{"id":138621,"date":"2018-05-20T06:30:05","date_gmt":"2018-05-19T22:30:05","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=138621"},"modified":"2018-05-20T04:06:53","modified_gmt":"2018-05-19T20:06:53","slug":"%e8%8b%8f%e5%b7%9e%e5%a4%a7%e5%ad%a6energy-environ-sci-%e5%9f%ba%e4%ba%8ec3n4%e5%82%ac%e5%8c%96%e5%89%82%e7%9a%84%e5%85%89%e7%94%b5%e5%8c%96%e5%ad%a6%e6%b1%a0%e5%ae%9e%e7%8e%b0%e5%a4%aa%e9%98%b3","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=138621","title":{"rendered":"\u82cf\u5dde\u5927\u5b66Energy Environ. Sci.: \u57fa\u4e8eC3N4\u50ac\u5316\u5242\u7684\u5149\u7535\u5316\u5b66\u6c60\u5b9e\u73b0\u592a\u9633\u80fd\u5230\u7535\u80fd\u76f4\u63a5\u8f6c\u6362"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u592a\u9633\u80fd\u662f\u53ef\u518d\u751f\u53ef\u6301\u7eed\u7684\u6e05\u6d01\u80fd\u6e90\uff0c\u5f53\u524d\u5df2\u7ecf\u6709\u5f88\u591a\u5173\u4e8e\u592a\u9633\u80fd\u8f6c\u6362\u7684\u7814\u7a76\uff0c\u5176\u4e2d\u6700\u91cd\u8981\u7684\u4e00\u4e2a\u8f6c\u6362\u76ee\u6807\u5c31\u662f\u628a\u592a\u9633\u80fd\u8f6c\u6362\u4e3a\u7535\u80fd\u3002\u5bf9\u6b64\uff0c\u592a\u9633\u80fd\u7535\u6c60\u7684\u7814\u7a76\u5df2\u7ecf\u505a\u5230\u4e86\u63a5\u8fd1\u706b\u7535\u7684\u6210\u672c\uff0c\u6709\u671b\u771f\u6b63\u5b9e\u73b0\u5927\u89c4\u6a21\u5e94\u7528\u3002\u592a\u9633\u5149\u7167\u7684\u95f4\u65ad\u6027\uff0c\u4e3a\u592a\u9633\u80fd\u7535\u6c60\u7684\u5e94\u7528\u5e26\u6765\u4e86\u4e00\u7cfb\u5217\u95ee\u9898\u3002\u76f8\u5bf9\u7684\uff0c\u71c3\u6599\u7535\u6c60\u53ef\u4ee5\u968f\u65f6\u5c06\u50a8\u5b58\u7684\u5316\u5b66\u80fd\u8f6c\u6362\u4e3a\u7535\u80fd\u4f9b\u4eba\u4eec\u4f7f\u7528\u3002\u672c\u6587\u6b63\u662f\u57fa\u4e8e\u8fd9\u4e00\u8003\u8651\uff0c\u8bbe\u8ba1\u4e86\u4e00\u79cd\u5149\u7535\u5316\u5b66\u6c60\u3002\u5b83\u53ef\u4ee5\u5229\u7528O2<\/sub>\/H2<\/sub>O\u6c27\u5316\u8fd8\u539f\u5bf9\u5728\u592a\u9633\u5149\u9a71\u52a8\u4e0b\u4ea7\u751f\u7535\u80fd\uff0c\u4e5f\u80fd\u4ee5\u5316\u5b66\u80fd\u5f62\u5f0f\u5b58\u50a8\u751f\u6210\u7684\u4e2d\u95f4\u4ea7\u7269H2<\/sub>O2<\/sub>\uff0c\u5728\u6ca1\u6709\u5149\u7167\u7684\u65f6\u5019\uff0c\u50cf\u71c3\u6599\u7535\u6c60\u4e00\u6837\u628a\u50a8\u5b58\u7684\u5316\u5b66\u80fd\u8f6c\u6362\u4e3a\u7535\u80fd\u3002\u8fd9\u79cd\u5149\u7535\u5316\u5b66\u6c60\u53ef\u4ee5\u542f\u53d1\u7814\u7a76\u8005\u601d\u8003\u5982\u4f55\u8bbe\u8ba1\u548c\u7814\u7a76\u592a\u9633\u80fd\u8f6c\u6362\u5668\u4ef6\uff0c\u4fc3\u8fdb\u5149\u50ac\u5316\u548c\u5149\u7535\u50ac\u5316\u7814\u7a76\u6df1\u5165\u62d3\u5c55\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u82cf\u5dde\u5927\u5b66\u529f\u80fd\u7eb3\u7c73\u4e0e\u8f6f\u7269\u8d28\u7814\u7a76\u9662\u7684\u5eb7\u632f\u8f89\u6559\u6388\u3001\u5218\u9633\u6559\u6388\u548cYeshayahu Lifshitz\u8bb2\u5ea7\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u5728Energy & Environmental Science<\/strong>\u4e0a\u53d1\u8868\u6700\u65b0\u7814\u7a76\u6210\u679c\u201cA g-C3<\/sub>N4<\/sub> based photoelectrochemical cell using O2<\/sub>\/H2<\/sub>O redox couples\u201d<\/strong>\u3002\u4ee5O2<\/sub>\/H2<\/sub>O\u4f5c\u4e3a\u6c27\u5316\u8fd8\u539f\u5bf9\uff0c\u7814\u7a76\u8bbe\u8ba1\u4e86\u4e00\u79cd\u57fa\u4e8eg-C3<\/sub>N4<\/sub>\u7684\u5149\u7535\u5316\u5b66\u6c60\uff0c\u514b\u670d\u8fc7\u7535\u52bf\u592a\u5927\u7684\u56f0\u96be\uff0c\u83b7\u5f970.91 V\u7684\u5f00\u8def\u7535\u538b\u4ee5\u53ca\u9ad8\u8fbe0.156 mW cm-2<\/sup>\u7684\u80fd\u91cf\u5bc6\u5ea6\u3002\u540c\u65f6\uff0c\u5b83\u53ef\u4ee5\u5728\u4e24\u6781\u5206\u79bb\u7684\u60c5\u51b5\u4e0b\u901a\u8fc7\u5149\u7167\u4ea7\u751fH2<\/sub>O2<\/sub>\u4f5c\u4e3a\u5316\u5b66\u80fd\u50a8\u5b58\uff0c\u6ca1\u6709\u5149\u6e90\u65f6\u5c31\u53ef\u4ee5\u50cf\u71c3\u6599\u7535\u6c60\u4e00\u6837\u6d88\u8017H2<\/sub>O2<\/sub>\u5de5\u4f5c\uff08\u9762\u79ef\u6bd4\u5bb9\u91cf\u8fbe\u5230350 mC cm-2<\/sup>\uff0c\u8d28\u91cf\u6bd4\u5bb9\u91cf\u8fbe\u5230237 C g-1<\/sup>\uff09\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe1\uff1a\u5149\u7535\u5316\u5b66\u6c60\u5de5\u4f5c\u673a\u7406\u56fe\u793a<\/strong><\/p>\n

