{"id":139329,"date":"2018-05-20T06:30:38","date_gmt":"2018-05-19T22:30:38","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=139329"},"modified":"2018-05-17T18:14:31","modified_gmt":"2018-05-17T10:14:31","slug":"nano-lett-%ef%bc%9a%e9%80%9a%e8%bf%87%e8%b0%83%e6%8e%a7%e7%a2%b3%e6%9d%90%e6%96%99%e7%9a%84%e5%8c%96%e5%ad%a6%e7%8e%af%e5%a2%83%e8%8e%b7%e5%be%97%e5%85%b7%e6%9c%89%e9%ab%98%e5%8e%8b%e3%80%81","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=139329","title":{"rendered":"Nano Lett.\uff1a\u901a\u8fc7\u8c03\u63a7\u78b3\u6750\u6599\u7684\u5316\u5b66\u73af\u5883\u83b7\u5f97\u5177\u6709\u201c\u9ad8\u538b\u3001\u9ad8\u80fd\u3001\u9ad8\u529f\u3001\u9ad8\u5bff\u547d\u201d\u7684\u65b0\u578b\u5168\u78b3\u9502\u79bb\u5b50\u7535\u5bb9\u5668"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u9502\u79bb\u5b50\u7535\u5bb9\u5668\uff08LIC\uff09\u7efc\u5408\u4e86\u9502\u79bb\u5b50\u7535\u6c60\u548c\u8d85\u7ea7\u7535\u5bb9\u5668\u7684\u7279\u70b9\uff0c\u6709\u671b\u83b7\u5f97\u826f\u597d\u7684\u529f\u7387\u5bc6\u5ea6\u3001\u80fd\u91cf\u5bc6\u5ea6\u548c\u5faa\u73af\u5bff\u547d\uff0c\u5177\u6709\u6781\u5927\u5e94\u7528\u524d\u666f\u3002LIC\u7684\u6b63\u8d1f\u6781\u901a\u5e38\u5177\u6709\u4e0d\u540c\u7684\u7535\u8377\u5b58\u50a8\u673a\u7406\uff0c\u5bfc\u81f4\u6b63\u8d1f\u7535\u6781\u4e4b\u95f4\u7684\u53cd\u5e94\u52a8\u529b\u5b66\u901f\u7387\u53ca\u5faa\u73af\u7a33\u5b9a\u6027\u4e0d\u4e00\u81f4\u3002\u4e3a\u4e86\u89e3\u51b3\u4e24\u7535\u6781\u4e4b\u95f4\u7535\u8377\u4f20\u9012\u52a8\u529b\u5b66\u53ca\u5bff\u547d\u7684\u5339\u914d\u95ee\u9898\uff0cLIC\u7684\u7535\u6781\u6750\u6599\u9664\u4e86\u63d0\u9ad8\u6b63\u6781\u6750\u6599\u7684\u6bd4\u5bb9\u91cf\u4e4b\u5916\uff0c\u8d1f\u6781\u6750\u6599\u8fd8\u5e94\u6709\u826f\u597d\u7684\u500d\u7387\u4e0e\u5faa\u73af\u6027\u80fd\uff0c\u4ee5\u53ca\u8f83\u4f4e\u7684\u653e\u7535\u5e73\u53f0\u6765\u4fdd\u8bc1LIC\u7684\u9ad8\u7535\u4f4d\u7a97\u53e3\u3002\u76ee\u524d\u5bf9LIC\u7684\u7814\u7a76\u591a\u4fa7\u91cd\u4e8e\u6b63\u8d1f\u6781\u7684\u4e0d\u540c\u7ec4\u5408\u53ca\u4f18\u5316\uff0c\u4f46\u8fd9\u4e9b\u6df7\u5408\u4f53\u7cfb\u5f88\u96be\u540c\u65f6\u5b9e\u73b0\u80