{"id":169275,"date":"2019-03-12T06:30:15","date_gmt":"2019-03-11T22:30:15","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=169275"},"modified":"2019-03-11T14:56:45","modified_gmt":"2019-03-11T06:56:45","slug":"%e6%ad%a6%e6%b1%89%e7%90%86%e5%b7%a5%e5%bc%a0%e9%ab%98%e7%a7%91%e6%95%99%e6%8e%88%e8%af%be%e9%a2%98%e7%bb%84%e5%92%8c%e4%b8%ad%e7%a7%91%e5%a4%a7%e5%ad%99%e6%b0%b8%e7%a6%8f%e6%95%99%e6%8e%88%e5%b8%b8","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=169275","title":{"rendered":"\u6b66\u6c49\u7406\u5de5\u5f20\u9ad8\u79d1\u6559\u6388\u8bfe\u9898\u7ec4\u548c\u4e2d\u79d1\u5927\u5b59\u6c38\u798f\u6559\u6388:\u5e38\u6e29\u3001\u5e38\u538b\u4e0b\u5168\u5149\u8c31\u76f4\u63a5\u5149\u50ac\u5316\u8fd8\u539f\u7a7a\u6c14\u4e2d\u7684CO2"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n

\u5927\u81ea\u7136\u4e2d\u7684\u5149\u5408\u4f5c\u7528\u4e3a\u4eba\u7c7b\u63d0\u4f9b\u4e86\u53d1\u5c55CO2<\/sub>\u6355\u83b7\u4e0e\u518d\u5faa\u73af\u5229\u7528\u6280\u672f\u7684\u7075\u611f\uff0c\u4ee5\u4eba\u5de5\u5149\u5408\u4f5c\u7528\u4e3a\u7814\u7a76\u5bf9\u8c61\uff0c\u79d1\u7814\u5de5\u4f5c\u8005\u5df2\u7ecf\u8bbe\u8ba1\u548c\u5408\u6210\u4e86\u591a\u79cd\u5149\u50ac\u5316\u5242\u7528\u4e8e\u8f6c\u5316CO2<\/sub>\u3002\u4f46\u662f\uff0c\u76ee\u524d\u5149\u50ac\u5316\u8fd8\u539fCO2<\/sub>\u4ecd\u7136\u5b58\u5728\u7740\u4e00\u4e9b\u96be\u70b9\u9700\u8981\u514b\u670d\u3002\u9996\u5148\u5b9e\u9a8c\u901a\u5e38\u9700\u8981\u5728\u65e0\u6c27\u6761\u4ef6\u4e0b\uff0c\u6216\u8005\u9700\u8981\u642d\u5efa\u989d\u5916\u7684CO2<\/sub>\u6355\u83b7\u63d0\u7eaf\u88c5\u7f6e\u3002\u6b64\u5916\uff0c\u7531\u4e8eCO2<\/sub>\u4e2d\u6781\u5f3a\u7684C\uff1dO\u53cc\u952e\u952e\u80fd\uff08750 kJ mol-1\uff09\uff0c\u514b\u670d\u5176\u80fd\u5792\u901a\u5e38\u9700\u8981\u80fd\u91cf\u8f83\u9ad8\u7684\u7d2b\u5916\u548c\u53ef\u89c1\u5149\uff0c\u800c\u5360\u6709\u592a\u9633\u80fd\u91cf\u5927\u591a\u6570\u4e14\u80fd\u91cf\u8f83\u4f4e\u7684\u8fd1\u7ea2\u5916\u5149\u5374\u5f88\u96be\u7528\u4e8e\u5149\u50ac\u5316\u8fd8\u539fCO2<\/sub>\u3002\u540c\u65f6\uff0c\u5149\u50ac\u5316\u8fd8\u539fCO2<\/sub>\u7684\u9009\u62e9\u6027\u53ca\u6700\u7ec8\u4ea7\u54c1\u7684\u7ecf\u6d4e\u6