{"id":118105,"date":"2017-12-21T14:00:07","date_gmt":"2017-12-21T06:00:07","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=118105"},"modified":"2017-12-20T22:18:24","modified_gmt":"2017-12-20T14:18:24","slug":"%e5%8d%97%e4%ba%ac%e7%90%86%e5%b7%a5%e5%a4%a7%e5%ad%a6%e5%a4%8f%e6%99%96adv-funct-mater-%ef%bc%9a-%e8%87%aa%e6%94%af%e6%92%91%e5%a4%9a%e5%ad%94licoo2%e7%ba%b3%e7%b1%b3%e7%89%87%e9%98%b5%e5%88%97","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=118105","title":{"rendered":"\u5357\u4eac\u7406\u5de5\u5927\u5b66\u590f\u6656Adv. Funct. Mater.\uff1a \u81ea\u652f\u6491\u591a\u5b54LiCoO2\u7eb3\u7c73\u7247\u9635\u5217\u7528\u4f5c\u67d4\u6027\u9502\u79bb\u5b50\u7535\u6c60\u4e09\u7ef4\u6b63\u6781"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u968f\u7740\u793e\u4f1a\u7684\u53d1\u5c55\uff0c\u5bf9\u67d4\u6027\u7535\u5b50\u4ea7\u54c1\u548c\u53ef\u7a7f\u6234\u8bbe\u5907\u9700\u6c42\u91cf\u7684\u4e0d\u65ad\u589e\u52a0\u63a8\u52a8\u7740\u67d4\u6027\u9502\u79bb\u5b50\u7535\u6c60\u7684\u53d1\u5c55\u3002\u67d4\u6027\u9502\u79bb\u5b50\u7535\u6c60\u9700\u8981\u5728\u4e00\u5b9a\u7a0b\u5ea6\u5f62\u53d8\uff08\u6298\u53e0\u6216\u5f2f\u66f2\uff09\u4e0b\u6b63\u5e38\u8fdb\u884c\u7535\u5316\u5b66\u80fd\u91cf\u7684\u5b58\u50a8\u3002\u5c31\u4f20\u7edf\u7684\u9502\u79bb\u5b50\u7535\u6c60\u7535\u6781\u800c\u8a00\uff0c\u5b83\u662f\u901a\u8fc7\u5728\u91d1\u5c5e\u7b94\u4e0a\u6d82\u8986\u542b\u6709\u6d3b\u6027\u7269\u8d28\u3001\u5bfc\u7535\u5242\u548c\u7c98\u5408\u5242\u7684\u6d46\u6599\u5236\u5907\u800c\u6210\uff0c\u56e0\u5176\u672c\u8eab\u662f\u975e\u67d4\u6027\u7684\u7535\u6781\u7ed3\u6784\uff0c\u56e0\u6b64\u4e0d\u80fd\u6ee1\u8db3\u67d4\u6027\u7535\u5b50\u5668\u4ef6\u7684\u9700\u6c42\u3002\u7136\u540e\uff0c\u4f7f\u7528\u78b3\u7eb3\u7c73\u7ba1\u548c\u7eb3\u7c73\u7ea4\u7ef4\u7ec7\u7269\u7b49\u81ea\u652f\u6491\u7684\u819c\u7535\u6781\u6216\u8005\u662f\u5728\u67d4\u6027\u886c\u5e95\u4e0a\u751f\u957f\u6d3b\u6027\u7269\u8d28\u7b49\u65b9\u6cd5\u4fc3\u8fdb\u4e86\u67d4\u6027\u9502\u79bb\u5b50\u7535\u6c60\u7684\u53d1\u5c55\u3002\u5728\u67d4\u6027\u886c\u5e95\u4e0a\u751f\u957f\u6d3b\u6027\u7269\u8d28\u7684\u7eb3\u7c73\u9635\u5217\u66f4\u662f\u53ef\u4ee5\u5f62\u6210\u4e00\u7c7b\u4e09\u7ef4\u67d4\u6027\u7535\u6781\u3002\u5176\u4e2d\uff0c\u7eb3\u7c73\u9635\u5217\u5728\u67d4\u6027\u886c\u5e95\u4e0a\u7684\u76f4\u63a5\u751f\u957f\u53ef\u4ee5\u4f7f\u5f97\u6d3b\u6027\u6750\u6599\u548c\u886c\u5e95\u4e4b\u95f4\u7d27\u5bc6\u63a5\u89e6\uff0c\u4ece\u800c\u6539\u5584\u5176\u673a\u68b0\u5f3a\u5ea6\u548c\u67d4\u6027\uff1b\u5bfc\u7535\u886c\u5e95\u7684\u7535\u5b50\u901a\u9053\uff0c\u51cf\u5c0f\u7684Li+<\/sup>\u6269\u6563\u8ddd\u79bb\u4ee5\u53ca\u4e09\u7ef4\u7eb3\u7c73\u7ed3\u6784\u7684\u5927\u6bd4\u8868\u9762\u79ef\u5f88\u597d\u5730\u6ee1\u8db3\u4e86\u5bf9\u4e8e\u9ad8\u80fd\u91cf\u548c\u9ad8\u529f\u7387\u7684\u67d4\u6027\u7535\u5b50\u4ea7\u54c1\u65e5\u76ca\u589e\u957f\u7684\u9700\u6c42\uff1b\u6b64\u5916\uff0c\u5355\u4e2a\u7eb3\u7c73\u9635\u5217\u4e4b\u95f4\u8db3\u591f\u7684\u81ea\u7531\u7a7a\u95f4\u8fd8\u53ef\u7528\u4e8e\u7f13\u89e3\u5145\u653e\u7535\u8fc7\u7a0b\u4e2d\u4f53\u79ef\u53d8\u5316\u5e26\u6765\u7684\u5e94\u53d8\uff0c\u4ece\u800c\u63d0\u9ad8\u7535\u6781\u7684\u957f\u671f\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u56e0\u6b64