{"id":119954,"date":"2018-01-06T06:30:18","date_gmt":"2018-01-05T22:30:18","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=119954"},"modified":"2018-01-04T23:15:16","modified_gmt":"2018-01-04T15:15:16","slug":"adv-energy-mater-%ef%bc%9amos2%e7%9f%b3%e5%a2%a8%e7%83%af%e7%ba%b3%e7%b1%b3%e7%89%87%e5%9c%a8%e9%ab%98%e5%80%8d%e7%8e%87%e6%80%a7%e8%83%bd%e9%92%a0%e7%a6%bb%e5%ad%90%e7%94%b5%e6%b1%a0%e4%b8%8a","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=119954","title":{"rendered":"Adv. Energy Mater.\uff1aMoS2\/\u77f3\u58a8\u70ef\u7eb3\u7c73\u7247\u5728\u9ad8\u500d\u7387\u6027\u80fd\u94a0\u79bb\u5b50\u7535\u6c60\u4e0a\u7684\u5e94\u7528\u7814\u7a76"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011
\n <\/strong><\/p>\n

\u5730\u7403\u4e0a\u4e30\u5bcc\u7684\u94a0\u8d44\u6e90\u50a8\u91cf\uff0c\u4f7f\u5f97\u53ef\u5145\u7535\u94a0\u79bb\u5b50\u7535\u6c60\u5728\u5927\u89c4\u6a21\u80fd\u91cf\u50a8\u5b58\u9886\u57df\u663e\u793a\u51fa\u5de8\u5927\u7684\u6f5c\u80fd\u3002\u4f46\u662f\uff0c\u76f8\u5bf9\u8f83\u5927\u7684\u79bb\u5b50\u534a\u5f84\u5bfc\u81f4\u94a0\u79bb\u5b50\u7535\u6c60\uff08SIBs\uff09\u7684\u6bd4\u5bb9\u91cf\u3001\u5faa\u73af\u6027\u80fd\u548c\u500d\u7387\u6027\u80fd\u4e0e\u9502\u79bb\u5b50\u7535\u6c60\uff08LIBs\uff09\u4e4b\u95f4\u5747\u5b58\u5728\u4e00\u5b9a\u7684\u5dee\u8ddd\u3002\u7814\u7a76\u53d1\u73b0\uff1a\u4e8c\u7ef4\u5c42\u72b6\u6750\u6599\u4e0e\u77f3\u58a8\u7684\u7ed3\u5408\u53ef\u4ee5\u6709\u6548\u6539\u5584\u6750\u6599\u7684\u50a8\u94a0\u6027\u80fd\u3002\u5728\u76ee\u524d\u5e7f\u6cdb\u7814\u7a76\u7684\u4e8c\u7ef4\u5c42\u72b6\u6750\u6599\u4e2d\uff0cMoS2<\/sub>\u7684\u7406\u8bba\u53ef\u9006\u5bb9\u91cf\u9ad8\u8fbe670 mAh\u00b7g-1<\/sup>\uff0c\u5177\u5907\u4f18\u5f02\u7684\u50a8\u94a0\u6f5c\u80fd\u3002\u9700\u8981\u6307\u51fa\u7684\u662f\uff1aMoS2<\/sub>\u7684\u5bfc\u7535\u6027\u8f83\u5dee\uff0c\u50a8\u94a0\u8fc7\u7a0b\u4e2d\u7ed3\u6784\u4f1a\u53d1\u751f\u660e\u663e\u7684\u53d8\u5316\uff0c\u56e0\u6b64\u5b9e\u9645\u7535\u5316\u5b66\u50a8\u94a0\u6027\u80fd\u5e76\u4e0d\u7406\u60f3\u3002\u77f3\u58a8\u70ef\u5177\u5907\u4f18\u5f02\u7684\u673a\u68b0\u6027\u80fd\u548c\u7535\u5b66\u6027\u80fd\uff0c\u901a\u8fc7\u4e0eMoS2<\/sub>\u7684\u590d\u5408\u53ef\u4ee5\u6709\u6548\u63d0\u9ad8MoS2<\/sub>\u7684\u7684\u50a8\u94a0\u6027\u80fd\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u4e2d\u5357\u5927\u5b66\u7684\u738b\u6d77\u71d5\u526f\u6559\u6388<\/strong>\u548c\u6606\u58eb\u5170\u5927\u5b66\u7684\u738b\u8fde\u6d32\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u7b49\uff0c\u5728Adv. Energy Mater.