{"id":144044,"date":"2018-06-29T06:46:40","date_gmt":"2018-06-28T22:46:40","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=144044"},"modified":"2018-06-28T10:49:07","modified_gmt":"2018-06-28T02:49:07","slug":"%e9%99%95%e8%a5%bf%e5%b8%88%e8%8c%83%e9%99%88%e7%85%9caem%ef%bc%9a%e5%a4%9a%e5%ad%94ptrhcu%e4%b8%89%e9%87%91%e5%b1%9e%e7%a9%ba%e5%bf%83%e7%ba%b3%e7%b1%b3%e7%ab%8b%e6%96%b9%e7%94%b5%e5%82%ac%e5%8c%96","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=144044","title":{"rendered":"\u9655\u897f\u5e08\u8303\u9648\u715cAEM\uff1a\u591a\u5b54PtRhCu\u4e09\u91d1\u5c5e\u7a7a\u5fc3\u7eb3\u7c73\u7acb\u65b9\u7535\u50ac\u5316\u4e59\u9187\u6c27\u5316"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n

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\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u9655\u897f\u5e08\u8303\u5927\u5b66\u6750\u6599\u79d1\u5b66\u4e0e\u5de5\u7a0b\u5b66\u9662\uff0c\u9655\u897f\u7701\u5927\u5206\u5b50\u79d1\u5b66\u91cd\u70b9\u5b9e\u9a8c\u5ba4\u9648\u715c\u6559\u6388\u8bfe\u9898\u7ec4<\/strong>\u9488\u5bf9EOR\u8fc7\u7a0b\u4e2d\u7684\u5404\u9879\u96be\u9898\uff0c\u8bbe\u8ba1\u5e76\u6210\u529f\u5236\u5907\u591a\u5b54PtRhCu\u4e09\u91d1\u5c5e\u7a7a\u5fc3\u7eb3\u7c73\u7acb\u65b9\uff08CNBs\uff09\u3002\u5176\u4e2d\uff0c\u4e2d\u7a7a\u58f3\u5c42\u7684\u539a\u5ea6\u53ef\u901a\u8fc7\u7b80\u5355\u7684\u63a7\u5236\u8d35\u91d1\u5c5e\u6295\u6599\u91cf\u6765\u8c03\u63a7\u3002\u5177\u6709\u4e0d\u540cPt\/Rh\u6bd4\u7684 PtRhCu-CNBs\u53ef\u4fbf\u5229\u5730\u901a\u8fc7\u6539\u53d8\u539f\u6599\u6bd4\u6765\u5236\u5907\u3002\u7814\u7a76\u663e\u793a\uff0cRh\u7684\u5f15\u5165\u53ef\u4ee5\u6709\u6548\u63d0\u5347\u50ac\u5316\u5242\u5288\u88c2C-C\u952e\u7684\u80fd\u529b\uff0cCu\u7684\u5f15\u5165\u53ef\u589e\u5f3a\u50ac\u5316\u5242\u5bf9CO\u4e2d\u95f4\u4f53\u7684\u50ac\u5316\u6c27\u5316\u6027\u80fd\u3002\u57fa\u4e8e\u8be5\u6750\u6599\u72ec\u7279\u7684\u7ed3\u6784\u6548\u5e94\u548c\u4e09\u91d1\u5c5e\u95f4\u7684\u534f\u540c\u6548\u5e94\uff0cPtRhCu-CNBs\u5bf9\u4e8e\u50ac\u5316EOR\u663e\u793a\u4f18\u5f02\u7684\u7535\u50ac\u5316\u6027\u80fd\u3002\u5728\u5177\u6709\u4e0d\u540cPt\/Rh\u6bd4\u7684PtRhCu-CNBs\u4e2d\uff0cPt54<\/sub>Rh4<\/sub>Cu42<\/sub>-CNBs \u5177\u6709\u6700\u9ad8\u7684\u50ac\u5316\u6d3b\u6027\u548c\u7a33\u5b9a\u6027\u3002\u6b64\u5916\uff0c\u5b9e\u9a8c\u7ed3\u679c\u4e5f\u663e\u793a\uff0c\u8be5\u79cd\u53d1\u5c55\u7684\u4f3d\u4f10\u5c3c\u8fd8\u539f\u6cd5\u5177\u6709\u901a\u7528\u6027\uff0c\u53ef\u7528\u6765\u5236\u5907\u5176\u5b83\u4e8c\u5143\u6216\u4e09\u5143\u6210\u5206\u7684\u4e2d\u7a7a\u7eb3\u7c73\u7acb\u65b9\uff0c\u4e3a\u8bbe\u8ba1\u5236\u5907\u7279\u5b9a\u7ec4\u5206\u548c\u7ed3\u6784\u7684\u7eb3\u7c73\u6750\u6599\u63d0\u4f9b\u4e86\u6709\u6548\u7684\u65b9\u6cd5\u3002\u8be5\u5de5\u4f5c\u65e5\u524d\u4ee5 \u201cPorous Trimetallic PtRhCu Cubic Nanoboxes for Ethanol Electrooxidation<\/strong>\u201d\u4e3a\u9898\u53d1\u8868\u4e8eAdvanced Energy Materials<\/strong>\u4e0a\u3002<\/p>\n

