{"id":152232,"date":"2018-08-31T06:52:18","date_gmt":"2018-08-30T22:52:18","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=152232"},"modified":"2018-08-30T23:42:12","modified_gmt":"2018-08-30T15:42:12","slug":"%e5%a4%a9%e5%a4%a7%e5%bc%a0%e6%99%93%e4%b8%9c%e5%8c%97%e5%a4%a7%e6%9d%8e%e7%be%8e%e4%bb%99science-bulletin%ef%bc%9a%e5%a2%9e%e5%bc%ba%e5%82%ac%e5%8c%96%e6%b4%bb%e6%80%a7%e7%9a%84au-mos2%e7%ba%b3","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=152232","title":{"rendered":"\u5929\u5927\u5f20\u6653\u4e1c&\u5317\u5927\u674e\u7f8e\u4ed9Science Bulletin\uff1a\u589e\u5f3a\u50ac\u5316\u6d3b\u6027\u7684Au-MoS2\u7eb3\u7c73\u56e2\u7c07\u6539\u5584\u8f90\u5c04\u9632\u62a4\u6027\u80fd"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n

\u8fd1\u5e74\u6765\uff0c\u50ac\u5316\u7eb3\u7c73\u6750\u6599\u5728\u6297\u6c27\u5316\u548c\u8f90\u5c04\u9632\u62a4\u65b9\u9762\u53d1\u6325\u4e86\u5de8\u5927\u7684\u6f5c\u529b\uff0c\u5927\u91cf\u7684\u7535\u5b50\u8f6c\u79fb\u6d3b\u6027\u4f4d\u70b9\u51b3\u5b9a\u4e86\u5b83\u4eec\u7684\u7535\u50ac\u5316\u6d3b\u6027\uff0c\u5982\u50ac\u5316\u6c27\u8fd8\u539f\u548c\u6c22\u5316\u53cd\u5e94\u7684\u6027\u80fd\u3002\u540c\u65f6\uff0c\u7535\u50ac\u5316\u8fc7\u7a0b\u4e2d\u7684\u6c27\u5316\u8fd8\u539f\u53cd\u5e94\u51b3\u5b9a\u4e86\u50ac\u5316\u7eb3\u7c73\u6750\u6599\u5206\u89e3\u8f90\u5c04\u8bf1\u5bfc\u4ea7\u751f\u7684\u8fc7\u91cfROS\u7684\u80fd\u529b\uff0c\u4e14\u8bb8\u591a\u7814\u7a76\u8bc1\u660e\u589e\u5f3a\u6750\u6599\u7684\u50ac\u5316\u6027\u80fd\u53ef\u4ee5\u589e\u5f3a\u5176\u8f90\u5c04\u9632\u62a4\u6027\u80fd\u3002\u4e8b\u5b9e\u4e0a\uff0c\u5df2\u6709\u5927\u91cf\u62a5\u9053\u63ba\u6742\u91d1\u5c5e\u539f\u5b50\u4ee5\u589e\u5f3a\u50ac\u5316\u6750\u6599\u50ac\u5316\u6d3b\u6027\u7684\u7814\u7a76\uff0c\u53d1\u73b0\u5728\u67d0\u4e9b\u50ac\u5316\u6750\u6599\u4e2d\u63ba\u5165\u91d1\u5c5e\u539f\u5b50\u53ef\u4ee5\u589e\u5f3a\u6750\u6599\u7684\u50ac\u5316\u6d3b\u6027\u30022-D\u5c42\u72b6\u50ac\u5316\u7eb3\u7c73\u6750\u6599MoS2<\/sub>\u662f\u591a\u79cd\u50ac\u5316\u53cd\u5e94\u7684\u6709\u6548\u50ac\u5316\u5242\u4e14\u5728\u8f90\u5c04\u9632\u62a4\u65b9\u9762\u5177\u6709\u5e7f\u9614\u7684\u5e94\u7528\u524d\u666f\u3002\u636e\u62a5\u9053\uff0c\u5982MoS2<\/sub>\u548cWS2<\/sub>\u8fd9\u7c7b\u7684\u50ac\u5316\u7eb3\u7c73\u6750\u6599\uff0c\u4e0eCeO2<\/sub>\u540c\u6837\u5177\u6709\u8f83\u5f3a\u7684\u50ac\u5316\u6d3b\u6027\uff0c\u53ef\u5728\u4f53\u5185\u5916\u6709\u6548\u6539\u5584\u8f90\u5c04\u8bf1\u5bfc\u7684\u635