<\/strong>\u4e0a\u53d1\u8868\u4e86\u9898\u4e3a\u201cMoS2<\/sub>\/Graphene Nanosheets from Commercial Bulky MoS2<\/sub> and Graphite as Anode Materials for High Rate Sodium-Ion Batteries\u201d <\/strong>\u7684\u7814\u7a76\u8bba\u6587\uff0c\u62a5\u9053\u4e86MoS2<\/sub>\/\u77f3\u58a8\u70ef\u590d\u5408\u6750\u6599\u5728\u9ad8\u6027\u80fd\u94a0\u79bb\u5b50\u7535\u6c60\u4e2d\u5e94\u7528\u7684\u6700\u65b0\u7814\u7a76\u8fdb\u5c55\u3002\u7814\u7a76\u4eba\u5458\u4ee5\u5e02\u552e\u7684MoS2<\/sub>\u5757\u4f53\u548c\u77f3\u58a8\u4e3a\u539f\u6599\uff0c\u501f\u52a9\u7403\u78e8\u5f15\u53d1\u7684\u5316\u5b66\u63d2\u5c42\u548c\u7269\u7406\u5265\u79bb\uff0c\u6210\u529f\u5236\u5907\u4e86MoS2<\/sub>\/\u77f3\u58a8\u70ef\u7eb3\u7c73\u7247\u590d\u5408\u6750\u6599\u3002\u7814\u7a76\u53d1\u73b0\uff1a\u8be5\u65b9\u6cd5\u83b7\u5f97\u7684MoS2<\/sub>\/\u77f3\u58a8\u70ef\u6750\u6599\u5177\u6709\u4f18\u5f02\u7684\u500d\u7387\u6027\u80fd\u548c\u5faa\u73af\u7a33\u5b9a\u6027\uff1b\u5f53\u7535\u6d41\u5bc6\u5ea6\u4e3a20 A\u00b7g-1<\/sup>\u65f6\uff0c\u50a8\u94a0\u5bb9\u91cf\u9ad8\u8fbe284 mAh\u00b7g-1<\/sup>\uff1b\u5f53\u7535\u6d41\u5bc6\u5ea6\u4e3a50 A\u00b7g-1<\/sup>\u65f6\uff0c\u4ecd\u53ef\u4fdd\u6301201 mAh\u00b7g-1<\/sup>\u7684\u9ad8\u653e\u7535\u5bb9\u91cf\uff1b\u5f53\u7535\u6d41\u5bc6\u5ea6\u4e3a0.3 A\u00b7g-1<\/sup>\u65f6\uff0c\u5faa\u73af250\u5708\u540e\u5bb9\u91cf\u4fdd\u6301\u7387\u9ad8\u8fbe95 %\u3002\u7406\u8bba\u8ba1\u7b97\u53d1\u73b0\uff1a\u7f3a\u9677\u53ca\u542b\u6c27\u5b98\u80fd\u56e2\u8f83\u5c11\u7684MoS2<\/sub>\/\u77f3\u58a8\u70ef\u590d\u5408\u6750\u6599\u5177\u6709\u66f4\u9ad8\u7684\u79bb\u5b50\u6269\u6563\u7cfb\u6570\u53ca\u7535\u5b50\u7535\u5bfc\u7387\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe-<\/strong>1. MoS2<\/sub>\/G<\/strong>\u7eb3\u7c73\u7247\u7684\u5408\u6210\u793a\u610f\u56fe<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

\u56fe-<\/strong>2. MoS2<\/sub><\/strong>\u53ca\u77f3\u58a8\u70ef\u7eb3\u7c73\u7247\u7684<\/strong>SEM<\/strong>\u56fe\u50cf<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

