{"id":155274,"date":"2018-10-05T08:00:47","date_gmt":"2018-10-05T00:00:47","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=155274"},"modified":"2018-10-04T20:40:06","modified_gmt":"2018-10-04T12:40:06","slug":"%e5%8a%a0%e6%8b%bf%e5%a4%a7%e6%bb%91%e9%93%81%e5%8d%a2%e5%a4%a7%e5%ad%a6%e9%99%88%e5%bf%a0%e4%bc%9f%e5%9b%a2%e9%98%9fadv-energy-mater-%ef%bc%9a%e8%bd%a8%e9%81%93%e7%9b%b8%e4%ba%92%e4%bd%9c%e7%94%a8","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=155274","title":{"rendered":"\u52a0\u62ff\u5927\u6ed1\u94c1\u5362\u5927\u5b66\u9648\u5fe0\u4f1f\u56e2\u961fAdv. Energy Mater. \uff1a\u8f68\u9053\u76f8\u4e92\u4f5c\u7528\u7684Bi-Sn\u53cc\u91d1\u5c5e\u7535\u50ac\u5316\u5242\u7528\u4e8e\u9ad8\u9009\u62e9\u6027\u7535\u5316\u5b66CO2\u8fd8\u539f\u751f\u4ea7\u7532\u9178\u76d0"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n

