{"id":121682,"date":"2018-01-16T06:30:03","date_gmt":"2018-01-15T22:30:03","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=121682"},"modified":"2018-01-15T23:27:09","modified_gmt":"2018-01-15T15:27:09","slug":"acs-nano-%e5%8a%a0%e5%88%a9%e7%a6%8f%e5%b0%bc%e4%ba%9a%e5%a4%a7%e5%ad%a6%e9%80%9a%e8%bf%87%e4%b8%80%e7%a7%8d%e5%8f%af%e6%8b%93%e5%b1%95%e7%9a%84%e9%80%94%e5%be%84%e5%90%88%e6%88%90%e7%ba%b3%e7%b1%b3","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=121682","title":{"rendered":"\u52a0\u5229\u798f\u5c3c\u4e9a\u5927\u5b66ACS Nano: \u901a\u8fc7\u4e00\u79cd\u53ef\u62d3\u5c55\u7684\u9014\u5f84\u5408\u6210\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u7ed3\u6784"},"content":{"rendered":"

\u3010\u5f15\u8a00<\/strong>\u3011<\/p>\n

\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u662f\u4e00\u79cd\u5177\u6709\u76f4\u5f84\u5927\u7ea61~100nm\u5b54\u9699\u7684\u7eaf\u91d1\u5c5e\u3002\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u56e0\u5176\u91d1\u5c5e\u7279\u6027\u548c\u7eb3\u7c73\u7ed3\u6784\u5c3a\u5bf8\u6548\u5e94\u7ed3\u5408\u7684\u7279\u70b9\u800c\u5907\u53d7\u8ffd\u6367\u3002\u4ed6\u4eec\u5373\u4fdd\u7559\u4e86\u5757\u72b6\u91d1\u5c5e\u7684\u70ed\/\u7535\u5bfc\u6027\uff0c\u5ef6\u5c55\u6027\u3001\u53ef\u5851\u6027\u7b49\u7279\u6027\u53c8\u6709\u826f\u597d\u7684\u7eb3\u7c73\u7ed3\u6784\u7279\u6027\uff0c\u5982\uff1a\u4f4e\u5bc6\u5ea6\u548c\u9ad8\u8868\u9762\u79ef\u3002\u4e0e\u4f20\u7edf\u5236\u5907\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u6750\u6599\u7684\u65b9\u6cd5\u76f8\u6bd4\uff0c\u53ef\u6269\u5c55\u7684\u5408\u6210\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u7684\u9014\u5f84\u5177\u6709\u64cd\u4f5c\u7b80\u5355\uff0c\u8fd0\u7528\u5e7f\u6cdb\u7b49\u7279\u70b9\u3002\u8fd9\u79cd\u65b9\u6cd5\u4e0d\u540c\u4e8e\u591a\u5b54\u7ed3\u6784\u5f62\u6210\u7684\u8131\u91d1\u5c5e\u8fc7\u7a0b\u540c\u65f6\u53bb\u9664\u539f\u5b50\u6df7\u5408\u5408\u91d1\u4e2d\u8f83\u4e0d\u8d35\u7684\u5143\u7d20\uff0c\u5b83\u9996\u5148\u7528\u671f\u671b\u7684\u7eaf\u91d1\u5c5e\u4e0e\u79bb\u5b50\u5316\u5408\u7269\u5f62\u6210\u7eb3\u7c73\u590d\u5408\u6750\u6599\u901a\u8fc7\u7528\u666e\u901a\u6709\u673a\u6eb6\u5242\u6eb6\u89e3\u800c\u9664\u53bb\u3002\u8fd9\u4e2a\u8fc7\u7a0b\u7684\u4f18\u70b9\u662f\u5b83\u5229\u7528\u4e86\u4e00\u4e2a\u6709\u673a\u7684\u6eb6\u5242\u800c\u4e0d\u662f\u9178\u4f5c\u4e3a\u8680\u523b\u5242\uff0c\u6240\u4ee5\u5b83\u9002\u7528\u4e8e\u8d35\u91d1\u5c5e\u3001\u975e\u8d35\u91d1\u5c5e\u4ee5\u53ca\u91d1\u5c5e\u6df7\u5408\u7269\u548c\u5408\u91d1\u7684\u63d0\u7eaf\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb<\/strong>\u3011<\/p>\n

