{"id":129003,"date":"2018-03-12T06:30:10","date_gmt":"2018-03-11T22:30:10","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=129003"},"modified":"2018-03-12T13:44:22","modified_gmt":"2018-03-12T05:44:22","slug":"%e6%ad%a6%e7%90%86%e8%8b%8f%e5%ae%9d%e8%bf%9e%e9%98%b3%e6%99%93%e5%ae%87nano-energy-%e7%ad%89%e7%ba%a7cdsm-tio2g%e4%b8%89%e5%85%83%e5%85%89%e5%82%ac%e5%8c%96%e5%89%82%e5%8f%8a%e5%85%b6","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=129003","title":{"rendered":"\u6b66\u7406\u82cf\u5b9d\u8fde&\u9633\u6653\u5b87Nano Energy : \u7b49\u7ea7CdS\/m-TiO2\/G\u4e09\u5143\u5149\u50ac\u5316\u5242\u53ca\u5176\u9ad8\u6d3b\u6027\u3001\u9ad8\u7a33\u5b9a\u6027\u53ef\u89c1\u5149\u8bf1\u5bfc\u5236\u6c22"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u786b\u5316\u9549(CdS)\u662f\u91cd\u8981\u7684\u53ef\u89c1\u5149\u9a71\u52a8\u534a\u5bfc\u4f53\u5149\u50ac\u5316\u5242\u4e4b\u4e00\uff0c\u7136\u800cCdS\u91cf\u5b50\u70b9(QDs)\u9971\u53d7\u5149\u8150\u8680\u4ee5\u53ca\u56e2\u805a\u73b0\u8c61\u7684\u56f0\u6270\uff0c\u5927\u5927\u9650\u5236\u4e86CdS\u5728\u592a\u9633\u80fd\u71c3\u6599\u751f\u4ea7\u65b9\u9762\u7684\u5b9e\u9645\u5e94\u7528\u3002\u4ee5\u5f80\u7684\u7814\u7a76\u4e2d\uff0c\u79d1\u7814\u4eba\u5458\u5229\u7528\u4e86\u5f88\u591a\u7b56\u7565\u6765\u63d0\u9ad8CdS\u7684\u7a33\u5b9a\u6027\uff0c\u5305\u62ec\u7eb3\u7c73\u8d1f\u8f7d\u3001\u7eb3\u7c73\u5305\u8986\u3001\u7eb3\u7c73\u5305\u57cb\u4ee5\u53ca\u7eb3\u7c73\u7ed3\u7b49\u3002\u8fd1\u6765\uff0c\u6838\u58f3\u7ed3\u6784\u7eb3\u7c73\u53cd\u5e94\u5668\u7531\u4e8e\u53ef\u5728\u7eb3\u7c73\u5c3a\u5ea6\u7efc\u5408\u5404\u79cd\u7ec4\u4ef6\u7684\u529f\u80fd\uff0c\u4ea7\u751f\u7684\u7eb3\u7c73\u9650\u57df\u6548\u5e94\u80fd\u63d0\u9ad8\u50ac\u5316\u5242\u7684\u50ac\u5316\u6d3b\u6027\u4ee5\u53ca\u50ac\u5316\u7a33\u5b9a\u6027\uff0c\u5f97\u5230\u4e86\u5f88\u591a\u7684\u5173\u6ce8\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u6b66\u6c49\u7406\u5de5\u5927\u5b66\u5362\u6bc5\u535a\u58eb\uff08\u7b2c\u4e00\u4f5c\u8005\uff09\uff0c\u82cf\u5b9d\u8fde\u6559\u6388\u3001\u9633\u6653\u5b87\u6559\u6388(\u5171\u540c\u901a\u8baf\u4f5c\u8005)\u7b49<\/strong>\u5229\u7528\u4e09\u7535\u5b50\u5c42\u9759\u7535\u7ec4\u88c5\u65b9\u6cd5\u5236\u5907\u4e86\u7b49\u7ea7CdS\/m-TiO2<\/sub>\/G\u4e09\u5143\u590d\u5408\u5149\u50ac\u5316\u5242\uff0c\u5176\u5177\u6709\u8f83\u9ad8\u7684\u5149\u50ac\u5316\u6d3b\u6027\u4ee5\u53ca\u4f18\u5f02\u7684\u5149\u50ac\u5316\u7a33\u5b9a\u6027\uff0c\u5e76\u5728Nano Energy<\/strong>\u4e0a\u53d1\u8868\u4e86\u9898\u4e3a\u201cHierarchical CdS\/m-TiO2<\/sub>\/G Ternary Photocatalyst for Highly Active Visible Light-induced Hydrogen Production from Water Splitting with High Stability<\/strong>\u201d\u7684\u7814\u7a76\u8bba\u6587\u3002\u4e0a\u8ff0\u4e09\u5143\u5149\u50ac\u5316\u5242\u7684\u6d3b\u6027\u662fCdS\u91cf\u5b50\u70b9\u6d3b\u6027\u7684\u4e24\u500d\u591a\uff0c\u572880 h \u5149\u716715\u6b21\u5faa\u73af\u540e\u4ecd\u80fd\u4fdd\u6301\u521d\u59cb\u6d3b\u6027\u768482%\u3002\u4f5c\u8005\u4ece\u8f68\u9053\u6742\u5316\u3001\u7ed3\u5408\u80fd\u3001\u539f\u5b50\u5e94\u529b\u626d\u66f2\u4ee5\u53ca\u7eb3\u7c73\u754c\u9762\u878d\u5408\u89d2\u5ea6\u7814\u7a76\u4e86\u5149\u50ac\u5316\u5242\u7684\u4e09\u5143\u7eb3\u7c73\u5f02\u8d28\u7ed3\u6548\u5e94\uff0c\u5e76\u5728\u539f\u5b50\/\u7eb3\u7c73\u5c3a\u5ea6\u63d0\u51fa\u4e86\u4e09\u5143\u4f53\u7cfb\u5185\u5149\u751f\u8f7d\u6d41\u5b50\u7684\u591a\u91cd\u4f20\u9012\u673a\u5236\u3002\u4e0a\u8ff0\u5de5\u4f5c\u4e3a\u6291\u5236CdS\u5149\u8150\u8680\u73b0\u8c61\u63d0\u4f9b\u4e86\u4e00\u79cd\u524d\u666f\u826f\u597d\u7684\u65b9\u6cd5\uff0c\u66f4\u91cd\u8981\u7684\u662f\uff0c\u4e5f\u4e3a\u8bbe\u8ba1\u5f02\u8d28\u7ed3\u7ed3\u6784\u7684\u4e09\u5143\u7eb3\u7c73\u50ac\u5316\u5242\u63d0\u4f9b\u4e86\u65b0\u7684\u89c1\u89e3\u3002<\/p>\n