 <\/p>\n

\"\"<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00\uff1aCu2<\/sub>O\u6a21\u677f\u7684\u8868\u5f81<\/p>\n


\n \"\"<\/b><\/strong><\/p>\n

a\uff09XRD\u56fe\uff1b<\/p>\n

b\uff09SEM\u7167\u7247\uff1b<\/p>\n

c\uff09TEM\u7167\u7247\uff1b<\/p>\n

d\uff09\u9ad8\u5206\u8fa8TEM\u7167\u7247\uff1b<\/p>\n

e\uff09d\u56fe\u4e2d\u968f\u673a\u9009\u53d6\u7684\u56db\u5e45\u5c40\u90e8\u653e\u5927\u7684TEM\u7167\u7247\u3002<\/p>\n

\u793a\u610f\u56fe\uff1aPtRhCu-CNBs\u5236\u5907\u8def\u7ebf\u3002<\/p>\n


\n \"\"<\/b><\/strong><\/p>\n

\u56fe\u4e8c\uff1aPtRhCu-CNBs\u8868\u5f81\uff08\u4e00\uff09<\/strong><\/p>\n


\n \"\"<\/b><\/strong><\/p>\n

a\uff09XRD\u56fe\uff1b<\/p>\n

b\uff09SEM\u7167\u7247\uff1b<\/p>\n

c\uff09TEM\u7167\u7247\uff1b<\/p>\n

d\uff09Pt\u3001Rh\u3001Cu\u4e09\u5143\u7d20maps\u56fe\u3002<\/p>\n

\u4e00\u7cfb\u5217\u8868\u5f81\u8bc1\u660e\u6211\u4eec\u4f7f\u7528\u4e0a\u8ff0\u5408\u6210\u8def\u7ebf\u53ef\u6210\u529f\u5236\u5907\u591a\u5b54PtRhCu\u4e09\u91d1\u5c5e\u7a7a\u5fc3\u7eb3\u7c73\u7acb\u65b9<\/b><\/strong>\u3002<\/b><\/strong><\/p>\n

\u56fe\u4e09\uff1aPtRhCu-CNBs\u8868\u5f81\uff08\u4e8c\uff09\uff1a\u7ec6\u8282\u8868\u5f81<\/strong><\/p>\n


\n \"\"<\/b><\/strong><\/p>\n

a\uff09\u5355\u4e2a\u7a7a\u5fc3\u7acb\u65b9\u7684TEM\u7167\u7247\uff1b<\/p>\n

b\uff09\u5b54\u5f84\u5206\u5e03\u66f2\u7ebf\uff1b<\/p>\n

c\uff09TEM\u5c40\u90e8\u653e\u5927\u56fe\uff0c\u63d2\u56fe\u4e3a\u76f8\u5e94\u4f4d\u7f6e\u7684\u7535\u5b50\u884d\u5c04\u7167\u7247\uff1b<\/p>\n

d\uff09\u9ad8\u5206\u8fa8TEM\u7167\u7247\u548c\u76f8\u5e94\u4f4d\u7f6e\u7684FFT\u53d8\u6362\u56fe\u3002<\/p>\n

