{"id":103749,"date":"2017-09-30T06:30:00","date_gmt":"2017-09-29T22:30:00","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=103749"},"modified":"2017-10-21T22:56:57","modified_gmt":"2017-10-21T14:56:57","slug":"%e8%a7%82%e7%82%b9%e4%ba%a4%e6%b5%81%e9%98%bb%e6%8a%97%e7%9b%b8%e5%85%b3%e7%9f%a5%e8%af%86%ef%bc%88%e6%96%b0%e6%89%8b%e5%bf%85%e5%a4%87%ef%bc%89","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=103749","title":{"rendered":"\u5e72\u8d27|\u4ea4\u6d41\u963b\u6297\u76f8\u5173\u77e5\u8bc6\uff08\u65b0\u624b\u5fc5\u5907\uff09"},"content":{"rendered":"

\u524d\u8a00<\/strong><\/span><\/p>\n

\u7535\u5316\u5b66\u963b\u6297\u8c31\uff08\u4ea4\u6d41\u963b\u6297\u6cd5\uff09\u662f\u7535\u5316\u5b66\u6d4b\u8bd5\u6280\u672f\u4e2d\u4e00\u7c7b\u5341\u5206\u91cd\u8981\u7684\u65b9\u6cd5\uff0c\u662f\u7814\u7a76\u7535\u6781\u8fc7\u7a0b\u52a8\u529b\u5b66\u548c\u8868\u9762\u73b0\u8c61\u7684\u91cd\u8981\u624b\u6bb5\u3002\u7279\u522b\u662f\u8fd1\u5e74\u6765\uff0c\u7531\u4e8e\u9891\u7387\u54cd\u5e94\u5206\u6790\u4eea\u7684\u5feb\u901f\u53d1\u5c55\uff0c\u4ea4\u6d41\u963b\u6297\u7684\u6d4b\u8bd5\u7cbe\u5ea6\u8d8a\u6765\u8d8a\u9ad8\uff0c\u8d85\u4f4e\u9891\u4fe1\u53f7\u963b\u6297\u8c31\u4e5f\u5177\u6709\u826f\u597d\u7684\u91cd\u73b0\u6027\uff0c\u518d\u52a0\u4e0a\u8ba1\u7b97\u673a\u6280\u672f\u7684\u8fdb\u6b65\uff0c\u5bf9\u963b\u6297\u8c31\u89e3\u6790\u7684\u81ea\u52a8\u5316\u7a0b\u5ea6\u8d8a\u6765\u8d8a\u9ad8\uff0c\u8fd9\u5c31\u4f7f\u6211\u4eec\u80fd\u66f4\u597d\u7684\u7406\u89e3\u7535\u6781\u8868\u9762\u53cc\u7535\u5c42\u7ed3\u6784\uff0c\u6d3b\u5316\u949d\u5316\u819c\u8f6c\u6362\uff0c\u5b54\u8680\u7684\u8bf1\u53d1\u3001\u53d1\u5c55\u3001\u7ec8\u6b62\u4ee5\u53ca\u6d3b\u6027\u7269\u8d28\u7684\u5438\u8131\u9644\u8fc7\u7a0b\u3002<\/p>\n

1 \u7535\u5316\u5b66\u963b\u6297\u8c31\u7684\u57fa\u7840<\/strong><\/span><\/p>\n

\u7535\u5316\u5b66\u963b\u6297\u8c31\uff08Electrochemical Impedance Spectroscopy\uff0cEIS\uff09\uff1a\u7ed9\u7535\u5316\u5b66\u7cfb\u7edf\u65bd\u52a0\u4e00\u4e2a\u9891\u7387\u4e0d\u540c\u7684\u5c0f\u632f\u5e45\u7684\u4ea4\u6d41\u6b63\u5f26\u7535\u52bf\u6ce2\uff0c\u6d4b\u91cf\u4ea4\u6d41\u7535\u52bf\u4e0e\u7535\u6d41\u4fe1\u53f7\u7684\u6bd4\u503c\uff08\u7cfb\u7edf\u7684\u963b\u6297\uff09\u968f\u6b63\u5f26\u6ce2\u9891\u7387w\u7684\u53d8\u5316\uff0c\u6216\u8005\u662f\u963b\u6297\u7684\u76f8\u4f4d\u89d2f<\/em>\u968fw\u7684\u7684\u53d8\u5316\u3002\u901a\u5e38\u4f5c\u4e3a\u6270\u52a8\u4fe1\u53f7\u7684\u7535\u52bf\u6b63\u5f26\u6ce2\u7684\u5e45\u5ea6\u57285mV\u5de6\u53f3\uff0c\u4e00\u822c\u4e0d\u8d85\u8fc710mV\u3002<\/p>\n

