{"id":133884,"date":"2018-04-10T06:30:46","date_gmt":"2018-04-09T22:30:46","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=133884"},"modified":"2018-04-08T18:16:07","modified_gmt":"2018-04-08T10:16:07","slug":"chem-mater-%ef%bc%9a%e4%bb%8e%e5%8e%9f%e5%ad%90%e5%b0%ba%e5%af%b8%e6%8f%ad%e7%a4%bazr%e8%a1%a8%e9%9d%a2%e4%bf%ae%e9%a5%b0%e6%8f%90%e5%8d%87%e9%ab%98%e5%ae%b9%e9%87%8f%e6%ad%a3%e6%9e%81%e6%9d%90","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=133884","title":{"rendered":"Chem. Mater.\uff1a\u4ece\u539f\u5b50\u5c3a\u5bf8\u63ed\u793aZr\u8868\u9762\u4fee\u9970\u63d0\u5347\u9ad8\u5bb9\u91cf\u6b63\u6781\u6750\u6599\u7535\u5316\u5b66\u6027\u80fd\u7684\u539f\u7406"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u968f\u7740\u5148\u8fdb\u4fbf\u643a\u5f0f\u7535\u5b50\u4ea7\u54c1\u3001\u7535\u52a8\u6c7d\u8f66\u7b49\u7684\u5feb\u901f\u53d1\u5c55\uff0c\u5bf9\u4e8e\u7535\u6c60\u7684\u80fd\u91cf\u5bc6\u5ea6\u63d0\u51fa\u4e86\u66f4\u9ad8\u7684\u8981\u6c42\u3002\u9ad8\u5bb9\u91cf\u7684\u6b63\u6781\u6750\u6599\uff0c\u5982\u9ad8\u954d\u4e09\u5143\u6b63\u6781\u6750\u6599\uff0c\u5bcc\u9502\u6b63\u6781\u6750\u6599\u7b49\uff0c\u56e0\u5176\u9ad8\u7684\u6bd4\u5bb9\u91cf\uff0c\u9ad8\u7684\u8131\u5d4c\u9502\u7535\u4f4d\uff0c\u4f4e\u7684\u94b4\u542b\u91cf\u7b49\uff0c\u6210\u4e3a\u8fd1\u671f\u5173\u6ce8\u7684\u7126\u70b9\u3002\u7136\u800c\uff0c\u4e0a\u8ff0\u9ad8\u5bb9\u91cf\u6b63\u6781\u6750\u6599\u666e\u904d\u5b58\u5728\u9633\u79bb\u5b50\u6df7\u6392\u4e25\u91cd\uff0c\u8868\u9762\u6676\u4f53\u7ed3\u6784\u4e0d\u7a33\u5b9a\u7b49\u95ee\u9898\uff0c\u7535\u5316\u5b66\u8131\u5d4c\u9502\u8fc7\u7a0b\u4e2d\uff0c\u8868\u9762\u5bb9\u6613\u88ab\u7535\u89e3\u6db2\u4fb5\u8680\uff0c\u53d1\u751f\u6c27\u6790\u51fa\u3001\u8fc7\u6e21\u91d1\u5c5e\u79bb\u5b50\u6eb6\u89e3\u7b49\u73b0\u8c61\uff0c\u9020\u6210\u4e25\u91cd\u7684\u5bb9\u91cf\u8870\u51cf\u3001\u5dee\u7684\u5faa\u73af\u6027\u80fd\u53ca\u500d\u7387\u6027\u80fd\u7b49\u3002<\/p>\n