027\uff0c\u4e5f\u4f1a\u9650\u5236CO2<\/sub>\u5149\u50ac\u5316\u8f6c\u6362\u6280\u672f\u7684\u4ea7\u4e1a\u5316\u3002\u4ece\u7ecf\u6d4e\u65b9\u9762\u6765\u8bb2\uff0c\u6295\u8d44\u8005\u66f4\u503e\u5411\u4e8e\u53d1\u5c55\u9009\u62e9\u6027\u8f6c\u5316CO2<\/sub>\u4e3a\u9ad8\u9644\u52a0\u503c\u7684\u7532\u9187\u3001\u7532\u9178\u7b49\u6709\u673a\u5316\u5de5\u539f\u6750\u6599\u7684\u50ac\u5316\u5242\u3002\u663e\u7136\uff0c\u5b9e\u73b0\u6709\u5de5\u4e1a\u5316\u524d\u666f\u7684CO2<\/sub>\u5149\u50ac\u5316\u8f6c\u6362\u6280\u672f\u4ecd\u7136\u9762\u4e34\u7740\u5de8\u5927\u7684\u6311\u6218\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u6b66\u6c49\u7406\u5de5\u5927\u5b66\u5f20\u9ad8\u79d1\u6559\u6388\u53ca\u5176\u8bfe\u9898\u7ec4<\/b><\/strong>\u5434\u6653\u52c7<\/b><\/strong>\u526f\u6559\u6388<\/b><\/strong>\u8bbe\u8ba1\u3001\u5408\u6210\u4e86\u66b4\u9732{010}\u6676\u9762\u7684\u516d\u65b9M0.33<\/sub>WO3<\/sub>(M=K,Rb,Cs)\u7eb3\u7c73\u68d2\uff0c\u9996\u6b21\u53d1\u73b0\u5176\u5177\u6709\u4f18\u5f02\u7684\u7ea2\u5916\u5149\u50ac\u5316\u8f6c\u5316\u7a7a\u6c14\u4e2dCO2<\/sub>\u4e3a\u7532\u9187\u7684\u6027\u80fd\uff0c\u800c\u4e14\u5728\u5168\u6d41\u52a8\u7a7a\u6c14\u76f8\u4e2d\uff0c\u5176\u4ecd\u5448\u73b0\u5f88\u9ad8\u7684\u5149\u50ac\u5316\u8f6c\u5316\u7a7a\u6c14\u4e2dCO2<\/sub>\u4e3a\u7532\u9187\u7684\u6d3b\u6027\u3002\u8bfe\u9898\u7ec4\u5df2\u5728\u00a0J. Am. Chem. Soc.<\/i><\/b><\/em><\/strong>\u4e0a\u5728\u7ebf\u53d1\u8868\u4e86\u9898\u4e3a\u201cPhotocatalytic CO<\/b><\/strong>2<\/b><\/sub><\/strong>\u00a0conversion of M<\/b><\/strong>0.33<\/b><\/sub><\/strong>WO<\/b><\/strong>3<\/b><\/sub><\/strong>\u00a0directly from the air with high selectivity: insight into full spectrum induced reaction mechanism<\/b><\/strong>\u00a0\u201d\u7684\u7814\u7a76\u76f8\u5173\u6210\u679c\u3002\u6587\u7ae0\u7684\u7b2c\u4e00\u4f5c\u8005\u4e3a\u6b66\u6c49\u7406\u5de5\u5927\u5b66\u526f\u6559\u6388\u5434\u6653\u52c7\u548c\u535a\u58eb\u7814\u7a76\u751f\u674e\u6e90\uff0c\u5f20\u9ad8\u79d1\u6559\u6388\u4e3a\u7b2c\u4e00\u901a\u8baf\u4f5c\u8005\uff0c\u6b66\u6c49\u7406\u5de5\u5927\u5b66\u8d75\u7131\u6559\u6388\u548c\u4e2d\u56fd\u79d1\u6280\u5927\u5b66\u7684\u