\"\"<\/p>\n

1.1<\/strong>\u5229\u7528<\/strong>EIS<\/strong>\u7814\u7a76\u4e00\u4e2a\u7535\u5316\u5b66\u7cfb\u7edf\u7684\u57fa\u672c\u601d\u8def<\/strong><\/p>\n

\u5c06\u7535\u5316\u5b66\u7cfb\u7edf\u770b\u4f5c\u662f\u4e00\u4e2a\u7b49\u6548\u7535\u8def\uff0c\u8fd9\u4e2a\u7b49\u6548\u7535\u8def\u662f\u7531\u7535\u963b\uff08R<\/em>\uff09\u3001\u7535\u5bb9\uff08C<\/em>\uff09\u3001\u7535\u611f\uff08L<\/em>\uff09\u7b49\u57fa\u672c\u5143\u4ef6\u6309\u4e32\u8054\u6216\u5e76\u8054\u7b49\u4e0d\u540c\u65b9\u5f0f\u7ec4\u5408\u800c\u6210\uff0c\u901a\u8fc7EIS\uff0c\u53ef\u4ee5\u6d4b\u5b9a\u7b49\u6548\u7535\u8def\u7684\u6784\u6210\u4ee5\u53ca\u5404\u5143\u4ef6\u7684\u5927\u5c0f\uff0c\u5229\u7528\u8fd9\u4e9b\u5143\u4ef6\u7684\u7535\u5316\u5b66\u542b\u4e49\uff0c\u6765\u5206\u6790\u7535\u5316\u5b66\u7cfb\u7edf\u7684\u7ed3\u6784\u548c\u7535\u6781\u8fc7\u7a0b\u7684\u6027\u8d28\u7b49\u3002<\/p>\n

1.2<\/strong>\u7535\u5316\u5b66\u7cfb\u7edf\u7684\u4ea4\u6d41\u963b\u6297\u7684\u542b\u4e49<\/strong><\/p>\n

\"\"<\/p>\n

\u7ed9\u9ed1\u7bb1\uff08\u7535\u5316\u5b66\u7cfb\u7edfM\uff09\u8f93\u5165\u4e00\u4e2a\u6270\u52a8\u51fd\u6570X\uff0c\u5b83\u5c31\u4f1a\u8f93\u51fa\u4e00\u4e2a\u54cd\u5e94\u4fe1\u53f7Y\u3002\u7528\u6765\u63cf\u8ff0\u6270\u52a8\u4e0e\u54cd\u5e94\u4e4b\u95f4\u5173\u7cfb\u7684\u51fd\u6570\uff0c\u79f0\u4e3a\u4f20\u8f93\u51fd\u6570G<\/em>(w)\u3002\u82e5\u7cfb\u7edf\u7684\u5185\u90e8\u7ed3\u6784\u662f\u7ebf\u6027\u7684\u7a33\u5b9a\u7ed3\u6784\uff0c\u5219\u8f93\u51fa\u4fe1\u53f7\u5c31\u662f\u6270\u52a8\u4fe1\u53f7\u7684\u7ebf\u6027\u51fd\u6570\u3002\"\"<\/p>\n

\u5982\u679cX<\/em>\u4e3a\u89d2\u9891\u7387\u4e3aw\u7684\u6b63\u5f26\u6ce2\u7535\u6d41\u4fe1\u53f7\uff0c\u5219Y<\/em>\u5373\u4e3a\u89d2\u9891\u7387\u4e5f\u4e3aw\u7684\u6b63\u5f26\u7535\u52bf\u4fe1\u53f7\uff0c\u6b64\u65f6\uff0c\u4f20\u8f93\u51fd\u6570G<\/em>(w)\u4e5f\u662f\u9891\u7387\u7684\u51fd\u6570\uff0c\u79f0\u4e3a\u9891\u54cd\u51fd\u6570\uff0c\u8fd9\u4e2a\u9891\u54cd\u51fd\u6570\u5c31\u79f0\u4e4b\u4e3a\u7cfb\u7edf\uff2d\u7684\u963b\u6297\uff08impedance)\uff0c\u7528Z<\/em>\u8868\u793a\u3002<\/p>\n

