{"id":105043,"date":"2017-10-03T06:30:17","date_gmt":"2017-10-02T22:30:17","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=105043"},"modified":"2018-02-21T01:05:59","modified_gmt":"2018-02-20T17:05:59","slug":"%e4%b8%ad%e7%a7%91%e9%99%a2%e7%90%86%e5%8c%96%e6%89%80%e5%bc%a0%e9%93%81%e9%94%90%e8%af%be%e9%a2%98%e7%bb%84adv-mater-%e6%b0%b4%e6%bb%91%e7%9f%b3%e7%94%a8%e4%ba%8e%e9%ab%98%e6%95%88%e5%8f%af","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=105043","title":{"rendered":"\u4e2d\u79d1\u9662\u7406\u5316\u6240\u5f20\u94c1\u9510 | Adv. Mater. : \u6c34\u6ed1\u77f3\u7528\u4e8e\u9ad8\u6548\u53ef\u89c1\u5149\u50ac\u5316\u56fa\u6c2e\u5408\u6210\u6c28"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/span><\/strong><\/p>\n

\u6c28\uff08NH3<\/sub>\uff09\u662f\u5927\u5b97\u5316\u5de5\u4e1a\u54c1\u4e4b\u4e00\uff0c\u5c06\u7a7a\u6c14\u4e2d\u7684\u6c2e\u6c14\uff08N2<\/sub>\uff09\u52a0\u6c22\u8fd8\u539f\u5408\u6210\u6c28\u5de5\u4e1a\u5728\u56fd\u6c11\u7ecf\u6d4e\u4e2d\u5360\u6709\u91cd\u8981\u5730\u4f4d\u3002\u519c\u4e1a\u4e0a\u4f7f\u7528\u7684\u6c2e\u80a5\u8bf8\u5982\uff1a\u5c3f\u7d20\u3001\u785d\u9178\u94f5\u3001\u78f7\u9178\u94f5\u3001\u6c2f\u5316\u94f5\u4ee5\u53ca\u5404\u79cd\u542b\u6c2e\u590d\u5408\u80a5\uff0c\u4ee5\u53ca\u78b1\uff08Na2<\/sub>CO3<\/sub>\uff09\u90fd\u662f\u4ee5\u6c28\u4e3a\u539f\u6599\u3002\u540c\u65f6\uff0c\u6240\u6709\u751f\u7269\u4f53\u90fd\u9700\u8981\u6c2e\u5143\u7d20\u6765\u5408\u6210\u4f53\u5185\u7684\u86cb\u767d\u8d28\u3001\u6838\u9178\u548c\u5176\u4ed6\u751f\u7269\u5206\u5b50\u3002\u8fd8\u539fN2<\/sub>\u5728\u5de5\u4e1a\u548c\u751f\u547d\u4f53\u7cfb\u5360\u6709\u91cd\u8981\u5730\u4f4d\u3002\u867d\u7136N2<\/sub>\u5360\u5730\u7403\u7a7a\u6c14\u768478\uff05\uff0c\u5982\u4f55\u6d3b\u5316\u89e3\u79bbN2<\/sub>\u4e2d\u6781\u5f3a\u7684\u975e\u6781\u6027N-N\u5171\u4ef7\u4e09\u952e\uff0c\u5177\u6709\u6781\u5927\u6311\u6218\u3002\u4f20\u7edf\u7684Haber-Bosch\u5de5\u827a\uff0c\u5728\u82db\u523b\u7684\u53cd\u5e94\u6761\u4ef6\u4e0b\uff0815-25 MPa\uff0c300-550\u2103\uff09\uff0c\u5229\u7528\u94c1\u57fa\u50ac\u5316\u5242\u5c06N2<\/sub>\u8fd8\u539f\u4e3aNH3<\/sub>\uff0c\u6d88\u8017\u5927\u91cf\u7684\u80fd\u6e90\uff0c\u4e0d\u53ef\u907f\u514d\u7684\u9020\u6210\u5927\u91cfCO2<\/sub>\u6392\u653e\u3002\u9274\u4e8e\u5316\u77f3\u71c3\u6599\u77ed\u7f3a\u548c\u5168\u7403\u6c14\u5019\u53d8\u5316\uff0c\u5f00\u53d1\u7eff\u8272\u53ef\u6301\u7eed\u7684\u56fa\u6c2e\u8fc7\u7a0b\u662f\u4e00\u9879\u5177\u6709\u6311\u6218\u6027\u548c\u957f\u671f\u6027\u7684\u76ee\u6807\u3002\u5176\u4e2d\uff0c\u5229\u7528\u592a\u9633\u80fd\u5149\u50ac\u5316\u6280\u672f\u5c06\u592a\u9633\u80fd\u8f6c\u5316\u4e3a\u5316\u5b66\u80fd\uff0c\u5df2\u88ab\u8ba4\u4e3a\u662f\u672a\u6765\u53ef\u518d\u751f\u80fd\u6e90\u7684\u6700\u4f73\u9014\u5f84\u4e4b\u4e00\u3002\u76ee\u524d\u5149\u56fa\u6c2e\u5408\u6210\u6c28\u50ac\u5316\u5242\u5927\u90fd\u53ea\u5bf9\u7d2b\u5916\u5149\u90e8\u5206\u6709\u5438\u6536\uff0c\u5f00\u53d1\u5bf9500 nm\u4ee5\u4e0a\u53ef\u89c1\u5149\u6709\u50ac\u5316\u6d3b\u6027\u7684\u50ac\u5316\u5242\u8fd8\u662f\u4e00\u4e2a\u6311\u6218\u3002<\/p>\n

