{"id":115022,"date":"2017-12-04T06:30:42","date_gmt":"2017-12-03T22:30:42","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=115022"},"modified":"2017-12-03T13:32:58","modified_gmt":"2017-12-03T05:32:58","slug":"%e5%90%89%e6%9e%97%e5%a4%a7%e5%ad%a6%e6%9d%9c%e8%8f%b2%e8%af%be%e9%a2%98%e7%bb%84adv-energy-mater-%e9%9d%9e%e6%99%b6%e9%94%a1%e5%9f%ba%e6%b0%a7%e5%8c%96%e7%89%a9%ef%bc%9a%e9%ab%98%e5%80%8d%e7%8e%87","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=115022","title":{"rendered":"\u5409\u6797\u5927\u5b66\u675c\u83f2\u8bfe\u9898\u7ec4Adv. Energy Mater.\u975e\u6676\u9521\u57fa\u6c27\u5316\u7269\uff1a\u9ad8\u500d\u7387\u8d85\u957f\u5bff\u547d\u94a0\u79bb\u5b50\u7535\u6c60\u8d1f\u6781\u6750\u6599"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u9502\u79bb\u5b50\u7535\u6c60\u5728\u5927\u89c4\u6a21\u50a8\u80fd\u9886\u57df\uff08\u7535\u52a8\u6c7d\u8f66\u548c\u50a8\u80fd\u7535\u7ad9\uff09\u7684\u53d1\u5c55\u52a0\u5feb\u4e86\u9502\u8d44\u6e90\u7684\u6d88\u8017\uff0c\u5f00\u53d1\u8d44\u6e90\u4e30\u5bcc\u3001\u5ec9\u4ef7\u7684\u50a8\u80fd\u4f53\u7cfb\u8feb\u5728\u7709\u776b\u3002\u94a0\u79bb\u5b50\u7535\u6c60\u7531\u4e8e\u8d44\u6e90\u7684\u4f18\u52bf\u4ee5\u53ca\u4e0e\u9502\u79bb\u5b50\u7535\u6c60\u7684\u76f8\u4f3c\u6027\u800c\u53d7\u5230\u5e7f\u6cdb\u5173\u6ce8\u3002\u6b63\u6781\u6750\u6599\u7535\u538b\u548c\u5bb9\u91cf\u5df2\u7ecf\u5230\u8fbe\u74f6\u9888\uff0c\u4e3a\u4e86\u63d0\u9ad8\u7535\u6c60\u4f53\u7cfb\u7684\u80fd\u91cf\u5bc6\u5ea6\u548c\u5faa\u73af\u5bff\u547d\uff0c\u5f00\u53d1\u6bd4\u5bb9\u91cf\u9ad8\u3001\u5faa\u73af\u7a33\u5b9a\u6027\u597d\u7684\u5408\u91d1\u8d1f\u6781\u6750\u6599\u5177\u6709\u91cd\u8981\u610f\u4e49\u3002\u65e9\u57281997\u5e74\uff0cY. Idota\u7b49\u4eba\u62a5\u9053\u7684\u975e\u6676\u9521\u57fa\u6c27\u5316\u7269\uff08ATCO\uff09\u5728\u9502\u79bb\u5b50\u7535\u6c60\u4e2d\u5c31\u8868\u73b0\u51fa\u826f\u597d\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002[1] <\/sup>\u4f46\u5728\u94a0\u79bb\u5b50\u7535\u6c60\u4e2d\uff0c\u7531\u4e8e\u79bb\u5b50\u7684\u534a\u5f84\u8f83\u5927\uff0c\u5bfc\u81f4\u53cd\u5e94\u8fc7\u7a0b\u4e2d\u6750\u6599\u7684\u4f53\u79ef\u81a8\u80c0\u5267\u70c8\uff0c\u7535\u6781\u66f4\u5bb9\u6613\u5f00\u88c2\u7c89\u5316\uff0c\u5faa\u73af\u5bff\u547d\u96be\u4ee5\u957f\u4e45\u3002\u6b64\u5916\uff0c\u975e\u7535\u5316\u5b66\u6d3b\u6027\u7684\u78f7\u9178\u76d0\u73bb\u7483\u57fa\u5e95\u88ab\u8ba4\u4e3a\u4f1a\u964d\u4f4e\u6750\u6599\u7684\u6bd4\u5bb9\u91cf\uff0c\u5982\u4f55\u6fc0\u6d3b\u8fd9\u90e8\u5206\u7ec4\u5206\u5bf9\u63d0\u5347\u6750\u6599\u7684\u6bd4\u5bb9\u91cf\u6709\u7740\u91cd\u8981\u610f\u4e49\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u5409\u6797\u5927\u5b66\u7269\u7406\u5b66\u9662\u65b0\u578b\u7535\u6c60\u7269\u7406\u4e0e\u6280\u672f\u6559\u80b2\u90e8\u91cd\u70b9\u5b9e\u9a8c\u5ba4\u675c\u83f2\uff08<\/strong>Fei Du<\/strong>\uff0c\u901a\u8baf\u4f5c\u8005\uff09\u6559\u6388\u7ec4<\/strong>\u62a5\u9053\u4e86\u4e00\u79cd\u975e\u6676\u9521\u57fa\u6c27\u5316\u7269\uff08ATCO\uff09\u4f5c\u4e3a\u94a0\u79bb\u5b50\u7535\u6c60\u8d1f\u6781\u6750\u6599\u53d6\u5f97\u4f18\u5f02\u7684\u7535\u5316\u5b66\u6027\u80fd\uff0c\u7814\u7a76\u4ee5\u9898\u4e3a\u201cAmorphous Tin-Based Composite Oxide: A High-Rate and Ultralong-Life Sodium-Ion-Storage Material\u201d<\/strong>\u7684\u7814\u7a76\u8bba\u6587\u53d1\u8868\u5728Advanced Energy Materials<\/strong> (doi:10.1002\/aenm.201701827 )\u4e0a\u3002<\/p>\n