\u901a\u8fc7\u7535\u5316\u5b66CO2<\/sub>\u8fd8\u539f\u53cd\u5e94\uff08CO2<\/sub>RR\uff09\u5c06CO2<\/sub>\u6c14\u4f53\u8f6c\u5316\u4e3a\u9644\u52a0\u503c\u5316\u5b66\u54c1\uff0c\u88ab\u8ba4\u4e3a\u662f\u4e00\u79cd\u5177\u6709\u7ecf\u6d4e\u6548\u76ca\u548c\u73af\u5883\u6548\u76ca\u7684CO2<\/sub>\u56de\u6536\u7b56\u7565\u3002\u7136\u800c\uff0cCO2<\/sub>RR\u4e00\u822c\u662f\u56f0\u96be\u7684\uff0c\u56e0\u4e3aCO2<\/sub>\u662f\u70ed\u529b\u5b66\u7a33\u5b9a\u7684\uff0c\u5728\u7535\u8fd8\u539f\u8fc7\u7a0b\u4e2d\u5bfc\u81f4\u53cd\u5e94\u52a8\u529b\u5b66\u975e\u5e38\u8fdf\u7f13\u548c\u5927\u91cf\u6fc0\u6d3b\u8fc7\u7535\u4f4d\u3002\u53e6\u5916\uff0cCO2<\/sub>\u7684\u8f6c\u5316\u4e0e\u5176\u4ed6\u53cd\u5e94\u7ade\u4e89\uff0c\u4f8b\u5982\u6790\u6c22\u53cd\u5e94\uff08HER\uff09\uff0c\u5176\u901a\u5e38\u663e\u7740\u51cf\u5c11\u8fd8\u539f\u78b3\u4ea7\u7269\u7684\u5f62\u6210\u3002\u7531CO2<\/sub>\u8f6c\u5316\u6210\u7532\u9178\u76d0\u4ea7\u54c1\uff0c\u5b83\u662f\u4e00\u79cd\u7a33\u5b9a\u7684\u65e0\u6bd2\u6db2\u4f53\uff0c\u5728\u5305\u62ec\u6c22\u8f7d\u4f53\u7cfb\u7edf\u548c\u7532\u9178\u71c3\u6599\u7535\u6c60\u5728\u5185\u7684\u5404\u79cd\u5e94\u7528\u9886\u57df\u5177\u6709\u5de8\u5927\u7684\u5e02\u573a\u6f5c\u529b\u3002\u7136\u800c\uff0c\u4ecd\u7136\u9700\u8981\u9ad8\u6d3b\u6027\u3001\u9009\u62e9\u6027\u548c\u7a33\u5b9a\u7684\u7535\u50ac\u5316\u5242\u6765\u4fc3\u8fdbCO2<\/sub>RR\uff0c\u4ee5\u514b\u670d\u5de8\u5927\u7684\u80fd\u91cf\u5c4f\u969c\uff0c\u5e76\u5c06\u53cd\u5e94\u8def\u5f84\u8f6c\u5411\u7532\u9178\u76d0\u7684\u5f62\u6210\u3002\u5c31\u50ac\u5316\u5242\u7ec4\u6210\u800c\u8a00\uff0c\u4ee5\u4e8c\u5143\u6216\u591a\u5143\u50ac\u5316\u5242\u7684\u5f62\u5f0f\u7ec4\u5408\u591a\u4e8e\u4e00\u79cd\u5143\u7d20\u5df2\u663e\u793a\u51fa\u662f\u8c03\u8282CO2<\/sub>RR\u50ac\u5316\u5242\u9009\u62e9\u6027\u7684\u6709\u6548\u65b9\u6cd5\u3002\u7406\u89e3\u4e8c\u5143\u7ec4\u5206\u4e4b\u95f4\u7684\u534f\u540c\u76f8\u4e92\u4f5c\u7528\u5bf9\u4e8e\u8bbe\u8ba1\u80fd\u591f\u5728\u9ad8\u6cd5\u62c9\u7b2c\u6548\u7387\u4e0b\u5c06CO2<\/sub>\u8f6c\u5316\u4e3a\u7532\u9178\u76d0\u7684\u50ac\u5316\u5242\u5177\u6709\u91cd\u8981\u610f\u4e49\u3002\u6b64\u5916\uff0c\u63d0\u9ad8CO2<\/sub>RR\u50ac\u5316\u5242\u6d3b\u6027\u548c\u9009\u62e9\u6027\u7684\u5176\u4ed6\u65b9\u6cd5\u8fd8\u5305\u62ec\u50ac\u5316\u5242\u8868\u9762\u7684\u5f62\u8c8c\u5de5\u7a0b\u548c\u6c27\u5316\u6001\u7684\u8c03\u8282\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u5728\u52a0\u62ff\u5927\u6ed1\u94c1\u5362\u5927\u5b66\u9648\u5fe0\u4f1f\u6559\u6388<\/b><\/strong>\u548c\u6cb3\u5357\u5e08\u8303\u5927\u5b66\u767d\u6b63\u5b87\u526f\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/b><\/strong>\u56e2\u961f\u7684\u5e26\u9886\u4e0b\uff0c\u5f00\u53d1\u4e86\u4e00\u79cd\u9ad8\u9009\u62e9\u6027\u548c\u8010\u7528\u7684\u4e8c\u6c27\u5316\u78b3\uff08CO2<\/sub>\uff09\u8f6c\u5316\u4e3a\u7532\u9178\u76d0\u7684\u7535\u50ac\u5316\u5242\uff0c\u7531\u7528\u94cb\uff08Bi\uff09\u7eb3\u7c73\u9897\u7c92\u4fee\u9970\u7684\u9521\uff08Sn\uff09\u7eb3\u7c73\u7247\u7ec4\u6210\u3002\u7531\u4e8e\u5728Sn-Bi\u754c\u9762\u901a\u8fc7\u6709\u5229\u7684\u8f68\u9053\u76f8\u4e92\u4f5c\u7528\u5f62\u6210\u6d3b\u6027\u4f4d\u70b9\uff0cBi-Sn\u53cc\u91d1\u5c5e\u50ac\u5316\u5242\u5c06CO2<\/sub>\u8f6c\u5316\u4e3a\u7532\u9178\u76d0\uff0c\u5728-1.1V\uff08vs.RHE\uff09\u5177\u6709\u975e\u5e38\u9ad8\u7684\u6cd5\u62c9\u7b2c\u6548\u7387\uff0896\uff05\uff09\u548c\u751f\u4ea7\u7387\uff080.74mmol h-1<\/sup>cm-2<\/sup>\uff09\u3002\u6b64\u5916\uff0c\u50ac\u5316\u5242\u8fd0\u884c100\u5c0f\u65f6\u4fdd\u6301\u5176\u521d\u59cb\u6548\u7387\u3002\u5bc6\u5ea6\u6cdb\u51fd\u7406\u8bba\u8868\u660e\uff0cBi\u7eb3\u7c73\u7c92\u5b50\u7684\u52a0\u5165\u4f7fSn\u7684\u7535\u5b50\u6001\u504f\u79bb\u8d39\u7c73\u80fd\u7ea7\uff0c\u4f7f\u5f97HCOO*\u4e2d\u95f4\u4f53\u4e0e\u7eafSn\u8868\u9762\u76f8\u6bd4\u6709\u5229\u5730\u5438\u9644\u5728Bi-Sn\u754c\u9762\u4e0a\u3002\u8fd9\u6709\u6548\u5730\u4fc3\u8fdb\u4e86\u7535\u5b50\u7684\u6d41\u52a8\uff0c\u4fc3\u8fdb\u4e86CO2<\/sub>\u9009\u62e9\u6027\u548c\u6301\u4e45\u5730\u8f6c\u5316\u4e3a\u7532\u9178\u76d0\u3002\u8be5\u7814\u7a76\u63d0\u4f9b\u4e86\u4e9a\u539f\u5b50\u7ea7\u7684\u89c1\u89e3\u548c\u7528\u4e8e\u9ad8\u9009\u62e9\u6027CO2<\/sub>\u7535\u8fd8\u539f\u7684\u53cc\u91d1\u5c5e\u50ac\u5316\u5242\u5f00\u53d1\u548c\u8868\u9762\u5de5\u7a0b\u7684\u4e00\u822c\u65b9\u6cd5\u3002\u76f8\u5173\u6210\u679c\u4ee5\u9898\u4e3a\u201cOrbital Interactions in Bi<\/b><\/strong>–<\/b><\/strong>Sn Bimetallic Electrocatalysts for Highly Selective Electrochemical CO<\/b><\/strong>2<\/b><\/sub><\/strong>\u00a0Reduction toward Formate Production<\/b><\/strong>\u201d\u53d1\u8868\u5728\u4e86Adv. Energy Mater. <\/b><\/strong>\u4e0a\u3002<\/p>\n

