{"id":114897,"date":"2017-12-06T06:30:18","date_gmt":"2017-12-05T22:30:18","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=114897"},"modified":"2017-12-01T21:44:50","modified_gmt":"2017-12-01T13:44:50","slug":"nano-energy%ef%bc%9a%e5%8e%9f%e5%ad%90%e5%b1%82%e6%b2%89%e7%a7%af%e5%88%b6%e5%a4%87%e9%ab%98%e8%b4%9f%e8%bd%bd%e9%87%8f%e8%b6%85%e7%a8%b3%e5%ae%9a%e8%87%aa%e6%94%af%e6%92%91%e7%a2%b3-%e7%a1%92","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=114897","title":{"rendered":"Nano Energy\uff1a\u539f\u5b50\u5c42\u6c89\u79ef\u5236\u5907\u9ad8\u8d1f\u8f7d\u91cf\u8d85\u7a33\u5b9a\u81ea\u652f\u6491\u78b3-\u7852\u6b63\u6781\u7528\u4e8e\u94a0-\u7852\u7535\u6c60"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u94a0-\u7852(Na-Se)\u7535\u6c60\u5177\u6709\u80fd\u91cf\u5bc6\u5ea6\u9ad8\u3001\u5b89\u5168\u6027\u80fd\u51fa\u8272\u3001\u5faa\u73af\u7a33\u5b9a\u6027\u80fd\u4f18\u5f02\u7b49\u7279\u70b9\uff0c\u6210\u4e3a\u80fd\u91cf\u50a8\u5b58\u9886\u57df\u7684\u70ed\u70b9\u7814\u7a76\u8bfe\u9898\u3002\u7136\u800c\u73b0\u9636\u6bb5Na-Se\u7535\u6c60\u7684\u53d1\u5c55\u53d7\u5230\u4ee5\u4e0b\u51e0\u65b9\u9762\u9650\u5236\uff1a(1)\u591a\u7852\u5316\u7269\u6eb6\u89e3\uff1b(2)\u5bfc\u7535\u6027\u4e0d\u7406\u60f3\uff1b(3)\u5faa\u73af\u7a33\u5b9a\u6027\u6b20\u4f73\u3002\u4e3a\u4e86\u89e3\u51b3Na-Se\u7535\u6c60\u5b58\u5728\u7684\u4e0a\u8ff0\u95ee\u9898\uff0c\u7814\u7a76\u4eba\u5458\u8fdb\u884c\u4e86\u5927\u91cf\u7684\u7814\u7a76\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0cNano Energy<\/strong>\u5728\u7ebf\u53d1\u8868\u4e86\u9898\u4e3a\u201cAtomic Layer Deposition-Enabled Ultrastable Freestanding Carbon-Selenium Cathodes with High Mass Loading for Sodium-Selenium Battery<\/strong>\u201d\u7684\u7814\u7a76\u8bba\u6587\uff0c\u62a5\u9053\u4e86\u94a0-\u7852\u7535\u6c60\u6b63\u6781\u6750\u6599\u7684\u6700\u65b0\u7814\u7a76\u8fdb\u5c55\u3002\u6df1\u5733\u5927\u5b66<\/strong>\u7684\u5f20\u57f9\u65b0\u6559\u6388<\/strong>\u548c\u4f50\u6cbb\u4e9a\u7406\u5de5\u5b66\u9662<\/strong>\u7684\u6797\u5fd7\u7fa4\u6559\u6388<\/strong>\u4e3a\u8bba\u6587\u7684\u5171\u540c\u901a\u8baf\u4f5c\u8005<\/strong>\uff0c\u8bba\u6587\u7684\u7b2c\u4e00\u4f5c\u8005\u4e3a\u6df1\u5733\u5927\u5b66\u7684\u9a6c\u5b9a\u6d9b\u548c\u674e\u6c38\u4eae\u535a\u58eb\u3002\u7814\u7a76\u4eba\u5458\u501f\u52a9\u7194\u878d\u6269\u6563\u3001\u6c14\u76f8\u6c89\u79ef\u548c\u539f\u5b50\u5c42\u6c89\u79ef\u5236\u5907\u5f97\u5230\u4e86\u53ef\u7528\u4e8e\u94a0-\u7852\u7535\u6c60\u7684\u6c27\u5316\u94dd\u5305\u8986\u7684\u7852\/\u591a\u5b54\u6c2e\u63ba\u6742\u78b3\u7eb3\u7c73\u7ea4\u7ef4\u590d\u5408\u7535\u6781(SC@Se-Al2O3)\u3002\u7814\u7a76\u53d1\u73b0\uff1a\u901a\u8fc7\u8c03\u8282\u7852(Se)\u542b\u91cf\u548c\u6c27\u5316\u94dd(Al2O3)\u8584\u819c\u7684\u539a\u5ea6\uff0c\u53ef\u4ee5\u5f97\u5230\u9ad8\u8d1f\u8f7d\u91cf\u3001\u9ad8\u7a33\u5b9a\u6027\u3001\u81ea\u652f\u6491\u7684\u78b3-\u7852\u6b63\u6781\u6750\u6599\uff1b\u5f53Se\u542b\u91cf\u4e3a67 wt%, Al2O3\u8584\u819c\u539a\u5ea6\u4e3a3 nm\u65f6\uff0c\u7535\u6781\u7684\u6027\u80fd\u6700\u4f18\uff1b\u57280.5 A\/g\u7684\u7535\u6d41\u5bc6\u5ea6\u4e0b\uff0c\u7535\u6781\u5728\u5faa\u73af1000\u6b21\u540e\u5e76\u672a\u8868\u73b0\u51fa\u660e\u663e\u7684\u5bb9\u91cf\u8870\u51cf\uff0c\u53ef\u9006\u5bb9\u91cf\u53ef\u8fbe503 mAh\/g\uff1b\u539f\u5b50\u5c42\u6c89\u79ef(ALD)\u53ef\u4ee5\u8c03\u8282\u7535\u6781\u7684\u7535\u5316\u5b66\u6027\u80fd\uff0c\u63d0\u9ad8\u6d3b\u6027\u7269\u8d28\u8d1f\u8f7d\u91cf\u548c\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u672c\u6587\u4e3a\u672a\u6765\u9ad8\u8d1f\u8f7d\u91cf\u3001\u9ad8\u7a33\u5b9a\u6027\u7535\u6781\u7684\u8bbe\u8ba1\u548c\u7814\u7a76\u63d0\u4f9b\u4e86\u4e00\u79cd\u65b0\u7684\u9009\u9879\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe<\/strong>-1. <\/strong>\u6837\u54c1\u5236\u5907\u793a\u610f\u56fe\u53ca\u5fae\u89c2\u5f62\u8c8c\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a)SC@Se-xAl2<\/sub>O3<\/sub>\u590d\u5408\u6750\u6599\u5236\u5907\u6d41\u7a0b\u793a\u610f\u56fe\uff1b<\/p>\n