\u3010\u56fe\u6587\u7b80\u4ecb\u3011<\/strong>
\n \u56fe1 CdS\/m-TiO2<\/sub>\/G\u5236\u5907\u8fc7\u7a0b\u793a\u610f\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

\u8d1f-\u6b63-\u8d1f\u4e09\u7535\u5b50\u5c42\u9759\u7535\u7ec4\u88c5\u5408\u6210CdS\/m-TiO2<\/sub>\/G\u8fc7\u7a0b\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe2 \u50ac\u5316\u5242\u7684\u5f62\u8c8c\u548c\u9ad8\u5206\u8fa8\u7ed3\u6784\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

a) CdS\/m-TiO2<\/sub>\/G\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

b) CdS\u3001m-TiO2<\/sub>\u548cCdS\/m-TiO2<\/sub>\/G\u7684XRD\u56fe\u8c31\uff1b<\/p>\n

c) CdS\/m-TiO2<\/sub>\/G\u7684HRTEM\u56fe\u50cf\uff1b<\/p>\n

d-g) CdS\/m-TiO2<\/sub>\/G\u7684HAADF-STEM\u56fe\u50cf\u548cEDS\u5143\u7d20\u5206\u5e03\uff1b<\/p>\n

h) \u9510\u949b\u77ffTiO2<\/sub>\u3001\u7acb\u65b9\u76f8CdS\u3001\u65e0\u5b9a\u578bTiO2<\/sub>\u548c\u6676\u4f53\u878d\u5408\u533a\u57df\u5728\u4e09\u5143\u7ed3\u6784\u4e2d\u7684HRTEM\u56fe\u50cf\uff0c\u4ee5\u56db\u79cd\u989c\u8272\u533a\u5206\u4e0d\u540c\u7684\u76f8\uff1b<\/p>\n

i) \u533a\u57dfI\u7684\u9006FFT\u56fe\u50cf\uff0c\u663e\u793a\u51faTiO2<\/sub>\u548cCdS\u4e4b\u95f4\u7684\u6676\u4f53\u878d\u5408\u533a\u57df\uff1b<\/p>\n

j) \u533a\u57dfII\u7684\u9006FFT\u56fe\u50cf\uff0c\u663e\u793a\u51faCdS\u548c\u65e0\u5b9a\u578bTiO2<\/sub>\u4e4b\u95f4\u7684\u878d\u5408\u8fc7\u6e21\u533a\u57df\u3002<\/p>\n

\u56fe3 \u50ac\u5316\u5242\u7684\u5236\u6c22\u5149\u7a33\u5b9a\u6027<\/strong><\/p>\n

\"\"<\/p>\n

CdS\/m-TiO2<\/sub>\/G\u548cCdS\u5728\u53ef\u89c1\u5149(\u03bb\u2265420 nm)\u7167\u5c04\u4e0b\u5236\u6c22\u7684\u5149\u7a33\u5b9a\u6027\uff0c\u5176\u4e2d\u727a\u7272\u5242\u4e3a0.1 M Na2<\/sub>SO3<\/sub>\u548c0.1 M Na2<\/sub>S \u6df7\u5408\u6eb6\u6db2\uff0c\u4ec5\u5728\u5236\u6c22\u5f00\u59cb\u524d\u52a0\u5165\u4e00\u6b21\uff1b\u5185\u63d2\u4e3aCdS\/m-TiO2<\/sub>\/G \u572880 h \u5236\u6c22\u6d4b\u8bd5\u540e\u7684HRTEM \u56fe\u50cf\u3002<\/p>\n

\u56fe4 \u50ac\u5316\u5242\u7684\u8f68\u9053\u6742\u5316\u548c\u5143\u7d20\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

a) CdS\/m-TiO2<\/sub>\/G\u7684XPS\u8c31\u56fe\uff1b<\/p>\n

b)\u4e0d\u540c\u6676\u76f8\u754c\u9762\u5f62\u6210\u65b0\u5316\u5b66\u952e\u7684\u6a21\u62df\u6a21\u578b\uff1b<\/p>\n

c) CdS\u3001CdS\/G\u3001CdS\/m-TiO2<\/sub>\u548cCdS\/m-TiO2<\/sub>\/G\u7684Cd 3d 5\/2\u5316\u5b66\u4f4d\u79fb\uff1b<\/p>\n

d) CdS\u3001CdS\/G\u3001CdS\/m-TiO2<\/sub>\u548cCdS\/m-TiO2<\/sub>\/G\u5728\u53ef\u89c1\u5149(\u03bb\u2265420 nm)\u4e0b\u7684\u5149\u7535\u6d41\u56fe\u3002<\/p>\n

\u56fe5 \u50ac\u5316\u5242\u7684\u5149\u751f\u8f7d\u6d41\u5b50\u5206\u79bb\u673a\u7406\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

