{"id":129746,"date":"2018-03-17T14:00:48","date_gmt":"2018-03-17T06:00:48","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=129746"},"modified":"2018-03-18T18:14:15","modified_gmt":"2018-03-18T10:14:15","slug":"%e6%b8%85%e5%8d%8e%e5%a4%a7%e5%ad%a6angew-chem-int-ed-%ef%bc%9a%e8%b0%83%e6%8e%a7%e9%94%82%e7%a6%bb%e5%ad%90%e6%ba%b6%e5%89%82%e5%8c%96%e5%b1%82%ef%bc%8c%e5%a2%9e%e5%bc%ba%e9%94%82%e9%87%91","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=129746","title":{"rendered":"\u6e05\u534e\u5927\u5b66\u5f20\u5f3aAngew. Chem. Int. Ed.\uff1a\u8c03\u63a7\u9502\u79bb\u5b50\u6eb6\u5242\u5316\u5c42\uff0c\u589e\u5f3a\u9502\u91d1\u5c5e\u7535\u6c60\u7a33\u5b9a\u6027"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u00a0<\/strong>\u65b0\u80fd\u6e90\u7535\u52a8\u6c7d\u8f66\u548c\u4fbf\u643a\u5f0f\u7535\u5b50\u8bbe\u5907\u7684\u5feb\u901f\u53d1\u5c55\uff0c\u6781\u5927\u5730\u63a8\u52a8\u4e86\u793e\u4f1a\u5bf9\u5b89\u5168\u7684\u3001\u9ad8\u6bd4\u80fd\u7684\u50a8\u80fd\u4f53\u7cfb\u7684\u9700\u6c42\u3002\u5728\u4f17\u591a\u7684\u8d1f\u6781\u6750\u6599\u4e2d\uff0c\u91d1\u5c5e\u9502\u7531\u4e8e\u7406\u8bba\u6bd4\u5bb9\u91cf\u6781\u9ad8\uff083860 mAh g\u22121<\/sup>\uff09\u548c\u7535\u6781\u7535\u52bf\u4f4e\uff08\u20133.040 V vs.\u6807\u51c6\u6c22\u7535\u6781\uff09\u7684\u7279\u6027\uff0c\u6210\u4e3a\u8d1f\u6781\u6750\u6599\u7684\u6700\u4f73\u9009\u62e9\u3002\u7136\u800c\uff0c\u9502\u5316\u5b66\u6027\u8d28\u6d3b\u6cfc\uff0c\u6613\u4e8e\u7535\u89e3\u6db2\u53cd\u5e94\u5728\u9502\u8d1f\u6781\u8868\u9762\u751f\u6210\u56fa\u6001\u7535\u89e3\u8d28\u754c\u9762\u819c\uff08SEI\uff09\u3002\u7531\u4e8eSEI\u7684\u7ec4\u6210\u548c\u7ed3\u6784\u4e0a\u7684\u4e0d\u5747\u5300\u6027\uff0c\u9502\u5728\u6c89\u79ef\u8fc7\u7a0b\u4e2d\u5bb9\u6613\u751f\u6210\u679d\u6676\uff0c\u4ece\u800c\u9020\u6210\u7535\u89e3\u6db2\u635f\u8017\u3001\u7535\u6781\u7c89\u5316\u4ee5\u53ca\u4f53\u79ef\u81a8\u80c0\u7b49\u95ee\u9898\uff0c\u5bfc\u81f4\u5176\u4e0d\u80fd\u5e94\u7528\u4e8e\u5546\u4e1a\u5316\u7535\u6c60\u3002\u56e0\u6b64\uff0c\u8c03\u63a7SEI\u5747\u5300\u6027\uff0c\u6291\u5236\u9502\u679d\u6676\u751f\u6210\uff0c\u589e\u5f3a\u9502\u91d1\u5c5e\u7535\u6c60\u5faa\u73af\u7a33\u5b9a\u6027\u6210\u4e3a\u5f53\u4e0b\u7684\u4e3b\u8981\u6311\u6218\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u00a0<\/strong>\u8fd1\u65e5\uff0c\u6e05\u534e\u5927\u5b66\u5f20\u5f3a\u6559\u6388\u8bfe\u9898\u7ec4<\/strong>\u901a\u8fc7\u8c03\u63a7\u6db2\u6001\u7535\u89e3\u6db2\u4e2d\u9502\u79bb\u5b50\u6eb6\u5242\u5316\u5