\u91c7\u7528Zr\u6216Zr\u57fa\u5316\u5408\u7269\u8868\u9762\u4fee\u9970\u6b63\u6781\u6750\u6599\u5df2\u88ab\u8bc1\u660e\u80fd\u591f\u6709\u6548\u4fc3\u8fdb\u5176\u7535\u5316\u5b66\u6027\u80fd\u63d0\u5347\u3002\u4f5c\u8005\u8bfe\u9898\u7ec4\u524d\u671f\u4e5f\u91c7\u7528Zr\u5143\u7d20\u5f00\u5c55\u4e86\u8868\u9762\u4fee\u9970LiNi1\/3<\/sub>Co1\/3<\/sub>Mn1\/3<\/sub>O2<\/sub>\u53caLiNi0.8<\/sub>Co0.1<\/sub>Mn0.1<\/sub>O2<\/sub>\u4e09\u5143\u6b63\u6781\u6750\u6599\u7684\u5de5\u4f5c\uff08Xing Li, Hui Peng, Ming-Shan Wang, XingZhao, Peng-XiaoHuang, WeiYang, JunXu, Zhi-QiangWang, Mei-Zhen Qu, Zuo-Long Yu, Enhanced Electrochemical Performance of Zr-Modified Layered LiNi1\/3<\/sub>Co1\/3<\/sub>Mn1\/3<\/sub>O2<\/sub> Cathode Material for Lithium-Ion Batteries, ChemElectroChem, 2016,3,130\u2013137<\/strong>; Xing Li, Kangjia Zhang, MingShan Wang, Yang Liu, MeiZhen Qu, Wengao Zhao, Jianming Zheng, Dual functions of Zirconium modification on improving the electrochemical performance of Ni-rich LiNi0.8<\/sub>Co0.1<\/sub>Mn0.1<\/sub>O2<\/sub>, Sustainable Energy & Fuels<\/strong>\uff0c<\/strong>2018, 2, 413-421.<\/strong>\uff09\u3002\u7814\u7a76\u8ba4\u4e3a\uff0cZr\u8868\u9762\u4fee\u9970\u53ef\u4ee5\u4fc3\u8fdb\u88ab\u4fee\u9970\u6b63\u6781\u6750\u6599\u7684\u6676\u4f53\u7ed3\u6784\u7a33\u5b9a\u6027\uff0c\u540c\u65f6\u5728\u6b63\u6781\u6750\u6599\u8868\u9762\u5f62\u6210\u4e00\u5c42Li2<\/sub>ZrO3<\/sub>\u5305\u8986\u5c42\uff0c\u4ece\u800c\u6709\u6548\u6291\u5236\u5176\u7535\u5316\u5b66\u5faa\u73af\u8fc7\u7a0b\u4e2d\u88ab\u7535\u89e3\u6db2\u4fb5\u8680\u3001\u6291\u5236\u8868\u9762\u6c27\u6790\u51fa\u53ca\u8fc7\u6e21\u91d1\u5c5e\u79bb\u5b50\u6eb6\u89e3\uff0c\u63d0\u5347\u5176\u7535\u5316\u5b66\u6027\u80fd\u3002\u7136\u800c\uff0c\u4e0a\u8ff0\u7814\u7a76\u9c9c\u6709\u4ece\u539f\u5b50\u5c3a\u5bf8\u6e05\u6670\u9610\u8ff0Zr\u8868\u9762\u4fee\u9970\u5bf9\u6b63\u6781\u6750\u6599\u8868\u9762\u6676\u4f53\u7ed3\u6784\u53ca\u6b63\u6781\u6750\u6599\/\u7535\u89e3\u6db2\u754c\u9762CEI\uff08Cathode Electrolyte Interface\uff09\u819c\u7684\u5f71\u54cd\u3002<\/p>\n

\u3010\u6210\u679c\u4ecb\u7ecd\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u897f\u5357\u77f3\u6cb9\u5927\u5b66\u674e\u661f\u535a\u58eb\u4e0e\u7f8e\u56fd\u897f\u5317\u592a\u5e73\u6d0b\u56fd\u5bb6\u5b9e\u9a8c\u5ba4\u90d1\u5efa\u660e\u535a\u58eb\u3001\u6768\u632f\u4e2d\u535a\u58eb\uff0c\u7f8e\u56fd<\/strong>Clarkson University<\/strong>\u7684<\/strong>David Mitlin<\/strong>\u535a\u58eb\u7b49<\/strong>\u5229\u7528STEM\uff08Aberration-corrected Scanning Transmission Electron microscopy\uff09\u53caEIS\uff08Electrochemical Impedance Spectroscopy\uff09\u4ece\u539f\u5b50\u5c3a\u5bf8\u89d2\u5ea6\u63ed\u793a\u4e86Zr\u8868\u9762\u4fee\u9970\u5bf9\u4e8eLi\/Mn-Rich\u6b63\u6781\u6750\u6599Li[Li0.2<\/sub>Ni0.13<\/sub>Co0.13<\/sub>Mn0.54<\/sub>]O2<\/sub>\uff08LMR\uff09\u7684\u6027\u80fd\u63d0\u5347\u539f\u7406\u3002<\/p>\n

