{"id":131779,"date":"2018-03-30T14:00:50","date_gmt":"2018-03-30T06:00:50","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=131779"},"modified":"2018-03-31T19:47:21","modified_gmt":"2018-03-31T11:47:21","slug":"%e4%b8%ad%e7%a7%91%e5%a4%a7nature-nanotechnology-%e4%ba%8c%e6%b0%a7%e5%8c%96%e7%a2%b3%e5%8a%a0%e6%b0%a2%e8%bf%87%e7%a8%8b%e4%b8%ad%e8%bf%91%e9%82%bbpt%e5%8d%95%e5%8e%9f%e5%ad%90%e9%97%b4%e5%8d%8f","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=131779","title":{"rendered":"\u4e2d\u79d1\u5927Nature Nanotechnology : \u4e8c\u6c27\u5316\u78b3\u52a0\u6c22\u8fc7\u7a0b\u4e2d\u8fd1\u90bbPt\u5355\u539f\u5b50\u95f4\u534f\u540c\u4f5c\u7528"},"content":{"rendered":"

\u3010<\/strong>\u5f15\u8a00<\/strong>\u3011<\/strong><\/p>\n

\u5355\u539f\u5b50\u50ac\u5316\u672c\u8eab\u56e0\u5176\u539f\u5b50\u5229\u7528\u7387\u9ad8\uff0c\u539f\u5b50\u914d\u4f4d\u6570\u4f4e\uff0c\u91d1\u5c5e-\u8f7d\u4f53\u5f3a\u76f8\u4e92\u4f5c\u7528\u7b49\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u50ac\u5316\u6027\u80fd\u800c\u5907\u53d7\u5173\u6ce8\u3002\u5728\u50ac\u5316\u5242\u4e2d\uff0c\u5f53\u4e24\u4e2a\u50ac\u5316\u6d3b\u6027\u4e2d\u5fc3\u7684\u8ddd\u79bb\u51cf\u5c0f\u5230\u539f\u5b50\u5c3a\u5ea6\u65f6\uff0c\u6d3b\u6027\u4e2d\u5fc3\u4e4b\u95f4\u7684\u76f8\u4e92\u4f5c\u7528\u5c31\u5c06\u4f1a\u6781\u5927\u5730\u5f71\u54cd\u5230\u50ac\u5316\u5242\u672c\u8eab\u7684\u50ac\u5316\u6027\u80fd\u3002\u7531\u4e8e\u5355\u539f\u5b50\u8868\u9762\u80fd\u5f88\u9ad8\uff0c\u4e3a\u4e86\u907f\u514d\u5355\u539f\u5b50\u5728\u8f7d\u4f53\u8868\u9762\u56e2\u805a\uff0c\u5176\u8d1f\u8f7d\u91cf\u4e00\u822c\u8f83\u4f4e\u3002\u56e0\u6b64\u4e24\u4e2a\u76f8\u90bb\u6d3b\u6027\u4f4d\u70b9\u4e4b\u95f4\u7684\u8ddd\u79bb\u76f8\u5bf9\u8f83\u8fdc\uff0c\u6b64\u65f6\u4e24\u5355\u539f\u5b50\u4e4b\u95f4\u7684\u76f8\u4e92\u4f5c\u7528\u5c31\u57fa\u672c\u88ab\u5ffd\u7565\u3002\u800c\u5982\u679c\u80fd\u591f\u63d0\u9ad8\u5355\u539f\u5b50\u50ac\u5316\u5242\u7684\u8d1f\u8f7d\u91cf\uff0c\u8ba9\u5176\u65e2\u6709\u5355\u539f\u5b50\u7684\u4f18\u70b9\uff0c\u53c8\u80fd\u589e\u52a0\u90bb\u8fd1\u539f\u5b50\u4e4b\u95f4\u7684\u76f8\u4e92\u4f5c\u7528\uff0c\u5c31\u6709\u671b\u5b9e\u73b0\u5355\u539f\u5b50\u95f4\u7684\u534f\u540c\u4f5c\u7528\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u4e2d\u56fd\u79d1\u6280\u5927\u5b66\u66fe\u6770\u6559\u6388\u548c\u5f20\u6587\u534e\u526f\u6559\u6388<\/strong>\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09\u5728Nat. Nanotech.\u4e0a\u53d1\u8868\u9898\u4e3a\u201cSynergetic interaction between neighbouring platinum monomers in CO2<\/sub> hydrogenation\u201d\u7684\u6587\u7ae0\u3002\u8be5\u7814\u7a76\u8868\u660eMoS2<\/sub>\u4e0a\u8fd1\u90bbPt\u5355\u539f\u5b50\u4e4b\u95f4\u7684\u534f\u540c\u4f5c\u7528\u53ef\u4ee5\u6781\u5927\u5730\u63d0\u9ad8CO2<\/sub>\u52a0\u6c22\u50ac\u5316\u6d3b\u6027\u5e76\u964d\u4f4e\u76f8\u5e94\u7684\u6d3b\u5316\u80fd\u3002\u901a\u8fc7\u5c06Pt\u7684\u8d28\u91cf\u8d1f\u8f7d\u589e\u52a0\u81f37.5\uff05\u540c\u65f6\u4fdd\u6301Pt\u7684\u539f\u5b50\u7ea7\u5206\u6563\uff0c\u5f97\u5230\u4e86\u8fd1\u90bbPt\u5355\u539f\u5b50\u3002\u673a\u7406\u7814\u7a76\u8868\u660e\uff0c\u8fd1\u90bbPt\u5355\u539f\u5b50\u4e0d\u4ec5\u534f\u540c\u50ac\u5316\u964d\u4f4e\u4e86\u53cd\u5e94\u80fd\u5792\uff0c\u800c\u4e14\u4e0e\u5b64\u7acb\u7684\u5355\u539f\u5b50\u76f8\u6bd4\u8fd8\u6539\u53d8\u4e86\u53cd\u5e94\u8def\u5f84\u3002\u5b64\u7acb\u7684Pt\u5355\u539f\u5b50\u5c06CO2<\/sub>\u76f4\u63a5\u8f6c\u5316\u4e3a\u7532\u9187\u800c\u4e0d\u4ea7\u751f\u7532\u9178\u4e2d\u95f4\u7269\u79cd\uff0c\u8fd1\u90bb\u5355\u539f\u5b50\u5219\u662f\u5c06CO2<\/sub>\u9010\u6b65\u52a0\u6c22\u6210\u7532\u9178\u548c\u7532\u9187\u3002\u8be5\u53d1\u73b0\u4e3a\u5355\u539f\u5b50\u50ac\u5316\u9886\u57df\u7684\u7814\u7a76\u5f00\u8f9f\u4e86\u65b0\u7684\u65b9\u5411\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb<\/strong>\u3011<\/p>\n

