{"id":127630,"date":"2018-03-04T06:30:48","date_gmt":"2018-03-03T22:30:48","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=127630"},"modified":"2018-03-03T10:46:21","modified_gmt":"2018-03-03T02:46:21","slug":"%e4%b8%ad%e5%9b%bd%e7%9f%b3%e6%b2%b9%e5%a4%a7%e5%ad%a6%ef%bc%88%e5%8d%8e%e4%b8%9c%ef%bc%89%e5%90%b4%e6%98%8e%e9%93%82%e5%9b%a2%e9%98%9facs-nano-%e9%87%91%e5%b1%9e%e6%9c%89%e6%9c%ba%e6%a1%86%e6%9e%b6","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=127630","title":{"rendered":"\u4e2d\u56fd\u77f3\u6cb9\u5927\u5b66\uff08\u534e\u4e1c\uff09\u5434\u660e\u94c2\u56e2\u961fACS Nano: \u91d1\u5c5e\u6709\u673a\u6846\u67b6\u6750\u6599\u8f85\u52a9\u5408\u6210\u5177\u6709\u9ad8\u50a8\u9502\u6027\u80fd\u7684\u4e00\u7ef4\u94bc\u57fa\u5316\u5408\u7269\/\u78b3\u590d\u5408\u6750\u6599"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u8fd1\u5e74\u6765\uff0c\u968f\u7740\u6d88\u8d39\u7c7b\u7535\u5b50\u4ea7\u54c1\u548c\u65b0\u80fd\u6e90\u6c7d\u8f66\u4ea7\u4e1a\u7684\u8fc5\u731b\u53d1\u5c55\uff0c\u5f00\u53d1\u5177\u6709\u9ad8\u80fd\u91cf\u5bc6\u5ea6\u3001\u5927\u500d\u7387\u7279\u6027\u4ee5\u53ca\u957f\u4f7f\u5f79\u5bff\u547d\u7684\u9502\u79bb\u5b50\u7535\u6c60\u5df2\u6210\u4e3a\u65b0\u80fd\u6e90\u9886\u57df\u7684\u7814\u7a76\u91cd\u70b9\u548c\u70ed\u70b9\u3002\u4f5c\u4e3a\u9502\u79bb\u5b50\u7535\u6c60\u7684\u5173\u952e\u6750\u6599\uff0c\u4f20\u7edf\u77f3\u58a8\u7c7b\u8d1f\u6781\u6027\u80fd\u5df2\u8d8b\u7a79\u9876\uff0c\u57fa\u4e8e\u77f3\u58a8\u8d1f\u6781\u7684\u9502\u79bb\u5b50\u7535\u6c60\u6027\u80fd\u5df2\u65e0\u6cd5\u6ee1\u8db3\u5b9e\u9645\u5e94\u7528\u65e5\u8d8b\u589e\u957f\u7684\u9700\u6c42\u3002\u56e0\u6b64\uff0c\u8bbe\u8ba1\u548c\u5f00\u53d1\u65b0\u7ed3\u6784\u3001\u9ad8\u6027\u80fd\u7684\u9502\u79bb\u5b50\u7535\u6c60\u7535\u6781\u6750\u6599\u6210\u4e3a\u4e86\u5f53\u524d\u7684\u8feb\u5207\u4efb\u52a1\u3002\u8fc7\u6e21\u91d1\u5c5e\u5316\u5408\u7269\u5177\u6709\u8fdc\u9ad8\u4e8e\u77f3\u58a8\u7535\u6781\u7684\u5bb9\u91cf\uff0c\u4f46\u5176\u5bfc\u7535\u6027\u5dee\u4ee5\u53ca\u660e\u663e\u7684\u4f53\u79ef\u81a8\u80c0\u6548\u5e94\u6781\u5927\u9650\u5236\u4e86\u5176\u4f5c\u4e3a\u9502\u79bb\u5b50\u7535\u6c60\u7535\u6781\u6750\u6599\u4f7f\u7528\u65f6\u7684\u6027\u80fd\u3002\u5c06\u8fc7\u6e21\u91d1\u5c5e\u5316\u5408\u7269\u4e0e\u7eb3\u7c73\u78b3\u6750\u6599\u8fdb\u884c\u6709\u673a\u8026\u5408\uff0c\u6784\u7b51\u5177\u6709\u5206\u7ea7\u591a\u5b54\u7ed3\u6784\u7684\u6742\u5316\u6750\u6599\u662f\u4ece\u6839\u672c\u4e0a\u63d0\u5347\u5176\u7535\u5316\u5b66\u6027\u80fd\u7684\u6709\u6548\u9014\u5f84\u3002\u7531\u4e8e\u4e0d\u540c\u7ec4\u5206\u95f4\u8868\u754c\u9762\u6027\u8d28\u8fe5\u5f02\uff0c\u5728\u5fae\u7eb3\u7c73\u5c3a\u5ea6\u4e0b\u5982\u4f55\u80fd\u7b80\u5355\u3001\u9ad8\u6548\u5730\u5b9e\u73b0\u4e0d\u540c\u7ec4\u5206\u7684\u5747\u5300\u53ef\u63a7\u