\u8fd1\u65e5\uff0c\u52a0\u5229\u798f\u5c3c\u4e9a\u5927\u5b66<\/strong>\u7684Ping Liu(\u901a\u8baf\u4f5c\u8005)<\/strong> \u7b49\u4eba\u5728ACS Nano<\/strong>\u4e0a\u53d1\u8868\u4e86\u9898\u4e3a\u201cA Scalable Synthesis Pathway to Nanoporous Metal Structures<\/strong>\u201d \u7684\u6587\u7ae0\u3002\u5728\u8fd9\u7bc7\u6587\u7ae0\u4e2d\uff0c\u7814\u7a76\u4eba\u5458\u53d1\u73b0\u4e00\u79cd\u64cd\u4f5c\u7b80\u5355\uff0c\u8fd0\u7528\u5e7f\u6cdb\u7684\u65b9\u6cd5\u3002\u5229\u7528\u91d1\u5c5e\u5364\u5316\u7269\u5316\u5408\u7269\u53d1\u751f\u53cd\u5e94\u4e0e\u6709\u673a\u9502\u8fd8\u539f\u5242\u5728\u975e\u6781\u6027\u6eb6\u5242\u4e2d\u53cd\u5e94\u4ee5\u5f62\u6210\u91d1\u5c5e\/\u9502\u5364\u5316\u7269\u7eb3\u7c73\u590d\u5408\u6750\u6599\uff0c\u7136\u540e\u5c06\u9502\u5364\u5316\u7269\u7528\u666e\u901a\u7684\u6709\u673a\u6eb6\u5242\u6eb6\u89e3\u5728\u7eb3\u7c73\u590d\u5408\u6750\u6599\u5916\u9762\uff0c\u7559\u4e0b\u5f62\u6210\u7eb3\u7c73\u591a\u5b54\u7684\u8fde\u7eed\u7684\u4e09\u7ef4\u91d1\u5c5e\u4e1d\u7f51\u7edc\u7ed3\u6784\u4f53\u3002\u8fd9\u79cd\u65b9\u6cd5\u9002\u7528\u4e8e\u8d35\u91d1\u5c5e\uff08\u94dc\uff0c\u91d1\uff0c\u94f6\uff09\u548c\u8f83\u4e0d\u8d35\u91cd\u7684\u8f6c\u53d8\u91d1\u5c5e\uff08\u94b4\uff0c\u94c1\uff0c\u954d\uff09\u3002\u800c\u4e14\u8fd9\u4e9b\u7eb3\u7c73\u591a\u5b54\u8fc7\u6e21\u91d1\u5c5e\u7684\u5fae\u89c2\u7ed3\u6784\u662f\u53ef\u8c03\u7684\u3002\u8fd9\u79cd\u53ef\u6269\u5c55\u548c\u591a\u529f\u80fd\u7684\u5408\u6210\u9014\u5f84\u5927\u5927\u6269\u5c55\u4e86\u6211\u4eec\u83b7\u5f97\u989d\u5916\u7684\u6210\u5206\u548c\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u7684\u5fae\u89c2\u7ed3\u6784\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb<\/strong>\u3011<\/p>\n

\u56fe<\/strong>1 <\/strong>\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u5236\u5907\u901a\u8fc7\u8f6c\u5316\u53cd\u5e94\u5408\u6210\u7684\u4f8b\u8bc1<\/strong><\/p>\n

\"\"<\/p>\n

\u4e00\u4e2a\u65e0\u6c34\u8fc7\u6e21\u91d1\u5c5e\u5364\u5316\u7269\u524d\u4f53\uff08\u5728\u672c\u7814\u7a76\u4e2d\u901a\u5e38\u4e3a\u6c2f\u5316\u7269\uff09\u4e0en-BuLi\u53cd\u5e94\u5e76\u8f6c\u5316\u4e3a\u91d1\u5c5e\/\u9502\u5364\u5316\u7269\u7eb3\u7c73\u590d\u5408\u6750\u6599\u3002\u9502\u901a\u8fc7\u7528\u7532\u9187\u6eb6\u89e3\u51fa\u53bb\u5364\u5316\u7269\uff0c\u7559\u4e0b\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u3002<\/p>\n

