{"id":134471,"date":"2018-04-20T09:34:30","date_gmt":"2018-04-20T01:34:30","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=134471"},"modified":"2018-04-20T09:34:14","modified_gmt":"2018-04-20T01:34:14","slug":"%e6%b8%85%e5%8d%8e%e5%a4%a7%e5%ad%a6%e6%9d%8e%e4%ba%9a%e6%a0%8b%e9%99%a2%e5%a3%abnat-commun-%ef%bc%9a%e9%87%91%e5%b1%9e%e9%94%82%e8%bf%98%e5%8e%9f%e8%b0%83%e8%8a%82%e6%b0%a7%e5%8c%96%e7%89%a9","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=134471","title":{"rendered":"\u6e05\u534e\u5927\u5b66\u674e\u4e9a\u680b\u9662\u58ebNat. Commun.\uff1a\u91d1\u5c5e\u9502\u8fd8\u539f\u8c03\u8282\u6c27\u5316\u7269\u7f3a\u9677\u7ed3\u6784"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n

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\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u5728\u6e05\u534e\u5927\u5b66\u674e\u4e9a\u680b\u9662\u58eb\u3001\u4f0d\u6656\u526f\u6559\u6388<\/b><\/strong>\u548c\u5317\u4eac\u822a\u7a7a\u822a\u5929\u5927\u5b66\u5218\u5229\u6c11\u6559\u6388<\/b><\/strong>\uff08<\/b><\/strong>\u5171\u540c<\/b><\/strong>\u901a\u8baf\u4f5c\u8005\uff09<\/b><\/strong>\u7684\u5e26\u9886\u4e0b\uff0c\u7814\u7a76\u4eba\u5458\u4e0e\u5317\u4eac\u8ba1\u7b97\u79d1\u5b66\u7814\u7a76\u4e2d\u5fc3\uff0c\u4e2d\u56fd\u79d1\u5b66\u9662\u7269\u7406\u7814\u7a76\u6240<\/b><\/strong>\u548c\u5317\u4eac\u822a\u7a7a\u822a\u5929\u5927\u5b66<\/b><\/strong>\u5408\u4f5c\uff0c\u5f00\u53d1\u4e86\u4e00\u79cd\u7b80\u4fbf\u6613\u884c\u7684\u91d1\u5c5e\u9502\u7814\u78e8\u8fd8\u539f\u65b9\u6cd5\uff0c\u63a7\u5236\u6c27\u5316\u7269\u6750\u6599\u7684\u6c27\u7a7a\u4f4d\u7f3a\u9677\u3002\u5728\u5e38\u6e29\u5e38\u538b\u4e0b\uff0c\u901a\u8fc7\u5c06\u9502\u4e0e\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u9897\u7c92\u5145\u5206\u7814\u78e8\uff0c\u5236\u5907\u51fa\u4e86\u7f3a\u9677\u542b\u91cf\u53ef\u8c03\u7684\u591a\u79cd\u5bcc\u7f3a\u9677\u6c27\u5316\u7269\u6750\u6599\uff0c\u5305\u62ec\u7f3a\u9677\u7684\u4e8c\u6c27\u5316\u949b\uff08TiO2<\/sub>\uff09\u3001\u6c27\u5316\u950c\uff08ZnO\uff09\u3001\u4e8c\u6c27\u5316\u9521\uff08SnO2<\/sub>\uff09\u548c\u4e8c\u6c27\u5316\u94c8\uff08CeO2<\/sub>\uff09\u7b49\u3002\u8be5\u65b9\u6cd5\u5177\u6709\u6761\u4ef6\u6e29\u548c\u3001\u64cd\u4f5c\u7b80\u5355\u3001\u5feb\u901f\u9ad8\u6548\u3001\u7f3a\u9677\u542b\u91cf\u53ef\u63a7\u53ca\u