590d\u5408\u4ecd\u7136\u5145\u6ee1\u6311\u6218\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u9488\u5bf9\u8fd9\u4e00\u96be\u9898\uff0c\u5434\u660e\u94c2\u6559\u6388\u56e2\u961f<\/strong>\u4ece\u91d1\u5c5e\u6709\u673a\u6846\u67b6\u6750\u6599\uff08MOFs\uff09\u51fa\u53d1\uff0c\u91c7\u7528\u5176\u4e0e\u8fc7\u6e21\u91d1\u5c5e\u6c27\u5316\u7269\u539f\u4f4d\u81ea\u7ec4\u88c5-\u70ed\u8f6c\u5316\u7684\u6280\u672f\u7b56\u7565\uff0c\u6210\u529f\u5236\u5907\u51fa\u4e86\u591a\u79cd\u5177\u6709\u4f18\u5f02\u50a8\u9502\u6027\u80fd\u7684\u94bc\u57fa\u5316\u5408\u7269\/\u7eb3\u7c73\u78b3\u590d\u5408\u6750\u6599\u3002\u5728\u6b64\u9879\u5de5\u4f5c\u4e2d\uff0c\u57fa\u4e8e\u5bf9MOFs\u5728\u91d1\u5c5e\u6c27\u5316\u7269\u8868\u9762\u751f\u957f\u673a\u7406\u7684\u6df1\u5165\u63a2\u7a76\uff0c\u8be5\u56e2\u961f\u7cbe\u786e\u8c03\u63a7\u4e86MOFs\u5728\u91d1\u5c5e\u6c27\u5316\u7269\u8868\u9762\u7684\u751f\u957f\u8fc7\u7a0b\uff0c\u5b9e\u73b0\u4e86\u5ba4\u6e29\u6761\u4ef6\u4e0b\u5bf9\u4e09\u6c27\u5316\u94bc\u7eb3\u7c73\u68d2\u524d\u9a71\u4f53\u7684\u5feb\u901f\u5747\u5300\u5305\u8986\uff0c\u5e76\u901a\u8fc7\u540e\u7eed\u70ed\u5904\u7406\u7b49\u8fc7\u7a0b\u53ef\u63a7\u5236\u5907\u4e86\u5177\u6709\u5206\u7ea7\u591a\u5b54\u7ed3\u6784\u7684\u6c2e\u63ba\u6742\u7eb3\u7c73\u78b3\u5305\u8986\u591a\u5b54\u6c27\u5316\u94bc\/\u78b3\u5316\u94bc\u7eb3\u7c73\u68d2\uff0c\u5448\u73b0\u660e\u663e\u7684\u6838\u58f3\u6216\u4e2d\u7a7a\u7ed3\u6784\u3002\u5177\u6709\u591a\u5b54\u7ed3\u6784\u7684\u6d3b\u6027\u7269\u8d28\u80fd\u6709\u6548\u7f13\u89e3\u50a8\u9502\u8fc7\u7a0b\u4e2d\u7684\u7ed3\u6784\u5e94\u529b\uff0c\u6781\u5927\u63d0\u9ad8\u4e86\u6750\u6599\u7684\u4f7f\u7528\u5bff\u547d\uff1b\u5747\u5300\u7684\u7eb3\u7c73\u78b3\u5305\u8986\u5219\u663e\u8457\u63d0\u9ad8\u4e86\u6750\u6599\u7684\u5bfc\u7535\u6027\u3002\u540c\u65f6\uff0c\u58f3\u5c42\u7684\u91d1\u5c5e\u6709\u673a\u6846\u67b6\u6750\u6599\u5728\u8be5\u8bbe\u8ba1\u4e2d\u53ef\u540c\u65f6\u4f5c\u4e3a\u78b3\u6e90\u524d\u9a71\u7269\u548c\u70ed\u89e3\u53cd\u5e94\u7269\uff0c\u5176\u5728\u70ed\u89e3\u8fc7\u7a0b\u4e2d\u7684\u9650\u57df\u8f6c\u5316\u6709\u6548\u7ef4\u6301\u4e86\u6d3b\u6027\u7ec4\u5206\u7684\u5927\u5c0f\u53ca\u7ed3\u6784\u7a33\u5b9a\u6027\uff0c\u4fdd\u8bc1\u4e86\u590d\u5408\u6750\u6599\u4f18\u5f02\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002\u8fdb\u4e00\u6b65\u52a8\u529b\u5b66\u8ba1\u7b97\u8868\u660e\uff0c\u590d\u5408\u6750\u6599\u7535\u5316\u5b66\u5bb9\u91cf\u4e2d\u5b58\u5728\u660e\u663e\u7684\u8d5d\u7535\u5bb9\u8d21\u732e\uff0c\u6709\u671b\u7528\u4e8e\u6784\u7b51\u9ad8\u6027\u80fd\u52a8\u529b\u578b\u9502\u79bb\u5b50\u7535\u6c60\u3002\u76f8\u5173\u5de5\u4f5c\u53d1\u8868\u5728\u7eb3\u7c73\u79d1\u5b66\u4e0e\u6280\u672f\u9886\u57df\u9876\u7ea7\u671f\u520aACS Nano<\/strong>\u4e0a\uff08IF=13.942\uff09\u3002<\/p>\n