\u3010\u672c\u6587\u4eae\u70b9\u3011<\/strong><\/p>\n

\u901a\u8fc7\u9ad8\u80fd\u7403\u78e8\u6cd5\u5c06\u7ed3\u6676\u6750\u6599\u975e\u6676\u5316\uff0c\u5229\u7528\u975e\u6676\u6750\u6599\u5404\u5411\u540c\u6027\u7684\u7279\u70b9\u524a\u5f31\u4e86Na-Sn\u5408\u91d1\u6cbf\u7279\u5b9a\u65b9\u5411\u7684\u4f53\u79ef\u81a8\u80c0\uff0c\u5e76\u5229\u7528\u7535\u5316\u5b66\u8fc7\u7a0b\u4e2d\u5f62\u6210\u7684\u7126\u78f7\u9178\u94a0\u8fdb\u4e00\u6b65\u7f13\u51b2\u5408\u91d1\u6750\u6599\u7684\u4f53\u79ef\u81a8\u80c0\u3002\u77f3\u58a8\u70ef\u6539\u6027\u540e\u7684ATCO\u53ef\u9006\u6bd4\u5bb9\u91cf\u53ef\u8fbe480 mAh g-1<\/sup>\uff0c\u5bf9\u5e94\u4e8e\u5408\u91d1\u5316\u548c\u8f6c\u6362\u4e24\u6b65\u53cd\u5e94\u7684\u5b9e\u73b0\uff1b2 A g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u6750\u6599\u5faa\u73af\u5bff\u547d\u53ef\u8fbe15000\u6b21\u3002\u5229\u7528ATCO\u7535\u52bf\u4f4e\u6bd4\u5bb9\u91cf\u9ad8\u7684\u4f18\u70b9\uff0c\u5206\u522b\u4e0eNa3<\/sub>V2<\/sub>(PO4<\/sub>)2<\/sub>F3<\/sub>\u548cNa3<\/sub>V2<\/sub>(PO4<\/sub>)3<\/sub>\u7ec4\u88c5\u4e86\u5168\u7535\u6c60\uff0c\u83b7\u5f97\u4e86\u8f83\u957f\u7684\u5faa\u73af\u5bff\u547d\u4e0e\u5353\u8d8a\u7684\u500d\u7387\u6027\u80fd\uff0c\u4e3a\u94a0\u79bb\u5b50\u7535\u6c60\u7684\u5b9e\u9645\u5e94\u7528\u63d0\u4f9b\u4e86\u501f\u9274\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\uff08\u6ce8\uff1a\u4ee5\u4e0b\u6240\u6709\u7684\u63d2\u56fe\u5747\u6765\u81ea\u6587\u540e\u6587\u732e\uff09<\/p>\n