\u6c34\u6ed1\u77f3\uff08Layered double hydroxides\uff08LDH\uff09\uff09,\u662f\u4e00\u7c7b\u4e8c\u7ef4\u5c42\u72b6\u9634\u79bb\u5b50\u578b\u5316\u5408\u7269\uff0c\u5176\u4e3b\u4f53\u5c42\u677f\u7ed3\u6784\u7c7b\u4f3c\u4e8e\u6c34\u9541\u77f3Mg(OH)2<\/sub>\uff0c\u5c42\u677f\u4e3a\u516b\u9762\u4f53MO6<\/sub>\u5171\u68f1\u8fb9\uff0c\u91d1\u5c5e\u79bb\u5b50\u5360\u636e\u516b\u9762\u4f53\u4e2d\u5fc3\u3002\u901a\u8fc7\u8c03\u63a7\u5c42\u677f\u91d1\u5c5e\u79bb\u5b50\u7684\u79cd\u7c7b\uff0c\u7ecf\u8fc7\u91d1\u5c5e-\u91d1\u5c5e\u7535\u8377\u8f6c\u79fb\uff0c\u53ef\u4ee5\u6709\u6548\u8c03\u63a7\u5176\u80fd\u5e26\u5438\u6536\u5f80\u53ef\u89c1\u5149\u4e43\u81f3\u7ea2\u5916\u8fc1\u79fb\u3002\u5728\u4e4b\u524d\u7684\u7814\u7a76\u4e2d\uff0c\u6c34\u6ed1\u77f3\u5df2\u7ecf\u5728\u5149\u5206\u89e3\u6c34\u3001\u8fd8\u539fCO2<\/sub>\u7b49\u65b9\u9762\u5c55\u73b0\u4e86\u4f18\u8d8a\u7684\u53ef\u8c03\u6027\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/span><\/strong><\/p>\n