fd\u91cf\u5bc6\u5ea6\u3001\u529f\u7387\u5bc6\u5ea6\u53ca\u5faa\u73af\u5bff\u547d\u7684\u534f\u540c\u6539\u5584\u3002\u6784\u5efa\u5bf9\u79f0\u9502\u79bb\u5b50\u7535\u5bb9\u5668\uff0c\u5229\u7528\u7eb3\u7c73\u6280\u672f\u3001\u63ba\u6742\u6280\u672f\u53ca\u590d\u5408\u6750\u6599\u6280\u672f\u7b49\uff0c\u6709\u671b\u83b7\u5f97\u4f18\u5f02\u7684\u7efc\u5408\u6027\u80fd\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u52a0\u5dde\u5927\u5b66\u6d1b\u6749\u77f6\u5206\u6821\u5362\u4e91\u5cf0\u6559\u6388\u548c\u54c8\u5c14\u6ee8\u5de5\u4e1a\u5927\u5b66\u9ad8\u7ee7\u6167\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u7814\u7a76\u56e2\u961f\u62a5\u9053\u4e86\u4e00\u79cd\u9ad8\u6d53\u5ea6\u6c2e\u63ba\u6742\u7684\u78b3\u7eb3\u7c73\u7403\uff08ANCS\uff09\u7ec4\u88c5\u7684LIC\u3002\u63ba\u6742\u4f18\u5316\u4e86\u78b3\u5fae\u6676\u7ed3\u6784\u7684\u5806\u79ef\u53c2\u6570\u3001\u63d0\u9ad8\u4e86\u78b3\u6750\u6599\u7684\u6d3b\u6027\u70b9\uff0c\u8fdb\u800c\u63d0\u9ad8\u4e86\u6b63\u8d1f\u6781\u6750\u6599\u5bf9Li+<\/sup>\u548cPF6<\/sub>\u2013<\/sup>\u7684\u5b58\u50a8\u6d3b\u6027\u3002\u5c06ANCS\u548c\u9884\u9502\u5316\u7684ANCS\u7ec4\u6210\u5168\u78b3LIC\uff0c\u83b7\u5f97\u4e86\u5177\u67094.5 V\u7684\u9ad8\u5de5\u4f5c\u7535\u538b\uff0c\u5176\u6027\u80fd\u80dc\u8fc7\u4e4b\u524d\u6240\u62a5\u9053\u8fc7\u7684LIC\uff0c\u5728\u9ad8\u500d\u7387\u5faa\u73af\u7a33\u5b9a\u6027\u65b9\u9762\u5c24\u5176\u7a81\u51fa\u3002\u8be5\u6210\u679c\u4ee5 \u201cIn Situ High-Level Nitrogen Doping into Carbon Nanospheres and Boosting of Capacitive Charge Storage in Both Anode and Cathode for a High-Energy 4.5 V Full-Carbon Lithium-Ion Capacitor<\/strong>\u201d \u4e3a\u9898\u4e8e4\u670830\u65e5\u520a\u53d1\u5728Nano letters<\/strong>\u4e0a\uff0c\u7b2c\u4e00\u4f5c\u8005\u4e3a\u54c8\u5c14\u6ee8\u5de5\u4e1a\u5927\u5b66\u80fd\u6e90\u5b66\u9662\u5b59\u98de\u535a\u58eb\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00<\/strong> ANCS<\/strong>\u9897\u7c92\u7684\u5f62\u6210\u793a\u610f\u56fe\u53ca\u5f62\u8c8c\u3001\u6210\u5206\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09ANCS\u5f62\u6210\u8fc7\u7a0b\u793a\u610f\u56fe<\/p>\n