\u56fe<\/strong>1 Pt\/MoS2<\/sub><\/strong>\u7684\u7ed3\u6784\u6027\u8d28<\/strong><\/p>\n

\"\"<\/p>\n

a) 0.2\uff05\u8d1f\u8f7d\u91cf\u4e0bPt\/MoS2<\/sub>\u7684HAADF-STEM\u56fe\uff1b<\/p>\n

b, c) 0.2\uff05\u8d1f\u8f7d\u91cf\u4e0bPt\/MoS2<\/sub>\u7684\u653e\u5927HAADF-STEM\u56fe\u53ca\u5176\u76f8\u5e94\u7ed3\u6784\u6a21\u578b(\u56fe\u4e2d\u53ef\u660e\u663e\u89c2\u5bdf\u5230\u5206\u6563\u7684Pt\u5355\u539f\u5b50)\uff1b<\/p>\n

d) 7.5%\u8d1f\u8f7d\u91cf\u4e0bPt\/MoS2<\/sub>\u7684HAADF-STEM\u56fe\uff1b<\/p>\n

e, f) 7.5\uff05\u8d1f\u8f7d\u91cf\u4e0bPt\/MoS2<\/sub>\u7684\u653e\u5927HAADF-STEM\u56fe\u50cf\u53ca\u5176\u76f8\u5e94\u7684\u7ed3\u6784\u6a21\u578b(\u56fe\u4e2d\u53ef\u89c2\u5bdf\u5230\u8fd1\u90bbPt\u5355\u539f\u5b50);<\/p>\n

g)\u4e0d\u540c Pt\/MoS2<\/sub>\u7684Pt K\u8fb9XANES\u5149\u8c31(\u4ee5Pt\u7b94\u4e3a\u53c2\u8003)\uff1b<\/p>\n

h\uff09\u4e0d\u540cPt \/MoS2<\/sub>\u7684Pt K-edge EXAFS (Pt\u7b94\u4e3a\u53c2\u8003\uff0c\u865a\u7ebf\u662f\u76f8\u5e94\u7684\u62df\u5408\u66f2\u7ebf)<\/p>\n