6613\u4e8e\u89c4\u6a21\u5316\u91cf\u4ea7\u7b49\u4f18\u70b9\u3002\u4f5c\u4e3a\u6f5c\u5728\u7684\u5e94\u7528\uff0c\u76f8\u5173\u4eba\u5458\u63a2\u8ba8\u4e86\u8be5\u7f3a\u9677TiO2<\/sub>\u6750\u6599\u7684\u5149\u50ac\u5316\u6790\u6c22\u6027\u80fd\u3002\u5728\u4e00\u4e2a\u592a\u9633\u5149\u5f3a\u5ea6\u7684\u7167\u5c04\u4e0b\uff0c\u6790\u6c22\u901f\u7387\u9ad8\u8fbe41.8 mmol g-1<\/sup>\u00a0h-1<\/sup>\uff0c\u8fd9\u6bd4\u539f\u59cbTiO2<\/sub>\u7eb3\u7c73\u7c92\u5b50\u9ad8\u51fa\u7ea63\u500d\u3002\u8fd9\u79cd\u73b0\u8c61\u7684\u539f\u56e0\u4e3b\u8981\u662f\u7f3a\u9677TiO2<\/sub>\u6750\u6599\u5177\u6709\u589e\u5f3a\u7684\u5149\u5438\u6536\uff0c\u6539\u5584\u7684\u7535\u5bfc\u7387\uff0c\u8868\u9762\u65e0\u5e8f\u5c42\uff0c\u5f15\u5165\u7684\u6c27\u7a7a\u4f4d\u4ee5\u53ca\u4f34\u751f\u7684Ti3+<\/sup>\u3002\u6b64\u5916\uff0c\u53ef\u4ee5\u5728\u7f3a\u9677TiO2<\/sub>\u7eb3\u7c73\u9897\u7c92\u7684\u6676\u4f53-\u65e0\u5b9a\u5f62\u754c\u9762\u5904\u5b9e\u73b0\u91d1\u5c5e\u5bfc\u7535\uff0c\u589e\u5f3aTiO2<\/sub>\u7684\u8868\u9762\u7535\u5b50\u4f20\u8f93\u6027\u8d28\u3002\u53e6\u4e00\u4e2a\u91cd\u8981\u56e0\u7d20\u662f\u690d\u5165\u7684\u6c27\u7a7a\u4f4d\u548c\u8868\u9762\u969c\u788d\uff0c\u53ef\u4ee5\u5145\u5f53\u7535\u5b50\u7ed9\u4f53\uff0c\u6539\u5584\u7535\u8377\u4f20\u8f93\u5e76\u4f7f\u8d39\u7c73\u80fd\u7ea7\u5411\u5bfc\u5e26\u79fb\u52a8\uff0c\u4fc3\u8fdb\u7535\u8377\u5206\u79bb\u5e76\u6539\u5584UV\u533a\u57df\u4e2d\u5165\u5c04\u5149\u5b50\u5bf9\u7535\u6d41\u6548\u7387\uff08IPCE\uff09\u3002\u6700\u540e\uff0c\u6709\u7f3a\u9677\u7684TiO2<\/sub>\u4e2d\u4ea7\u751f\u7684Ti3+<\/sup>\u53ef\u4ee5\u51cf\u5c11\u5149\u751f\u7535\u5b50-\u7a7a\u7a74\u5bf9\u7684\u590d\u5408\uff0c\u4ece\u800c\u63d0\u9ad8\u9502\u8fd8\u539fTiO2<\/sub>\u7684\u5149\u50ac\u5316\u6d3b\u6027\u7eb3\u7c73\u9897\u7c92\u3002\u76f8\u5173\u6210\u679c\u9898\u4e3a\u201cTuning defects in oxides at room temperature by lithium reduction<\/b><\/strong>\u201d\u53d1\u8868\u5728Nat. Commun.<\/b><\/strong>\u4e0a\uff0c\u7b2c\u4e00\u4f5c\u8005\u4e3a\u6e05\u534e\u5927\u5b66\u535a\u58eb\u540e\u6b27\u521a\u3001\u7855\u58eb\u7814\u7a76\u751f\u8bb8\u4e8e\u5e05\u548c\u5317\u4eac\u8ba1\u7b97\u79d1\u5b66\u7814\u7a76\u4e2d\u5fc3\u535a\u58eb\u7814\u7a76\u751f\u95fb\u6ce2\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/b><\/strong><\/p>\n