\u53ef\u5f97\u51fa\u7ed3\u8bba\uff1a<\/b><\/strong>\u00a0PtRhCu-CNBs<\/b><\/strong>\u4e3a\u7a7a\u5fc3\u591a\u5b54\u6750\u6599\uff0c\u540c\u65f6\u6709\u7740\u826f\u597d\u7684\u7ed3\u6676\u5ea6\u3002\u6240\u66b4\u9732\u7684\u6676\u9762\u4e3a\u5408\u91d1\u7684{111}\u6676\u9762<\/b><\/strong>\u3002<\/p>\n

\u56fe\u56db\uff1a\u5408\u6210\u65b9\u6cd5\u7684\u901a\u7528\u6027<\/strong>\u3002<\/p>\n


\n \"\"<\/b><\/strong><\/p>\n

a\uff09PtAuCu-CNBs\u548cb\uff09PtIrCu-CNBs\u7684\u6697\u573a\u900f\u5c04\u7167\u7247\u53ca\u5143\u7d20maps\u5206\u5e03\u56fe\u3002<\/p>\n

\u53ef\u4ee5\u770b\u51fa\uff0c\u672c\u6587\u7684\u5236\u5907\u65b9\u6cd5\u5bf9\u4e8e\u5176\u4ed6\u4e8c\u5143\u3001\u4e09\u5143\u8d35\u91d1\u5c5e\u5408\u91d1\u7a7a\u5fc3\u7eb3\u7c73\u7acb\u65b9\u7684\u5408\u6210\u5177\u6709\u826f\u597d\u7684\u901a\u7528\u6027\u3002\u8fd9\u4e5f\u4e3a\u5176\u5b83\u4e2d\u7a7a\u6750\u6599\u7684\u5236\u5907\u63d0\u4f9b\u4e86\u826f\u597d\u7684\u5408\u6210\u8def\u7ebf\u3002<\/b><\/strong><\/p>\n

\u56fe\u4e94\uff1a\u4e59\u9187\u7535\u6c27\u5316\u6027\u80fd\u6d4b\u8bd5\uff08\u4e00\uff09\uff1a\u4e09\u79cd\u5143\u7d20\u7684\u4f5c\u7528\u63a2\u7a76<\/strong><\/p>\n


\n \"\"<\/b><\/strong><\/p>\n

a\uff09Pt54<\/sub>Rh4<\/sub>Cu42<\/sub>-CNBs\u3001Pt58<\/sub>Cu42<\/sub>-CNBs\u548c\u81ea\u5236Pt\u7eb3\u7c73\u7c92\u5b50\u7684CV\u66f2\u7ebf\uff0c\u7535\u89e3\u8d28\u6eb6\u6db2\u4e3a1M KOH\u6eb6\u6db2\uff1b<\/p>\n

b\uff09Pt54<\/sub>Rh4<\/sub>Cu42<\/sub>-CNBs\u3001Pt58<\/sub>Cu42<\/sub>-CNBs\u548c\u81ea\u5236Pt\u7eb3\u7c73\u7c92\u5b50\u7684\u8d35\u91d1\u5c5e\u8d28\u91cf\u6bd4\u6d3b\u6027CV\u66f2\u7ebf\uff0c\u7535\u89e3\u8d28\u6eb6\u6db2\u4e3aN2<\/sub>\u9971\u548c\u76841M KOH+1M CH3<\/sub>CH2<\/sub>OH\uff1b<\/p>\n

c\uff09Pt54<\/sub>Rh4<\/sub>Cu42<\/sub>-CNBs\u3001Pt58<\/sub>Cu42<\/sub>-CNBs\u548c\u81ea\u5236Pt\u7eb3\u7c73\u7c92\u5b50\u7684ECSA\u9762\u79ef\u6bd4\u6d3b\u6027CV\u66f2\u7ebf\uff0c\u7535\u89e3\u8d28\u6eb6\u6db2\u4e3aN2<\/sub>\u9971\u548c\u76841M KOH+1M CH3<\/sub>CH2<\/sub>OH\uff1b<\/p>\n