\uff0c\u81f4\u529b\u4e8e\u5728\u5404\u79cd\u67d4\u6027\u886c\u5e95\uff08\u5982\uff1a\u78b3\u5e03\u548c\u91d1\u5c5e\u7b94\uff09\u4e0a\u5236\u9020\u4e09\u7ef4\u81ea\u652f\u6491\u7eb3\u7c73\u9635\u5217\u7535\u6781\u6210\u4e3a\u4e86\u7814\u7a76\u8005\u4eec\u7814\u7a76\u7684\u91cd\u70b9\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u5357\u4eac\u7406\u5de5\u5927\u5b66\u590f\u6656\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09\u548c\u859b\u4eae\u535a\u58eb\u7b49\u4eba<\/strong>\u5728Advanced Functional Materials<\/strong>\u4e0a\u53d1\u8868\u4e86\u4e00\u7bc7\u9898\u4e3a\u201cSelf-Standing Porous LiCoO2<\/sub> Nanosheet Arrays as 3D Cathodes for Flexible Li-Ion Batteries<\/strong>\u201d\u7684\u7814\u7a76\u6210\u679c\u3002\u5728\u8fd9\u9879\u5de5\u4f5c\u4e2d\uff0c\u8be5\u7814\u7a76\u56e2\u961f\u901a\u8fc7\u7b80\u5355\u7684\u201c\u6c34\u70ed\u9502\u5316\u201d\u6cd5\uff0c\u4f7f\u7528Co3<\/sub><\/strong>O4<\/sub><\/strong>\u7eb3\u7c73\u7247\u9635\u5217\u4f5c\u4e3a\u6a21\u677f\uff0c\u7136\u540e\u5728\u7a7a\u6c14\u4e2d\u5feb\u901f\u9000\u706b\uff0c\u5c06\u591a\u5b54LiCoO2<\/sub><\/strong>\u7eb3\u7c73\u7247\u9635\u5217\u751f\u957f\u5728\u9540\u91d1\u4e0d\u9508\u94a2\uff08Au\/SS\uff09\u886c\u5e95\u4e0a\u3002\u4e0d\u542b\u7c98\u5408\u5242\u7684\u81ea\u652f\u6491LiCoO2<\/sub><\/strong>\u7eb3\u7c73\u7247\u9635\u5217\u7684\u4e09\u7ef4\u6b63\u6781\u53ef\u4ee5\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u500d\u7387\u6027\u80fd\u548c\u5faa\u73af\u7a33\u5b9a\u6027\uff1b\u5f53\u5176\u572810C\u901f\u7387\u4e0b\u5faa\u73af\u65f6\u53ef\u4ee5\u63d0\u4f9b104.6mA h g-1<\/sup>\u7684\u9ad8\u53ef\u9006\u5bb9\u91cf\uff0c\u57280.1C\u500d\u7387\u4e0b\u5faa\u73af1000\u5468\u671f\u540e\u4ecd\u53ef\u5b9e\u73b081.8\uff05\u7684\u5bb9\u91cf\u4fdd\u6301\u7387\u3002\u6b64\u5916\uff0c\u901a\u8fc7\u4e0eLi4<\/sub>Ti5<\/sub>O12<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\u8d1f\u6781\u76f8\u7ed3\u5408\uff0c\u8be5\u7814\u7a76\u56e2\u961f\u8fd8\u6784\u5efa\u4e86\u57fa\u4e8eLiCoO2<\/sub>\/\/Li4<\/sub>Ti5<\/sub>O12<\/sub>\u5168\u7eb3\u7c73\u7247\u9635\u5217\u7684\u67d4\u6027\u9502\u79bb\u5b50\u7535\u6c60\u3002\u5f97\u76ca\u4e8e\u6b63\u8d1f\u6781\u6240\u63d0\u4f9b\u7684\u7684\u4e09\u7ef4\u7eb3\u7c73\u7ed3\u6784\u7684\u4f18\u52bf\uff0c\u67d4\u6027LiCoO2<\/sub>\/\/Li4<\/sub>Ti5<\/sub>O12<\/sub>\u5168\u7535\u6c60\u53ef\u4ee5\u57280.1C\u500d\u7387\u4e0b\u63d0\u4f9b130.7 mA h g-1<\/sup>\u7684\u8f83\u5927\u53ef\u9006\u5bb9\u91cf\uff0c\u5faa\u73af1000\u5468\u671f\u540e\u4ecd\u5177\u670980.5\uff05\u7684\u5bb9\u91cf\u4fdd\u6301\u7387\uff0c\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u5faa\u73af\u7a33\u5b9a\u6027\uff0c\u8fd9\u4f7f\u5176\u5728\u67d4\u6027\u9502\u79bb\u5b50\u7535\u6c60\u4e2d\u7684\u5e94\u7528\u4e2d\u8868\u73b0\u51fa\u4e86\u826f\u597d\u7684\u5e94\u7528\u524d\u666f\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00<\/strong> L-LiCoO2<\/sub><\/strong>\u7eb3\u7c73\u7247\u9635\u5217\u5408\u6210\u8fc7\u7a0b\u793a\u610f\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe\u4e8c<\/strong> (I) Co3<\/sub>O4<\/sub><\/strong>\uff0c<\/strong>(II) S-LiCoO2<\/sub><\/strong>\u548c<\/strong>(III) L-LiCoO2<\/sub><\/strong>\u7eb3\u7c73\u7247\u9635\u5217\u7684\u7ed3\u6784\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