\u56fe<\/b><\/strong>1 <\/b><\/strong>\u539f\u59cb\u548c\u9502\u8fd8\u539f\u7684\u6c27\u5316\u7269\u7eb3\u7c73\u7c92\u5b50\u7684XRD<\/b><\/strong>\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

a.TiO2<\/sub>\u7684\u56fe\u7247\uff1b<\/p>\n

b.TiO2<\/sub>\u7684XRD\u56fe\uff1b<\/p>\n

c.\u5206\u522b\u4e3aZnO\uff0cSnO2<\/sub>\u548cCeO2<\/sub>\u7684\u56fe\u7247\uff1b<\/p>\n

d-f.\u5206\u522b\u4e3aZnO\uff0cSnO2<\/sub>\u548cCeO2<\/sub>\u7684XRD\u56fe\u3002<\/p>\n

\u56fe<\/b><\/strong>2 <\/b><\/strong>\u539f\u59cb\u548c\u9502\u8fd8\u539f\u7684<\/b><\/strong>TiO<\/b><\/strong>2<\/b><\/sub><\/strong>\u7eb3\u7c73\u7c92\u5b50\u7684\u7f3a\u9677\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

a-c\u5206\u522b\u4e3a\u539f\u59cb\u548c\u9502\u8fd8\u539f\u7684TiO2<\/sub>\u7eb3\u7c73\u7c92\u5b50\u7684XPS\u5149\u8c31\u548cEPR\u5149\u8c31\uff1b<\/p>\n

d\uff0ce.\u539f\u59cb\u548c5\uff05Li\u5904\u7406\u7684TiO2<\/sub>\u7684\u9ad8\u89d2\u5ea6\u73af\u5f62\u6697\u573a\uff08HAADF\uff09\u56fe\u50cf\u3002\u6807\u5c3a\uff1a5nm\u3002<\/p>\n

\u56fe<\/b><\/strong>3 <\/b><\/strong>\u539f\u59cb\u548c\u9502\u8fd8\u539f\u7684<\/b><\/strong>TiO<\/b><\/strong>2<\/b><\/sub><\/strong>\u7eb3\u7c73\u7c92\u5b50\u7684\u5149\u50ac\u5316\u6027\u80fd<\/b><\/strong>\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

a\uff0cb.\u539f\u59cb\u548c\u9502\u8fd8\u539f\u7684TiO2<\/sub>\u7eb3\u7c73\u7c92\u5b50\u5149\u50ac\u5316\u964d\u89e3RhB\u7684\u6d3b\u6027\u548c\u7a33\u5b9a\u6027\uff1b<\/p>\n

c\uff0cd.\u539f\u59cb\u548c\u9502\u8fd8\u539f\u7684TiO2<\/sub>\u7eb3\u7c73\u7c92\u5b50\u5149\u50ac\u5316\u6790\u6c22\u6d3b\u6027\u548c\u7a33\u5b9a\u6027\u3002<\/p>\n

\u56fe<\/b><\/strong>4 <\/b><\/strong>\u6709\u7f3a\u9677\u7684\u9510\u949b\u77ffTiO<\/b><\/strong>2<\/b><\/sub><\/strong>\u7684<\/b><\/strong>\u72b6\u6001\u5bc6\u5ea6\uff08DOS\uff09<\/b><\/strong>\u548c<\/b><\/strong>\u632f\u8361<\/b><\/strong>\u5f3a\u5ea6\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

a\u2013c.\u5206\u522b\u5177\u67091Ov<\/sub>\uff0c2Ov<\/sub>\u548c4Ov<\/sub>\u7684TiO2<\/sub>\u8868\u9762\u7684DOS\uff1b<\/p>\n

d-f\u5206\u522b\u5177\u67091Ov<\/sub>\uff0c2Ov<\/sub>\u548c4Ov<\/sub>\u7684TiO2<\/sub>\u8868\u9762\u7684\u632f\u8361\u5f3a\u5ea6\u3002<\/p>\n