d\uff09c\u56fe\u7684\u5c40\u90e8\u653e\u5927\u56fe\u3002<\/p>\n

\u7ed3\u8bba\uff1aRh\u3001Cu\u539f\u5b50\u7684\u5f15\u5165\u6709\u5229\u4e8eEOR\u8d77\u59cb\u6c27\u5316\u7535\u4f4d\u7684\u8d1f\u79fb\u3002\u540c\u65f6\uff0cRh\u7684\u5f15\u5165\u53ef\u6709\u6548\u964d\u4f4e\u6b63\u53cd\u5411\u5cf0\u7535\u6d41\u4e4b\u6bd4\uff0c\u6307\u51faRh\u5f15\u5165\u53ef\u80fd\u5f71\u54cdEOR\u9014\u5f84\u3002<\/b><\/strong><\/p>\n

\u968f\u540e\u6211\u4eec\u5bf9\u7535\u89e3\u8d28\u6eb6\u6db2\u8fdb\u884c\u4e86\u6210\u5206\u5206\u6790\uff0c\u7ed3\u679c\u663e\u793a\uff0cRh\u7684\u5f15\u5165\u786e\u5b9e\u6709\u53ef\u4ee5\u6709\u6548\u964d\u4f4e\u7535\u89e3\u6db2\u4e2dC2\u4ea7\u7269\u7684\u542b\u91cf\uff0c\u8fdb\u800c\u8bc1\u660eRh\u7684\u5f15\u5165\u786e\u5b9e\u53ef\u4ee5\u63d0\u9ad8C-C\u952e\u5288\u88c2\u80fd\u529b\uff0c\u4ece\u800c\u63d0\u5347C1\u9014\u5f84\u7684\u9009\u62e9\u6027\u3002<\/b><\/strong><\/p>\n

\u56fe\u516d\uff1a\u4e59\u9187\u7535\u6c27\u5316\u6027\u80fd\u6d4b\u8bd5\uff08\u4e8c\uff09\uff1a\u5bf9\u4e2d\u95f4\u4f53\u7535\u6c27\u5316\u7684\u63a2\u7a76<\/strong><\/p>\n


\n \"\"<\/b><\/strong><\/p>\n

a\uff09Pt54<\/sub>Rh4<\/sub>Cu42<\/sub>-CNBs\u3001Pt58<\/sub>Cu42<\/sub>-CNBs\u548c\u81ea\u5236Pt\u7eb3\u7c73\u7c92\u5b50\u7684 ECSA \u9762\u79ef\u6bd4\u6d3b\u6027CV \u66f2\u7ebf\uff0c\u7535\u89e3\u8d28\u6eb6\u6db2\u4e3a N2<\/sub>\u9971\u548c\u76841M KOH+1M CH3<\/sub>CHO\u3002<\/p>\n

b\uff09Pt54<\/sub>Rh4<\/sub>Cu42<\/sub>-CNBs\u3001Pt58<\/sub>Cu42<\/sub>-CNBs\u548c\u81ea\u5236Pt\u7eb3\u7c73\u7c92\u5b50\u7684CO\u9884\u5438CV\u66f2\u7ebf\u3002\u7535\u89e3\u8d28\u6eb6\u6db2\u4e3aN2<\/sub>\u9971\u548c\u76841M KOH\u3002<\/p>\n

\u7ed3\u8bba\uff1a\u5bf9\u4e8e\u4e59\u919b\u4e2d\u95f4\u4f53\uff0cRh\u7684\u5f15\u5165\u4e5f\u53ef\u4fc3\u8fdbC-C\u952e\u7684\u65ad\u88c2\u3002Cu\u7684\u5f15\u5165\u53ef\u4ee5\u4fc3\u8fdbCO\u6c27\u5316\u3002<\/b><\/strong><\/p>\n

\u56fe\u4e03\uff1a\u4e59\u9187\u7535\u6c27\u5316\u6027\u80fd\u6d4b\u8bd5\uff08\u4e09\uff09\uff1a\u7a33\u5b9a\u6027\u6d4b\u8bd5<\/strong><\/p>\n