(b) Se\/PCNFs\u7684FE-SEM\u56fe\u50cf\uff1b<\/p>\n

(c) SC@Se \u590d\u5408\u6750\u6599\u7684FE-SEM\u56fe\u50cf\u3002<\/p>\n

\u56fe<\/strong>-2. <\/strong>\u6837\u54c1\u7684\u5fae\u89c2\u5f62\u8c8c\u8868\u5f81\u548c\u5143\u7d20\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

\u901a\u8fc7ALD\u6c89\u79ef\u4e0d\u540c\u5faa\u73af\u7684Al2<\/sub>O3<\/sub>\u5f97\u5230\u7684SC@Se-xAl2<\/sub>O3<\/sub>\u590d\u5408\u7269\u7684C\uff0cSe\uff0cAl\u548cC\u7684HRTEM\u56fe\u50cf\u548c\u5177\u6709\u7535\u5b50\u80fd\u91cf\u635f\u5931\u8c31(EELS)\u5143\u7d20\u56fe\u7684\u9ad8\u89d2\u5ea6\u73af\u5f62\u6697\u573a(HAADF)\u56fe\u50cf\u3002<\/p>\n

(a, b)\u5f53x = 10\u65f6\uff0c\u4ea7\u7269\u7684HRTEM\u56fe\u50cf\u548cHAADF\u56fe\u50cf\uff1b<\/p>\n

(c, d)\u5f53x = 25\u65f6\uff0c\u4ea7\u7269\u7684HRTEM\u56fe\u50cf\u548cHAADF\u56fe\u50cf\uff1b<\/p>\n

(e, f)\u5f53x = 40\u65f6\uff0c\u4ea7\u7269\u7684HRTEM\u56fe\u50cf\u548cHAADF\u56fe\u50cf\u3002<\/p>\n

\u56fe<\/strong>-3.<\/strong>\u4e0d\u540c\u6837\u54c1\u7684\u8868\u5f81\u7ed3\u679c<\/strong><\/p>\n