5b59\u6c38\u798f\u6559\u6388\u5206\u522b\u8fdb\u884c\u4e86\u8ba1\u7b97\u548c\u5b9e\u9a8c\u6570\u636e\u6d4b\u8bd5\u5206\u6790\u7b49\u65b9\u9762\u7684\u5408\u4f5c\u7814\u7a76\uff0c\u4f5c\u4e3a\u5171\u540c\u901a\u8baf\u4f5c\u8005\u3002\u4f5c\u8005\u9996\u5148\u91c7\u7528\u6c34\u63a7\u5236\u7f13\u6162\u91ca\u653e\u6cd5\u5236\u5907\u4e86M0.33<\/sub>WO3<\/sub>\u7eb3\u7c73\u68d2\u5149\u50ac\u5316\u5242\u3002\u6c14\u4f53\u5438\u9644\u3001\u8131\u9644\u5b9e\u9a8c\u4e0eCO2<\/sub>\u5438\u9644\u80fd\u8ba1\u7b97\u7ed3\u679c\u8bc1\u5b9e\uff0cM0.33<\/sub>WO3<\/sub>\u4e2d\u7684\u78b1\u91d1\u5c5e\u80fd\u6781\u5927\u5730\u589e\u5f3aCO2<\/sub>\u7684\u9009\u62e9\u6027\u5438\u9644\u80fd\u529b\uff0c\u4f7f\u5f97\u5149\u50ac\u5316\u8f6c\u5316\u7a7a\u6c14\u4e2d\u7684CO2<\/sub>\u5f97\u4ee5\u5b9e\u73b0\u3002\u5176\u6b21X\u5c04\u7ebf\u5149\u7535\u5b50\u80fd\u8c31\u3001\u540c\u6b65\u8f90\u5c04X\u5c04\u7ebf\u5438\u6536\u7cbe\u7ec6\u7ed3\u6784\u8bc1\u660eM0.33<\/sub>WO3<\/sub>\u4e2d\u90e8\u5206\u516d\u4ef7\u94a8\u88ab\u8fd8\u539f\u4e3a\u4e94\u4ef7\u94a8\uff0c\u6210\u4e3aCO2<\/sub>\u6d3b\u5316\u548c\u6c34\u7684\u8d28\u5b50\u5316\u7684\u6d3b\u6027\u4f4d\u70b9\uff0c\u8fd9\u4e00\u70b9\u901a\u8fc7\u539f\u4f4d\u5085\u91cc\u53f6\u53d8\u6362\u7ea2\u5916\u5149\u8c31\u5206\u6790\u548c\u5409\u5e03\u65af\u81ea\u7531\u80fd\u8ba1\u7b97\u5747\u5f97\u5230\u4e86\u8bc1\u5b9e\u3002\u6b64\u5916\uff0c\u4ecb\u7535\u51fd\u6570\u8ba1\u7b97\u548c\u8fd1\u7ea2\u5916\u5149\u50ac\u5316\u8fd8\u539fCO2<\/sub>\u673a\u7406\u7814\u7a76\u8868\u660e\uff0c\u8fd1\u7ea2\u5916\u5149\u8bf1\u5bfc\u7684\u5c0f\u6781\u5b50\u8dc3\u8fc1\u80fd\u591f\u5728\u5149\u50ac\u5316\u5242\u8868\u9762\u751f\u6210\u4e30\u5bcc\u7684\u7535\u5b50\uff0c\u4ee5\u8fd8\u539f\u88ab\u5438\u9644\u5728\u5176\u8868\u9762\u7684CO2<\/sub>\u3002\u8be5\u7814\u7a76\u5de5\u4f5c\u4e3a\u63a2\u7d22\u591a\u529f\u80fd\u6750\u6599\u5728CO2<\/sub>\u8fd8\u539f\u4e0e\u4eba\u5de5\u5149\u5408\u4f5c\u7528\u7b49\u65b9\u9762\u63d0\u4f9b\u4e86\u65b0\u7684\u601d\u8def\u548c\u5960\u5b9a\u4e86\u5b9e\u8df5\u57fa\u7840\uff0c\u5176\u6210\u679c\u6709\u671b\u4f7f\u5f97\u4eba\u5de5\u5149\u5408\u4f5c\u7528\u53d8\u7684\u66f4\u7b80\u5355\u53ef\u884c\u3002<\/p>\n