\uff08b\uff09ANCS\u9897\u7c92\u7684SEM\u56fe\u3002\u63d2\u56fe\u4e3aANCS\u9897\u7c92\u7684TEM\u56fe<\/p>\n

\uff08c\uff09ANCS\u9897\u7c92\u7684HRTEM\u56fe\u3002\u63d2\u56fe\u4e3a\u5bf9\u5e94\u7684FFT\u56fe<\/p>\n

\uff08d\uff09ANCS\u7684HAADF-STEM\u56fe\u4ee5\u53ca\u5bf9\u5e94\u7684C\uff0cN\u548cO\u5143\u7d20\u7684EDS mapping<\/p>\n

\u00a0<\/strong>\u56fe\u4e8c<\/strong> ANCS<\/strong>\u548c<\/strong>CS<\/strong>\uff08\u975e\u6c2e\u63ba\u6742\u78b3\u7eb3\u7c73\u7403\uff09\u7684\u7ed3\u6784\u6210\u5206\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09ANCS\u7684\u6c2e\u6c14\u7b49\u6e29\u7ebf\u53ca\u5bf9\u5e94\u7684NLDFT\u5b54\u5c3a\u5bf8\u5206\u5e03<\/p>\n

\uff08b\uff09ANCS\u548cCS\u7684XRD\u56fe\u3002\u63d2\u56fe\u662f\u653e\u5927\u7684XRD\u56fe\u3002\u63d2\u8868\u662f\u6839\u636e\u8c22\u4e50\u516c\u5f0f\u8ba1\u7b97\u7684\u78b3\u5fae\u6676\u53c2\u6570<\/p>\n

\uff08c\uff09\u6c2e\u63ba\u6742\u524d\u540e\u7684\u78b3\u5c42\u6a21\u578b\u53ca\u5176\u53c2\u6570\u7684\u793a\u610f\u56fe<\/p>\n

\uff08d\uff09ANCS\u548cCS\u7684\u62c9\u66fc\u5149\u8c31<\/p>\n

\uff08e\uff09ANCS\u548cCS\u7684XPS\u5168\u626b\u8c31\u56fe<\/p>\n

\uff08f\uff09ANCS\u7684\u6c2e1s\u9ad8\u5206\u8fa8XPS\u8c31\u56fe\u3002\u63d2\u56fe\u662f\u6c2e\u63ba\u6742\u78b3\u7684\u8868\u9762\u6a21\u578b<\/p>\n

\u00a0<\/strong>\u56fe\u4e09<\/strong> \u7ec4\u88c5\u6210\u534a\u7535\u6c60\u7684\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09ANCS\u8d1f\u6781\u57280.02-3.0 V\u5bf9\u9502\u7535\u52bf\u8303\u56f4\u5185\u4ee50.5 mV s-1<\/sup>\u626b\u63cf\u901f\u5ea6\u4e0b\u7684\u5178\u578bCV\u66f2\u7ebf<\/p>\n

\uff08b\uff09ANCS\u8d1f\u6781\u57280.1 A g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7b2c\u4e00\u3001\u7b2c\u4e8c\u3001\u7b2c\u4e09\u6b21\u7684\u5145\u653e\u7535\u66f2\u7ebf<\/p>\n

\uff08c\uff09ANCS\u548cCS\u8d1f\u6781\u7684\u500d\u7387\u6027\u80fd<\/p>\n

\uff08d\uff09ANCS\u548cCS\u7535\u6781\u7684\u4ea4\u6d41\u963b\u6297\u56fe<\/p>\n

\uff08e\uff09ANCS\u8d1f\u6781\u57282 A g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u5faa\u73af\u7a33\u5b9a\u6d4b\u8bd5\u56fe<\/p>\n

\uff08f\uff09ANCS\u6b63\u6781\u57282.0-4.5 V\u5bf9\u9502\u7535\u52bf\u8303\u56f4\u5185\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u5145\u653e\u7535\u66f2\u7ebf<\/p>\n

\uff08g\uff09ANCS\u6b63\u6781\u57282 A g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u5faa\u73af\u7a33\u5b9a\u6d4b\u8bd5\u56fe<\/p>\n

\u00a0<\/strong>\u56fe\u56db<\/strong> \u4ee5<\/strong>1 M TEABF4-AN<\/strong>\u4e3a\u7535\u89e3\u6db2<\/strong> \u5728<\/strong>3V<\/strong>\u5de5\u4f5c\u7535\u538b\u4e0b<\/strong>ANCS-EDLC<\/strong>\uff08<\/strong>ANCS<\/strong>\u53cc\u7535\u5c42\u7535\u5bb9\u5668\uff09\u548c<\/strong>CS-EDLC<\/strong>\uff08\u78b3\u7eb3\u7c73\u7403\u53cc\u7535\u5c42\uff09\u7684\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u4e0d\u540c\u626b\u63cf\u901f\u5ea6\u4e0bANCS-EDLC\u7684CV\u66f2\u7ebf<\/p>\n