\"\"<\/p>\n

(a) Se, PCNFs\u548cSC@Se-xAl2<\/sub>O3<\/sub>\u590d\u5408\u6750\u6599 (x=10, 25, 40)\u7684XRD\u56fe\u8c31\uff1b<\/p>\n

(b) PCNFs, Se\/PCNFs\u548cSC@Se\u7684TGA\u66f2\u7ebf\uff1b<\/p>\n

(c) PCNFs, Se\/PCNFs\u548cSC@Se\u7684N2<\/sub>\u5438\u8131\u9644\u7b49\u6e29\u7ebf\u548c\u5b54\u5f84\u5206\u5e03\u66f2\u7ebf\uff1b<\/p>\n

(d) Se, PCNFs\u548cSC@Se-xAl2<\/sub>O3<\/sub>\u590d\u5408\u6750\u6599\u7684Raman\u5149\u8c31\u3002<\/p>\n

\u56fe<\/strong>-4. <\/strong>\u4e0d\u540c\u6837\u54c1\u7684<\/strong>XPS<\/strong>\u8868\u5f81\u7ed3\u679c<\/strong><\/p>\n

\"\"<\/p>\n

(a) Se, PCNFs\u548cSC@Se-xAl2<\/sub>O3<\/sub>\u590d\u5408\u6750\u6599 (x=10, 25, 40)\u7684XPS\u5149\u8c31\uff1b<\/p>\n

(b) SC@Se-xAl2<\/sub>O3<\/sub>\u590d\u5408\u6750\u6599\u4e2dAl 2p\u7684XPS\u5149\u8c31\uff1b<\/p>\n

(c) PCNFs\u4e2dN 1s\u7684XPS\u5149\u8c31\u3002<\/p>\n

\u56fe<\/strong>-5. <\/strong>\u4ea7\u7269\u7684\u7535\u5316\u5b66\u6027\u80fd\u6d4b\u8bd5\u7ed3\u679c<\/strong><\/p>\n

\"\"<\/p>\n

(a) SC@Se-xAl2<\/sub>O3<\/sub>\u590d\u5408\u6750\u6599\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u66f2\u7ebf\uff1b<\/p>\n

(b) SC@Se-xAl2<\/sub>O3<\/sub>\u590d\u5408\u6750\u6599\u76f8\u5bf9\u521d\u59cb\u7535\u6d41\u5bc6\u5ea6\u4e3a0.1 C\u65f6\u5bb9\u91cf\u7684\u500d\u7387\u6027\u80fd\u5bf9\u6bd4\uff1b<\/p>\n

(c) PCNFs, SC@Se\u548cSC@Se-25Al2<\/sub>O3<\/sub>\u590d\u5408\u6750\u6599\u7684\u957f\u671f\u5faa\u73af\u7a33\u5b9a\u6027\u80fd\u5bf9\u6bd4\uff1b<\/p>\n

(d) SC@Se\u548cSC@Se-xAl2<\/sub>O3<\/sub>\u7535\u6781\u5faa\u73af\u524d\u7684Nyquist\u66f2\u7ebf\uff1b<\/p>\n