STEM\u89c2\u5bdf\u8868\u660e\uff0cZr\u5143\u7d20\u80fd\u591f\u5728LMR\u6b63\u6781\u6750\u6599\u8868\u9762\u5f62\u6210\u4e00\u5c421~2 nm\u7684Zr\u57fa\u5ca9-\u76d0\u76f8\uff08Rock-salt\uff09\uff0c\u7531\u4e8eZr-O\u952e\u7684\u5f3a\u952e\u5408\u80fd\u4f5c\u7528\uff0c\u5176\u5728\u7535\u5316\u5b66\u5faa\u73af\u8fc7\u7a0b\u4e2d\u80fd\u591f\u5145\u5f53\u4fdd\u62a4\u5c42\u89d2\u8272\uff0c\u4ece\u800c\u6709\u6548\u6291\u5236\u4e86\u6c27\u6790\u51fa\u3001\u8fc7\u6e21\u91d1\u5c5e\u6eb6\u89e3\u3002\u800c\u5bf9\u4e8e\u672a\u88ab\u4fee\u9970\u7684LMR\u6b63\u6781\u6750\u6599\uff0c\u5176\u5728\u7535\u5316\u5b66\u5faa\u73af\u8fc7\u7a0b\u4e2d\uff0c\u8868\u9762\u5219\u53d1\u751f\u7531\u4e8e\u6c27\u6790\u51fa\u3001\u8fc7\u6e21\u91d1\u5c5e\u6eb6\u89e3\u800c\u5bfc\u81f4\u7684\u76f8\u8f6c\u53d8\uff0c\u5982\u8868\u97623~4 nm\u4f1a\u8f6c\u53d8\u4e3a\u6709\u7f3a\u9677\u7684\u5c16\u6676\u77f3\uff08Defect Spinel-like\uff09\u76f8\uff0c\u4e9a\u8868\u97624~5 nm\u4f1a\u8f6c\u53d8\u4e3a\u626d\u66f2\u7684\u5ca9-\u76d0\uff08Disordered Rock-salt\uff09\u76f8\u3002\u6b64\u5916\uff0cEIS\u7ed3\u679c\u8fd8\u8868\u660e\uff0c\u8868\u9762\u5f62\u6210\u76841~2 nm\u7684Zr\u57fa\u5ca9-\u76d0\u76f8\u5e76\u6ca1\u4fc3\u8fdbLMR\u9502\u79bb\u5b50\u8fc1\u79fb\u6548\u7387\u7684\u63d0\u5347\uff0c\u5176\u53ea\u662f\u6709\u6548\u4fdd\u62a4\u4e86LMR\u5c42\u72b6\u7ed3\u6784\u5728\u7535\u5316\u5b66\u5faa\u73af\u8fc7\u7a0b\u4e2d\u4e0d\u88ab\u7834\u574f\uff0c\u4fdd\u6301\u4e86\u8f83\u901a\u7545\u7684Li+<\/sup>\u8fc1\u79fb\u901a\u9053\uff0c\u4ece\u800c\u6709\u6548\u904f\u5236\u4e86\u56e0\u5c42\u72b6\u7ed3\u6784\u88ab\u7834\u574f\u800c\u5bfc\u81f4\u7684\u5bb9\u91cf\u8870\u51cf\u53ca\u5faa\u73af\u6027\u80fd\u6076\u5316\u3002\uff08Xing Li, Kangjia Zhang, David Mitlin, Zhenzhong Yang, Mingshan Wang, Yao Tang, Fei Jiang, Yingge Du, Jianming Zheng, Fundamental Insight into Zr Modification of Li- and Mn-Rich Cathodes: Combined Transmission Electron Microscopy and Electrochemical Impedance Spectroscopy Study, Chem. Mater. 2018, DOI: 10.1021\/acs.chemmater.7b04861\uff09<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