\u00a0<\/b><\/strong>\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/b><\/strong><\/p>\n

\u56fe1 <\/b><\/strong>Bi-Sn\/CF\u50ac\u5316\u5242<\/b><\/strong>\u7684\u5fae\u89c2\u7ed3\u6784\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

a\uff09\u5728\u591a\u5b54\u78b3\u7ec7\u7269\u57fa\u5e95\u4e0a\u751f\u957f\u7684Bi-Sn\u50ac\u5316\u5242\u7ed3\u6784\u548c\u901a\u8fc7Bi\u7eb3\u7c73\u9897\u7c92\u6c89\u79ef\u5728Sn\u7eb3\u7c73\u7247\u4e0a\u5f62\u6210\u7684\u6d3b\u6027\u754c\u9762\u7684\u793a\u610f\u56fe\u3002<\/p>\n

b,c\uff09\u5206\u522b\u5728\u539f\u4f4d\u9884\u5904\u7406\u8fd8\u539f\u6b65\u9aa4\u4e4b\u524db\uff09\u548c\u4e4b\u540ec\uff09\u7684Bi-Sn\/CF\u50ac\u5316\u5242\u7684SEM\u56fe\u50cf\u3002<\/p>\n

d\uff09Bi-SnO2<\/sub>\u7eb3\u7c73\u7247\u8868\u9762\u7684STEM\u56fe\u50cf\u3002<\/p>\n