c42\u7684\u7ec4\u6210\u548c\u7ed3\u6784\uff0c\u6539\u5584SEI\u548c\u9502\u6c89\u79ef\u7684\u5747\u5300\u6027\uff0c\u4ece\u800c\u589e\u5f3a\u4e86\u9502\u91d1\u5c5e\u7535\u6c60\u5728\u6db2\u6001\u7535\u89e3\u6db2\u4e2d\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u5728\u6db2\u6001\u7535\u89e3\u6db2\u4e2d\uff0cSEI\u7684\u7ec4\u5206\u4e3b\u8981\u6765\u6e90\u4e8e\u9502\u79bb\u5b50\u7684\u6eb6\u5242\u5316\u5c42\u3002\u56e0\u6b64\uff0c\u8c03\u63a7\u9502\u79bb\u5b50\u6eb6\u5242\u5316\u5c42\u53ef\u663e\u8457\u6539\u5584SEI\u7684\u5747\u5300\u6027\uff0c\u6291\u5236\u9502\u679d\u6676\u751f\u6210\u3002\u672c\u5de5\u4f5c\u4e2d\uff0c\u6c1f\u4ee3\u78b3\u9178\u4e59\u70ef\u916f\uff08FEC\uff09\u548c\u785d\u9178\u9502(LiNO3<\/sub>)\u901a\u8fc7\u919a\u916f\u6df7\u5408\u6eb6\u6db2\u7684\u6eb6\u5242\u5316\u4f5c\u7528\u540c\u65f6\u5f15\u5165\u7535\u89e3\u6db2\u4e2d\uff0c\u6539\u53d8\u9502\u79bb\u5b50\u7684\u6eb6\u5242\u5316\u5c42\u7684\u7ec4\u6210\u548c\u7ed3\u6784\uff0c\u4ece\u800c\u751f\u6210\u5bcc\u542bLiF\u548cLiNx<\/sub>Oy<\/sub>\u7684SEI\uff0c\u589e\u5f3aSEI\u7684\u5747\u5300\u6027\uff0c\u83b7\u5f97\u5747\u5300\u7684\u9502\u6c89\u79ef\u5f62\u8c8c\u3002\u5c06\u8be5\u7535\u89e3\u6db2\u8fd0\u7528\u4e8e\u7ebd\u6263\u548c\u8f6f\u5305\u7535\u6c60\u4e2d\uff0c\u5747\u53ef\u4ee5\u83b7\u5f97\u9ad8\u5e93\u4ed1\u6548\u7387\u548c\u957f\u5faa\u73af\u5bff\u547d\uff0c\u5e76\u4e14\u53ef\u4ee5\u5728\u4f4e\u6e29\u548c\u9ad8\u6e29\u6761\u4ef6\u4e0b\u7a33\u5b9a\u8fd0\u884c\uff0c\u6781\u5927\u63d0\u9ad8\u4e86\u9502\u91d1\u5c5e\u7535\u6c60\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u5206\u5b50\u52a8\u529b\u5b66\u548c\u7b2c\u4e00\u6027\u539f\u7406\u7684\u8ba1\u7b97\u6a21\u62df\uff0c\u8fdb\u4e00\u6b65\u63ed\u793a\u4e86\u65b0\u578b\u7535\u89e3\u6db2\u4e2d\u9502\u79bb\u5b50\u7684\u6eb6\u5242\u5316\u5c42\u7684\u7ec4\u6210\u548c\u7ed3\u6784\uff0c\u52a0\u5f3a\u4e86\u4eba\u4eec\u5bf9\u4e8e\u6eb6\u5242\u5316\u5c42\u5728\u5206\u5b50\u5c42\u9762\u7684\u8ba4\u8bc6\uff0c\u4e3a\u4e4b\u540e\u7535\u89e3\u6db2\u7684\u8bbe\u8ba1\u63d0\u4f9b\u4e86\u65b0\u7684\u601d\u8def\u3002\u76f8\u5173\u6210\u679c\u4ee5\u201cHighly Stable Lithium Metal Batteries Enabled by Regulating the Solvation of Lithium Ions in Nonaqueous Electrolytes<\/strong>\u201d\u4e3a\u9898\u53d1\u8868\u5728Angew. Chem. Int. Ed.<\/strong>\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u00a0<\/strong>\u56fe<\/strong>1. <\/strong>\u539f\u4f4d\u5149\u5b66\u663e\u5fae\u955c\u89c2\u5bdf\u9502\u6c89\u79ef\u8fc7\u7a0b<\/strong><\/p>\n