f\u4f24\u3002\u540c\u65f6\u6709\u7814\u7a76\u663e\u793a\uff0c\u7eb3\u7c73\u6750\u6599\u7684\u50ac\u5316\u6027\u80fd\u4e0e\u8f90\u5c04\u9632\u62a4\u6548\u679c\u5448\u6b63\u76f8\u5173\u3002\u56e0\u6b64\uff0c\u589e\u5f3a\u6750\u6599\u7684\u50ac\u5316\u6d3b\u6027\u662f\u53d6\u5f97\u6700\u4f73\u8f90\u5c04\u9632\u62a4\u6548\u679c\u7684\u5173\u952e\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u5728\u5929\u6d25\u5927\u5b66\u5f20\u6653\u4e1c\u6559\u6388<\/b><\/strong>\u548c\u5317\u4eac\u5927\u5b66\u674e\u7f8e\u4ed9\u6559\u6388<\/b><\/strong>\uff08<\/b><\/strong>\u5171\u540c<\/b><\/strong>\u901a\u8baf\u4f5c\u8005\uff09<\/b><\/strong>\u56e2\u961f\u7684\u5e26\u9886\u4e0b\uff0c\u4e0e\u4e2d\u5c71\u5927\u5b66<\/b><\/strong>\u5408\u4f5c\uff0c\u91c7\u7528\u4e86\u6eb6\u5242\u70ed\u6cd5\uff0c\u5c06\u7eb3\u7c73\u6750\u6599MoS2<\/sub>\u4e0e\u91d1\u56e2\u7c07\u8fdb\u884c\u6742\u4ea4\uff0c\u5f62\u6210\u5177\u6709\u66f4\u5f3a\u50ac\u5316\u6d3b\u6027\u7684Au-MoS2<\/sub>\u56e2\u7c07\uff0c\u6210\u529f\u5b9e\u73b0\u4e86\u63d0\u9ad8\u6750\u6599\u6e05\u9664ROS\u6d3b\u6027\u53ca\u589e\u5f3a\u8f90\u5c04\u9632\u62a4\u6027\u80fd\u7684\u76ee\u7684\u3002\u8be5\u7814\u7a76\u56e2\u961f\u9996\u5148\u63a2\u7d22\u53d1\u73b0\uff0c\u4e0e\u7eb3\u7c73\u6750\u6599MoS2<\/sub>\u76f8\u6bd4\uff0cAu-MoS2<\/sub>\u56e2\u7c07\u5177\u6709\u66f4\u5f3a\u7684\u50ac\u5316H2<\/sub>O2<\/sub>\u5206\u89e3\u7684\u80fd\u529b\u3002\u5728\u6b64\u57fa\u7840\u4e0a\uff0c\u4ed6\u4eec\u8fdb\u4e00\u6b65\u7814\u7a76\u53d1\u73b0\uff0c\u00a0Au-MoS2<\/sub>\u56e2\u7c07\u5177\u6709\u66f4\u5f3a\u7684\u6e05\u9664\u8f90\u5c04\u8bf1\u5bfc\u4ea7\u751fROS\u7684\u6027\u80fd\u3002\u6b64\u5916\uff0c\u4e0eMoS2<\/sub>\u76f8\u6bd4\uff0cAu-MoS2<\/sub>\u56e2\u7c07\u53ef\u4ee5\u901a\u8fc7\u66f4\u663e\u8457\u5730\u63d0\u9ad8DNA\u6c34\u5e73\u53ca\u589e\u52a0\u80a1\u9aa8\u6709\u6838\u7ec6\u80de\u7684\u6570\u91cf\uff0c\u4ece\u800c\u66f4\u597d\u5730\u4fdd\u62a4\u5bf9\u8f90\u5c04\u9ad8\u5ea6\u654f\u611f\u7684\u9aa8\u9ad3\u9020\u8840\u7cfb\u7edf\u3002\u4ee5\u4e0a\u7ed3\u679c\u8bc1\u660e\u4e86\u50ac\u5316\u7eb3\u7c73\u6750\u6599Au-MoS2<\/sub>\u6709\u671b\u5e94\u7528\u4e8e\u6539\u5584\u8f90\u5c04\u8bf1\u5bfc\u7684\u635f\u4f24\u3002\u76f8\u5173\u6210\u679c\u4ee5\u9898\u4e3a\u201cEnhanced catalysis of ultrasmall Au-MoS<\/b><\/strong>2<\/b><\/sub><\/strong>\u00a0clusters against reactive oxygen species for radiation protection<\/b><\/strong>\u201d\u53d1\u8868\u5728\u4e86Science Bulletin<\/b><\/strong>\u4e0a\u3002<\/p>\n