a\uff09(I) Au\/SS\u886c\u5e95\uff0c(II) Co3<\/sub>O4<\/sub>\uff0c(III) S-LiCoO2<\/sub>\u548c(IV) L-LiCoO2<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\u7684XRD\u56fe\u8c31\uff1b<\/p>\n

b\uff09(I) Co3<\/sub>O4<\/sub>\uff0c(II) S-LiCoO2<\/sub>\u548c(III) L-LiCoO2<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\u7684\u62c9\u66fc\u5149\u8c31\uff1b<\/p>\n

c\uff09Co3<\/sub>O4<\/sub>\uff0cS-LiCoO2<\/sub>\u548cL-LiCoO2<\/sub>\u7684\u539f\u5b50\u4f4d\u7f6e\uff0c\u5316\u5408\u4ef7\u548c\u5149\u5b66\u632f\u52a8\u6a21\u5f0f\u7684\u603b\u7ed3\uff1bd\uff09\u4eceCo3<\/sub>O4<\/sub>\u5230S-LiCoO2<\/sub>\u548c\u4eceS-LiCoO2<\/sub>\u5230L-LiCoO2<\/sub>\u7684\u76f8\u53d8\u548c\u7ed3\u6784\u91cd\u6392\u7684\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe\u4e09<\/strong> Co3<\/sub>O4<\/sub><\/strong>\uff0c<\/strong>S-LiCoO2<\/sub><\/strong>\u548c<\/strong>L-LiCoO2<\/sub><\/strong>\u7eb3\u7c73\u7247\u9635\u5217\u7684\u5f62\u8c8c\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