\u8fd1\u671f\uff0c\u4e2d\u79d1\u9662\u7406\u5316\u6280\u672f\u7814\u7a76\u6240\u5f20\u94c1\u9510\u7814\u7a76\u5458\u7b49\u4eba\u5728Adv. Mater.<\/i>\u4e0a\u53d1\u8868\u4e00\u7bc7\u9898\u4e3aLayered double hydroxide nanosheets as efficient visible-light-driven photocatalysts for dinitrogen fixation<\/strong>\u7684\u6587\u7ae0\u3002\u672c\u8bba\u6587\u901a\u8fc7\u5229\u7528\u7b80\u5355\u7684\u53ef\u4ee5\u89c4\u6a21\u5316\u7684\u5171\u6c89\u6dc0\u65b9\u6cd5\uff0c\u6210\u529f\u5236\u5907\u4e86\u4e00\u7cfb\u5217MII<\/sup>MIII<\/sup>-LDH\uff08MII<\/sup>\u00a0= Mg\uff0cZn\uff0cNi\uff0cCu; MIII<\/sup>\u00a0= Al\uff0cCr\uff09\u7eb3\u7c73\u7247\u5149\u50ac\u5316\u5242\uff0c\u5b9e\u73b0\u4e86\u53ef\u89c1\u5149\u4e0bN2<\/sub>\u548c\u6c34\u5408\u6210\u6c28\u3002X\u5c04\u7ebf\u5438\u6536\u7cbe\u7ec6\u7ed3\u6784\uff0c\u4f4e\u6e29\u7535\u5b50\u987a\u78c1\u5171\u632f\u548c\u6b63\u7535\u5b50\u6e6e\u706d\u5bff\u547d\u6d4b\u91cf\u8868\u660e\uff0c\u8d85\u8584LDH\u7eb3\u7c73\u7247\u7531\u4e8e\u5bcc\u6c27\u7f3a\u9677\uff0c\u4ee5\u53ca\u660e\u663e\u7684\u7ed3\u6784\u626d\u66f2\u548c\u538b\u7f29\u5e94\u53d8\uff0c\u589e\u5f3a\u4e86\u5bf9N2<\/sub>\u5206\u5b50\u7684\u5438\u9644\u548c\u53ef\u89c1\u5149\u751f\u7535\u5b50\u4eceLDH\u5149\u50ac\u5316\u5242\u8f6c\u79fb\u5230N2<\/sub>\u7684\u6548\u7387\uff0c\u4ece\u800c\u4fc3\u8fdb\u4e86NH3<\/sub>\u7684\u6709\u6548\u5408\u6210\uff08\u7279\u522b\u662fCuCr-LDH\u7eb3\u7c73\u7247\u5728500\u00a0nm\u5904\uff0c\u91cf\u5b50\u4ea7\u7387\u4ecd\u80fd\u8fbe\u52300.10\uff05\uff09\u3002\u8fd9\u9879\u7814\u7a76\u5de5\u4f5c\u663e\u793a\uff0c\u5728\u5e38\u6e29\u5e38\u538b\u548c\u53ef\u89c1\u5149\u6216\u76f4\u63a5\u592a\u9633\u8f90\u5c04\u4e0b\uff0c\u57fa\u4e8eLDH\u5c06N2<\/sub>\u8fd8\u539f\u6210NH3<\/sub>\u662f\u4e00\u79cd\u6781\u5176\u6709\u6f5c\u529b\u548c\u5e0c\u671b\u7684\u65b0\u9014\u5f84\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/span><\/p>\n

LDH\u8d85\u8584\u7eb3\u7c73\u7247\u5149\u50ac\u5316\u5408\u6210\u6c28\u793a\u610f\u56fe<\/span><\/strong><\/p>\n

\"\"<\/p>\n

\u56fe1 LDH\u7684\u5f62\u8c8c\u53ca\u6676\u4f53\u7ed3\u6784\u8868\u5f81<\/strong><\/span><\/p>\n

\"\"<\/p>\n

(A)\u3001(B)\u548c(C) CuCr-LDH\u7684TEM\u548cHRTEM\u56fe\uff1b<\/p>\n

(D)\u3001(E)\u548c(F)\u00a0ZnAl-LDH\u7684TEM\u548cHRTEM\u56fe\u3002<\/p>\n

\u56fe2\u00a0LDH\u7684\u7ed3\u6784\u8868\u5f81<\/span><\/strong><\/p>\n

\"\"<\/p>\n

(A)\u3001(B)\u548c(C) CuCr-LDH\u53ca\u5feb\u4f53\u5bf9\u6bd4\u6837\u7684Cr\u8fb9XANES\u548cEXAFS\u56fe\u8c31\uff1b<\/p>\n

(D) ZnAl-LDH\u53ca\u5feb\u4f53\u5bf9\u6bd4\u6837\u7684Zn\u8fb9EXAFS\u56fe\u8c31\uff1b<\/p>\n

(E) CuCr-LDH\u53ca\u5bf9\u6bd4\u6837\u548cZnAl-LDH\u53ca\u5bf9\u6bd4\u6837\u7684XRD\u56fe\u8c31\uff1b<\/p>\n

(D) LDH\u7684110\u9762\u7684\u538b\u7f29\u5e94\u53d8\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe3 \u56fa\u6c2e\u6027\u80fd\u8868\u5f81<\/span><\/strong><\/p>\n

\"\"<\/p>\n

(A) \u5149\u50ac\u5316\u5408\u6210\u6c28\u793a\u610f\u56fe\uff1b<\/p>\n

(B) \u5728\u5168\u5149\u8c31\u4e0b\u53cd\u5e941 h\u4e0d\u540cLDH\u50ac\u5316\u5242\u7684\u5408\u6210\u6c28\u6027\u80fd\uff1b<\/p>\n

(C) \u5728\u53ef\u89c1\u5149(l<\/i><\/em>\u00a0> 400 nm)\u4e0b\u53cd\u5e941 h\u4e0d\u540cLDH\u50ac\u5316\u5242\u7684\u5408\u6210\u6c28\u6027\u80fd\uff1b<\/p>\n

(D) CuCr-LDH\u5149\u50ac\u5316\u56fa\u6c2e\u6027\u80fd\u7684\u7a33\u5b9a\u6027\uff1b<\/p>\n