\u00a0<\/b><\/strong>\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/b><\/strong><\/p>\n

\u56fe1 Au-MoS<\/b><\/strong>2<\/b><\/sub><\/strong>\u7684\u8868\u5f81<\/b><\/strong>\"\"<\/b><\/strong><\/p>\n

\uff08a\uff09Au-MoS2<\/sub>\u56e2\u7c07\u7684TEM\u56fe\u3002<\/p>\n

\uff08b\uff09\u5728350\uff0c380\u548c410nm\u7684\u4e0d\u540c\u6fc0\u53d1\u6ce2\u957f\u4e0bAu-MoS2<\/sub>\u56e2\u7c07\u7684\u5149\u81f4\u53d1\u5149\u5149\u8c31\u3002\uff08c-e\uff09\u5206\u522b\u4e3aAu-MoS2<\/sub>\u7684Au 4f\uff0cMo 3d\u548cS 2p\u7684XPS\u5149\u8c31\u3002<\/p>\n

\uff08f\uff09Au-MoS2<\/sub>\u56e2\u7c07\u7684XPS\u603b\u8c31\u3002<\/p>\n

\u00a0<\/b><\/strong>\u56fe2 <\/b><\/strong>Au-MoS<\/b><\/strong>2<\/b><\/sub><\/strong>\u56e2<\/b><\/strong>\u7c07<\/b><\/strong>\u7684\u7535\u50ac\u5316\u6d3b\u6027<\/b><\/strong>\"\"<\/b><\/strong><\/p>\n

\uff08a\uff09\u5728N2<\/sub>\u9971\u548c\u76840.1mol\/L\u00a0PBS\u4e2d\u542b\u6709\u548c\u4e0d\u542b5.00mmol\/L\u00a0H2<\/sub>O2<\/sub>\u7684GCE\u7684CV\u3002<\/p>\n

\uff08b\uff09\u5728N2<\/sub>\u9971\u548c\u76840.1mol\/L\u00a0PBS\u4e2d\u4ee550mV\/s\u7684\u626b\u63cf\u901f\u7387\u7684Au-MoS2<\/sub>\u56e2\u7c07\u548cCys-MoS2<\/sub>\u4fee\u9970\u7684GCE\u7684CV\uff0c\u5305\u62ec\u542b\u6709\u548c\u4e0d\u542b5.00mmol\/L\u00a0H2<\/sub>O2<\/sub>\u3002<\/p>\n

\uff08c\uff09\u5728N2<\/sub>\u548cO2<\/sub>\u9971\u548c\u76840.1mol\/L\u00a0PBS\u4e2d\u4ee550mV\/s\u7684\u626b\u63cf\u901f\u7387\u7684GCE\u7684CV\u3002<\/p>\n

\uff08d\uff09\u5728N2<\/sub>\u548cO2<\/sub>\u9971\u548c\u76840.1mol\/LPBS\u4e2d\u4ee550mV\/s\u7684\u626b\u63cf\u901f\u7387\u7684Au-MoS2<\/sub>\u56e2\u7c07\u548cCys-MoS2<\/sub>\u4fee\u9970\u7684GCE\u7684CV\u3002<\/p>\n