i) \u57fa\u4e8eHAADF-STEM\u56fe\u7684\u76f4\u63a5\u89c2\u5bdf\uff0c\u5728\u4e0d\u540cPt\u8d1f\u8f7d\u91cf\u7684Pt\/MoS2<\/sub>\u4e2d\u5b64\u7acbPt\u5355\u539f\u5b50\u3001\u8fd1\u90bbPt\u5355\u539f\u5b50\u548c\u5c0f\u7247Pt\u5355\u539f\u5b50\u7684\u7edf\u8ba1\u76f4\u65b9\u56fe<\/p>\n

\uff08c\u548cf\u4e2d\u7684\u84dd\u8272\uff0c\u9752\u8272\u548c\u9ec4\u8272\u7403\u5206\u522b\u4ee3\u8868Pt\uff0cMo\u548cS\u539f\u5b50\uff09<\/p>\n

\u5c0f\u7ed3\uff1a<\/strong><\/p>\n

1.(a-c)\u76f4\u63a5\u89c2\u6d4b\u5230\u5b64\u7acbPt\u5355\u539f\u5b50\u3002<\/p>\n

2.(b-f)\u76f4\u63a5\u89c2\u6d4b\u5230\u8fd1\u90bbPt\u5355\u539f\u5b50\u3002<\/p>\n

3.g\u8868\u660e\u5355\u539f\u5b50\u5904\u4e8e\u6c27\u5316\u6001\u3002<\/p>\n

4.h\u56fe\u8bc1\u660ePt\u8d1f\u8f7d\u91cf\u57282%\u81f37.5%\u65f6\uff0c\u4e0d\u5b58\u5728Pt-Pt\u952e\uff0c\u5373Pt\u5747\u4ee5\u5355\u539f\u5b50\u5f62\u5f0f\u5b58\u5728\u3002<\/p>\n

5.\u53ea\u6709\u4e0ePt\u914d\u4f4d\u7684S\u539f\u5b50\u6709\u5229\u4e8e\u5438\u9644H\uff0c\u56e0\u6b64Pt\u548c\u4e0e\u5176\u914d\u4f4d\u7684S\u539f\u5b50\u6784\u6210\u4e00\u4e2a\u6d3b\u6027\u4e2d\u5fc3\u3002<\/p>\n

\"\"<\/p>\n

Pt\/MoS2<\/sub>\u5355\u539f\u5b50\u50ac\u5316\u5242\u4e2d\uff0cH\u539f\u5b50\u5728\u4e0d\u540cS\u539f\u5b50\u4e0a\u7684\u5438\u9644\u80fd\u3002<\/p>\n

\u56fe<\/strong>2<\/strong> Pt\/MoS2<\/sub><\/strong>\u7684<\/strong>CO2<\/sub><\/strong>\u50ac\u5316\u52a0\u6c22\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

a\uff09\u4e0d\u540cPt\/MoS2<\/sub>\u5f97\u5230\u7684\u4ea7\u7269\u6bd4\u8f83\uff1b<\/p>\n

b\uff090.2\uff05Pt\/MoS2<\/sub>\u548c7.5\uff05Pt\/MoS2<\/sub>\u7684TOF\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684\u6bd4\u8f83\uff1b<\/p>\n

c\uff090.2\uff05\u8d1f\u8f7d\u91cf\u7684Pt\/MoS2<\/sub>\u548c7.5\uff05Pt\/MoS2<\/sub>\u7684Arrhenius\u56fe\uff1b<\/p>\n

d\uff09\u4f7f\u75280.2\uff05Pt\/MoS2<\/sub>\u548c7.5\uff05Pt\/MoS2<\/sub>\u4f5c\u4e3a\u50ac\u5316\u5242\u4e14\u5728\u4e0d\u540c\u6bd4\u4f8b\u7684CO2<\/sub>\u4e0eH2<\/sub>\u4e0b3\u5c0f\u65f6\u540e\u83b7\u5f97\u7684\u4ea7\u7269\u7684\u9009\u62e9\u6027\u6bd4\u8f83\uff08\u8bef\u5dee\u7ebf\u4ee3\u8868\u4e09\u6b21\u72ec\u7acb\u6d4b\u91cf\u7684\u6807\u51c6\u504f\u5dee\uff09\uff1b<\/p>\n