\uff08b\uff09\u572850 mV s-1<\/sup>\u626b\u63cf\u901f\u5ea6\u4e0bANCS-EDLC\u548cCS-EDLC\u7684CV\u66f2\u7ebf<\/p>\n

\uff08c\uff09\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0bANCS-EDLC\u7684\u6052\u7535\u6d41\u5145\u653e\u7535\u66f2\u7ebf<\/p>\n

\uff08d\uff09\u57282 A g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0bANCS-EDLC\u548cCS-EDLC\u7684\u6052\u7535\u6d41\u5145\u653e\u7535\u66f2\u7ebf<\/p>\n

\uff08e\uff09ANCS-EDLC\u548cCS-EDLC\u7684\u4ea4\u6d41\u963b\u6297\u56fe<\/p>\n

\uff08f\uff09ANCS-EDLC\u548cCS-EDLC\u7684\u80fd\u91cf\u5bc6\u5ea6\u56fe<\/p>\n

\u00a0<\/strong>\u56fe\u4e94<\/strong> ANCS\/\/ANCS LIC<\/strong>\u7684\u5de5\u4f5c\u673a\u7406\u548c\u7535\u5316\u5b66\u6027\u80fd\uff08<\/strong>ANCS<\/strong>\u5728\u8d1f\u6781\u548c\u6b63\u6781\u7684\u8d1f\u8f7d\u91cf\u5206\u522b\u4e3a<\/strong>1.2<\/strong>\u548c<\/strong>3.6 mg cm-2<\/sup><\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u5de5\u4f5c\u673a\u7406\u793a\u610f\u56fe<\/p>\n

\uff08b\uff09\u5728\u7535\u538b\u8303\u56f40-4.5V\u8303\u56f4\u5185\u4e0d\u540c\u626b\u63cf\u901f\u7387\u4e0b\u7684\u5178\u578bCV\u66f2\u7ebf<\/p>\n

\uff08c\uff09\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u6052\u7535\u6d41\u5145\u653e\u7535\u66f2\u7ebf<\/p>\n

\uff08d\uff09\u4e0e\u6587\u732e\u5df2\u62a5\u9053\u7684\u80fd\u91cf\u5bc6\u5ea6\u7684\u5bf9\u6bd4\u56fe<\/p>\n

\uff08e\uff09\u57284 A g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0bANCS\/\/ANCS\u7684\u5faa\u73af\u6027\u80fd\u3002\u63d2\u56fe\u662f\u57282 A g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u77f3\u58a8\/\/ANCS\u7684\u5faa\u73af\u6027\u80fd<\/p>\n