\u56fe<\/strong>2 <\/strong>\u6765\u81ea\u6c2f\u548c\u6eb4\u5316\u524d\u4f53\u7684\u7eb3\u7c73\u591a\u5b54\u7eaf\u91d1\u5c5e\u7684\u626b\u63cf\u7535\u5b50\u663e\u5fae\u56fe\uff08<\/strong>SEM<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

(a)Fe from FeCl2; <\/sub><\/p>\n

(b) Co From CoCl2;<\/sub><\/p>\n

(c) Ni from NiCl2<\/sub>;<\/p>\n

(d) Cu from CuCl2; <\/sub><\/p>\n

(e) Ag from AgCl;<\/p>\n

(f) Au from AuCl3;<\/sub><\/p>\n

(g) Cu from CuBr2;<\/sub><\/p>\n

(h) Cu from CuBr<\/p>\n

\u56fe\u4e2d\u6240\u8868\u793a\u7684\u540d\u79f0\u662f\u5176\u76f8\u5e94\u7684\u5728\u5176\u76f8\u5e94\u7684\u5728n-BuLi\u8f6c\u5316\u4e4b\u540e\u7684\u7eaf\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u4ea7\u7269\uff1b\u56fe\u7247\u7684\u6bd4\u4f8b\u5c3a\u662f200nm<\/p>\n

\u56fe<\/strong>3 <\/strong>\u900f\u5c04\u7535\u955c\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

\u4eceFeCl3\u524d\u4f53\u4e2d\u5408\u6210\u7684\u7eb3\u7c73\u591a\u5b54\u94c1\u7684\u900f\u5c04\u7535\u955c\u56fe\uff08TEM\uff09<\/p>\n

\u56fe<\/strong>4 <\/strong>\u4e09\u79cd\u91d1\u5c5e<\/strong>\/LiCl <\/strong>\u7eb3\u7c73\u590d\u5408\u6750\u6599\u7684<\/strong>X<\/strong>\u5c04\u7ebf\u884d\u5c04\u56fe\uff08<\/strong>XRD<\/strong>\uff09\u53ca\u5176\u76f8\u5bf9\u5e94\u7684\u7532\u9187\u7eaf\u5316\u540e\u76f8\u5e94\u7684\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u3002\u5305\u62ec\u6807\u51c6\u6765\u81ea\u65e0\u673a\u6676\u4f53\u7ed3\u6784\u6570\u636e\u5e93\uff08<\/strong>ICSD<\/strong>\uff09\u7684\u6bcf\u79cd\u91d1\u5c5e\u7684\u884d\u5c04\u56fe\u6848\u8868\u793a\u5206\u914d\u7ed9<\/strong>LiCl<\/strong>\u7684\u5cf0\u3002<\/strong><\/p>\n

\"\"<\/p>\n

a\uff09\u6765\u81eaCuCl 2<\/sub>\u7684\u7eb3\u7c73\u591a\u5b54Cu\uff1b<\/p>\n

b\uff09\u6765\u81eaCoCl2<\/sub>\u7684\u7eb3\u7c73\u591a\u5b54Co\uff1b<\/p>\n

c\uff09\u6765\u81eaFeCl 3<\/sub>\u7684\u7eb3\u7c73\u591a\u5b54Fe\u3002<\/p>\n

\u56fe<\/strong>5 <\/strong>\u6c2f\u5316\u7269\u524d\u4f53\u5408\u6210\u7684\u4e09\u79cd\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u7684<\/strong>BET N2<\/strong>\u5438\u9644<\/strong> – <\/strong>\u89e3\u5438\u7b49\u6e29\u7ebf<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u548c(d)\u7eb3\u7c73\u591a\u5b54Cu;<\/p>\n