e\uff09Bi\u4fee\u9970SnO2<\/sub>\u7eb3\u7c73\u7247\u7684HRTEM\u56fe\u50cf\u3002<\/p>\n

f\uff09\u65e0Bi\u4fee\u9970SnO2<\/sub>\u7eb3\u7c73\u7247\u7684HRTEM\u56fe\u50cf\u3002<\/p>\n

g\uff09Bi-SnO2<\/sub>\/CF\uff0cBi-Sn\/CF\u548cCF\u7684XRD\u56fe\u6848\u3002<\/p>\n

\u56fe2 <\/b><\/strong>\u4e0d\u540c\u50ac\u5316\u5242\u7684<\/b><\/strong>XPS\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

a\uff09Bi(3)-SnO2<\/sub>\/CF\uff0cBi-SnO2<\/sub>\/CF\uff0cBi(3)-SnO2<\/sub>\/CF\u548cSnO2<\/sub>\/CF\u7684Sn 3d\u6838\u5fc3\u80fd\u7ea7XPS\u5149\u8c31\u3002<\/p>\n

b\uff09Bi(3)-SnO2<\/sub>\/CF\uff0cBi-SnO2<\/sub>\/CF\uff0cBi(3)-SnO2<\/sub>\/CF\u548cSnO2<\/sub>\/CF\u7684Bi 4f\u6838\u5fc3\u80fd\u7ea7XPS\u5149\u8c31\u3002<\/p>\n

\u00a0<\/b><\/strong>\u56fe3<\/b><\/strong>\u00a0\u4e0d\u540c\u50ac\u5316\u5242<\/b><\/strong>\u7684\u7535\u5316\u5b66\u6027\u80fd\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

a\uff09\u5236\u5907\u7684\u7535\u6781\uff08Bi-Sn\/CF\uff0cSn\/CF\u548cCF\uff09\u57280.5 m KHCO3<\/sub>\u7535\u89e3\u8d28\u4e2d\uff0c\u626b\u63cf\u901f\u7387\u4e3a20 mV s -1<\/sup>\u65f6\u7684N2<\/sub>\uff08\u865a\u7ebf\uff09\u548cCO2<\/sub>\u00a0\u5439\u626b\uff08\u5b9e\u7ebf\uff09\u7684CO2<\/sub>RR\u6d3b\u6027\u3002<\/p>\n

b\uff09\u5728-0.64\u81f3-1.34V\u7684\u4e00\u7cfb\u5217\u7535\u4f4d\u4e0b\u5728\u7535\u6781\uff08Bi-Sn\/CF\uff0cSn\/CF\u548cCF\uff09\u4e0a\u4ea7\u751f\u7684\u7532\u9178\u76d0\u7684\u6cd5\u62c9\u7b2c\u6548\u7387\u3002<\/p>\n

c\uff09\u5728\u6c27\u5316\u7269\u884d\u751f\u7684Bi-Sn\/CF\u7535\u6781\u5728-0.64\u81f3-1.34V\u7684\u4e00\u7cfb\u5217\u7535\u4f4d\u4e0b\u7684\u7532\u9178\u76d0\uff0cCO\u548cH2<\/sub>\u7684\u6cd5\u62c9\u7b2c\u6548\u7387\u3002<\/p>\n

d\uff09\u5177\u6709\u4e0d\u540c\u6bd4\u7387\u7684Bi\u548cSn\u7684\u7532\u9178\u76d0\u5728-1.14V\u00a0vs. RHE\u65f6\u7684\u6cd5\u62c9\u7b2c\u6548\u7387\u3002\u8bef\u5dee\u68d2\u8868\u793a\u540c\u4e00\u6837\u54c1\u7684\u4e09\u6b21\u72ec\u7acb\u6d4b\u91cf\u7684\u6807\u51c6\u504f\u5dee\u3002<\/p>\n