\"\"<\/p>\n

\u9633\u6781\uff1a\u8d1f\u8f7dg-C3<\/sub>N4<\/sub>\u7684Ni\u7f51\u3002g-C3<\/sub>N4<\/sub>\u6355\u5149\u5e76\u5c06H2<\/sub>O\u6c27\u5316\u4e3aH2<\/sub>O2<\/sub>\uff0c\u63a5\u7740Ni\u7f51\u5c06H2<\/sub>O2<\/sub>\u6c27\u5316\u4e3aO2<\/sub>\u3002<\/p>\n

\u9634\u6781\uff1a[Fe\u2162<\/sup>(Pc)Cl]\u4e0eg-C3<\/sub>N4<\/sub>\u6df7\u5408\u7269\u55b7\u6d82\u5728\u78b3\u7eb8\u4e0a\u3002\u4ece\u5916\u7535\u8def\u8fc7\u6765\u7684\u9633\u6781\u7535\u5b50\u50ac\u5316g-C3<\/sub>N4<\/sub>\u5c06O2<\/sub>\u8fd8\u539f\u4e3aH2<\/sub>O2<\/sub>\uff0c[Fe\u2162<\/sup>(Pc)Cl]\u8fdb\u4e00\u6b65\u5c06H2<\/sub>O2<\/sub>\u8fd8\u539f\u4e3aH2<\/sub>O\uff08\u8fd8\u539f\u8fc7\u7a0b\u4e09\u4ef7Fe\u53d8\u4e3a\u56db\u4ef7\uff0c\u800c\u56db\u4ef7Fe\u53c8\u53ef\u4ee5\u901a\u8fc7\u7535\u5b50\u8fc1\u79fb\u56de\u5230\u4e09\u4ef7\uff09\u3002<\/p>\n