\"\"<\/p>\n

EIS\u6280\u672f\u5c31\u662f\u6d4b\u5b9a\u4e0d\u540c\u9891\u7387w\uff08f<\/em>\uff09\u7684\u6270\u52a8\u4fe1\u53f7X<\/em>\u548c\u54cd\u5e94\u4fe1\u53f7Y<\/em>\u7684\u6bd4\u503c\uff0c\u5f97\u5230\u4e0d\u540c\u9891\u7387\u4e0b\u963b\u6297\u7684\u5b9e\u90e8Z<\/em>\u2019\u3001\u865a\u90e8Z<\/em>\u201d\u3001\u6a21\u503c|Z<\/em>|\u548c\u76f8\u4f4d\u89d2f<\/em>\uff0c\u7136\u540e\u5c06\u8fd9\u4e9b\u91cf\u7ed8\u5236\u6210\u5404\u79cd\u5f62\u5f0f\u7684\u66f2\u7ebf\uff0c\u5c31\u5f97\u5230EIS\u6297\u8c31\u3002\u5e38\u7528\u7684\u7535\u5316\u5b66\u963b\u6297\u8c31\u6709\u4e24\u79cd\uff1a\u4e00\u79cd\u53eb\u505a\u5948\u594e\u65af\u7279\u56fe\uff08Nyquist plot\uff09\uff0c \u4e00\u79cd\u53eb\u505a\u6ce2\u7279\u56fe\uff08Bode plot\uff09\u3002<\/p>\n

\"\"<\/p>\n

1.3 EIS<\/strong>\u7684\u7279\u70b9<\/strong><\/p>\n

\u4f18\u70b9\uff1a<\/strong>\u4f53\u7cfb\u5e72\u6270\u5c0f\uff1b\u63d0\u4f9b\u591a\u89d2\u5ea6\u7684\u754c\u9762\u72b6\u6001\u4e0e\u8fc7\u7a0b\u7684\u4fe1\u606f\uff0c\u4fbf\u4e8e\u5206\u6790\u8150\u8680\u7f13\u8680\u4f5c\u7528\u673a\u7406\uff1b\u6570\u636e\u5206\u6790\u8fc7\u7a0b\u76f8\u5bf9\u7b80\u5355\uff0c\u7ed3\u679c\u53ef\u9760\u3002<\/p>\n

\u7f3a\u70b9\uff1a<\/strong>\u590d\u6742\u7684\u963b\u6297\u8c31\u7684\u89e3\u91ca\u3002<\/p>\n

2 <\/strong>\u7535\u6781\u8fc7\u7a0b\u7684\u7b49\u6548\u7535\u8def<\/strong><\/span><\/p>\n

2.1 <\/strong>\u7535\u8377\u4f20\u9012\u8fc7\u7a0b\u63a7\u5236\u7684<\/strong>EIS<\/strong><\/p>\n

\u5982\u679c\u7535\u6781\u8fc7\u7a0b\u7531\u7535\u8377\u4f20\u9012\u8fc7\u7a0b\uff08\u7535\u5316\u5b66\u53cd\u5e94\u6b65\u9aa4\uff09\u63a7\u5236\uff0c\u6269\u6563\u8fc7\u7a0b\u5f15\u8d77\u7684\u963b\u6297\u53ef\u4ee5\u5ffd\u7565\uff0c\u5219\u7535\u5316\u5b66\u7cfb\u7edf\u7684\u7b49\u6548\u7535\u8def\u53ef\u7b80\u5316\u4e3a\uff1a<\/p>\n

\"\"<\/p>\n

\u7b49\u6548\u7535\u8def\u7684\u963b\u6297\uff1a\"\"<\/p>\n

\"\"<\/p>\n

\u7535\u6781\u8fc7\u7a0b\u7684\u63a7\u5236\u6b65\u9aa4\u4e3a\u7535\u5316\u5b66\u53cd\u5e94\u6b65\u9aa4\u65f6\uff0cNyquist\u56fe\u4e3a\u534a\u5706\uff0c\u636e\u6b64\u53ef\u4ee5\u5224\u65ad\u7535\u6781\u8fc7\u7a0b\u7684\u63a7\u5236\u6b65\u9aa4\u3002\u4eceNyquist\u56fe\u4e0a\u53ef\u4ee5\u76f4\u63a5\u6c42\u51faR<\/em>W<\/sub>\u548cR<\/em>ct<\/sub>\u3002\u7531\u534a\u5706\u9876\u70b9\u7684w\u53ef\u6c42\u5f97C<\/em>d<\/sub>\u3002<\/p>\n