\uff08f\uff09ANCS\/\/ANCS\u548c\u77f3\u58a8\/\/ANCS\u7684\u7535\u538b\u964d-\u7535\u6d41\u5bc6\u5ea6\u5750\u6807\u56fe<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u672c\u6587\u4ecb\u7ecd\u4e86\u4e00\u79cd\u5177\u6709\u4f18\u5f02\u6027\u80fd\u7684\u65b0\u578b\u5168\u78b3\u9502\u79bb\u5b50\u7535\u5bb9\u5668\u3002\u8be5LIC\u4ee5\u9ad8\u6d53\u5ea6\u6c2e\u63ba\u6742\u7684\u65e0\u5b9a\u578b\u591a\u5b54\u78b3\u7403\u540c\u65f6\u7528\u4e3a\u6b63\u8d1f\u6781\u6750\u6599\uff0c\u9ad8\u6d53\u5ea6\u6c2e\u63ba\u6742\u589e\u52a0\u4e86\u78b3\u7403\u7684\u6d3b\u6027\u70b9\uff0c\u4f7f\u5176\u7528\u4f5c\u6b63\u8d1f\u6781\u6750\u6599\u53ef\u4ee5\u63d0\u4f9b\u66f4\u591a\u7684\u7535\u5bb9\u6027\u7535\u8377\u5b58\u50a8\u5bb9\u91cf\uff0c\u8fd9\u6709\u6548\u5730\u5316\u89e3\u4e86\u8d1f\u6781\u50a8Li+<\/sup>\u548c\u6b63\u6781\u50a8PF6<\/sub>–<\/sup>\u7684\u7535\u5316\u5b66\u52a8\u529b\u5b66\u53ca\u7a33\u5b9a\u6027\u77db\u76fe\uff0c\u5b9e\u73b0\u4e86\u8d1f\u6781\u7684\u9ad8\u500d\u7387\u957f\u5bff\u547d\u548c\u6b63\u6781\u7684\u9ad8\u5bb9\u91cf\uff0c\u5c55\u73b0\u4e86\u9ad8\u538b\u5168\u78b3\u5bf9\u79f0\u9502\u79bb\u5b50\u7535\u5bb9\u5668\u7684\u53d1\u5c55\u6f5c\u529b\u548c\u5e94\u7528\u524d\u666f\u3002\u8be5\u5de5\u4f5c\u53ef\u4e3a\u901a\u8fc7\u8c03\u63a7\u78b3\u7eb3\u7c73\u6750\u6599\u7684\u5316\u5b66\u73af\u5883\u6765\u8bbe\u8ba1\u9ad8\u538b\u9502\u79bb\u5b50\u7535\u5bb9\u5668\u63d0\u4f9b\u601d\u8def\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong> In Situ High-Level Nitrogen Doping into Carbon Nanospheres and Boosting of Capacitive Charge Storage in Both Anode and Cathode for a High-Energy 4.5 V Full-Carbon Lithium-Ion Capacitor<\/a> (Nano Lett., 2018, DOI: 10.1021\/acs.nanolett.8b00134)<\/p>\n

\u56e2\u961f\u76f8\u5173\u7814\u7a76\u4ecb\u7ecd\uff1a<\/strong>\u5362\u4e91\u5cf0\u6559\u6388\u7814\u7a76\u56e2\u961f\u957f\u671f\u4ece\u4e8b\u7535\u5316\u5b66\u50a8\u80fd\u6750\u6599\u53ca\u5668\u4ef6\u7814\u53d1\u76f8\u5173\u5de5\u4f5c\uff0c\u8fd1\u4e24\u6765\u5728\u78b3\u57fa\u6750\u6599\u5fae\u7eb3\u7ed3\u6784\u5b9a\u5411\u8c03\u63a7\u53ca\u5176\u5728\u7535\u5316\u5b66\u50a8\u80fd\u65b9\u9762\u7684\u5e94\u7528\uff0c\u7279\u522b\u662f\u78b3\u6750\u6599\u5316\u5b66\u73af\u5883\u7684\u6539\u5584\u53ca\u5176\u5728\u8d85\u7ea7\u7535\u5bb9\u5668\u3001\u9502\u79bb\u5b50\u7535\u6c60\u3001\u7535\u50ac\u5316\u3001\u6c14\u4f53\u5438\u9644\u7b49\u65b9\u9762\u7684\u6027\u80fd\u4f18\u5316\u53ca\u673a\u5236\u63ed\u793a\u65b9\u9762\u5f00\u5c55\u4e86\u8f83\u4e3a\u6df1\u5165\u7684\u7814\u7a76\u5de5\u4f5c\uff0c\u76f8\u5173\u7814\u7a76\u5df2\u53d1\u8868Adv. Energy. Mater., 2017, 7\u00a0(22)\u00a0:1701154, Nano Energy, 2016\u00a0,\u00a021,80, Nano Res., 2016, 9(11), 3209, JMCA, 2016, 4(47): 18248.<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u65b0\u80fd\u6e90\u7ec4\u9a6c\u5143\u6574\u7406\u7f16\u8f91\uff0c\u70b9\u6211\u52a0\u5165\u6750\u6599\u4eba\u7f16\u8f91\u90e8<\/a>\u3002<\/p>\n

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