(E) CuCr-LDH\u53ca\u5bf9\u6bd4\u6837\u968f\u65f6\u95f4\u53d8\u5316\uff0c\u5728\u4e0d\u540c\u6c14\u6c1b\u4e0b\u5408\u6210\u6c28\u6027\u80fd\uff1b<\/p>\n

(F) CuCr-LDH\u5408\u6210\u6c28\u53cd\u5e94\u7684\u539f\u4f4d\u7ea2\u5916\u56fe\u8c31\u3002<\/p>\n

\u56fe4 CuCr-LDH\u672c\u5f81\u7279\u6027\u8868\u5f81<\/span><\/strong><\/p>\n

\"\"<\/p>\n

(A) CuCr-LDH\u53ca\u5bf9\u6bd4\u6837\u7684\u7d2b\u5916\u53ef\u89c1\u6f2b\u53cd\u5c04\u56fe\u548cCuCr-LDH\u5149\u50ac\u5316\u5408\u6210\u6c28\u7684\u91cf\u5b50\u6548\u7387\u56fe\uff1b<\/p>\n

(B) CuCr-LDH\u53ca\u5bf9\u6bd4\u6837\u7684ESR\u8c31\u56fe\uff1b<\/p>\n

(C) CuCr-LDH\u53ca\u5bf9\u6bd4\u6837\u7684Mott-Schottky\u66f2\u7ebf\uff1b<\/p>\n

(D)\u548c(E) CuCr-LDH\u53ca\u5bf9\u6bd4\u6837\u7684EIS\u548cBode-phase\u66f2\u7ebf\uff1b<\/p>\n

(F) CuCr-LDH\u53ca\u5bf9\u6bd4\u6837\u7684\u5149\u7535\u6d41\u6d4b\u8bd5\u66f2\u7ebf\u3002<\/p>\n

\u56fe5 \u7406\u8bba\u8ba1\u7b97<\/span><\/strong><\/p>\n

\"\"<\/p>\n

(A) CuCr-LDH\u7684\u80fd\u5e26\uff1b<\/p>\n

(B)\u00a0\u6676\u683c\u5f15\u5165\u6c27\u7f3a\u9677\u540eCuCr-LDH\u7684\u80fd\u5e26\uff1b<\/p>\n

(C)\u00a0\u6676\u683c\u5e94\u529b\u53d8\u5316\u540eCuCr-LDH\u7684\u80fd\u5e26\uff1b<\/p>\n

(D) \u4e0d\u540cCuCr-LDH\u5bf9\u4e8eN2<\/sub>\u7684\u5438\u9644\u80fd\u8ba1\u7b97\uff1b<\/p>\n

(E)\u00a0\u4e0d\u540cCuCr-LDH\u5bf9\u4e8eN2<\/sub>\u7684\u952e\u957f\u53d8\u5316\uff1b<\/p>\n

(F) CuCr-LDH \u5f15\u5165\u6c27\u7f3a\u9677\u548c\u5e94\u529b\u7684\u7535\u8377\u5bc6\u5ea6\u5206\u5e03\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/span><\/strong><\/p>\n

\u7814\u7a76\u4eba\u5458\u6210\u529f\u5236\u5907\u4e86\u4e00\u7cfb\u5217MII<\/sup>MIII<\/sup>-LDH\uff08MII<\/sup>\u00a0= Mg\uff0cZn\uff0cNi\uff0cCu; MIII<\/sup>\u00a0= Al\uff0cCr\uff09\u8d85\u8584\u7eb3\u7c73\u7247\u5149\u50ac\u5316\u5242\uff0c\u901a\u8fc7\u7cbe\u7ec6\u7ed3\u6784\u8868\u5f81\u548c\u7406\u8bba\u8ba1\u7b97\u8868\u660e\uff0c\u8d85\u8584LDH\u7eb3\u7c73\u7247\u7531\u4e8e\u5bcc\u6c27\u7f3a\u9677\uff0c\u7ed3\u6784\u626d\u66f2\u548c\u538b\u7f29\u5e94\u53d8\uff0c\u589e\u5f3a\u4e86\u5bf9N2<\/sub>\u5206\u5b50\u7684\u5438\u9644\u548c\u5149\u751f\u7535\u5b50\u4eceLDH\u5149\u50ac\u5316\u5242\u8f6c\u79fb\u5230N2<\/sub>\uff0c\u4ece\u800c\u4fc3\u8fdb\u4e86\u5149\u50ac\u5316\u5408\u6210\u6c28\u6027\u80fd\u7684\u63d0\u9ad8\u3002\u901a\u8fc7\u8c03\u63a7\u91d1\u5c5e\u79bb\u5b50\u79cd\u7c7b\uff0cCuCr-LDH\u5728500 nm\u4ecd\u7136\u5177\u6709\u53ef\u89c1\u5149\u56fa\u6c2e\u7279\u6027\u3002\u8be5\u7b56\u7565\u4e3a\u5408\u6210\u9ad8\u6548\u5149\u50ac\u5316\u5242\u7684\u5408\u6210\u63d0\u4f9b\u4e86\u601d\u8def\uff0c\u53ef\u5e7f\u6cdb\u5e94\u7528\u4e8e\u5149\u50ac\u5316\u5408\u6210\u6c28\uff0cCO2<\/sub>\u8fd8\u539f\u4ee5\u53ca\u5176\u4ed6\u50ac\u5316\u548c\u80fd\u6e90\u9886\u57df\u3002<\/p>\n