\u6b64\u9879\u5de5\u4f5c\u5f97\u5230\u4e86\u5305\u62ec\u56fd\u5bb6\u81ea\u7136\u79d1\u5b66\u57fa\u91d1\u3001\u5c71\u4e1c\u7701\u6cf0\u5c71\u5b66\u8005\u5de5\u7a0b\u4e13\u9879\u7ecf\u8d39\u4ee5\u53ca\u4e2d\u592e\u9ad8\u6821\u57fa\u672c\u79d1\u7814\u4e1a\u52a1\u4e13\u9879\u8d44\u91d1\u7b49\u8d44\u52a9\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe1 \u94bc\u57fa\u5316\u5408\u7269\/\u7eb3\u7c73\u78b3\u590d\u5408\u6750\u6599\u5408\u6210\u8def\u68d2\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe2 \u6c27\u5316\u94bc\u7eb3\u7c73\u68d2\/\u91d1\u5c5e\u6709\u673a\u6846\u67b6\u590d\u5408\u7269\u7684\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a<\/strong>)\u6c27\u5316\u94bc\u7eb3\u7c73\u68d2\u7684\u900f\u5c04\u7535\u955c\u7167\u7247<\/p>\n

(b-c<\/strong>) \u6c27\u5316\u94bc\u7eb3\u7c73\u68d2\/\u91d1\u5c5e\u6709\u673a\u6846\u67b6\u590d\u5408\u7269\u7684\u626b\u63cf\u7535\u955c\u53ca\u900f\u5c04\u7535\u955c\u7167\u7247<\/p>\n

(d<\/strong>) \u91d1\u5c5e\u6709\u673a\u6846\u67b6\u5728\u6c27\u5316\u94bc\u7eb3\u7c73\u68d2\u4e0a\u5305\u8986\u8fc7\u7a0b\u7684XRD\u5206\u6790\uff1aI-\u6c27\u5316\u94bc\uff0cII-\u53cd\u5e9415\u5206\u949f\uff0c III-\u53cd\u5e9430\u5206\u949f\uff0c IV-\u53cd\u5e94120\u5206\u949f\uff0cV-\u91d1\u5c5e\u6709\u673a\u6846\u67b6<\/p>\n