\u56fe3<\/b><\/strong>\u00a0<\/b><\/strong>\u7ec6\u80de\u6d3b\u529b\u6d4b<\/b><\/strong>\u8bd5<\/b><\/strong>\"\"<\/b><\/strong><\/p>\n

\uff08a\uff09CHO\u7ec6\u80de\u4e0eAu-MoS2<\/sub>\u5b75\u531624\u5c0f\u65f6\u548c48\u5c0f\u65f6\u540e\u7684\u6d3b\u529b\u3002<\/p>\n

\uff08b\uff09CHO\u7ec6\u80de\u4e0eAu-MoS2<\/sub>\uff08100\u03bcg\/mL\uff09\u548cCys-MoS2<\/sub>\uff08100\u03bcg\/mL\uff09\u5b75\u531624\u5c0f\u65f6\u548c48\u5c0f\u65f6\u540e\u7684\u6d3b\u529b\u3002<\/p>\n

\uff08c\uff09\u7528\u6d53\u5ea6\u4e3a0\uff0c25\uff0c50\u548c100\u03bcg\/mL\u7684Au-MoS2<\/sub>\u5904\u7406\u7684CHO\u7ec6\u80de\uff0c\u5728\u66b4\u9732\u4e8e0\uff0c2\uff0c4\u548c8\u00a0Gy\u8f90\u5c04\u5242\u91cf\u4e4b\u524d\u7684\u6d3b\u529b\u3002*\u8868\u793aP\u202f<0.05\u3002<\/p>\n

\uff08d\uff09\u7528\u6d53\u5ea6\u4e3a0\uff0c25\uff0c50\u548c100\u03bcg\/mL\u7684Au-MoS2<\/sub>\u5904\u7406\u7684\u548cCys-MoS2<\/sub>\u5904\u7406\u7684CHO\u7ec6\u80de\uff0c\u5728\u66b4\u9732\u4e8e4\u00a0Gy\u8f90\u5c04\u5242\u91cf\u4e4b\u524d\u7684\u6d3b\u529b\u3002*\u8868\u793aP\u202f<0.05\u3002<\/p>\n

\u56fe<\/b><\/strong>4 <\/b><\/strong>\u8f90\u5c04\u8bf1\u5bfc\u7684\u7ec6\u80de\u5185ROS\u6c34\u5e73<\/b><\/strong>\u6d4b\u8bd5<\/b><\/strong>\"\"<\/p>\n

\uff08a\uff0cb\uff09\u5206\u522b\u4e3aCHO\u7ec6\u80de\u5bf9\u7167\u548c\u8f90\u5c04\u7167\u5c04\u540e\u7684\u8367\u5149\u56fe\u50cf\u3002<\/p>\n

\uff08c\uff0cd\uff09\u5206\u522b\u4e3a\u6ce8\u5c04Au-MoS2<\/sub>\u7684CHO\u7ec6\u80de\u5bf9\u7167\u56fe\u548c\u8f90\u5c04\u540e\u7684\u8367\u5149\u56fe\u50cf\u3002<\/p>\n

\uff08e\uff0cf\uff09\u5206\u522b\u4e3a\u6ce8\u5c04Cys-MoS2<\/sub>\u7684CHO\u7ec6\u80de\u5bf9\u7167\u56fe\u548c\u8f90\u5c04\u540e\u7684\u8367\u5149\u56fe\u50cf\u3002\u5728\u6210\u50cf\u4e4b\u524d\u5c06\u6240\u6709\u6837\u54c1\u4e0eDCFH-DA\u4e00\u8d77\u5b75\u5316\u3002<\/p>\n

\u56fe<\/b><\/strong>5 <\/b><\/strong>\u9aa8\u9ad3DNA\u548c\u6709\u6838\u7ec6\u80de\u68c0\u6d4b<\/b><\/strong>\"\"<\/p>\n

\uff08a\uff09\u66b4\u9732\u4e8e5\u00a0Gy\u8f90\u5c04\u540e\uff0c\u6ce8\u5c04Au-MoS2<\/sub>\u548cCys-MoS2<\/sub>\u7684\u9aa8\u9ad3DNA\u57287\u5929\u540e\u7684\u635f\u4f24\u548c\u6062\u590d\u3002\u901a\u8fc7\u5728268nm\u5904\u7684UV-vis\u5438\u6536\u8fdb\u884c\u6d4b\u91cf\u3002<\/p>\n