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\u56fe<\/strong>1<\/strong> a\u548cb\u4e3a\u7535\u5316\u5b66\u5faa\u73af\u4e4b\u524d\u7684LMR\u6b63\u6781\u6750\u6599\u7684STEM\u56fe\uff1bc\u548cd\u4e3a\u7535\u5316\u5b66\u5faa\u73af\u4e4b\u540e\u7684STEM\u56fe\u3002\u4ecea\u548cb\u56fe\u4e2d\u53ef\u4ee5\u89c2\u5bdf\u5230\uff0c\u5faa\u73af\u4e4b\u524d\uff0cLMR\u4f53\u73b0\u51fa\u4e86\u5178\u578b\u7684\u5c42\u72b6\u7ed3\u6784\u6b63\u6781\u6750\u6599\u7684\u7279\u5f81\uff1b\u4ecec\u548cd\u56fe\u4e2d\u53ef\u4ee5\u89c2\u5bdf\u5230\uff0c\u5faa\u73af\u4e4b\u540e\uff0cLMR\u8868\u9762\u53ca\u4e9a\u8868\u9762\u53d1\u751f\u4e86\u7531\u4e8e\u6c27\u6790\u51fa\u3001\u8fc7\u6e21\u91d1\u5c5e\u6eb6\u89e3\u5bfc\u81f4\u7684\u5c42\u72b6\u7ed3\u6784\u8f6c\u53d8\uff0c\u5373\u5206\u522b\u8f6c\u53d8\u4e3a\u6709\u7f3a\u9677\u7684\u5c16\u6676\u77f3\u76f8\u548c\u626d\u66f2\u7684\u5ca9-\u76d0\u76f8\u3002<\/p>\n

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\u56fe<\/strong>2<\/strong> a\uff0cb\u548cc\u4e3a\u7535\u5316\u5b66\u5faa\u73af\u4e4b\u524d\u7684Zr\u8868\u9762\u4fee\u9970\u7684LMR\u6b63\u6781\u6750\u6599\u7684STEM\u56fe\uff1bd\uff0ce\u548cf\u4e3a\u7535\u5316\u5b66\u5faa\u73af\u4e4b\u540e\u7684STEM\u56fe\u3002\u4ecea\uff0cb\u548cc\u56fe\u4e2d\u53ef\u4ee5\u89c2\u5bdf\u5230\uff0c\u5faa\u73af\u4e4b\u524d\uff0cZr\u8868\u9762\u4fee\u9970\u7684LMR\u4e5f\u4f53\u73b0\u51fa\u4e86\u5178\u578b\u7684\u5c42\u72b6\u7ed3\u6784\u6b63\u6781\u6750\u6599\u7684\u7279\u5f81\uff0c\u540c\u65f6\u5728\u5176\u8868\u9762\u5f62\u6210\u4e861~2 nm\u539a\u7684Zr\u57fa\u5ca9-\u76d0\u76f8\uff08\u56fec\uff09\uff1b\u4eced\uff0ce\u548cf\u56fe\u4e2d\u53ef\u4ee5\u89c2\u5bdf\u5230\uff0c\u5faa\u73af\u4e4b\u540e\uff0c\u5f62\u6210\u76841~2 nm\u539a\u7684Zr\u57fa\u5ca9-\u76d0\u76f8\u80fd\u591f\u8f83\u597d\u7684\u88ab\u4fdd\u6301\uff08\u56fef\uff09\uff0c\u4ece\u800c\u80fd\u591f\u8d77\u5230\u4fdd\u62a4\u5c42\u4f5c\u7528\uff0c\u6291\u5236LMR\u7684\u5c42\u72b6\u7ed3\u6784\u5728\u7535\u5316\u5b66\u5faa\u73af\u8fc7\u7a0b\u4e2d\u88ab\u7834\u574f\u3002<\/p>\n

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\u56fe<\/strong>3<\/strong> a\u4e3aZr\u8868\u9762\u4fee\u9970\u7684LMR\u6b63\u6781\u6750\u6599\u7684STEM\u56fe\uff0cb\uff0cc\uff0cd\uff0ce\u548cf\u4e3a\u5bf9\u5e94\u7684Mn\u3001Co\u3001Ni\u3001O\u548cZr\u7684EDX mapping\u56fe\u3002<\/p>\n