\"\"<\/p>\n

a) EC\/DEC\u548cb) FEC\/LiNO3<\/sub>\u7535\u89e3\u6db2\u4e2d\u9502\u7684\u6c89\u79ef\u5f62\u8c8c\uff0c\u6c89\u79ef\u7535\u6d41\u5bc6\u5ea6\u4e3a1.0 mA cm-2<\/sup>\u3002<\/p>\n

\u56fe<\/strong>2. Li | LiFePO4<\/sub><\/strong>\u7ebd\u6263\u53ca\u8f6f\u5305\u7535\u6c60\u7684\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

Li | LiFePO4<\/sub>\u7ebd\u6263\u53ca\u8f6f\u5305\u7535\u6c60\u5728EC\/DEC\u6216FEC\/LiNO3<\/sub>\u7535\u89e3\u6db2\u4e2d\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002a) Li | LiFePO4<\/sub>\u7ebd\u6263\u7535\u6c60\u57280 C\u500d\u7387\u4e0b\u7684\u5faa\u73af\u6027\u80fd\u548c\u5e93\u4ed1\u6548\u7387\u3002b) Li | LiFePO4<\/sub>\u8f6f\u5305\u7535\u6c60\u57282 C\u500d\u7387\u4e0b\u7684\u5faa\u73af\u6027\u80fd\uff0c\u8f6f\u5305\u7535\u6c60\u4f7f\u752850 \u03bcm\u539a\u7684\u9502\u7b94\u4e3a\u8d1f\u6781\u3002c) Li | LiFePO4<\/sub>\u7ebd\u6263\u7535\u6c60\u7684\u7535\u538b-\u5bb9\u91cf\u66f2\u7ebf\u3002d) Li | LiFePO4<\/sub>\u7ebd\u6263\u7535\u6c60\u7684\u7535\u5316\u5b66\u963b\u6297\u8c31(EIS)\u3002e) Li | LiFePO4<\/sub>\u7ebd\u6263\u7535\u6c60\u5728\u221210\u2103\u65f6\uff0c\u4e0d\u540c\u500d\u7387\u4e0b\u7684\u6bd4\u5bb9\u91cf\u548c\u5e93\u4ed1\u6548\u7387\u3002f) Li | LiFePO4<\/sub>\u7ebd\u6263\u7535\u6c60\u572860\u00b0C\u7684\u9ad8\u6e29\u6027\u80fd\u548c\u5e93\u4ed1\u6548\u7387\u3002<\/p>\n

\u56fe<\/strong>3. SEI<\/strong>\u7684\u7ec4\u6210\u548c\u7ed3\u6784\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

\u9502\u91d1\u5c5e\u8d1f\u6781\u5728FEC\/LiNO3<\/sub>\u7535\u89e3\u6db2\u4e2d\u5f62\u6210SEI\u7684\u7ec4\u6210\u548c\u7ed3\u6784\u5206\u6790\u3002a) Li 1s\u8c31\u56fe\uff0cb) N 1s \u8c31\u56fe\u3002c) \u5728FEC\/LiNO3<\/sub>\u7535\u89e3\u6db2\u4e2d\u5f62\u6210\u7684SEI\u7684TEM\u56fe\u50cfd) \u4e0d\u540c\u7535\u89e3\u6db2\u4e0b\uff0c\u9502\u79bb\u5b50\u7a7f\u8fc7SEI\u9700\u8981\u7684\u6d3b\u5316\u80fd\u3002<\/p>\n

\u56fe<\/strong>4. <\/strong>\u8ba1\u7b97\u6a21\u62df\u9502\u79bb\u5b50\u6eb6\u5242\u5316\u5c42<\/strong><\/p>\n