\"\"<\/p>\n

\u6ce8\u610f\uff1a<\/strong>\u5728\u56fa\u4f53\u7535\u6781\u7684EIS\u6d4b\u91cf\u4e2d\u53d1\u73b0\uff0c\u66f2\u7ebf\u603b\u662f\u6216\u591a\u6216\u5c11\u7684\u504f\u79bb\u534a\u5706\u8f68\u8ff9\uff0c\u800c\u8868\u73b0\u4e3a\u4e00\u6bb5\u5706\u5f27\uff0c\u88ab\u79f0\u4e3a\u5bb9\u6297\u5f27\uff0c\u8fd9\u79cd\u73b0\u8c61\u88ab\u79f0\u4e3a\u201c\u5f25\u6563\u6548\u5e94\u201d\uff0c\u539f\u56e0\u4e00\u822c\u8ba4\u4e3a\u540c\u7535\u6781\u8868\u9762\u7684\u4e0d\u5747\u5300\u6027\u3001\u7535\u6781\u8868\u9762\u7684\u5438\u9644\u5c42\u53ca\u6eb6\u6db2\u5bfc\u7535\u6027\u5dee\u6709\u5173\uff0c\u5b83\u53cd\u6620\u4e86\u7535\u6781\u53cc\u7535\u5c42\u504f\u79bb\u7406\u60f3\u7535\u5bb9\u7684\u6027\u8d28\u3002\u6eb6\u6db2\u7535\u963bR<\/em>W<\/sub>\u9664\u4e86\u6eb6\u6db2\u7684\u6b27\u59c6\u7535\u963b\u5916\uff0c\u8fd8\u5305\u62ec\u4f53\u7cfb\u4e2d\u7684\u5176\u5b83\u53ef\u80fd\u5b58\u5728\u7684\u6b27\u59c6\u7535\u963b\uff0c\u5982\u7535\u6781\u8868\u9762\u819c\u7684\u6b27\u59c6\u7535\u963b\u3001\u7535\u6c60\u9694\u819c\u7684\u6b27\u59c6\u7535\u963b\u3001\u7535\u6781\u6750\u6599\u672c\u8eab\u7684\u6b27\u59c6\u7535\u963b\u7b49\u3002<\/p>\n

2.2<\/strong>\u7535\u8377\u4f20\u9012\u548c\u6269\u6563\u8fc7\u7a0b\u6df7\u5408\u63a7\u5236\u7684<\/strong>EIS<\/strong><\/p>\n

\u5982\u679c\u7535\u8377\u4f20\u9012\u52a8\u529b\u5b66\u4e0d\u662f\u5f88\u5feb\uff0c\u7535\u8377\u4f20\u9012\u8fc7\u7a0b\u548c\u6269\u6563\u8fc7\u7a0b\u5171\u540c\u63a7\u5236\u603b\u7684\u7535\u6781\u8fc7\u7a0b\uff0c\u7535\u5316\u5b66\u6781\u5316\u548c\u6d53\u5dee\u6781\u5316\u540c\u65f6\u5b58\u5728\uff0c\u5219\u7535\u5316\u5b66\u7cfb\u7edf\u7684\u7b49\u6548\u7535\u8def\u53ef\u7b80\u5355\u8868\u793a\u4e3a\uff1a<\/p>\n

\"\"<\/p>\n

\u7535\u8def\u7684\u963b\u6297\uff1a\"\"<\/p>\n

Nyquist\u56fe\u4e0a\u6269\u6563\u63a7\u5236\u8868\u73b0\u4e3a\u503e\u659c\u89d2\u03c0<\/em>\/4\uff0845\u00b0\uff09\u7684\u76f4\u7ebf\u3002<\/p>\n