\uff08b\uff09\u548c\uff08e\uff09\u7eb3\u7c73\u591a\u5b54Co;<\/p>\n

\uff08c\uff09\u548c\uff08f\uff09\u7eb3\u7c73\u591a\u5b54Fe\u3002<\/p>\n

\u56fe<\/strong>6<\/strong>\uff08<\/strong>a<\/strong>\uff09<\/strong>Fe<\/strong>\u548c<\/strong>Fe \/ LiCl<\/strong>\uff0c\uff08<\/strong>b<\/strong>\uff09<\/strong>Co<\/strong>\u548c<\/strong>Co \/ LiCl <\/strong>\uff08<\/strong>c<\/strong>\uff09<\/strong>Ni<\/strong>\u548c<\/strong>Ni \/ LiCl<\/strong>\u7684\u77eb\u987d\u529b\uff08<\/strong>Hc<\/strong>\uff09\u548c\u5269\u78c1\uff08<\/strong>Mr \/ Ms <\/strong>\u9664\u53bb<\/strong>LiCl<\/strong>\u540e\uff0c<\/strong>Fe \/ LiCl<\/strong>\u548c<\/strong>Co \/ LiCl<\/strong>\u7684<\/strong>Hc<\/strong>\u548c<\/strong>Mr \/ Ms<\/strong>\u964d\u4f4e\u4ee5\u589e\u52a0\u91d1\u5c5e\u7eb3\u7c73\u9897\u7c92\u4e4b\u95f4\u7684\u5076\u6781\u76f8\u4e92\u4f5c\u7528\u3002\u76f8\u53cd\uff0c\u90a3\u4e9b\u4ef7\u503c\u7531\u4e8e\u5fae\u5f31\u7684\u5076\u6781\u76f8\u4e92\u4f5c\u7528\u548c\u6676\u4f53\uff0c<\/strong>Ni \/ LiCl<\/strong>\u5728\u53bb\u9664<\/strong>LiCl<\/strong>\u540e\u589e\u52a0\u751f\u957f\u3002<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>7<\/strong>\u7531\u5171\u6c89\u6dc0\u6cd5\u5408\u6210\u7684\u6df7\u5408\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u6c2f\u5316\u7269\u524d\u4f53\u7684<\/strong>SEM<\/strong>\u56fe\u50cf<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u6765\u81ea\u5171\u6c89\u6dc0\u7684AuCl 3<\/sub> + CuCl 2<\/sub>\u7684\u7eb3\u7c73\u591a\u5b54AuCu\uff1b<\/p>\n

\uff08b\uff09\u7eb3\u7c73\u591a\u5b54CuCo\uff0c\u5171\u6c89\u6dc0CuCl2 + CoCl2\uff1b<\/sub><\/p>\n

\uff08c\uff09\u7eb3\u7c73\u591a\u5b54CoFe\uff0c\u6765\u81ea\u5171\u6c89\u6dc0\u7684CoCl2<\/sub>\u548cFeCl2<\/sub><\/p>\n

\u56fe<\/strong>8\u00a0<\/strong>\u6df7\u5408\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u6837\u54c1\u7684<\/strong>X<\/strong>\u5c04\u7ebf\u884d\u5c04\u56fe\uff0c\u5305\u62ec\u5171\u6c89\u6dc0\u524d\u4f53\u3001\u91d1\u5c5e<\/strong>\/<\/strong>\u5364\u5316\u9502\u7eb3\u7c73\u590d\u5408\u6750\u6599\u548c\u6700\u7ec8\u6df7\u5408\u7269\u7eb3\u7c73\u591a\u5b54\u91d1\u5c5e\u4ea7\u54c1<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u901a\u8fc7AuCl 3<\/sub> + CuCl 2<\/sub>\u7684\u7eb3\u7c73\u591a\u5b54AuCu;<\/p>\n

\uff08b\uff09\u901a\u8fc7CuCl 2 <\/sub>+ CoCl 2<\/sub>\u7684\u7eb3\u7c73\u5b54CuCl;<\/p>\n

\uff08c\uff09\u901a\u8fc7FeCl 2<\/sub> + CoCl 2<\/sub>\u7684\u7eb3\u7c73\u591a\u5b54FeCo<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1aA Scalable Synthesis Pathway to Nanoporous Metal Structures<\/a>\uff08ACS Nano.,2018,DOI:10.1021\/acsnano.7b06667\uff09<\/p>\n

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