\u3010\u5c0f\u7ed3<\/b><\/strong>\u3011<\/p>\n

\u8be5\u7814\u7a76\u56e2\u961f\u8ba4\u4e3a\uff0c\u6b64\u91d1\u5c5e\u9502\u8fd8\u539f\u6cd5\u9002\u7528\u4e8e\u591a\u79cd\u6c27\u5316\u7269\u7eb3\u7c73\u6750\u6599\u7684\u7f3a\u9677\u8c03\u63a7\uff0c\u8fd9\u4e9b\u6750\u6599\u5728\u91d1\u5c5e\u9502\u8fd8\u539f\u540e\u8868\u73b0\u51fa\u663e\u8457\u589e\u5f3a\u7684\u5149\u50ac\u5316\u6027\u80fd\u3002\u672a\u6765\u53ef\u4ee5\u5c06\u8fd9\u79cd\u65b9\u6cd5\u5e94\u7528\u5230 \u66f4\u5e7f\u6cdb\u7684\u6750\u6599\u4e2d\uff0c\u6bd4\u5982\u591a\u91d1\u5c5e\u6c27\u5316\u7269\u3001\u786b\u5316\u7269\u53ca\u7852\u5316\u7269\u7b49\u3002\u76f8\u5173\u7684\u5e94\u7528\u4e5f\u53ef\u4ee5\u8fdb\u4e00\u6b65\u62d3\u5c55\u5230\u7535\u50ac\u5316\u3001\u7535\u6c60\u3001\u4f20\u611f\u5668\u7b49\u9886\u57df\u4e2d\u3002<\/p>\n

\u6b64\u5916\uff0c\u76f8\u5173\u4f5c\u8005\u5728\u524d\u671f\u5de5\u4f5c\u4e2d\u62a5\u9053\u4e86\u591a\u79cd\u7f3a\u9677\u8c03\u63a7\u7684\u65b9\u6cd5\uff0c\u5305\u62ec\u7535\u5f27\u7194\u878d\u6cd5\uff08Adv. Mater., 2015, 27,\u00a02589.; Nano Res.,\u00a02016, 9,\u00a01236.; Chem. Commun.,\u00a02017, 53, 5048.\uff09\u548c\u6fc0\u5149\u70e7\u8680\u6cd5\uff08Nano Energy, 2017, 35, 207.; Nano Res.,\u00a02017, 11,\u00a0751.; RSC Adv.,\u00a02016, 6, 107158.\uff09\uff0c\u5e76\u5c06\u5236\u5907\u7684\u5bcc\u7f3a\u9677\u7eb3\u7c73\u6750\u6599\u5e94\u7528\u4e8e\u5149\u50ac\u5316\u3001\u7535\u50ac\u5316\u3001\u5149\u70ed\u8f6c\u6362\u548c\u5149\u70ed\u6cbb\u7597\u7b49\u8bf8\u591a\u9886\u57df\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/b><\/strong>Tuning defects in oxides at room temperature by lithium reduction<\/u><\/a>\uff08Nat. Commun.,\u00a02018, DOI: 10.1038\/s41467-018-03765-0\uff09<\/p>\n

\u6587\u732e\u63a8\u4ecb\uff1a<\/b><\/strong><\/p>\n

Nature Communications<\/strong>\u00a09 (1), 1302,\u00a02018;<\/p>\n

Nature Communications\u00a0<\/strong>8 (1), 1490\uff0c 2018;<\/p>\n

Angew.\u00a0Chem. Int. Ed.<\/strong>\u00a057,\u00a03354, 2018;<\/p>\n

Science Advances<\/strong>\u00a03 (6), e1603170\uff0c 2017;<\/p>\n

Advanced Materials<\/strong> 29 (41), 2017;\u00a0<\/p>\n

Advanced Materials\u00a0<\/strong>28 (37), 8170-8176\uff0c 2016;\u00a0<\/p>\n

Nature communications<\/strong>\u00a07, 12543, 2016;<\/p>\n

\u00a0Advanced Materials<\/strong>\u00a027 (16), 2589-2594,\u00a02015<\/p>\n

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