\u56fe2\uff1a g-C3<\/sub>N4<\/sub>\u5f62\u8c8c\u53ca\u5149\u7535\u5316\u5b66\u6c60\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

a. \u591a\u5b54g-C3<\/sub>N4<\/sub> TEM\u56fe<\/p>\n

b. I-V\uff08\u9ed1\u8272\uff09\u548cI-P\uff08\u84dd\u8272\uff09\u66f2\u7ebf\u56fe\uff0c0.1 M HCl\uff08light\uff1a100 mW cm-2<\/sup> AM 1.5G\uff1bFuel cell\uff1a\u6697\u72b6\u6001\uff0c\u542b\u6709300 mM H2<\/sub>O2<\/sub>\uff09<\/p>\n

\u56fe3\uff1a \u5149\u7535\u5316\u5b66\u6c60\u53d8\u91cf\u8c03\u63a7\u53ca\u7a33\u5b9a\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

Seawater \u8868\u793a\u7528HCl\u5c06pH\u8c03\u6574\u81f31\u540e\u7684\u6d77\u6c34<\/p>\n

a. OCP\uff08\u5f00\u8def\u7535\u538b\uff09\u548c\u529f\u7387\u5bc6\u5ea6\u5728\u4e0d\u540cpH\u503c\u7684\u76d0\u9178\u6eb6\u6db2\u4e2d<\/p>\n

b. OCP\u548c\u529f\u7387\u5bc6\u5ea6\u5728\u4e0d\u540cNaCl\u6d53\u5ea6\u4e2d\uff080.1 M HCl\uff09<\/p>\n

c. I-V\u548cI-P\u66f2\u7ebf\u56fe\u57280.1 M HCl\u4e0epH 1\u6d77\u6c34\u6eb6\u6db2\u4e2d<\/p>\n

d. \u529f\u7387\u5bc6\u5ea6\u6d4b\u8bd5\u4e09\u4e2a\u5faa\u73af\u57280.1 M HCl\u4e0epH 1\u6d77\u6c34\u6eb6\u6db2\u4e2d<\/p>\n

\u56fe4\uff1a H2<\/sub>O2<\/sub>\u5b58\u50a8\/\u5229\u7528\u5b9e\u9a8c<\/strong><\/p>\n

\"\"<\/p>\n

a. \u4e0d\u540c\u8d1f\u8f7d\u4e0b\u7684\u653e\u7535\u66f2\u7ebf\uff08\u5149\u50a8\u5b58-\u5149\u716730\u5206\u949f\u5b58\u50a8\u5f97H2<\/sub>O2<\/sub>\uff09<\/p>\n

b. 50 \u2126\u8d1f\u8f7d\u4e0b\u7684\u7535\u6c60\u5bb9\u91cf-\u5149\u50a8\u5b58\u65f6\u95f4\u5173\u7cfb\u56fe<\/p>\n

c. 50 \u2126\u8d1f\u8f7d\u4e0b\u7684\u4e09\u6b21\u8fde\u7eed\u5149\u50a8\u5b58-\u653e\u7535\u5faa\u73af<\/p>\n

d. 50 \u2126\u8d1f\u8f7d\u4e0b\u5149\u50a8\u5b5830\u5206\u949f\u5f97\u5230H2<\/sub>O2<\/sub>\u7684\u4fdd\u6301\u65f6\u95f4\u5bf9\u7535\u6c60\u5bb9\u91cf\u7684\u5f71\u54cd<\/p>\n

\u56fe5\uff1a \u5149\u7535\u5316\u5b66\u6c60\u88c5\u7f6e\u793a\u610f\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

a. \u5149\u7535\u5316\u5b66\u6c60\uff08O2<\/sub>\/H2<\/sub>O\u6c27\u5316\u8fd8\u539f\u5bf9\uff09<\/p>\n