\"\"<\/p>\n

\u7535\u6781\u8fc7\u7a0b\u7531\u7535\u8377\u4f20\u9012\u548c\u6269\u6563\u8fc7\u7a0b\u5171\u540c\u63a7\u5236\u65f6\uff0c\u5728\u6574\u4e2a\u9891\u7387\u57df\u5185\uff0c\u5176Nyquist\u56fe\u662f\u7531\u9ad8\u9891\u533a\u7684\u4e00\u4e2a\u534a\u5706\u548c\u4f4e\u9891\u533a\u7684\u4e00\u676145\u5ea6\u7684\u76f4\u7ebf\u6784\u6210\u3002\u9ad8\u9891\u533a\u4e3a\u7535\u6781\u53cd\u5e94\u52a8\u529b\u5b66\uff08\u7535\u8377\u4f20\u9012\u8fc7\u7a0b\uff09\u63a7\u5236\uff0c\u4f4e\u9891\u533a\u7531\u7535\u6781\u53cd\u5e94\u7684\u53cd\u5e94\u7269\u6216\u4ea7\u7269\u7684\u6269\u6563\u63a7\u5236\u3002<\/p>\n

\"\"<\/p>\n

\"\"<\/p>\n

\u6269\u6563\u963b\u6297\u7684\u76f4\u7ebf\u53ef\u80fd\u504f\u79bb45\u00b0\uff0c\u539f\u56e0\uff1a\u7535\u6781\u8868\u9762\u5f88\u7c97\u7cd9\uff0c\u4ee5\u81f4\u6269\u6563\u8fc7\u7a0b\u90e8\u5206\u76f8\u5f53\u4e8e\u7403\u9762\u6269\u6563\uff1b\u9664\u4e86\u7535\u6781\u7535\u52bf\u5916\uff0c\u8fd8\u6709\u53e6\u5916\u4e00\u4e2a\u72b6\u6001\u53d8\u91cf\uff0c\u8fd9\u4e2a\u53d8\u91cf\u5728\u6d4b\u91cf\u7684\u8fc7\u7a0b\u4e2d\u5f15\u8d77\u611f\u6297\u3002<\/p>\n

2.3<\/strong>\u590d\u6742\u6216\u7279\u6b8a\u7684\u7535\u5316\u5b66\u4f53\u7cfb<\/strong><\/p>\n

\u5bf9\u4e8e\u590d\u6742\u6216\u7279\u6b8a\u7684\u7535\u5316\u5b66\u4f53\u7cfb\uff0cEIS\u8c31\u7684\u5f62\u72b6\u5c06\u66f4\u52a0\u590d\u6742\u591a\u6837\u3002\u53ea\u7528\u7535\u963b\u3001\u7535\u5bb9\u7b49\u8fd8\u4e0d\u8db3\u4ee5\u63cf\u8ff0\u7b49\u6548\u7535\u8def\uff0c\u9700\u8981\u5f15\u5165\u611f\u6297\u3001\u5e38\u76f8\u4f4d\u5143\u4ef6\u7b49\u5176\u5b83\u7535\u5316\u5b66\u5143\u4ef6\u3002<\/p>\n

\"\"<\/p>\n

3 EIS<\/strong>\u7684\u6570\u636e\u5904\u7406\u4e0e\u89e3\u6790<\/strong><\/span><\/p>\n

EIS<\/strong>\u5206\u6790\u5e38\u7528\u7684\u65b9\u6cd5\uff1a\u7b49\u6548\u7535\u8def\u66f2\u7ebf\u62df\u5408\u6cd5<\/strong><\/p>\n

\u7b2c\u4e00\u6b65\uff1a<\/strong>\u5b9e\u9a8c\u6d4b\u5b9aEIS\u3002<\/p>\n

\"\"<\/p>\n

\u7b2c\u4e8c\u6b65\uff1a<\/strong>\u6839\u636e\u7535\u5316\u5b66\u4f53\u7cfb\u7684\u7279\u5f81\uff0c\u5229\u7528\u7535\u5316\u5b66\u77e5\u8bc6\uff0c\u4f30\u8ba1\u8fd9\u4e2a\u7cfb\u7edf\u4e2d\u53ef\u80fd\u6709\u54ea\u4e9b\u4e2a\u7b49\u6548\u7535\u8def\u5143\u4ef6\uff0c\u5b83\u4eec\u4e4b\u95f4\u6709\u53ef\u80fd\u600e\u6837\u7ec4\u5408\uff0c\u7136\u540e\u63d0\u51fa\u4e00\u4e2a\u53ef\u80fd\u7684\u7b49\u6548\u7535\u8def\u3002<\/p>\n

\"\"<\/p>\n

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