CdS\/m-TiO2<\/sub>\/G\u7ed3\u6784\u4e2d\u5149\u751f\u7535\u5b50\u548c\u7a7a\u7a74\u7684\u8fc1\u79fb\u548c\u5206\u79bb\u793a\u610f\u56fe\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u4f5c\u8005\u901a\u8fc7\u8d1f-\u6b63-\u8d1f\u4e09\u7535\u5b50\u5c42\u9759\u7535\u7ec4\u88c5\u6cd5\u6210\u529f\u5236\u5907CdS\/m-TiO2<\/sub>\/G\u4e09\u5143\u590d\u5408\u5149\u50ac\u5316\u5242\uff0c\u8be5\u4e09\u5143\u5149\u50ac\u5316\u5242\u5177\u6709\u8f83\u9ad8\u7684\u5236\u6c22\u901f\u7387\u4ee5\u53ca\u4f18\u5f02\u7684\u5149\u7a33\u5b9a\u6027\u3002\u7814\u7a76\u53d1\u73b0\u6709\u5982\u4e0b\u9762\u4e09\u4e2a\u539f\u56e0\u3002\u9996\u5148\uff0cm-TiO2<\/sub>\/Cd2+<\/sup>\/GO\u7684\u4e09\u7535\u5c42\u6709\u5229\u4e8eCdS\/m-TiO2<\/sub>\/G\u754c\u9762\u7eb3\u7c73\u878d\u5408\u4ee5\u53ca\u63d0\u9ad8CdS\u91cf\u5b50\u70b9\u5728\u6838\u58f3\u7ed3\u6784\u4e2d\u7684\u5206\u6563\uff0c\u4f7f\u5f97\u7ed3\u6784\u7a33\u5b9a\u6027\u5927\u5927\u63d0\u9ad8\uff0cCdS\u6eb6\u51fa\u51cf\u5c11\u3002\u5176\u6b21\uff0cCdS\/m-TiO2<\/sub>\/G\u4e2d\u7684\u539f\u5b50\u5c3a\u5ea6\u5f02\u8d28\u7ed3\u6709\u5229\u4e8e\u5149\u751f\u8f7d\u6d41\u5b50\u4ece\u534a\u5bfc\u4f53\u591a\u91cd\u9ad8\u6548\u8f6c\u79fb\uff0c\u4ece\u800c\u5927\u5927\u63d0\u9ad8\u4e86CdS\u7684\u5149\u6d3b\u6027\u548c\u7a33\u5b9a\u6027\u3002\u7b2c\u4e09\uff0c\u5149\u751f\u7a7a\u7a74\u8fc5\u901f\u8f6c\u79fb\u5230\u975e\u6676\u6001\u7684Ti(IV)\u533a\u57df\uff0c\u589e\u5f3a\u5176\u6c27\u5316\u53cd\u5e94\u6d3b\u6027\u548c\u5149\u7a33\u5b9a\u6027\u3002<\/p>\n