(a) \u5e02\u552e\u5757\u72b6\u77f3\u58a8\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

(b) \u5b9e\u9a8c\u5236\u5907\u7684\u77f3\u58a8\u70ef\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

(c) \u5b9e\u9a8c\u5236\u5907\u7684\u77f3\u58a8\u70ef\u7684AFM\u56fe\u50cf\uff1b<\/p>\n

(d) \u5e02\u552eMoS2<\/sub>\u5757\u4f53\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

(e) \u5b9e\u9a8c\u5236\u5907\u7684MoS2<\/sub>\u7eb3\u7c73\u7247\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

(f) \u5b9e\u9a8c\u5236\u5907MoS2<\/sub>\u7684AFM\u56fe\u50cf\uff1b<\/p>\n

(g) MoS2<\/sub>\/G\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

(h) MoS2<\/sub>\/GO\u7684SEM\u56fe\u50cf\u3002<\/p>\n

\u56fe-<\/strong>3.\u00a0<\/strong>\u5b9e\u9a8c\u6d4b\u5f97\u7684<\/strong>TEM<\/strong>\u3001<\/strong>HRTEM<\/strong>\u53ca<\/strong>STEM-EDS<\/strong>\u56fe\u50cf<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

(a)-(b) \u5b9e\u9a8c\u5236\u5907\u7684\u77f3\u58a8\u70ef\u7684TEM\u56fe\u50cf\uff1b<\/p>\n

(c) \u5b9e\u9a8c\u5236\u7684\u77f3\u58a8\u70ef\u7684HRTEM\u56fe\u50cf\uff1b<\/p>\n

(d)-(e) \u5b9e\u9a8c\u5236\u5907\u7684MoS2<\/sub>\u7684TEM\u56fe\u50cf\uff1b<\/p>\n

(f) \u5b9e\u9a8c\u5236\u5907\u7684MoS2<\/sub>\u7684HRTEM\u56fe\u50cf\uff1b<\/p>\n

(g)-(h) MoS2<\/sub>\/G\u7684TEM\u56fe\u50cf\uff1b<\/p>\n

(i) MoS2<\/sub>\/G\u7684HRTEM\u56fe\u50cf\uff1b<\/p>\n

(j) (k) (l) (m) MoS2<\/sub>\/G\u7684STEM-EDS\u56fe\u50cf\u3002<\/p>\n

\u56fe-<\/strong>4.<\/strong>\u00a0MoS2<\/sub>\/<\/strong>\u77f3\u58a8\u70ef\u7eb3\u7c73\u7247\u7684\u5faa\u73af\u6027\u80fd\u7814\u7a76<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

(a) \u7535\u6d41\u5bc6\u5ea6\u4e3a 100 mA.g-1<\/sup>\u65f6\uff0cMoS2<\/sub>\/G\u590d\u5408\u6750\u6599\u7684\u5faa\u73af\u6027\u80fd\uff1b<\/p>\n

(b) \u7535\u6d41\u5bc6\u5ea6\u4e3a300 mA.g-1<\/sup>\u65f6\uff0cMoS2<\/sub>\/G\u590d\u5408\u6750\u6599\u7684\u5faa\u73af\u6027\u80fd\uff1b<\/p>\n

(c) \u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\uff0cMoS2<\/sub>\/G\u7eb3\u7c73\u7247\u548cMoS2<\/sub>\/GO\u7eb3\u7c73\u7247\u7684\u500d\u7387\u6027\u80fd\uff1b<\/p>\n

(d) \u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\uff0c\u6587\u732e\u548c\u5b9e\u9a8c\u7684MoS2<\/sub>\u57fa\u94a0\u79bb\u5b50\u8d1f\u6781\u6750\u6599\u7684\u500d\u7387\u6027\u80fd\u5bf9\u6bd4\u56fe\u3002<\/p>\n

\u56fe-<\/strong>5. MoS2<\/sub>\/<\/strong>\u77f3\u58a8\u70ef\u7eb3\u7c73\u7247\u7684\u7ed3\u6784\u8868\u5f81<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