\uff08b\uff09\u66b4\u9732\u4e8e5\u00a0Gy\u8f90\u5c04\u540e\uff0c\u6ce8\u5c04Au-MoS2<\/sub>\u548cCys-MoS2<\/sub>\u7684\u5c0f\u9f20\u57287\u5929\u540e\u7684BMNC\u8ba1\u6570\u3002**\u8868\u793aP <0.01\uff0c*\u8868\u793aP\u202f<0.05\u3002<\/p>\n

\u56fe<\/b><\/strong>6<\/b><\/strong>\u00a0<\/b><\/strong>\u809d\u810f\u548c\u80ba\u90e8\u7684SOD\uff0cMDA\u6c34\u5e73<\/b><\/strong>\"\"<\/p>\n

\uff08a\uff0cb\uff09\u66b4\u9732\u4e8e5\u00a0Gy\u8f90\u5c047\u5929\u540e\u809d\u810f\uff08a\uff09\u548c\u80ba\u90e8\uff08b\uff09\u7684SOD\u6c34\u5e73\u3002<\/p>\n

\uff08c\uff0cd\uff09\u66b4\u9732\u4e8e5Gy\u8f90\u5c047\u5929\u540e\u809d\u810f\uff08c\uff09\u548c\u80ba\u90e8\uff08d\uff09\u4e2d\u7684MDA\u6c34\u5e73\u3002*\u8868\u793aP<0.01\u3002<\/p>\n

\u56fe<\/b><\/strong>7<\/b><\/strong>\u00a0<\/b><\/strong>Au-MoS<\/b><\/strong>2<\/b><\/sub><\/strong>\u7684\u4f53\u5185\u6bd2\u6027\u7279\u5f81<\/b><\/strong>\"\"<\/p>\n

\uff08a\uff09\u8179\u8154\u6ce8\u5c04Au-MoS2<\/sub>\u540e\u5c0f\u9f20\u57281\u5929\uff0c7\u5929\u548c30\u5929\u7684\u8840\u6db2\u5206\u6790\u3002\u6307\u6807\u5305\u62ecRBC\uff0cWBC\uff0cHGB\uff0cMCHC \uff0cHCT\uff0c\u5e73\u5747\u7ea2\u7ec6\u80de\u8840\u7ea2\u86cb\u767d\uff08MCH\uff09\u548cPLT\u3002<\/p>\n

\uff08b\uff09\u8179\u8154\u6ce8\u5c04Au-MoS2<\/sub>\u540e\u5c0f\u9f20\u57281\u5929\uff0c7\u5929\u548c30\u5929\u7684ALT\uff0cAST\uff0cTP\uff0cALB\uff0cTBIL\uff0c BUN\uff0cGLOB\u548cA\/G\u7684\u8840\u6db2\u751f\u5316\u5206\u6790\u3002*\u8868\u793a P<0.05\u3002<\/p>\n

\u56fe<\/b><\/strong>8<\/b><\/strong>\u00a0<\/b><\/strong>Au-MoS<\/b><\/strong>2<\/b><\/sub><\/strong>\u7684\u4f53\u5185\u6bd2\u6027<\/b><\/strong>\"\"<\/p>\n

\u4ece\u5bf9\u7167\u5c0f\u9f20\u548c\u6ce8\u5c04Au-MoS2<\/sub>\u540e1\u5929\u548c30\u5929\u7684\u5c0f\u9f20\u7684\u4e3b\u8981\u5668\u5b98\uff08\u5fc3\u810f\uff0c\u809d\u810f\uff0c\u813e\u810f\uff0c\u80ba\u810f\uff0c\u80be\u810f\u548c\u777e\u4e38\uff09\u7684\u75c5\u7406\u5b66\u8bc4\u4ef7\u3002<\/p>\n