(e<\/strong>)\u91d1\u5c5e\u6709\u673a\u6846\u67b6\u5728\u6c27\u5316\u94bc\u7eb3\u7c73\u68d2\u4e0a\u5747\u5300\u5305\u8986\u7684\u673a\u7406\u5206\u6790<\/p>\n

\u56fe3 \u94bc\u57fa\u5316\u5408\u7269\/\u7eb3\u7c73\u78b3\u590d\u5408\u6750\u6599\u7ed3\u6784\u5206\u6790<\/strong><\/p>\n

\"\"
\n (a<\/strong>) 600 o<\/sup>C\u3001700 o<\/sup>C\u4e0b\u78b3\u5316\u5f97\u5230\u7684MoO2<\/sub>\/C-600\u548cMo2<\/sub>C\/C-700\u7684XRD\u56fe\u8c31<\/p>\n

(b<\/strong>)\u4e0d\u540c\u6761\u4ef6\u4e0b\u5236\u5f97\u6837\u54c1\u7684Raman\u56fe\u8c31\uff1aa. MoO2<\/sub>\/C-600, b. Mo2<\/sub>C\/C-700, c. Mo2<\/sub>C\/C-800, d. H-MoO2<\/sub>\/C<\/p>\n

(c-f)<\/strong>MoO2<\/sub>\/C-600\u3001Mo2<\/sub>C\/C-700\u3001Mo2<\/sub>C\/C-800\u53caH-MoO2<\/sub>\/C\u7684\u6c2e\u6c14\u5438\u9644\/\u8131\u9644\u66f2\u68d2<\/p>\n

\u56fe4 \u6c27\u5316\u94bc\/\u7eb3\u7c73\u78b3\u590d\u5408\u7269\u7684\u5f62\u8c8c\u5206\u6790<\/strong><\/p>\n

\"\"
\n (a<\/strong>) MoO2<\/sub>\/C-600\u7684\u626b\u63cf\u7535\u955c\u7167\u7247<\/p>\n

(b-e<\/strong>) MoO2<\/sub>\/C-600\u7684\u900f\u5c04\u7535\u955c\u7167\u7247<\/p>\n

(f<\/strong>) H-MoO2<\/sub>\/C\u7684\u626b\u63cf\u7535\u955c\u7167\u7247<\/p>\n

(g-j<\/strong>) H-MoO2<\/sub>\/C\u7684\u900f\u5c04\u7535\u955c\u7167\u7247<\/p>\n

\u56fe5 \u78b3\u5316\u94bc\/\u7eb3\u7c73\u78b3\u590d\u5408\u7269\u7684\u5f62\u8c8c\u5206\u6790<\/strong><\/p>\n

\"\"
\n (a<\/strong>) Mo2<\/sub>C\/C-700\u7684\u626b\u63cf\u7535\u955c\u7167\u7247<\/p>\n

(b-d<\/strong>) Mo2<\/sub>C\/C-700\u7684\u900f\u5c04\u7535\u955c\u7167\u7247<\/p>\n

\u56fe6 \u4e0d\u540c\u6837\u54c1\u7684\u7535\u5316\u5b66\u50a8\u9502\u6027\u80fd\u5206\u6790<\/strong><\/p>\n

\"\"
\n (a-c<\/strong>) MoO2<\/sub>\/C-600, H-MoO2<\/sub>\/C, Mo2<\/sub>C\/C-700\u7684\u5faa\u73af\u4f0f\u5b89\u66f2\u68d2<\/p>\n

(d<\/strong>) MoO2<\/sub>\/C-600, H-MoO2<\/sub>\/C, Mo2<\/sub>C\/C-700\u7684\u500d\u7387\u6027\u80fd\u6bd4\u8f83<\/p>\n