(a) MoS2<\/sub>\uff0c\u77f3\u58a8\u70ef\uff0cMoS2<\/sub>\/G\u548cMoS2<\/sub>\/GO\u7684\u62c9\u66fc\u56fe\u8c31\uff1b<\/p>\n

(b) MoS2<\/sub>\/G\u4e2dC-C\u952e\u7684XPS\u56fe\u8c31\uff1b<\/p>\n

(c) \u7145\u70e7\u524dMoS2<\/sub>\/GO\u7684XPS\u56fe\u8c31\uff1b<\/p>\n

(d) MoS2<\/sub>\/GO\u7684XPS\u56fe\u8c31\uff1b<\/p>\n

(e) \u77f3\u58a8\u70ef\u7684\u5408\u6210 (i) MoS2<\/sub>\/GO (ii) MoS2<\/sub>\/G\u3002<\/p>\n

\u56fe-<\/strong>6.\u00a0<\/strong>\u94a0\u79bb\u5b50\u7535\u6c60\u7684<\/strong>CV<\/strong>\u66f2\u7ebf<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

(a) MoS2<\/sub>\/G\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

(b) MoS2<\/sub>\/GO\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

(c) MoS2<\/sub>\/G\u7684\u5cf0\u7535\u6d41\u5bc6\u5ea6\u4e0e\u626b\u63cf\u901f\u7387\u5e73\u65b9\u6839\u66f2\u7ebf\uff1b<\/p>\n

(d) MoS2<\/sub>\/GO\u7684\u5cf0\u7535\u6d41\u5bc6\u5ea6\u4e0e\u626b\u63cf\u901f\u7387\u5e73\u65b9\u6839\u66f2\u7ebf\u3002<\/p>\n

\u56fe-<\/strong>7.\u00a0<\/strong>\u5355\u5c42<\/strong>MoS2<\/sub><\/strong>\u548c\u77f3\u58a8\u70ef\u7684\u539f\u5b50\u6392\u5217\u65b9\u5f0f\u53ca\u5176\u4e2d\u94a0\u79bb\u5b50\u7684\u6269\u6563\u65b9\u5f0f<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

(a) \u5355\u5c42\u7684MoS2<\/sub>\u548c\u77f3\u58a8\u70ef\u7684\u4fef\u89c6\u56fe\uff1b<\/p>\n

(b) \u5355\u5c42\u7684MoS2<\/sub>\u548c\u77f3\u58a8\u70ef\u7684\u4fa7\u89c6\u56fe\uff1b<\/p>\n

(c) (d) (e) \u94a0\u79bb\u5b50\u4ee5\u6700\u4f4e\u80fd\u91cf\uff0c\u901a\u8fc7\u5355\u5c42\u7684MoS2<\/sub>\u548c\u77f3\u58a8\u70ef\u76843\u79cd\u65b9\u5f0f\u3002<\/p>\n

\u56fe-<\/strong>8.\u00a0<\/strong>\u5e26\u6709\u4e0d\u540c\u5b98\u80fd\u56e2\u7684\u5355\u5c42<\/strong>MoS2<\/sub><\/strong>\u548c\u77f3\u58a8\u70ef\u7684\u539f\u5b50\u6392\u5217\u65b9\u5f0f\u53ca\u5176\u4e2d\u94a0\u79bb\u5b50\u7684\u6269\u6563\u65b9\u5f0f<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

(a) \u5e26\u6709\u73af\u6c27\u57fa\u7684\u5355\u5c42MoS2<\/sub>\u548c\u77f3\u58a8\u70ef\u7684\u539f\u5b50\u6392\u5217\u65b9\u5f0f\uff1b<\/p>\n

(b) \u5e26\u6709\u73af\u6c27\u57fa\u7684\u5355\u5c42MoS2<\/sub>\u548c\u77f3\u58a8\u70ef\u4e2d\u94a0\u79bb\u5b50\u7684\u6269\u6563\u8def\u5f84\uff1b<\/p>\n

(c) \u5e26\u6709\u7f9f\u57fa\u7684\u5355\u5c42MoS2<\/sub>\u548c\u77f3\u58a8\u70ef\u7684\u539f\u5b50\u6392\u5217\u65b9\u5f0f\uff1b<\/p>\n