\u3010<\/b><\/strong>\u5c0f\u7ed3<\/b><\/strong>\u3011<\/b><\/strong><\/p>\n

\u7efc\u4e0a\u6240\u8ff0\uff0c\u56e2\u961f\u5408\u6210\u4e86\u5177\u6709\u4f18\u5f02\u7535\u50ac\u5316\u6027\u80fd\u7684\u8d85\u5c0f\u578bAu-MoS2<\/sub>\u56e2\u7c07\u3002\u4e0eCys-MoS2<\/sub>\u76f8\u6bd4\uff0cAu-MoS2<\/sub>\u5bf9H2<\/sub>O2<\/sub>\u548cO2<\/sub>\u7684\u8fd8\u539f\u6709\u66f4\u5f3a\u7684\u6fc0\u53d1\u6ce2\u957f\u4f9d\u8d56\u6027\u8367\u5149\u548c\u66f4\u9ad8\u7684\u50ac\u5316\u6d3b\u6027\u3002\u56e0\u6b64\uff0c\u89c2\u5bdf\u5230\u901a\u8fc7Au-NCs\u4fee\u9970\u6539\u5584MoS2<\/sub>\u7684\u7535\u50ac\u5316\u6d3b\u6027\uff0c\u53ef\u4ee5\u6709\u6548\u5730\u589e\u5f3a\u5176\u6297\u6c27\u5316\u6d3b\u6027\u548c\u8f90\u5c04\u9632\u62a4\u6548\u679c\u3002\u7ec6\u80de\u5b9e\u9a8c\u8868\u660e\uff0cAu-MoS2<\/sub>\u53ef\u4ee5\u6539\u5584\u7ec6\u80de\u6d3b\u529b\uff0c\u6e05\u9664\u53d7\u8f90\u5c04\u7ec6\u80de\u4e2d\u7684ROS\uff0c\u9632\u6b62\u7531\u9ad8\u80fd\u91cf\u03b3\u5c04\u7ebf\u8bf1\u5bfc\u7684DNA\u76f8\u5173\u635f\u4f24\u3002\u540c\u65f6\uff0cAu-MoS2<\/sub>\u8fd8\u53ef\u4ee5\u901a\u8fc7\u6e05\u9664\u81ea\u7531\u57fa\u548c\u4fdd\u62a4\u5c0f\u9f20\u7684\u9aa8\u9ad3\u9020\u8840\u7cfb\u7edf\u514d\u53d7\u8f90\u5c04\uff0c\u4ece\u800c\u6062\u590d\u5668\u5b98\u4e2d\u7684SOD\u548cMDA\u6c34\u5e73\u3002\u56e0\u6b64\uff0c\u901a\u8fc7Au-NCs\u6539\u6027\u63d0\u9ad8MoS2<\/sub>\u7eb3\u7c73\u6750\u6599\u7684\u50ac\u5316\u6d3b\u6027\u5177\u6709\u91cd\u8981\u7684\u5b9e\u9645\u610f\u4e49\u3002\u56e0\u6b64\uff0c\u53ef\u4ee5\u5f97\u51fa\u7ed3\u8bba\uff0cAu-MoS2<\/sub>\u662f\u4e00\u79cd\u6709\u524d\u9014\u7684\u8f90\u5c04\u9632\u62a4\u5242\uff0c\u53ef\u7528\u4e8e\u80bf\u7624\u5316\u7597\uff0c\u8bf1\u53d8 \u9884\u9632\uff0c\u6297\u7ec6\u80de\u8f6c\u5316\u548c\u51cf\u5c11\u764c\u53d8\u7b49\u4e34\u5e8a\u5e94\u7528\u3002<\/p>\n

\u00a0<\/b><\/strong>\u6587\u732e\u94fe\u63a5<\/b><\/strong>\uff1a<\/b><\/strong>Enhanced catalysis of ultrasmall Au-MoS<\/u>2<\/sub><\/u>\u00a0clusters against reactive oxygen species for radiation protection<\/u><\/a>\uff08Science Bulletin, 2018, DOI\uff1a10.1016\/j.scib.2018.05.008\uff09<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u5b66\u672f\u7ec4\u6728\u6587\u97ec<\/b><\/strong>\u7ffb\u8bd1\uff0c\u6750\u6599\u725b\u6574\u7406\u7f16\u8f91\u3002<\/p>\n

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