a,d) Co3<\/sub>O4<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\uff0cb,e) S-LiCoO2<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\u548cc,f) L-LiCoO2<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\u7684FESEM\u56fe\u50cf\uff1b<\/p>\n

g\uff09\u5355\u4e00Co3<\/sub>O4<\/sub>\u7eb3\u7c73\u7247\u7684TEM\u56fe\u50cf\uff1b<\/p>\n

h\uff09\u5355\u4e2aCo3<\/sub>O4<\/sub>\u7eb3\u7c73\u9897\u7c92\u7684HRTEM\u56fe\u50cf\uff08\u5de6\u4e0b\u63d2\u56fe\uff1a\u7ea2\u8272\u6b63\u65b9\u5f62\u533a\u57df\u7684\u653e\u5927\u56fe\u50cf\uff1b\u53f3\u4e0b\u63d2\u56fe\uff1a\u5bf9\u5e94\u7684FFT\u56fe\u50cf\uff09\uff1b<\/p>\n

i\uff09Co3<\/sub>O4<\/sub>\u7eb3\u7c73\u7247\u7684SAED\u56fe\u6848\uff1b<\/p>\n

j\uff09\u5355\u4e2aL-LiCoO2<\/sub>\u7eb3\u7c73\u7247\u7684TEM\u56fe\u50cf\uff1b<\/p>\n

k\uff09\u5355\u4e2aL-LiCoO2<\/sub>\u7eb3\u7c73\u9897\u7c92\u7684HRTEM\u56fe\u50cf\uff08\u5de6\u4e0b\u63d2\u56fe\uff1a\u84dd\u8272\u65b9\u5f62\u533a\u57df\u7684\u653e\u5927\u56fe\u50cf\uff1b\u53f3\u4e0b\u63d2\u56fe\uff1a\u5bf9\u5e94\u7684FFT\u56fe\u50cf\uff09\uff1b<\/p>\n

l\uff09L-LiCoO2<\/sub>\u7eb3\u7c73\u7247\u7684SAED\u56fe\u6848\u3002\u00a0<\/strong><\/p>\n

\u56fe\u56db \u4e0d\u540c\u6e29\u5ea6\u4e0b\u5236\u5907\u6240\u5f97<\/strong>L-LiCoO2<\/sub><\/strong>\u7eb3\u7c73\u7247\u9635\u5217\u7684\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

a\uff09\u4e0d\u540c\u6e29\u5ea6\u4e0b\u5236\u5907\u6240\u5f97L-LiCoO2<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\u5176\u7535\u6781\u7684\u5145\u7535\/\u653e\u7535\u66f2\u7ebf\uff08\u7535\u538b\u8303\u56f4\u4e3a3~4.2 V\uff0c0.1C\u500d\u7387\uff09\uff1b<\/p>\n

b\uff09750\u2103 L-LiCoO2<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\u7535\u6781\u5728\u7535\u538b\u8303\u56f43~4.2V\u4e4b\u95f4\u4e0d\u540c\u626b\u63cf\u901f\u7387\u4e0b\u7684CV\u66f2\u7ebf\uff08\u5206\u522b\u4e3a0.1 mV s-1<\/sup>, 0.2 mV s-1<\/sup>, 0.5 mV s-1<\/sup>\uff09\uff1b<\/p>\n

c\uff09650 \u2103,700 \u2103,750 \u2103\u548c800 \u2103 L-LiCoO2<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\u7535\u6781\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u6bd4\u8f83\uff1b<\/p>\n

d\uff09750 \u2103 L-LiCoO2<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\u7535\u6781\u7684\u500d\u7387\u6027\u80fd\u3002<\/p>\n