\u3010\u56e2\u961f\u5de5\u4f5c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u82cf\u5b9d\u8fde\u9662\u58eb\u56e2\u961f<\/strong>\u957f\u671f\u81f4\u529b\u4e8e\u7b49\u7ea7\u5b54\u6750\u6599\u8bbe\u8ba1\u7406\u8bba\u53ca\u5176\u5728\u50ac\u5316\u3001\u80fd\u6e90\u8f6c\u5316\u4e0e\u5b58\u50a8\u3001\u4eba\u5de5\u5149\u5408\u4f5c\u7528\u7b49\u5e94\u7528\u9886\u57df\u7684\u7814\u7a76\u3002\u63d0\u51fa\u4e86\u751f\u547d\u590d\u5408\u6750\u6599\u7684\u6982\u5ff5\uff0c\u5373\u5c06\u5177\u6709\u7279\u6b8a\u529f\u80fd\u7684\u751f\u547d\u4f53\u548c\u65e0\u751f\u547d\u7684\u6750\u6599\u590d\u5408\uff0c\u53d1\u5c55\u5177\u6709\u751f\u547d\u529f\u80fd\u7684\u4eff\u751f\u590d\u5408\u6750\u6599\uff0c\u4e3a\u89e3\u51b3\u80fd\u6e90\u3001\u73af\u5883\u3001\u533b\u7597\u5065\u5eb7\u3001\u751f\u547d\u79d1\u5b66\u4e2d\u7684\u6311\u6218\u63d0\u4f9b\u4e86\u5168\u65b0\u65b9\u6848\u3002\u9488\u5bf9\u751f\u547d\u590d\u5408\u6750\u6599\u7684\u7269\u8d28\u4f20\u8f93\u548c\u4ea4\u6362\u95ee\u9898\uff0c\u521b\u65b0\u6027\u5730\u5c06\u7269\u8d28\u4f20\u8f93\u548c\u4ea4\u6362\u4e2d\u7684\u8d28\u91cf\u53d8\u5316\u5f15\u8fdb\u72ed\u4e49\u9ed8\u91cc\u5b9a\u5f8b\uff0c\u63a8\u5bfc\u51fa\u5e7f\u4e49\u9ed8\u91cc\u5b9a\u5f8b(General Murray\u2019s Law)<\/strong>\uff0c\u5e76\u7ed3\u5408\u751f\u547d\u4f53\u4e2d\u65e0\u5904\u4e0d\u5728\u7684\u7b49\u7ea7\u7ed3\u6784\u5f52\u7eb3\u6210\u5d2d\u65b0\u7684\u6750\u6599\u8bbe\u8ba1\u65b0\u7406\u8bba\uff1a\u7b49\u7ea7\u5b9a\u5f8b\uff0c\u63d0\u51fa\u4e86\u9ed8\u91cc\u6750\u6599(Murray Materials)<\/strong>\u65b0\u6982\u5ff5\u3002\u5e76\u6309\u7167\u7b49\u7ea7\u5b9a\u5f8b\uff0c\u6a21\u62df\u4e86\u6811\u53f6\u4e2d\u53f6\u8109\u7684\u7b49\u7ea7\u5b54\u7ed3\u6784\uff0c\u8bbe\u8ba1\u5e76\u5236\u5907\u4e86\u65b0\u578b\u7684\u5177\u6709\u5927\u5b54-\u4ecb\u5b54-\u5fae\u5b54\u4e09\u7ea7\u7b49\u7ea7\u5b54\u7ed3\u6784\u7684\u6c27\u5316\u950c\u9ed8\u91cc\u6750\u6599\u3002\u8be5\u65b0\u578b\u7b49\u7ea7\u5b54\u5fae\u7eb3\u7ed3\u6784\u9ed8\u91cc\u6750\u6599\u53ef\u4ee5\u5f88\u5927\u7a0b\u5ea6\u5730\u63d0\u9ad8\u7269\u8d28\u7684\u4f20\u8f93\u53ca\u79bb\u5b50\u8fc1\u79fb\uff0c\u4f7f\u5176\u5728\u6c14\u76f8\u3001\u6db2\u76f8\u53ca\u6db2\u56fa\u76f8\u53cd\u5e94\u4e2d\u5177\u6709\u975e\u5e38\u9ad8\u7684\u6027\u80fd\u548c\u6548\u7387\u3002\u8be5\u7814\u7a76\u6210\u679c\u53d1\u8868\u5728Nat. Commun.