\"\"<\/p>\n

a) FEC\/LiNO3<\/sub>\u548cb) EC\/DEC\u7535\u89e3\u8d28\u6db2\u7684\u5206\u5b50\u52a8\u529b\u5b66\u6a21\u62df\u7ed3\u679c\u3002\u5143\u7d20\u989c\u8272\uff1aH\u767d\uff0cLi\u7d2b\uff0cC\u7070\uff0cO\u7ea2\uff0cN\u84dd\uff0cF\u7eff\u548cP\u9ec4\u3002\u672a\u6eb6\u5242\u5316\u7684\u6eb6\u5242\u5206\u5b50\u4e3a\u6d45\u7070\u8272\u3002c) FEC\/LiNO3<\/sub>\u548cEC\/DEC\u7535\u89e3\u8d28\u4e2dLi\u2013O\u548cLi\u2013F\u5f84\u5411\u5206\u5e03\u51fd\u6570g(r)\u7684\u6a21\u62df\u7ed3\u679c\u3002d) \u57fa\u4e8e\u7b2c\u4e00\u6027\u539f\u7406\u8ba1\u7b97\u7684\u6eb6\u5242\u548c\u9502\u79bb\u5b50\u4e4b\u95f4\u7684\u7ed3\u5408\u80fd\u3002e) FEC\/LiNO3<\/sub>\u548cf) EC\/DEC\u7535\u89e3\u6db2\u4e2d\u5f62\u6210\u7684\u9502\u79bb\u5b50\u6eb6\u5242\u5316\u5c42\u3001\u5f62\u6210SEI\u7684\u793a\u610f\u56fe\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u00a0<\/strong>\u57fa\u4e8e\u8c03\u63a7\u9502\u79bb\u5b50\u6eb6\u5242\u5316\u5c42\u7684\u601d\u8def\uff0cFEC\u548cLiNO3<\/sub>\u88ab\u540c\u65f6\u5f15\u5165\u5230\u7535\u89e3\u6db2\u4e2d\uff0c\u5f62\u6210\u4e00\u79cd\u65b0\u578b\u7684\u7535\u89e3\u6db2\u3002FEC\u66ff\u4ee3\u4f20\u7edf\u7684EC\u4f5c\u4e3a\u5171\u6eb6\u5242\u53c2\u4e0e\u6eb6\u5242\u5316\u5c42\uff0c\u540c\u65f6\uff0cLiNO3<\/sub> \u901a\u8fc7\u6eb6\u5242\u5316\u4f5c\u7528\u6eb6\u4e8e\u919a\u916f\u6df7\u5408\u7535\u89e3\u6db2\u5e76\u53c2\u4e0e\u6eb6\u5242\u5316\u5c42\u3002\u7531\u4e8e\u6eb6\u5242\u5316\u5c42\u7ec4\u6210\u548c\u7ed3\u6784\u7684\u6539\u53d8\uff0c\u5bfc\u81f4\u751f\u6210\u7684SEI\u4e2d\u5bcc\u542bLiF\u548cLiNx<\/sub>Oy<\/sub>, \u4ece\u800c\u589e\u5f3aSEI\u7684\u5747\u5300\u6027\uff0c\u6291\u5236\u9502\u679d\u6676\u7684\u751f\u957f\u3002\u8be5\u65b0\u578b\u7535\u89e3\u6db2\u5728\u7ebd\u6263\u7535\u6c60\u548c\u8f6f\u5305\u7535\u6c60\u4e2d\u5747\u5c55\u73b0\u51fa\u9ad8\u5e93\u4f26\u6548\u7387\u548c\u957f\u5faa\u73af\u5bff\u547d\u7684\u7279\u6027\uff0c\u9502\u91d1\u5c5e\u7535\u6c60\u7a33\u5b9a\u6027\u663e\u8457\u589e\u5f3a\u3002\u540c\u65f6\uff0c\u8be5\u65b0\u578b\u7535\u89e3\u6db2\u5728\u9ad8\u4f4e\u6e29\u6761\u4ef6\u4e0b\u4ecd\u53ef\u4fdd\u6301\u7a33\u5b9a\u5faa\u73af\u6027\u80fd\uff0c\u5177\u6709\u8f83\u5bbd\u7684\u5de5\u4f5c\u6e29\u5ea6\u7a97\u53e3\u3002\u7406\u8bba\u6a21\u62df\u5219\u8fdb\u4e00\u6b65\u63ed\u793a\u4e86\u6eb6\u5242\u5316\u5c42\u7ec4\u6210\u548c\u7ed3\u6784\u7684\u6539\u53d8\uff0c\u4e3a\u4e4b\u540e\u65b0\u578b\u7535\u89e3\u6db2\u7684\u7814\u53d1\u63d0\u4f9b\u4e86\u65b0\u7684\u601d\u8def\u3002<\/p>\n

\u672c\u5de5\u4f5c\u7684\u4f5c\u8005\u4f9d\u6b21\u662f\u5f20\u5b66\u5f3a\u3001\u9648\u7fd4\u3001\u7a0b\u65b0\u5175\u3001\u674e\u535a\u6743\u3001\u6c88\u99a8\u3001\u95eb\u5d07\u3001\u9ec4\u4f73\u7426\u548c\u5f20\u5f3a\u3002<\/strong><\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a <\/strong>Highly Stable Lithium Metal Batteries Enabled by Regulating the Solvation of Lithium Ions in Nonaqueous Electrolytes <\/a>(Angew. Chem. Int. Ed. 2018, DOI: 10.1002\/anie.201801513, \u7b2c\u4e00\u4f5c\u8005\u4e3a\u5f20\u5b66\u5f3a\uff0c\u901a\u8baf\u4f5c\u8005\u4e3a\u5f20\u5f3a\u6559\u6388)<\/p>\n