\u5c0f\u7ed3\uff1a<\/strong><\/p>\n

1.\u8fd1\u90bbPt\u5355\u539f\u5b50\u50ac\u5316\u6d3b\u6027\u9ad8\u4e8e\u5b64\u7acbPt\u5355\u539f\u5b50\u3002<\/p>\n

2.\u8fd1\u90bbPt\u5355\u539f\u5b50\u5bf9\u7532\u9187\u7684\u9009\u62e9\u6027\u4f4e\u4e8e\u5b64\u7acbPt\u5355\u539f\u5b50\u3002<\/p>\n

\u56fe<\/strong>3 <\/strong>\u53cd\u5e94\u7269\u4e0e<\/strong>Pt\/MoS2<\/sub><\/strong>\u4e4b\u95f4\u7684\u76f8\u4e92\u4f5c\u7528<\/strong><\/p>\n

\"\"<\/p>\n

a) \u5177\u6709\u4e0d\u540cPt\u8d1f\u8f7d\u7684\u539f\u5b50\u5206\u6563\u7684Pt\/MoS2<\/sub>\u7684H2<\/sub>-TPD\u5206\u5e03\u56fe\uff1b<\/p>\n

b) 0.2\uff05Pt\/MoS2<\/sub>\u548c5\uff05Pt\/MoS2<\/sub>\u7684\u539f\u4f4dDRIFT\u8c31,\u5728150\u2103\u4e0b\u5c06\u6837\u54c1\u66b4\u9732\u4e8e\u6df7\u5408\u6c14\u4f53\uff08CO2<\/sub>\uff1aH2<\/sub> = 1\uff1a3, 1bar\uff090.5\u5c0f\u65f6\u540e\u83b7\u5f97\u5149\u8c31;<\/p>\n

c, d) 0.2\uff05Pt\/MoS2<\/sub>\u548c7.5\uff05Pt\/MoS2<\/sub>\u7684C1s<\/sub>\u548cO1s<\/sub>\u7684\u539f\u4f4dXPS\u8c31(\u5728\u7528\u6df7\u5408\u6c14\u4f53\uff08CO2<\/sub>\uff1aH2<\/sub> = 1\uff1a3\uff0c1bar\uff09\u5728150\u2103\u4e0b\u5904\u7406\u6837\u54c10.5\u5c0f\u65f6\u540e\u83b7\u5f97\u539f\u4f4dXPS\u8c31);<\/p>\n

\u00a0<\/strong>\u5c0f\u7ed3\uff1a<\/strong><\/p>\n

1.\u5b64\u7acbPt\u5355\u539f\u5b50\u4e3b\u8981\u4e2d\u95f4\u7269\u79cd\u4e3aCOOH*\u3002<\/p>\n

2.\u8fd1\u90bbPt\u5355\u539f\u5b50\u4e3b\u8981\u4e2d\u95f4\u7269\u79cd\u4e3aCH2<\/sub>OH*\u3002<\/p>\n

\u56fe<\/strong>4 <\/strong>\u91cf\u5316\u8ba1\u7b97<\/strong><\/p>\n

\"\"<\/p>\n

a, b) \u5206\u522b\u9488\u5bf9Pt1<\/sub>\/MoS2<\/sub>\u548cPt2iii<\/sub>\/MoS2<\/sub>\u5728CO2<\/sub>\u52a0\u6c22\u4e2d\u4f18\u5316\u7684\u53cd\u5e94\u8def\u5f84\uff1b<\/p>\n

c, d) \u5206\u522b\u5728Pt1<\/sub> \/ MoS2<\/sub>\u548cPt2iii<\/sub>\/MoS2<\/sub>\u4e0a\u5411COOH *\u6dfb\u52a0H\u539f\u5b50\u7684\u6b65\u9aa4\uff1b<\/p>\n

\u5c0f\u7ed3\uff1a<\/strong><\/p>\n

1.\u5b64\u7acbPt\u5355\u539f\u5b50\u8def\u5f84\u5728CO2<\/sub>\u52a0\u6c22\u5236\u7532\u9187\u8fc7\u7a0b\u4e2d\u4e0d\u7ecf\u5386\u7532\u9178\u4e2d\u95f4\u7269\u79cd\uff0c\u9650\u901f\u6b65\u5728CH2<\/sub>OH*-CH3<\/sub>OH\uff0c\u56e0\u6b64CH2<\/sub>OH*\u4e3a\u4e3b\u8981\u4e2d\u95f4\u7269\u79cd\u3002<\/p>\n