(Nat. Commun., 2017, 8, 14921<\/a><\/strong>)\u3002\u9488\u5bf9\u751f\u547d\u4f53\u548c\u65e0\u751f\u547d\u7684\u590d\u5408\u539f\u7406\u4e0e\u6280\u672f\u95ee\u9898\uff0c\u56e2\u961f\u53d1\u5c55\u4e86\u4ee5\u6c22\u952e\u4e3a\u57fa\u7840\u7684\u4eff\u751f\u754c\u9762\u590d\u5408\u6280\u672f\uff0c\u4ee5\u7ec6\u80de\u4e0e\u4eff\u751f\u7b49\u7ea7\u5b54\u6750\u6599\u4e3a\u6a21\u578b\uff0c\u5b9e\u73b0\u4e86\u6750\u6599\u4e0e\u529f\u80fd\u751f\u547d\u4f53\u7684\u590d\u5408(Chem. Commun., 2014,50, 15407<\/a><\/strong>\uff1bChem. Sci., 2015, 6, 486<\/a><\/strong>\uff1bSmall, 2015, 11, 2003<\/a><\/strong>)\u3002\u9488\u5bf9\u672a\u6765\u53ef\u6301\u7eed\u6d01\u51c0\u80fd\u6e90\u548c\u7eff\u8272\u73af\u5883\u7684\u91cd\u5927\u9700\u6c42\u53ca\u751f\u547d\u590d\u5408\u6750\u6599\u201c\u957f\u5bff\u547d\u9ad8\u6548\u7387\u201d\u8fd9\u4e00\u91cd\u5927\u79d1\u5b66\u76ee\u6807\uff0c\u5728\u6750\u6599\u8bbe\u8ba1\u548c\u754c\u9762\u8c03\u63a7\u57fa\u7840\u4e0a\uff0c\u6211\u4eec\u8fdb\u4e00\u6b65\u5229\u7528\u975e\u57fa\u56e0\u6539\u9020\u6280\u672f\uff0c\u5c06\u5916\u754c\u529f\u80fd\u4fe1\u606f\u5f15\u5bfc\u5230\u7ec6\u80de\u5185\u90e8\uff0c\u76f8\u5bf9\u4e8e\u81ea\u7136\u7ec6\u80de\u63d0\u9ad8\u6548\u7387\u6700\u9ad8\u5230500%(Chem. Commun., 2017, 53, 6617<\/a><\/strong>)\u3002\u8fd9\u4e9b\u6210\u679c\u4e3a\u751f\u547d\u590d\u5408\u6750\u6599\u7684\u8fdb\u4e00\u6b65\u53d1\u5c55\u6253\u4e0b\u4e86\u575a\u5b9e\u7684\u79d1\u5b66\u57fa\u7840\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a Hierarchical CdS\/m-TiO2<\/sub>\/G Ternary Photocatalyst for Highly Active<\/a><\/strong>
\n Visible Light-induced Hydrogen Production from Water Splitting with High Stability<\/strong><\/a> (Nano Energy<\/strong>, 2018, DOI: 10.1016\/ j.nanoen.2018.02.021)<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u65b0\u80fd\u6e90\u5c0f\u7ec4abc940504\u7f16\u8bd1\u6574\u7406\uff0c\u53c2\u4e0e\u65b0\u80fd\u6e90\u8bdd\u9898\u8ba8\u8bba\u8bf7\u52a0\u5165\u201c\u6750\u6599\u4eba\u65b0\u80fd\u6e90\u6750\u6599\u4ea4\u6d41\u7fa4 422065953\u201d\u3002<\/p>\n