\u3010\u56fe\u6587\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n

\u56fe1 \u5149\u50ac\u5316\u8fd8\u539fCO<\/b><\/strong>2<\/b><\/sub><\/strong>\u6027\u80fd<\/b><\/strong><\/p>\n

\"\"<\/p>\n

A) \u5bbd\u8c31\u5149\u7167\u5c04\u4e0b\uff0c\u5149\u50ac\u5316\u8fd8\u539f\u7a7a\u6c14\u4e2dCO2<\/sub>\u6027\u80fd\uff1b<\/p>\n

B)\u8fd1\u7ea2\u5916\u5149\uff08800 nm~2500 nm\uff09\u7167\u5c04\u4e0b\uff0c\u5149\u50ac\u5316\u8fd8\u539f\u7a7a\u6c14\u4e2dCO2<\/sub>\u6027\u80fd\uff1b<\/p>\n

C)\u5bbd\u8c31\u5149\u7167\u5c04\u4e0b\uff0cRb0.33<\/sub>WO3<\/sub>\u5149\u50ac\u5316\u8fd8\u539f\u7a7a\u6c14\u4e2dCO2<\/sub>\u7684\u7a33\u5b9a\u6027\uff1b<\/p>\n

D) \u5bbd\u8c31\u5149\u7167\u5c04\u4e0b\uff0cRb0.33<\/sub>WO3<\/sub>\u5728\u5168\u6d41\u52a8\u76f8\u4e0b\u5149\u50ac\u5316\u8fd8\u539f\u7a7a\u6c14\u4e2dCO2<\/sub>\u6027\u80fd\u3002<\/p>\n

\u56fe2 DFT\u8ba1\u7b97\u6a21\u62df\u7684Rb<\/b><\/strong>0.33<\/b><\/sub><\/strong>WO<\/b><\/strong>3<\/b><\/sub><\/strong>\u5149\u50ac\u5316\u8fd8\u539fCO<\/b><\/strong>2<\/b><\/sub><\/strong>\u53cd\u5e94\u6b65\u9aa4\u793a\u610f\u56fe<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\u56fe3 Rb<\/b><\/strong>0.33<\/b><\/sub><\/strong>WO<\/b><\/strong>3<\/b><\/sub><\/strong>\u7684\u5f62\u8c8c\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

A) TEM\u56fe\u50cf\uff1b<\/p>\n

B) HAADF-STEM\u56fe\u50cf\u4ee5\u53ca\u76f8\u5e94\u7684\u5143\u7d20\u5206\u5e03\u56fe\u50cf\uff1b<\/p>\n

C) \u653e\u5927\u7684HRTEM\u56fe\u50cf\uff1b<\/p>\n

D) SEAD\u56fe\u8c31\u3002<\/p>\n

\u56fe4 \u4f7f\u7528N\u63ba\u6742\u77f3\u58a8\u70ef\u4e0a\u5355\u539f\u5b50Sn<\/b><\/strong>\u03b4+<\/b><\/sup><\/strong>\u8fdb\u884cCO<\/b><\/strong>2<\/b><\/sub><\/strong>\u7535\u8fd8\u539f\u7684\u4f18\u52bf<\/b><\/strong><\/p>\n

\"\"<\/p>\n

A) Rb33<\/sub>WO3<\/sub>\u3001W18<\/sub>O49<\/sub>\u7684CO2<\/sub>\u5438\u9644\u7b49\u538b\u7ebf\uff1b<\/p>\n

B) Rb33<\/sub>WO3<\/sub>\u3001W18<\/sub>O49<\/sub>\u7684CO2<\/sub>\u8131\u9644\u7b49\u6e29\u7ebf\uff1b<\/p>\n