\u8fd1\u5e74\u6765\uff0c\u6e05\u534e\u5927\u5b66\u5f20\u5f3a\u6559\u6388\u7814\u7a76\u56e2\u961f<\/strong>\u5728\u91d1\u5c5e\u9502\u8d1f\u6781\u7684\u7814\u7a76\u4e0d\u65ad\u53d6\u5f97\u65b0\u7684\u8fdb\u5c55\u3002\u901a\u8fc7\u539f\u4f4d\u624b\u6bb5\u7814\u7a76\u56fa\u6001\u7535\u89e3\u8d28\u754c\u9762\u819c\uff0c\u5e76\u91c7\u7528\u7eb3\u7c73\u9aa8\u67b6\u3001\u4eba\u5de5SEI\u3001\u8868\u9762\u56fa\u6001\u7535\u89e3\u8d28\u4fdd\u62a4\u8c03\u63a7\u91d1\u5c5e\u9502\u7684\u6c89\u79ef\u884c\u4e3a\uff0c\u6291\u5236\u9502\u679d\u6676\u7684\u751f\u957f\uff0c\u5b9e\u73b0\u91d1\u5c5e\u9502\u7684\u9ad8\u6548\u5b89\u5168\u5229\u7528\u3002\u8fd9\u4e9b\u76f8\u5173\u7814\u7a76\u5de5\u4f5c\u53d1\u8868\u5728Nat. Commun., Adv. Mater., Adv. Funct. Mater., Chem, Joule, Energy Storage Mater.<\/em>\u7b49\u671f\u520a\u3002\u6700\u8fd1\uff0c\u5f20\u5f3a\u6559\u6388\u56e2\u961f\u56f4\u7ed5\u7740\u5b89\u5168\u3001\u9ad8\u6bd4\u80fd\u91d1\u5c5e\u9502\u7535\u6c60\uff0c\u5728Chem. Rev. <\/em>(10.1021\/acs.chemrev.7b00115), Adv. Sci. <\/em>(10.1002\/advs.201600445), Adv. Mater. Interfaces <\/em>(10.1002\/admi.201701097)\u4e0a\u53d1\u8868\u7efc\u8ff0\u6587\u7ae0\uff0c\u7cfb\u7edf\u9610\u8ff0\u4e86\u91d1\u5c5e\u9502\u7684\u7814\u7a76\u8109\u7edc\u548c\u8fdb\u5c55\uff0c\u53d7\u5230\u5e7f\u6cdb\u5173\u6ce8\u3002<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u8ba1\u7b97\u6750\u6599\u7ec4Annay\u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u6574\u7406\u7f16\u8f91\u3002<\/p>\n

\u6750\u6599\u725b\u7f51\u4e13\u6ce8\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u53ca\u884c\u4e1a\u8fdb\u5c55\uff0c\u8fd9\u91cc\u6c47\u96c6\u4e86\u5404\u5927\u9ad8\u6821\u7855\u535a\u751f\u3001\u4e00\u7ebf\u79d1\u7814\u4eba\u5458\u4ee5\u53ca\u884c\u4e1a\u4ece\u4e1a\u8005\uff0c\u5982\u679c\u60a8\u5bf9\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u8fdb\u5c55\uff0c\u89e3\u8bfb\u9ad8\u6c34\u5e73\u6587\u7ae0\u6216\u662f\u8bc4\u8ff0\u884c\u4e1a\u6709\u5174\u8da3\uff0c\u70b9\u6211\u52a0\u5165\u7f16\u8f91\u90e8\u5927\u5bb6\u5ead<\/a>\u3002<\/p>\n

\u6b22\u8fce\u5927\u5bb6\u5230\u6750\u6599\u4eba\u5ba3\u4f20\u79d1\u6280\u6210\u679c\u5e76\u5bf9\u6587\u732e\u8fdb\u884c\u6df1\u5165\u89e3\u8bfb\uff0c\u6295\u7a3f\u90ae\u7bb1tougao@cailiaoren.com<\/a>\u3002<\/p>\n

\u6295\u7a3f\u4ee5\u53ca\u5185\u5bb9\u5408\u4f5c\u53ef\u52a0\u7f16\u8f91\u5fae\u4fe1\uff1a<\/strong>RDD-2011-CHERISH<\/strong>\uff0c\u4efb\u4e39\u4e39\uff0c\u6211\u4eec\u4f1a\u9080\u8bf7\u5404\u4f4d\u8001\u5e08\u52a0\u5165\u4e13\u5bb6\u7fa4\u3002<\/strong><\/p>\n

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