(e) SC@Se\u7535\u6781\u5faa\u73af\u793a\u610f\u56fe\u3002<\/p>\n

(f) ALD\u6c89\u79efAl2<\/sub>O3<\/sub>\u8584\u819c\u7a33\u5b9aSC@Se\u7535\u6781\u5faa\u73af\u793a\u610f\u56fe\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u672c\u6587\u8fd0\u7528\u4e24\u6b65\u6e17\u900f\u6cd5\u548c\u539f\u5b50\u5c42\u6c89\u79ef\u5de5\u827a\u6210\u529f\u5236\u5907\u4e86\u53ef\u7528\u4e8e\u94a0-\u7852\u7535\u6c60\u7684\u9ad8\u6027\u80fd\u590d\u5408\u7535\u6781\u6750\u6599\u3002\u4e24\u6b65\u6e17\u900f\u6cd5\u7684\u5e94\u7528\u6709\u6548\u63d0\u9ad8\u4e86\u6d3b\u6027\u7269\u8d28\u7684\u8d1f\u8f7d\u91cf\uff0c\u539f\u5b50\u5c42\u6c89\u79ef\u7684Al2<\/sub>O3<\/sub>\u4fdd\u62a4\u5c42\u6709\u6548\u63d0\u9ad8\u4e86\u7535\u6781\u7684\u7a33\u5b9a\u6027\u3002\u6c2e\u63ba\u6742\u5bfc\u7535\u78b3\u57fa\u4f53\u548cAl2<\/sub>O3<\/sub>\u4fdd\u62a4\u5c42\u7684\u534f\u540c\u4f5c\u7528\u4e0d\u4ec5\u53ef\u4ee5\u786e\u4fdd\u7535\u5b50\u3001\u79bb\u5b50\u7684\u5feb\u901f\u8fc1\u79fb\uff0c\u6291\u5236\u591a\u7852\u5316\u7269\u5411\u7535\u89e3\u8d28\u7684\u6eb6\u89e3\uff0c\u800c\u4e14\u53ef\u4ee5\u6709\u6548\u6291\u5236\u5145\u653e\u7535\u8fc7\u7a0b\u4e2d\u7684\u4f53\u79ef\u81a8\u80c0\u3002\u8fd9\u79cd\u901a\u8fc7\u6784\u5efa\u591a\u7ea7\u7ed3\u6784\u7684\u7b56\u7565\u4e3a\u5176\u4ed6\u9ad8\u6027\u80fd\u50a8\u80fd\u5668\u4ef6\u7684\u8bbe\u8ba1\u548c\u7814\u7a76\u63d0\u4f9b\u4e86\u65b0\u7684\u601d\u8def\u53c2\u8003\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Atomic Layer Deposition-Enabled Ultrastable Freestanding Carbon-Selenium Cathodes with High Mass Loading for Sodium-Selenium Battery\u00a0<\/a>(Nano Energy, 2017, DOI: 10.1016\/j.nanoen.2017.11.042)<\/p>\n

\u3010\u56e2\u961f\u7b80\u4ecb<\/strong>\u3011<\/p>\n

\u5f20\u57f9\u65b0<\/strong>\uff0c\u4e8c\u7ea7\u6559\u6388\uff0c\u535a\u58eb\u751f\u5bfc\u5e08\uff0c\u6df1\u5733\u5927\u5b66\u5316\u5b66\u4e0e\u73af\u5883\u5de5\u7a0b\u5b66\u9662\u9662\u957f\uff0c\u5e7f\u4e1c\u7701\u67d4\u6027\u53ef\u7a7f\u6234\u80fd\u6e90\u4e0e\u5668\u4ef6\u5de5\u7a0b\u6280\u672f\u7814\u7a76\u4e2d\u5fc3\u4e3b\u4efb\u3002\u5148\u540e\u4e3b\u6301\u6216\u53c2\u52a0\u4e86\u56fd\u5bb6\u81ea\u7136\u79d1\u5b66\u57fa\u91d1\u91cd\u70b9\u9879\u76ee\u53ca\u9762\u4e0a\u9879\u76ee\u3001\u201c973\u8ba1\u5212\u201d\u8bfe\u9898\u3001\u6559\u80b2\u90e8\u79d1\u5b66\u6280\u672f\u7814\u7a76\u91cd\u70b9\u9879\u76ee\u3001\u5e7f\u4e1c\u7701\u81ea\u7136\u79d1\u5b66\u57fa\u91d1\u7b4940\u591a\u9879\u8bfe\u9898\u3002\u5728\u65e0\u673a\u7eb3\u7c73\u6750\u6599\u3001\u9502\uff08\u94a0\uff09\u79bb\u5b50\u7535\u6c60\u3001\u592a\u9633\u80fd\u7535\u6c60\u548c\u8d85\u7ea7\u7535\u5bb9\u5668\u7b49\u9886\u57df\u505a\u51fa\u4e86\u9887\u5177\u7279\u8272\u7684\u7814\u7a76\u6210\u679c\uff0c\u5728\u56fd\u5185\u5916\u671f\u520a\u53d1\u8868\u8bba\u6587200\u591a\u7bc7\u3002<\/p>\n