\u56fe\u4e00\uff1a<\/strong>ATCO<\/strong>\u7684\u7ed3\u6784\u4e0e\u5f62\u8c8c\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a-b) \u9521\u57fa\u6c27\u5316\u7269\u7684X\u5c04\u7ebf\u884d\u5c04\u56fe\u53ca\u62c9\u66fc\u56fe\u8c31\uff0c\u7ed3\u6676Sn2<\/sub>P2<\/sub>O7<\/sub>\u3001\u77f3\u58a8\u70ef\u590d\u5408\u7ed3\u6676Sn2<\/sub>P2<\/sub>O7<\/sub>\u3001\u975e\u6676Sn2<\/sub>P2<\/sub>O7<\/sub>\u4ee5\u53ca\u77f3\u58a8\u70ef\u590d\u5408\u975e\u6676Sn2<\/sub>P2<\/sub>O7<\/sub>\u5206\u522b\u8bb0\u4e3a(c-Sn2<\/sub>P2<\/sub>O7<\/sub>\u3001c-Sn2<\/sub>P2<\/sub>O7<\/sub>\/RGO\u3001a-Sn2<\/sub>P2<\/sub>O7<\/sub>\u4ee5\u53caa-Sn2<\/sub>P2<\/sub>O7<\/sub>\/RGO)\u3002\u7ecf\u8fc7\u9ad8\u80fd\u7403\u78e8\uff0cSn2<\/sub>P2<\/sub>O7<\/sub>\u957f\u7a0b\u6709\u5e8f\u7ed3\u6784\u88ab\u7834\u574f\uff0c\u5f62\u6210\u975e\u6676\u73bb\u7483\u6001\uff0c\u4fdd\u7559\u77ed\u7a0b\u6709\u5e8f\u7ed3\u6784\uff1b<\/p>\n

(c) \u7403\u78e8\u5904\u7406\u540e\u6750\u6599\u5448\u73b0\u591a\u5b54\u7ed3\u6784\uff0c\u6709\u5229\u4e8e\u7535\u89e3\u6db2\u7684\u6d78\u6da6\uff1b<\/p>\n

(d-e) \u900f\u5c04\u7535\u955c\u7167\u7247\u8bc1\u5b9e\u4e86\u6750\u6599\u7684\u975e\u6676\u5c5e\u6027\uff1b<\/p>\n

(f) \u7403\u78e8\u540e\u975e\u6676\u6750\u6599\u76f8\u6bd4\u7ed3\u6676\u6750\u6599\u963b\u6297\u6709\u6240\u964d\u4f4e\u3002<\/p>\n

\u56fe\u4e8c\uff1aa-Sn2<\/sub>P2<\/sub>O7<\/sub>\/RGO\u7684\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

(a-b) a-Sn2<\/sub>P2<\/sub>O7<\/sub>\/RGO\u57280-3.0 V\u7535\u538b\u533a\u95f4\u7684\u5145\u653e\u7535\u66f2\u7ebf\u4ee5\u53ca\u5faa\u73af\u4f0f\u5b89\u66f2\u7ebf\u3002\u6750\u6599\u572850mA g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u53ef\u9006\u5bb9\u91cf\u53ef\u4ee5\u8fbe\u5230480 mAh g-1<\/sup>\u30021.3\/1.5 V\u548c0\/0.6 V\u7684\u6c27\u5316\u8fd8\u539f\u7535\u5b50\u5bf9\u5206\u522b\u5bf9\u5e94\u4e8e\u53cd\u5e941\u548c\u53cd\u5e942\uff1a<\/p>\n