\u6295\u7a3f\u4ee5\u53ca\u5185\u5bb9\u5408\u4f5c\u53ef\u52a0\u7f16\u8f91\u5fae\u4fe1\uff1aRDD-2011-CHERISH\uff0c\u4efb\u4e39\u4e39\uff0c\u6211\u4eec\u4f1a\u9080\u8bf7\u5404\u4f4d\u8001\u5e08\u52a0\u5165\u4e13\u5bb6\u7fa4\u3002<\/strong><\/p>\n

\u6750\u6599\u725b\u7f51\u4e13\u6ce8\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u53ca\u884c\u4e1a\u8fdb\u5c55\uff0c\u5982\u679c\u60a8\u5bf9\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u8fdb\u5c55\uff0c\u89e3\u8bfb\u9ad8\u6c34\u5e73\u6587\u7ae0\u6216\u662f\u8bc4\u8ff0\u884c\u4e1a\u6709\u5174\u8da3\uff0c\u70b9\u6211\u52a0\u5165\u7f16\u8f91\u90e8<\/a><\/strong>\u3002\u6b22\u8fce\u5927\u5bb6\u5230\u6750\u6599\u4eba\u5ba3\u4f20\u79d1\u6280\u6210\u679c\u5e76\u5bf9\u6587\u732e\u8fdb\u884c\u6df1\u5165\u89e3\u8bfb\uff0c\u6295\u7a3f\u90ae\u7bb1tougao@cailiaoren.com\u3002<\/p>\n

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