b. Nafion\u819c\u9694\u79bb\u7684\u53cc\u7ec4\u4ef6\u5149\u7535\u5316\u5b66\u6c60<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u7814\u7a76\u57fa\u4e8eg-C3<\/sub>N4<\/sub>\u8bbe\u8ba1\u4e86\u4e00\u79cd\u4ee5O2<\/sub>\/H2<\/sub>O\u4f5c\u4e3a\u6c27\u5316\u8fd8\u539f\u5bf9\u7684\u5149\u7535\u5316\u5b66\u6c60\uff08\u4ee5H2<\/sub>O2<\/sub>\u4f5c\u4e3a\u53cd\u5e94\u4e2d\u95f4\u4f53\uff09\u3002\u5728\u5149\u7167\u4e0b\uff0c\u82e5\u662f\u9009\u62e9\u6027\u5730\u751f\u6210\u5e76\u5b58\u50a8H2<\/sub>O2<\/sub>\uff0c\u90a3\u4e48\uff0c\u5728\u65e0\u5149\u6761\u4ef6\u4e0b\uff0cH2<\/sub>O2<\/sub>\u53ef\u4ee5\u628a\u5316\u5b66\u80fd\u8f6c\u5316\u4e3a\u7535\u80fd\u2014\u2014\u4ee5\u71c3\u6599\u7535\u6c60\u7684\u65b9\u5f0f\u5de5\u4f5c\u3002\u8fd9\u79cd\u65b0\u578b\u7684\u5149\u7535\u5316\u5b66\u6c60\u5668\u4ef6\u7ed3\u5408\u4e86\u524d\u4eba\u7684\u76f8\u5173\u7814\u7a76\u5de5\u4f5c\uff0c\u9996\u6b21\u5b9e\u73b0\u4ee5\u5316\u5b66\u80fd\u4e3a\u4e2d\u8f6c\u5f62\u5f0f\uff0c\u5c06\u592a\u9633\u80fd\u8f6c\u6362\u4e3a\u7535\u80fd\uff0c\u514b\u670d\u4e86\u592a\u9633\u80fd\u7535\u6c60\u4f9d\u8d56\u5149\u6e90\u7684\u5f0a\u7aef\u3002\u540c\u65f6\uff0c\u5668\u4ef6\u4e5f\u83b7\u5f97\u4e86\u8f83\u597d\u7684\u7535\u6c60\u6027\u80fd\uff0c\u4e3a\u592a\u9633\u80fd\u8f6c\u6362\u7814\u7a76\u548c\u5668\u4ef6\u8bbe\u8ba1\u63d0\u4f9b\u4e86\u65b0\u601d\u8def\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5<\/strong>\uff1aA g-C3<\/sub>N4<\/sub> based photoelectrochemical cell using O2<\/sub>\/H2<\/sub>O redox couples<\/a>\uff08Energy Environ. Sci. 2018, DOI: 10.1039\/C7EE03459H\uff09<\/p>\n

\u3010\u56e2\u961f\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u5eb7\u632f\u8f89\u6559\u6388\u79d1\u7814\u56e2\u961f\u7acb\u8db3\u4e8e\u82cf\u5dde\u5927\u5b66\u529f\u80fd\u7eb3\u7c73\u4e0e\u8f6f\u7269\u8d28\u7814\u7a76\u9662\uff0c\u957f\u671f\u4ee5\u78b3\u3001\u7845\u7eb3\u7c73\u7ed3\u6784\u548c\u91d1\u5c5e\/\u534a\u5bfc\u4f53\u7eb3\u7c73\u7c92\u5b50\u7b49\u4e3a\u7814\u7a76\u6838\u5fc3\uff0c\u81f4\u529b\u4e8e\u63ed\u793a\u4ecb\u89c2\u4f53\u7cfb\u4e2d\u7eb3\u7c73\u7c92\u5b50\u7684\u8868\u9762\u5316\u5b66\u3001\u50ac\u5316\u7279\u6027\u3001\u5149\u7535\u5316\u5b66\u6027\u8d28\u7b49\u3002\u6784\u7b51\u7eb3\u7c73\u590d\u5408\u4f53\u7cfb\uff0c\u5e76\u5bf9\u5176\u8fdb\u884c\u8bbe\u8ba1\u4e0e\u529f\u80fd\u8c03\u63a7\uff0c\u5b9e\u73b0\u4e86\u9ad8\u6548\u80fd\u6e90\u8f6c\u5316\u4e0e\u5b58\u50a8\u5e94\u7528\uff0c\u5305\u62ec\u592a\u9633\u80fd\u5149\u89e3\u6c34\u3001\u4e8c\u6c27\u5316\u78b3\u8fd8\u539f\u548c\u71c3\u6599\u7535\u6c60\u7b49\u3002<\/p>\n

\u3010\u56e2\u961f\u5728\u8be5\u9886\u57df\u5de5\u4f5c\u6c47\u603b\u3011<\/strong><\/p>\n