\n \"\"<\/b><\/strong><\/p>\n

a\uff09Pt54<\/sub>Rh4<\/sub>Cu42<\/sub>-CNBs\u3001Pt58<\/span>Cu42<\/sub>-CNBs\u548c\u81ea\u5236Pt\u7eb3\u7c73\u7c92\u5b50\u7684\u8ba1\u65f6\u7535\u6d41\u6d4b\u8bd5\uff0c\u7535\u89e3\u8d28\u6eb6\u6db2\u4e3aN2<\/sub>\u9971\u548c\u76841M KOH+1M\u00a0CH3<\/sub>CH2<\/sub>OH\u3002\u00a0<\/p>\n

b\uff09\u4e09\u79cd\u50ac\u5316\u5242\u7684\u81ea\u8eab\u7a33\u5b9a\u6027\u6d4b\u8bd5\u7edf\u8ba1\u56fe\uff0c\u7535\u89e3\u8d28\u6eb6\u6db2\u4e3aN2<\/sub>\u9971\u548c\u76841M KOH\u3002<\/p>\n

\u56fe\u516b\uff1a\u4e59\u9187\u7535\u6c27\u5316\u6027\u80fd\u6d4b\u8bd5\uff08\u56db\uff09\uff1a\u4e0d\u540c\u6bd4\u4f8b\u5bf9\u6d3b\u6027\u7684\u5f71\u54cd<\/strong><\/p>\n


\n \"\"<\/b><\/strong><\/p>\n

a\uff09\u4e0d\u540c\u6210\u5206\u7684PtRhCu-CNBs\u7684ECSA\u9762\u79ef\u6bd4CV\u66f2\u7ebf\uff0c\u7535\u89e3\u8d28\u6eb6\u6db2\u4e3aN2<\/sub>\u9971\u548c\u76841M KOH+1M\u00a0CH3<\/sub>CH2<\/sub>OH\u3002<\/p>\n

b\uff09a\u56fe\u7684\u6c27\u5316\u5cf0\u7535\u6d41\u503c\u548c\u6b63\u53cd\u5411\u5cf0\u6bd4\u503c\u7684\u7edf\u8ba1\u56fe\u3002<\/p>\n

\u56fe\u4e5d\uff1a\u4e59\u9187\u7535\u6c27\u5316\u6027\u80fd\u6d4b\u8bd5\uff08\u4e94\uff09\uff1a\u5546\u4e1a\u5316\u5e94\u7528\u7684\u6f5c\u529b<\/strong><\/p>\n


\n \"\"<\/b><\/strong><\/p>\n

a\uff09Pt54<\/sub>Rh4<\/sub>Cu42<\/sub>-CNBs\u548c\u5546\u4e1a\u5316Pt\u9ed1\u7684Pt\u8d28\u91cf\u6bd4CV\u66f2\u7ebf\uff0c\u7535\u89e3\u8d28\u6eb6\u6db2\u4e3aN2<\/sub>\u9971\u548c\u76841M KOH+1M\u00a0CH3<\/sub>CH2<\/sub>OH\uff0c\u63d2\u56fe\u4e3aa\u56fe\u7684\u5c40\u90e8\u653e\u5927\u56fe\u3002<\/p>\n

b\uff09Pt54<\/sub>Rh4<\/sub>Cu42<\/sub>-CNBs\u548c\u5546\u4e1a\u5316Pt\u9ed1\u8ba1\u65f6\u7535\u6d41\u6d4b\u8bd5\uff0c\u7535\u89e3\u8d28\u6eb6\u6db2\u4e3aN2<\/sub>\u9971\u548c\u76841M KOH+1M\u00a0CH3<\/sub>CH2<\/sub>OH\u3002<\/p>\n

\u3010\u81f4\u8c22\u3011<\/b><\/strong><\/p>\n

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\u8bba\u6587\u94fe\u63a5\uff1ahttps:\/\/onlinelibrary.wiley.com\/doi\/abs\/10.1002\/aenm.201801326<\/p>\n

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