C) Rb33<\/sub>WO3<\/sub>\u3001W18<\/sub>O49<\/sub>\u7684O2<\/sub>\u8131\u9644\u7b49\u6e29\u7ebf\uff1b<\/p>\n

D) Rb33<\/sub>WO3<\/sub>{001}\u6676\u9762\u5438\u9644CO2<\/sub>\u6a21\u62df\u793a\u610f\u56fe<\/p>\n

E) Rb33<\/sub>WO3<\/sub>{010}\u6676\u9762\u5438\u9644CO2<\/sub>\u6a21\u62df\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe5 Rb<\/b><\/strong>0.33<\/b><\/sub><\/strong>WO<\/b><\/strong>3<\/b><\/sub><\/strong>\u7684<\/b><\/strong>X<\/b><\/strong>PS<\/b><\/strong>\u3001X<\/b><\/strong>ANE\u8868\u5f81\u4e0e<\/b><\/strong>in situ<\/i><\/b><\/em><\/strong>\u00a0FT-IR\u56fe\u8c31<\/b><\/strong><\/p>\n

\"\"<\/p>\n

A) \u9ad8\u5206\u8fa8W 4f XPS\u5149\u8c31\uff1b<\/p>\n

B) W L3\u8fb9XANES\u5149\u8c31\uff1b<\/p>\n

C) Rb33<\/sub>WO3.165<\/sub>\uff08\u65e0W5+<\/sup>\u7ec4\uff09\u5149\u50ac\u5316\u8fd8\u539fCO2<\/sub>\u7684in situ<\/i><\/em>FT-IR\u5149\u8c31\uff1b<\/p>\n

D) Rb33<\/sub>WO3<\/sub>\uff08\u5bccW5+<\/sup>\u7ec4\uff09\u5149\u50ac\u5316\u8fd8\u539fCO2<\/sub>\u7684in situ<\/i><\/em>FT-IR\u5149\u8c31\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/b><\/strong><\/p>\n