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1.Juan Liu, Yang Liu, Nai-Yun Liu, Yu-Zhi Han, Xing Zhang, Hui Huang, Yeshayahu Lifshitz,* Shuit-Tong Lee,* Jun Zhong, Zhen-Hui Kang,* “Metal-free efficient photocatalyst for stable visible water splitting via a two-electron pathway”, Science, 2015, 347, 970.<\/p>\n

2.Sijie Guo, Siqi Zhao, Xiuqin Wu, Hao Li, Yunjie Zhou, Cheng Zhu, Nianjun Yang, Xin Jiang,* Jin Gao, Liang Bai, Yang Liu,* Yeshayahu Lifshitz, Shuit-Tong Lee* & Zhenhui Kang*, A Co3<\/sub>O4<\/sub>-CDots-C3<\/sub>N4<\/sub> three component electrocatalyst design concept for efficient and tunable CO2<\/sub> reduction to syngas, Nat Commun., 2017, 8, 1828.<\/p>\n

3.Siqi Zhao, Zeyuan Tang, Sijie Guo, Mumei Han, Cheng Zhu, Yunjie Zhou, Liang Bai, Jin Gao, Hui Huang , Youyong Li* , Yang Liu*, and Zhenhui Kang* , Enhanced Activity for CO2<\/sub> Electroreduction on a Highly Active and Stable Ternary Au-CDots-C3<\/sub>N4<\/sub> Electrocatalyst, ACS Catal., 2018, 8, 188.<\/p>\n

4.Juan Liu, Naiyun Liu, Hao Li, Liping Wang, Xiuqin Wu, Hui Huang, Yang Liu,* Feng Bao, Yeshayahu Lifshitz,* Shuit-Tong Lee, and Zhenhui Kang,* A critical study of the generality of the two step two electron pathway for water splitting by application of a C3<\/sub>N4<\/sub>\/MnO2<\/sub> photocatalyst, Nanoscale, 2016, 8, 11956.<\/p>\n

5.Feng Guo, Weilong Shi, Cheng Zhu, Hao Li, ZhenhuiKang*, CoO and g-C3<\/sub>N4<\/sub> complement each other for highly efficient overall water splitting under visible light, Applied Catalysis B: Environmental, 2018, 226, 412.<\/p>\n

6.Yue Sun, Yunjie Zhou, Cheng Zhu, Lulu Hu, Mumei Han, Aoqi Wang, Hui Huang, * Yang Liu,* Zhenhui Kang,* A Pt-Co3<\/sub>O4<\/sub>-CDs electrocatalyst with enhanced electrocatalytic performance and resistance to CO poisoning achieved by carbon dots and Co3O4 for direct methanol fuel cell, Nanoscale, 2017, 9, 5467.<\/p>\n

7.Mumei Han, Huibo Wang, Siqi Zhao, Lulu Hu, Hui Huang* and Yang Liu*, One-step synthesis of CoO\/g-C3<\/sub>N4<\/sub> composites by thermal decomposition for overall water splitting without sacrificial reagents, Inorg. Chem. Front., 2017, 4, 1691.<\/p>\n

8.Sun-Yan Zhao, Juan Liu, Chuan-Xi Li, Wen-Bin Ji, Yan-Mei Yang, Hui Huang, Yang Liu,* Zhen-Hui Kang,* “Tunable-ternary (N, P, B)-doped Porous Nanocarbon and Their Catalytic Properties for Oxygen Reduction Reaction, ACS Appl. Mater. Interface, 2014, 6, 22297.<\/p>\n

9.Yijun Fu, Cheng Zhu, Chang’an Liu, Mengling Zhang, Huibo Wang, Weilong Shi, Hui Huang,* Yang Liu,* Zhenhui Kang*, CoMn-S\/CDs nanocomposite for effective long wavelength visible-light-driven photocatalytic water splitting, Applied Catalysis B: Environmental, 2018, 226, 295.<\/p>\n

10.Chang’an Liu, Yijun Fu, Yujian Xia, Cheng Zhu, Lulu Hu, Kai Zhang, Haihua Wu, Hui Huang, Yang Liu,* Tengfeng Xie,* Jun Zhong* and Zhenhui Kang*, Cascaded photo-potential in a carbon dot-hematite system driving overall water splitting under visible light, Nanoscale, 2018, 10, 2454.<\/p>\n

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