\u56fe<\/b><\/strong>4<\/b><\/strong>\u00a0Bi-Sn\/CF\u7535\u6781\u7684\u7a33\u5b9a\u6027<\/b><\/strong>\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\u90e8\u5206\u7535\u6d41\u5bc6\u5ea6\uff08PCD\uff09\u548c\u6cd5\u62c9\u7b2c\u6548\u7387\u5728-1.14V\u00a0vs. RHE\u7684\u5ef6\u957f\u64cd\u4f5c\uff08100h\uff09\u671f\u95f4\u5bf9\u7532\u9178\u76d0\u7684\u7a33\u5b9a\u6027\u3002\u63d2\u56fe\uff1a\u7a33\u5b9a\u6027\u6d4b\u8bd5\u4e4b\u524d\uff08\u5de6\uff09\u548c\u4e4b\u540e\uff08\u53f3\uff09\u7684Bi-SnO2<\/sub>\/CF\u7684SEM\u56fe\u50cf\u3002<\/p>\n

\u56fe<\/b><\/strong>5<\/b><\/strong>\u00a0Sn\uff08101\uff09\u8868\u9762\u548cBi-Sn\uff08101\uff09\u8868\u9762<\/b><\/strong>\u7684<\/b><\/strong>\u53cd\u5e94\u80fd\u91cf\u5206\u5e03<\/b><\/strong>\u56fe<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\u8ba1\u7b97CO2<\/sub>RR\u5728a\uff09Sn\uff08101\uff09\u8868\u9762\u548cb\uff09Bi-Sn\uff08101\uff09\u8868\u9762\u4e0a\u5f62\u6210CO\uff08\u9876\u90e8\uff09\u548cHCOOH\uff08\u5e95\u90e8\uff09\u7684\u53cd\u5e94\u80fd\u91cf\u5206\u5e03\u3002\u6240\u6709\u80fd\u91cf\u90fd\u53c2\u8003\u5438\u9644\u5728Sn\uff08101\uff09\u6216Bi-Sn\uff08101\uff09\u8868\u9762\u4e0a\u7684CO3<\/sub>H\u7684\u80fd\u91cf\u3002<\/p>\n

\u56fe<\/b><\/strong>6<\/b><\/strong>\u00a0Sn\uff08101\uff09\u548cBi-Sn\uff08101\uff09\u8868\u9762\u4e0a\u7684Sn\u539f\u5b50<\/b><\/strong>\u7684<\/b><\/strong>PDOS<\/b><\/strong>\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

a\uff09\u5438\u9644HCOO*\u7684Sn\uff08101\uff09\u548cBi-Sn\uff08101\uff09\u8868\u9762\u4e0a\u7684Sn\u539f\u5b50\u7684s\uff0cp\u548cd\u8f68\u9053\u548cO\u539f\u5b50\u7684p\u8f68\u9053\u7684\u72b6\u6001\u5bc6\u5ea6\uff08PDOS\uff09\u3002<\/p>\n

b,c\uff09\u5728HCOO *\u5438\u9644\u4e4b\u524dSn\uff08101\uff09\u548cBi-Sn\uff08101\uff09\u8868\u9762\u4e0a\u7684Sn\u539f\u5b50\u7684b\uff09p\u8f68\u9053\u548cc\uff09d\u8f68\u9053\u7684PDOS\u3002<\/p>\n

\u3010<\/b><\/strong>\u5c0f\u7ed3<\/b><\/strong>\u3011<\/b><\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5<\/b><\/strong>\uff1a<\/b><\/strong>Orbital Interactions in Bi<\/u>–<\/u>Sn Bimetallic Electrocatalysts for Highly Selective Electrochemical CO<\/u>2<\/sub><\/u>\u00a0Reduction toward Formate Production<\/u><\/a>\uff08Adv. Energy Mater. \u00a0,2018,DOI\uff1a10.1002\/aenm.201802427\uff09<\/p>\n

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