Sn2<\/sub>P2<\/sub>O7<\/sub> + 4 Na+<\/sup> + 4 e–<\/sup> \u2194 2 Sn + a-Na4<\/sub>P2<\/sub>O7<\/sub>\u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 (1)<\/p>\n

4 Sn + 9 Na+<\/sup> + 9 e–<\/sup> \u2194 a-Na9<\/sub>Sn4<\/sub>\u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 (2)<\/p>\n

(c) \u6a2a\u6d41\u95f4\u6b47\u6ef4\u5b9a\u66f2\u7ebf\uff08GITT\uff09\u8868\u660e\u6750\u6599\u7684\u6b27\u59c6\u6781\u5316\u5f88\u5c0f\uff0c\u52a8\u529b\u5b66\u6027\u8d28\u826f\u597d\uff1b<\/p>\n

(d) a-Sn2<\/sub>P2<\/sub>O7<\/sub>\/RGO\u500d\u7387\u6027\u80fd\u4f18\u5f02\uff0c10 A g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u6bd4\u5bb9\u91cf\u4ecd\u6709165 mAh g-1<\/sup>\uff1b<\/p>\n

(e) \u6750\u6599\u57282 A g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u5faa\u73af\u5bff\u547d\u53ef\u8fbe15000\u6b21\u3002<\/p>\n

\u56fe\u4e09\uff1a<\/strong>a-Sn2<\/sub>P2<\/sub>O7<\/sub>\/RGO\u7684\u52a8\u529b\u5b66\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a-b) a-Sn2<\/sub>P2<\/sub>O7<\/sub>\/RGO\u4ece0.05\u5230200 mV s-1<\/sup>\u626b\u901f\u4e0b\u7684\u5faa\u73af\u4f0f\u5b89\u66f2\u7ebf\uff1b<\/p>\n

(c) \u5cf0\u7535\u6d41i<\/em>\u4e0e\u626b\u901fv<\/em>\u53ef\u4ee5\u7528power law: i <\/em>= avb<\/sup><\/em>\u6216\u8005log (i<\/em>) = log (a<\/em>) + b<\/em> log (v<\/em>)\u6765\u8868\u8ff0\uff0c\u56fec\u4e2d\u901a\u8fc7\u62df\u5408Log(i<\/em>)\u4e0eLog(v<\/em>)\u7684\u7ebf\u6027\u5173\u7cfb\u53d1\u73b0\uff0c\u5f53\u626b\u901f\u4f4e\u4e8e10mV s-1<\/sup>\u65f6\u659c\u7387\u4e3a0.9\uff0c\u5bf9\u5e94\u4e8e\u8868\u9762\u63a7\u5236\u8fc7\u7a0b\uff0c\u800c\u5f53\u626b\u901f\u9ad8\u4e8e10mV s-1<\/sup>\u65f6\u659c\u7387\u63a5\u8fd10.5\uff0c\u5bf9\u5e94\u4e8e\u6269\u6563\u63a7\u5236\u8fc7\u7a0b\uff1b<\/p>\n

(d) \u5f52\u4e00\u5316\u5bb9\u91cf\u4e0ev<\/em>1\/2<\/sup>\u7684\u5173\u7cfb\uff0c\u5f53\u626b\u901f\u5c0f\u65f6\uff0c\u6750\u6599\u7684\u5bb9\u91cf\u4e0ev<\/em>1\/2<\/sup>\u65e0\u7ebf\u6027\u5173\u7cfb\uff0c\u800c\u5f53\u626b\u901f\u53d8\u5927\u540e\u6750\u6599\u7684\u5bb9\u91cf\u4e0e\u626b\u901f\u6210\u7ebf\u6027\u5173\u7cfb\uff0c\u8fd9\u8868\u660e\u94a0\u79bb\u5b50\u5728\u6750\u6599\u5185\u90e8\u7684\u6269\u6563\u8fc7\u7a0b\u662f\u7535\u5316\u5b66\u53cd\u5e94\u7684\u51b3\u901f\u6b65\u9aa4\uff1b<\/p>\n