\u5f20\u94c1\u9510\u535a\u58eb\u7b80\u4ecb<\/strong><\/p>\n

\u5f20\u94c1\u9510\uff0c\u4e2d\u56fd\u79d1\u5b66\u9662\u7406\u5316\u6280\u672f\u7814\u7a76\u6240\u7814\u7a76\u5458\uff0c\u535a\u58eb\u751f\u5bfc\u5e08\uff1b\u4e2d\u79d1\u9662\u7279\u8058\u7814\u7a76\u5458\u30022003\u5e74\u4e8e\u5409\u6797\u5927\u5b66\u53d6\u5f97\u535a\u58eb\u5b66\u4f4d\uff0c\u57282004-2009\u5e74\u95f4\u66fe\u5148\u540e\u4e8e\u5fb7\u56fd\u9a6c\u666e\u80f6\u4f53\u754c\u9762\u7814\u7a76\u6240\u3001\u52a0\u62ff\u5927\u56fd\u5bb6\u7eb3\u7c73\u7814\u7a76\u6240\u548c\u963f\u5c14\u4f2f\u5854\u5927\u5b66\u3001\u963f\u80af\u8272\u5927\u5b66\u53ca\u52a0\u5dde\u5927\u5b66\u6cb3\u6ee8\u5206\u6821\u8fdb\u884c\u535a\u58eb\u540e\u8bbf\u95ee\uff0c2009\u5e7411\u6708\u8d77\u5c31\u804c\u4e8e\u4e2d\u56fd\u79d1\u5b66\u9662\u7406\u5316\u6280\u672f\u7814\u7a76\u6240\u30022017\u5e74\u5f53\u9009\u82f1\u56fd\u7687\u5bb6\u5316\u5b66\u4f1a\u4f1a\u58eb\u3002\u66fe\u83b7\u5f97\u82f1\u56fd\u7687\u5bb6\u5b66\u4f1a\u725b\u987f\u5b66\u8005\u3001\u4e07\u4eba\u8ba1\u5212\u9996\u6279\u9752\u5e74\u62d4\u5c16\u4eba\u624d\u3001\u56fd\u5bb6\u81ea\u7136\u79d1\u5b66\u57fa\u91d1\u59d4\u4f18\u79c0\u9752\u5e74\u79d1\u5b66\u57fa\u91d1\u7b49\u5956\u52b1\u3002<\/p>\n

\u4e3b\u8981\u7814\u7a76\u9886\u57df\u4e3a\u7528\u4e8e\u6c22\u9ad8\u6548\u6e05\u6d01\u5236\u5907\u548c\u5229\u7528\u7684\u7eb3\u7c73\u50ac\u5316\u6750\u6599\uff0c\u5171\u53d1\u8868SCI\u8bba\u6587140\u4f59\u7bc7\uff0c\u6b63\u9762\u5f15\u75285000\u4f59\u6b21\uff0c\u7533\u8bf7\u4e2d\u56fd\u4e13\u522927\u9879(15\u9879\u5df2\u6388\u6743)\u3002\u76ee\u524d\u62c5\u4efbScience Bulletin\u671f\u520a\u526f\u4e3b\u7f16\uff0cScientific Reports\u3001Chinese Chemical Letters\u7b49\u671f\u520a\u7f16\u59d4\u3002<\/p>\n

\u6587\u7ae0\u94fe\u63a5\uff1aLayered-Double-Hydroxide Nanosheets as Efficient Visible-Light-Driven Photocatalysts for Dinitrogen Fixation<\/u>\u00a0<\/u><\/a>(Adv. Mater.\u00a0<\/i>2017, 1703828. https:\/\/doi.org\/10.1002\/adma.201703828)<\/p>\n

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