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\u56fe<\/strong>4<\/strong> a\u548cb\u4e3aLMR\u53caZr\u8868\u9762\u4fee\u9970\u7684LMR\u5728\u4e0d\u540c\u5faa\u73af\u6b21\u6570\u4e0b\u7684EIS\u8c31\u56fe\uff1bc\u548cd\u4e3aa\u548cb\u56fe\u4e2d\u7ea2\u8272\u957f\u65b9\u4f53\u7684\u653e\u5927\u56fe\u3002\u4ece\u56fe\u4e2d\u53ef\u4ee5\u89c2\u5bdf\u5230\uff0cZr\u57fa\u5ca9-\u76d0\u76f8\u5e76\u672a\u5bf9CEI\u819c\u4ea7\u751f\u660e\u663e\u5f71\u54cd\uff0c\u7136\u800cZr\u8868\u9762\u4fee\u9970LMR\u7684Rct<\/sub>\u968f\u7740\u5faa\u73af\u6b21\u6570\u7684\u589e\u52a0\u5374\u660e\u663e\u5c0f\u4e8e\u672a\u88abZr\u8868\u9762\u4fee\u9970\u7684LMR\u3002<\/p>\n

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\u56fe<\/strong>5<\/strong> a\u56fe\u4e3aLMR\u53caZr\u8868\u9762\u4fee\u9970\u7684LMR\u5728C\/3\u4e0b\u7684\u5faa\u73af\u7a33\u5b9a\u6027\uff0cb\u548cc\u56fe\u5206\u522b\u4e3aLMR\u53caZr\u8868\u9762\u4fee\u9970\u7684LMR\u5728\u4e0d\u540c\u5faa\u73af\u6b21\u6570\u4e0b\u7684\u5145\u653e\u7535\u66f2\u7ebf\u3002\u4ece\u56fe\u4e2d\u53ef\u4ee5\u89c2\u5bdf\u5230Zr\u8868\u9762\u4fee\u9970\u80fd\u591f\u8d77\u5230\u660e\u663e\u6291\u5236\u5bb9\u91cf\u8870\u51cf\u53ca\u5faa\u73af\u7a33\u5b9a\u6027\u6076\u5316\u7684\u4f5c\u7528\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u672c\u6587\u91c7\u7528STEM\u4e0eEIS\u76f8\u7ed3\u5408\u7684\u65b9\u5f0f\uff0c\u4ece\u539f\u5b50\u5c3a\u5bf8\u63ed\u793a\u4e86Zr\u8868\u9762\u4fee\u9970\u63d0\u5347LMR\u6b63\u6781\u6750\u6599\u7535\u5316\u5b66\u6027\u80fd\u7684\u539f\u7406\u3002\u5bf9\u4e8e\u6df1\u5165\u8ba4\u8bc6\u91c7\u7528Zr\u6216Zr\u57fa\u5316\u5408\u7269\u8868\u9762\u4fee\u9970\u6b63\u6781\u6750\u6599\u6709\u4e00\u5b9a\u7684\u4fc3\u8fdb\u4f5c\u7528\u3002\u540c\u65f6\uff0c\u4e5f\u5e0c\u671b\u4e3a\u5f00\u5c55\u91c7\u7528\u5176\u5b83\u6750\u6599\u8868\u9762\u4fee\u9970\u9ad8\u5bb9\u91cf\u6b63\u6781\u7684\u7814\u7a76\u63d0\u4f9b\u4e00\u4e9b\u501f\u9274\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Fundamental Insight into Zr Modification of Li- and Mn-Rich Cathodes: Combined Transmission Electron Microscopy and Electrochemical Impedance Spectroscopy Study<\/a> (Chem. Mater., 2018, DOI: 10.1021\/acs.chemmater.7b04861)<\/p>\n

\u76f8\u5173\u6587\u732e\uff1a<\/p>\n

    \n
  1. Enhanced Electrochemical Performance of Zr-Modified Layered LiNi1\/3<\/sub>Co1\/3<\/sub>Mn1\/3<\/sub>O2<\/sub> Cathode Material for Lithium-Ion Batteries<\/a> (ChemElectroChem, 2016, DOI: 10.1002\/celc.201500360)<\/li>\n
  2. Dual functions of Zirconium modification on improving the electrochemical performance of Ni-rich LiNi0.8<\/sub>Co0.1<\/sub>Mn0.1<\/sub>O2<\/sub><\/a> (Sustainable Energy & Fuels, 2018, DOI: 10.1039\/C7SE00513J)<\/li>\n<\/ol>\n

    \u672c\u6587\u7531\u897f\u5357\u77f3\u6cb9\u5927\u5b66\u674e\u661f\u4f9b\u7a3f\uff0c\u7279\u6b64\u611f\u8c22\u3002<\/p>\n

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