(d) \u5e26\u6709\u7f9f\u57fa\u7684\u5355\u5c42MoS2<\/sub>\u548c\u77f3\u58a8\u70ef\u4e2d\u94a0\u79bb\u5b50\u7684\u6269\u6563\u8def\u5f84\uff1b<\/p>\n

(e) \u5e26\u6709\u7f3a\u9677\u7684\u5355\u5c42MoS2<\/sub>\u548c\u77f3\u58a8\u70ef\u7684\u539f\u5b50\u6392\u5217\u65b9\u5f0f\uff1b<\/p>\n

(f) \u5e26\u6709\u7f3a\u9677\u7684\u5355\u5c42MoS2<\/sub>\u548c\u77f3\u58a8\u70ef\u4e2d\u94a0\u79bb\u5b50\u7684\u6269\u6563\u8def\u5f84\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u672c\u6587\u91c7\u7528\u4e24\u6b65\u7403\u78e8\u6cd5\u5236\u5907\u5f97\u5230\u4e86\u53ef\u7528\u4e8e\u9ad8\u500d\u7387\u6027\u80fd\u94a0\u79bb\u5b50\u7535\u6c60\u7684MoS2<\/sub>\/\u77f3\u58a8\u70ef\u7eb3\u7c73\u7247\u8d1f\u6781\u6750\u6599\uff0c\u8be5\u65b9\u6cd5\u5177\u6709\u4ef7\u683c\u4f4e\u3001\u9ad8\u4ea7\u80fd\u7b49\u4f18\u70b9\u3002\u5b9e\u9a8c\u7ed3\u679c\u548cDFT\u8ba1\u7b97\u8868\u660e\uff0c\u4f4e\u7f3a\u9677\u7a0b\u5ea6\u7684\u77f3\u58a8\u70ef\u53ef\u4ee5\u589e\u52a0\u6750\u6599\u7684\u7535\u5b50\u7535\u5bfc\u7387\uff0c\u51cf\u5c0f\u94a0\u79bb\u5b50\u6269\u6563\u80fd\u5792\u3002\u56e0\u6b64\uff0cMoS2<\/sub>\/\u77f3\u58a8\u70ef\u6750\u6599\u5177\u5907\u51fa\u8272\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002\u8fd9\u9879\u5de5\u4f5c\u8868\u660e\uff0c\u901a\u8fc7\u5bf9\u5f02\u8d28\u754c\u9762\u7684\u529f\u80fd\u5316\u8bbe\u8ba1\uff0c\u80fd\u591f\u6709\u6548\u63d0\u9ad8MoS2<\/sub>\/\u77f3\u58a8\u70ef\u7535\u6781\u7684\u7535\u5316\u5b66\u6027\u80fd\uff0c\u540c\u65f6\u4e5f\u4e3a\u5176\u5b83\u77f3\u58a8\u70ef\u590d\u5408\u6750\u6599\u7684\u5f00\u53d1\u548c\u8bbe\u8ba1\u63d0\u4f9b\u4e86\u4e00\u5b9a\u7684\u601d\u8def\u53c2\u8003\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>“MoS2\/Graphene Nanosheets from Commercial Bulky MoS2 and Graphite as Anode Materials for High Rate Sodium-Ion Batteries”<\/strong><\/a> (Adv. Energy Mater., 2017, DOI: 10.1002\/aenm.201702383)\u3002<\/p>\n

\u6b22\u8fce\u5927\u5bb6\u5230\u6750\u6599\u4eba\u5ba3\u4f20\u79d1\u6280\u6210\u679c\u5e76\u5bf9\u6587\u732e\u8fdb\u884c\u6df1\u5165\u89e3\u8bfb\uff0c\u6295\u7a3f\u90ae\u7bb1tougao@cailiaoren.com<\/a>\u3002<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u5f20\u91d1\u9633\u7f16\u8bd1\uff0c\u5f20\u6770\u5ba1\u6838\u3002<\/p>\n

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