\u56fe\u4e94<\/strong> \u67d4\u6027<\/strong>LiCoO2<\/sub>\/\/Li4<\/sub>Ti5<\/sub>O12<\/sub><\/strong>\u5168\u7535\u6c60\u7684\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

a\uff09\u67d4\u6027LiCoO2<\/sub>\/\/Li4<\/sub>Ti5<\/sub>O12<\/sub>\u5168\u7535\u6c60\u5c01\u88c5\u5de5\u827a\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

b\uff09L-LiCoO2<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\u7535\u6781\uff0cLi4<\/sub>Ti5<\/sub>O12<\/sub>\u7eb3\u7c73\u7247\u9635\u5217\u7535\u6781\u548c\u57fa\u4e8e\u5168\u7eb3\u7c73\u7247\u9635\u5217\u7684LiCoO2<\/sub>\/\/Li4<\/sub>Ti5<\/sub>O12<\/sub>\u5168\u7535\u6c60\u7684\u5145\u7535\/\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

c\uff09LiCoO2<\/sub>\/\/Li4<\/sub>Ti5<\/sub>O12<\/sub>\u5168\u7535\u6c60\u7684\u5faa\u73af\u7a33\u5b9a\u6027\uff08\u63d2\u56fe\uff1a\u5168\u7535\u6c60\u8bbe\u5907\u70b9\u4eae\u4e86\u4e00\u4e2aLED\uff09\uff1b<\/p>\n

d\uff09LiCoO2<\/sub>\/\/Li4<\/sub>Ti5<\/sub>O12<\/sub>\u5168\u7535\u6c60\u4e0d\u540c\u500d\u7387\u4e0b\u7684\u5145\u7535\/\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

e\uff09LiCoO2<\/sub>\/\/Li4<\/sub>Ti5<\/sub>O12<\/sub>\u5168\u7535\u6c60\u7684\u500d\u7387\u6027\u80fd\u3002<\/p>\n

\u56fe\u516d<\/strong> LiCoO2<\/sub>\/\/Li4<\/sub>Ti5<\/sub>O12<\/sub><\/strong>\u5168\u7535\u6c60\u7684\u67d4\u6027\u6d4b\u8bd5<\/strong><\/p>\n

\"\"<\/p>\n

a\uff09LiCoO2<\/sub>\/\/Li4<\/sub>Ti5<\/sub>O12<\/sub>\u5168\u7535\u6c60\u5728\u4e0d\u540c\u5f2f\u66f2\u72b6\u6001\u4e0b\u70b9\u4eaeLED\u7684\u7167\u7247\uff1b<\/p>\n

b\uff09\u4e0e\u5e38\u89c4\u7535\u6781\u76f8\u6bd4\uff0c\u81ea\u652f\u6491\u4e09\u7ef4\u7535\u6781\u5177\u6709\u4f18\u5f02\u67d4\u6027\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

c\uff09\u572810 mm\u548c14 mm\u7684\u4e0d\u540c\u5f2f\u66f2\u534a\u5f84\u4e0b\uff0cLiCoO2<\/sub>\/\/Li4<\/sub>Ti5<\/sub>O12<\/sub>\u5168\u7535\u6c60\u7684\u5faa\u73af\u7a33\u5b9a\u6027\uff1b<\/p>\n

d\uff09\u57fa\u4e8e\u5168\u7eb3\u7c73\u7247\u9635\u5217\u7684\u5168\u7535\u6c60\u5176\u9ad8\u6548\u6c27\u5316\u8fd8\u539f\u53cd\u5e94\u548c\u5feb\u901f\u7535\u8377\u4f20\u8f93\u7684\u793a\u610f\u56fe\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Self-Standing Porous LiCoO2<\/sub><\/strong>\u00a0Nanosheet Arrays as 3D Cathodes for Flexible Li-Ion Batteries\u00a0<\/a>\uff08Adv. Funct. Mater. 2018, DOI: 10.1002\/adfm.201705836\uff09<\/p>\n

\u7b2c\u4e00\u4f5c\u8005\u7b80\u4ecb<\/strong><\/p>\n

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\u901a\u8baf\u4f5c\u8005\u7b80\u4ecb<\/strong><\/p>\n

\u590f\u6656<\/strong> \u7537<\/strong> \u6559\u6388<\/strong> \u535a\u58eb\u751f\u5bfc\u5e08<\/strong> \u5357\u4eac\u7406\u5de5\u5927\u5b66\u683c\u83b1\u7279\u7eb3\u7c73\u79d1\u6280\u7814\u7a76\u6240\u7eb3\u7c73\u80fd\u6e90\u6750\u6599\uff08<\/strong>NEM<\/strong>\uff09\u7814\u7a76\u7ec4\u8d1f\u8d23\u4eba<\/strong><\/p>\n

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