2.\u8fd1\u90bbPt\u5355\u539f\u5b50\u8def\u5f84\u5728CO2<\/sub>\u52a0\u6c22\u5236\u7532\u9187\u8fc7\u7a0b\u4e2d\u6709\u7532\u9178\u4e2d\u95f4\u7269\u79cd\uff0c\u9650\u901f\u6b65\u5728COOH*-HCOOH\uff0c\u56e0\u6b64COOH*\u4e3a\u4e3b\u8981\u4e2d\u95f4\u7269\u79cd\u3002<\/p>\n

3.\u4e24\u79cd\u5355\u539f\u5b50\u7684\u53cd\u5e94\u8def\u5f84\u4e0d\u540c\u3002<\/p>\n

\u3010\u603b\u7ed3\u3011<\/strong><\/p>\n

\u8be5\u7814\u7a76\u6210\u679c\u8868\u660e\uff0c\u8fd1\u90bbPt\u5355\u539f\u5b50\u4e4b\u95f4\u7684\u534f\u540c\u4f5c\u7528\u4f1a\u8bf1\u5bfc\u4e0d\u540c\u7684\u53cd\u5e94\u8def\u5f84\uff0c\u5e76\u6539\u5584CO2<\/sub>\u52a0\u6c22\u7684\u50ac\u5316\u6027\u80fd\u3002\u4e3a\u5c06\u4e8c\u6c27\u5316\u78b3\u8f6c\u5316\u4e3a\u6709\u7528\u7684\u5316\u5b66\u54c1\u6216\u71c3\u6599\u63d0\u4f9b\u4f9d\u636e\uff0c\u4e0d\u4ec5\u6709\u52a9\u4e8e\u7f13\u89e3\u5168\u7403\u53d8\u6696\uff0c\u800c\u4e14\u8fd8\u5c06\u51cf\u8f7b\u5bf9\u77f3\u5316\u4ea7\u54c1\u7684\u4f9d\u8d56\u4ee5\u6ee1\u8db3\u5f53\u524d\u80fd\u6e90\u9700\u6c42\u3002\u7814\u7a76\u4e2d\u901a\u8fc7\u589e\u52a0Pt\u8d28\u91cf\u8d1f\u8f7d\u52307.5\uff05\uff0c\u540c\u65f6\u4ecd\u7136\u4fdd\u6301Pt\u7684\u539f\u5b50\u5206\u6563\uff0c\u83b7\u5f97\u4e86\u8fd1\u90bb\u7684Pt\u5355\u539f\u5b50\u3002\u8fd1\u90bbPt\u5355\u539f\u5b50\u5728CO2<\/sub>\u52a0\u6c22\u5230\u7532\u9187\u4e2d\u8868\u73b0\u51fa\u6bd4\u5b64\u7acb\u5355\u539f\u5b50\u66f4\u9ad8\u7684\u50ac\u5316\u6d3b\u6027\u548c\u66f4\u4f4e\u7684\u6d3b\u5316\u80fd\u3002\u8fd1\u90bb\u5355\u539f\u5b50\u4e4b\u95f4\u534f\u540c\u4f5c\u7528\u7684\u53d1\u73b0\u5c06\u4e3a\u64cd\u7eb5\u50ac\u5316\u6027\u8d28\u521b\u9020\u65b0\u7684\u9014\u5f84\uff0c\u5e76\u63a8\u8fdb\u5bf9\u591a\u76f8\u50ac\u5316\u673a\u7406\u7684\u7406\u89e3\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5<\/strong>\uff1aSynergetic interaction between neighbouring platinum monomers in CO2<\/sub> hydrogenation<\/strong><\/a> (Nature Nanotechnology,<\/em> 2018, doi:10.1038\/s41565-018-0089-z)<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u65b0\u80fd\u6e90\u7ec4\u8fde\u5a77\u5a77\u4f9b\u7a3f\uff0c\u70b9\u6211\u52a0\u5165\u6750\u6599\u4eba\u7f16\u8f91\u90e8<\/a>\u3002<\/p>\n

\u6295\u7a3f\u4ee5\u53ca\u5185\u5bb9\u5408\u4f5c\u53ef\u52a0\u7f16\u8f91\u5fae\u4fe1\uff1acailiaokefu<\/strong>\u3002<\/strong><\/p>\n

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