\u6797\u5fd7\u7fa4<\/strong>\uff0c\u7f8e\u56fd\u4f50\u6cbb\u4e9a\u7406\u5de5\u5b66\u9662\u6559\u6388\u3001\u82f1\u56fd\u7687\u5bb6\u5316\u5b66\u5b66\u4f1a\u4f1a\u58eb\uff0c\u4ece\u4e8b\u80fd\u6e90\u8f6c\u6362\u548c\u5b58\u50a8\u7eb3\u7c73\u529f\u80fd\u6750\u6599\u3001\u534a\u5bfc\u4f53\u6709\u673a-\u65e0\u673a\u7eb3\u7c73\u590d\u5408\u6750\u6599\u3001\u590d\u6742\u7ed3\u6784\u529f\u80fd\u805a\u5408\u7269\u7b49\u65b9\u9762\u7684\u7814\u7a76\u3002\u5176\u7814\u7a76\u5df2\u83b7\u5f97\u7f8e\u56fdNSF\u3001AFOSR\u3001DOD-MURI\u7b49\u673a\u6784\u7684\u8d44\u52a9\uff0c\u5df2\u5728Science\u3001Nat. Mater.\u3001Nat. Nanotech.\u3001Sci. Adv.\u3001Phys. Rev. Lett.\u3001J. Am. Chem. Soc.\u3001Angew. Chem. Int. Ed.\u3001Adv. Mater.\u7b49\u56fd\u9645\u4e00\u6d41\u671f\u520a\u4e0a\u53d1\u8868\u5b66\u672f\u8bba\u6587185\u7bc7\u3002\u76ee\u524d\uff0c\u62c5\u4efbJournal of Materials Chemistry A\u526f\u4e3b\u7f16\u4ee5\u53caNanoscale\u7f16\u8f91\u987e\u95ee\u59d4\u5458\u4f1a\u6210\u5458\u3002<\/p>\n

\u3010\u56e2\u961f\u76f8\u5173\u9886\u57df\u5de5\u4f5c\u4ecb\u7ecd<\/strong>\u3011<\/p>\n

\u7814\u7a76\u56e2\u961f\u957f\u671f\u4ee5\u6765\u4e00\u76f4\u81f4\u529b\u4e8e\u5148\u8fdb\u7eb3\u7c73\u6750\u6599\u7684\u8bbe\u8ba1\u3001\u5408\u6210\u53ca\u5176\u5728\u65b0\u80fd\u6e90\u5668\u4ef6\u9886\u57df\u4e2d\u5e94\u7528\u7684\u7814\u7a76\u3002\u5176\u4e2d\uff0c\u5229\u7528\u9759\u7535\u7eba\u4e1d\u6cd5\uff08electrospinning\uff09\u5236\u5907\u4e86\u591a\u79cd\u9502\u79bb\u5b50\u7535\u6c60\u7684\u6b63\u3001\u8d1f\u6781\u6750\u6599\uff0c\u5982Li1.2<\/sub>Mn0.54<\/sub>Ni0.13<\/sub>Co0.13<\/sub>O2<\/sub>\/C\u53caSi\/Ni17<\/sub>Si3<\/sub>\/C\u590d\u5408\u6750\u6599\u7b49\uff0c\u4e00\u7ef4\u78b3\u7ea4\u7ef4\u9aa8\u67b6\u80fd\u591f\u6709\u6548\u63d0\u9ad8\u7535\u6781\u7684\u7535\u5b50\u3001\u79bb\u5b50\u5bfc\u7535\u6027\uff0c\u5e76\u63d0\u9ad8\u5176\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u8be5\u7cfb\u5217\u5de5\u4f5c\u53d1\u8868\u5728Acta Mater., 2016, 112, 11; J. Power Sources, 2016, 311, 35; Electrochim. Acta, 2016, 192, 385; RSC Adv., 2016, 6, 52746<\/em><\/strong>\u3002\u91c7\u7528\u539f\u5b50\u5c42\u6c89\u79ef\u6280\u672f\uff08atomic layer deposition\uff09\u53ef\u63a7\u5236\u5907\u4e86\u591a\u79cd\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u6750\u6599\uff0c\u5e76\u5c06\u5176\u5e94\u7528\u4e8e\u94a0\u79bb\u5b50\u7535\u6c60\u53ca\u9502\u7a7a\u6c14\u7535\u6c60\u7b49\u80fd\u6e90\u5668\u4ef6\u4e2d\uff0c\u8be5\u65b9\u6cd5\u80fd\u591f\u6709\u6548\u63a7\u5236\u6750\u6599\u7684\u751f\u957f\u8fc7\u7a0b\uff0c\u5e76\u53ef\u901a\u8fc7\u7b49\u79bb\u5b50\u4f53\u539f\u4f4d\u5bf9\u6750\u6599\u8fdb\u884c\u5f02\u8d28\u539f\u5b50\u63ba\u6742\uff0c\u63d0\u9ad8\u5176\u7535\u5316\u5b66\u6027\u80fd\u3002\u8be5\u7cfb\u5217\u5de5\u4f5c\u53d1\u8868\u5728J. Power Sources, 2017, 360, 215; J. Power Sources, 2017, 368, 88; Dalton Trans., 2017, 46,13101<\/em><\/strong>\u3002<\/p>\n

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