(e-f<\/strong>) MoO2<\/sub>\/C-600, H-MoO2<\/sub>\/C, Mo2<\/sub>C\/C-700\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u5206\u6790<\/p>\n

\u56fe7 \u78b3\u5316\u94bc\/\u7eb3\u7c73\u78b3\u590d\u5408\u7269\u7684\u50a8\u9502\u52a8\u529b\u5b66\u6027\u80fd\u5206\u6790<\/strong><\/p>\n

\"\"
\n (a<\/strong>) \u4e0d\u540c\u626b\u63cf\u901f\u7387\u4e0b\u7684\u5faa\u73af\u4f0f\u5b89\u66f2\u68d2<\/p>\n

(b<\/strong>) \u9634\u6781\u626b\u63cf\u8fc7\u7a0b\u4e2d\u7684b\u503c\u53d8\u5316<\/p>\n

(c<\/strong>) 1 mV s-1<\/sup>\u626b\u901f\u4e0b\u7684\u7535\u5bb9\u8d21\u732e\u5206\u6790<\/p>\n

(d<\/strong>)\u4e0d\u540c\u626b\u63cf\u901f\u7387\u4e0b\u7535\u5bb9\u8d21\u732e\u5206\u6790<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u672c\u5de5\u4f5c\u5f00\u53d1\u4e86\u4e00\u79cd\u65b0\u578b\u3001\u9ad8\u6548\u7684\u94bc\u57fa\u5316\u5408\u7269\/\u7eb3\u7c73\u78b3\u590d\u5408\u6750\u6599\u7684\u6784\u7b51\u65b0\u65b9\u6cd5\u3002\u901a\u8fc7\u65b0\u9896\u6709\u6548\u7684\u5408\u6210\u7b56\u7565\u548c\u4f18\u5316\u7684\u7ed3\u6784\u8bbe\u8ba1\uff0c\u6709\u6548\u89e3\u51b3\u4e86\u91d1\u5c5e\u5316\u5408\u7269\u7528\u4f5c\u9502\u79bb\u5b50\u7535\u6c60\u7535\u6781\u6750\u6599\u4f7f\u7528\u65f6\u7684\u4f4e\u7535\u5bfc\u7387\u548c\u4f53\u79ef\u81a8\u80c0\u7b49\u74f6\u9888\u6027\u96be\u9898\u3002\u5f97\u76ca\u4e8e\u590d\u5408\u6750\u6599\u5408\u7406\u7684\u7eb3\u7c73\u7ed3\u6784\u8bbe\u8ba1\u53ca\u4e0d\u540c\u7ec4\u5206\u95f4\u7684\u9ad8\u6548\u534f\u540c\u4f5c\u7528\uff0c\u6240\u5408\u6210\u7684\u4e00\u7cfb\u5217\u6c2e\u63ba\u6742\u7eb3\u7c73\u78b3\u5305\u8986\u7684\u591a\u5b54\u6c27\u5316\u94bc\/\u78b3\u5316\u94bc\u7eb3\u7c73\u68d2\u8868\u73b0\u51fa\u8f83\u9ad8\u7684\u6bd4\u5bb9\u91cf\u3001\u826f\u597d\u7684\u500d\u7387\u7279\u6027\u4ee5\u53ca\u4f18\u5f02\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u540c\u65f6\uff0c\u8be5\u5de5\u4f5c\u4e2d\u7684\u57fa\u4e8eMOFs\u6750\u6599\u7684\u539f\u4f4d\u751f\u957f-\u70ed\u8f6c\u5316\u7b56\u7565\u4e5f\u4e3a\u6784\u7b51\u5176\u4ed6\u7c7b\u578b\u8fc7\u6e21\u91d1\u5c5e\u5316\u5408\u7269\/\u78b3\u57fa\u590d\u5408\u6750\u6599\u63d0\u4f9b\u4e86\u65b0\u7684\u8bbe\u8ba1\u601d\u8def\u3002\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Metal\u2013Organic Frameworks Mediated Synthesis of One-Dimensional Molybdenum-Based\/Carbon Composites for Enhanced Lithium Storage<\/a>(ACS Nano, 2018, DOI:10.1021\/acsnano.7b09175)<\/p>\n

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