(e-f) \u5b9a\u91cf\u5206\u6790\u8868\u660e\u968f\u7740\u626b\u901f\u7684\u589e\u5927\uff0c\u53d7\u6269\u6563\u63a7\u5236\u7684\u5bb9\u91cf\u90e8\u5206\u660e\u663e\u964d\u4f4e\uff0c\u800c\u8d5d\u7535\u5bb9\u90e8\u5206\u7531\u4e8e\u52a8\u529b\u5b66\u6027\u8d28\u597d\u800c\u51e0\u4e4e\u4e0d\u53d7\u626b\u901f\u5f71\u54cd\uff0c\u56e0\u6b64\u8d5d\u7535\u5bb9\u90e8\u5206\u6240\u5360\u6bd4\u91cd\u660e\u663e\u63d0\u9ad8\u3002<\/p>\n

\u56fe\u56db\uff1a\u5168\u7535\u6c60\u7684\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

(a) a-Sn2<\/sub>P2<\/sub>O7<\/sub>\/RGO\u4e0eNa3<\/sub>V2<\/sub>(PO4<\/sub>)2<\/sub>F3<\/sub>\/C\u5168\u7535\u6c60(\u7b80\u8bb0\u4e3aSPO||NVPF)\u572850 mA g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u5145\u653e\u7535\u66f2\u7ebf\uff0c\u653e\u7535\u4e2d\u503c\u7535\u538b\u53ef\u4ee5\u8fbe\u52303.3 V\uff1b<\/p>\n

(b) a-Sn2<\/sub>P2<\/sub>O7<\/sub>\/RGO\u4e0eNa3<\/sub>V2<\/sub>(PO4<\/sub>)3<\/sub>\/C\u5168\u7535\u6c60(\u7b80\u8bb0\u4e3aSPO||NVP)\u572850 mA g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u5145\u653e\u7535\u66f2\u7ebf\uff0c\u653e\u7535\u4e2d\u503c\u7535\u538b\u53ef\u4ee5\u8fbe\u52302.9 V\uff1b<\/p>\n

(c) SPO||NVPF\u4ee5\u53caSPO||NVP\u5168\u7535\u6c60\u7684\u500d\u7387\u6027\u80fd\uff0c\u572860 C (6 A g-1<\/sup>)\u7684\u500d\u7387\u4e0b\u6bd4\u5bb9\u91cf\u4ecd\u5206\u522b\u53ef\u4ee580\u548c60 mAh g-1<\/sup>\uff1b<\/p>\n

(d) \u5168\u7535\u6c60\u7684\u62c9\u8d21\u66f2\u7ebf\uff0c\u529f\u7387\u5bc6\u5ea6\u53ef\u4ee5\u8fbe\u52309000 W kg-1<\/sup>\uff0c\u80fd\u91cf\u5bc6\u5ea6\u5206\u522b\u4e3a160\u548c140 Wh kg-1<\/sup>\uff1b<\/p>\n

(e) \u5168\u7535\u6c60\u572810 C\u500d\u7387\u4e0b\u7684\u5faa\u73af\u6027\u80fd\uff0cSPO||NVP\u7ecf\u8fc71000\u6b21\u5faa\u73af\u5bb9\u91cf\u4fdd\u6301\u7387\u63a5\u8fd1100%\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1aAmorphous Tin-Based Composite Oxide: A High-Rate and Ultralong-Life Sodium-Ion-Storage Material<\/a>\uff08Advanced Energy Materials\uff0c2017\uff0cdoi:10.1002\/aenm.201701827\uff09<\/p>\n

\u53c2\u8003\u6587\u732e<\/p>\n

[1] Y. Idota, T. Kubota, et al.<\/em> Tin-Based Amorphous Oxide: A High-Capacity Lithium-Ion-Storage Material, Science<\/em>\u00a0,\u00a01997, 276<\/em>, 1395.<\/p>\n

\u3010\u5bfc\u5e08\u4ecb\u7ecd\u3011<\/strong><\/p>\n

\"\"<\/p>\n

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