\u7efc\u4e0a\u6240\u8ff0\uff0c\u4f5c\u8005\u8bbe\u8ba1\u4e86\u66b4\u9732{010}\u6676\u9762\u3001\u5bcc\u542b\u8fd8\u539f\u6001W5+<\/sup>\u7684M0.33<\/sub>WO3<\/sub>(M=K,\u00a0Rb,\u00a0Cs)\u7eb3\u7c73\u68d2\uff0c\u53d1\u73b0\u5176\u5177\u6709\u4f18\u5f02\u7684\u7ea2\u5916\u5149\u50ac\u5316\u8f6c\u5316\u7a7a\u6c14\u4e2dCO2<\/sub>\u4e3a\u7532\u9187\u7684\u6027\u80fd\u3002\u901a\u8fc7CO2<\/sub>\u3001O2<\/sub>\u7684\u5438\u9644\u8131\u9644\u5b9e\u9a8c\u548cDFT\u8ba1\u7b97\uff0c\u8bc1\u5b9e\u4e86\u66b4\u9732{010}\u6676\u9762\u7684M0.33<\/sub>WO3<\/sub>\u5149\u50ac\u5316\u5242\u4e2d\u7684\u78b1\u91d1\u5c5e\u5bf9\u7a7a\u6c14\u4e2d\u7684CO2<\/sub>\u6709\u9009\u62e9\u6027\u5438\u9644\uff0c\u5e76\u4e14\u8fd9\u79cd\u9009\u62e9\u6027\u5438\u9644\u80fd\u529b\u968f\u7740\u78b1\u91d1\u5c5e\u79bb\u5b50\u534a\u5f84\u7684\u589e\u5927\u800c\u589e\u5f3a\u3002DFT\u8ba1\u7b97\u548cin situ <\/i><\/em>FT-IR\u7ed3\u679c\u8868\u660e\uff0c\u5728\u5149\u50ac\u5316\u8f6c\u5316CO2<\/sub>\u53cd\u5e94\u4e2d\uff0cM0.33<\/sub>WO3<\/sub>\u6837\u54c1\u4e2d\u7684W5+<\/sup>\u4f4d\u70b9\u5728\u6d3b\u5316CO2<\/sub>\u5206\u5b50\u7684\u540c\u65f6\uff0c\u4e5f\u6d3b\u5316\u4e86\u6c34\u5206\u5b50\u3002\u5149\u50ac\u5316\u5242\u4e2d\u7684\u78b1\u91d1\u5c5e\u4e0eW5+<\/sup>\u534f\u540c\u4f5c\u7528\uff0c\u589e\u5f3a\u4e86\u5176\u5bbd\u8c31\u5149\u9a71\u52a8\u7684\u5149\u50ac\u5316\u8f6c\u5316CO2<\/sub>\u7684\u6d3b\u6027\u3002\u5e76\u901a\u8fc7\u4ecb\u7535\u51fd\u6570\u8ba1\u7b97\u548c\u5149\u50ac\u5316\u6761\u4ef6\u5b9e\u9a8c\u7684\u7ed3\u679c\uff0c\u63a2\u7d22\u4e86\u8fd1\u7ea2\u5916\u5149\u8bf1\u5bfc\u7684\u5149\u50ac\u5316\u8fd8\u539fCO2<\/sub>\u673a\u7406\uff0c\u7ed3\u679c\u8bc1\u5b9e\u8fd1\u7ea2\u5916\u5149\u8bf1\u5bfc\u7684\u5c0f\u6781\u5b50\u8dc3\u8fc1\u53ef\u4ee5\u5728\u5149\u50ac\u5316\u5242\u8868\u9762\u751f\u6210\u81ea\u7531\u7535\u5b50\uff0c\u4ee5\u8fd8\u539f\u88ab\u5438\u9644\u5728\u5176\u8868\u9762\u7684CO2<\/sub>\uff0c\u5b9e\u73b0\u4e86\u4f18\u5f02\u7684\u7ea2\u5916\u5149\u50ac\u5316\u8f6c\u5316\u7a7a\u6c14\u4e2dCO2<\/sub>\u4e3a\u7532\u9187\u7684\u6027\u80fd\uff0c\u540c\u65f6\uff0c\u8be5\u5149\u50ac\u5316\u6750\u6599\u5728\u5bbd\u8c31\u5149\u7167\u5c04\u4e0b\u7684\u5168\u6d41\u52a8\u76f8\u4e2d\u4ecd\u7136\u5448\u73b0\u5f88\u9ad8\u7684\u5149\u50ac\u5316\u8f6c\u5316\u7a7a\u6c14\u4e2dCO2<\/sub>\u4e3a\u7532\u9187\u7684\u6d3b\u6027\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1aPhotocatalytic CO<\/b><\/strong>2<\/b><\/sub><\/strong>\u00a0Conversion of M<\/b><\/strong>0.33<\/b><\/sub><\/strong>WO<\/b><\/strong>3<\/b><\/sub><\/strong>\u00a0Directly from the Air with High Selectivity: Insight into Full Spectrum Induced Reaction Mechanism<\/b><\/strong>\u00a0(J. Am. Chem. Soc.<\/b><\/strong>, 2019, DOI: 10.1021\/jacs.8b12928)<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u6b66\u6c49\u7406\u5de5\u5927\u5b66\u5f20\u9ad8\u79d1\u6559\u6388\u8bfe\u9898\u7ec4<\/b><\/strong>\u4f9b\u7a3f\uff0c<\/b><\/strong>\u6750\u6599\u4eba\u7f16\u8f91\u90e8Alisa\u7f16\u8f91\u3002<\/p>\n

\u6b22\u8fce\u5927\u5bb6\u5230\u6750\u6599\u4eba\u5ba3\u4f20\u79d1\u6280\u6210\u679c\u5e76\u5bf9\u6587\u732e\u8fdb\u884c\u6df1\u5165\u89e3\u8bfb\uff0c\u6295\u7a3f\u90ae\u7bb1: tougao@cailiaoren.com.<\/p>\n

\u6295\u7a3f\u4ee5\u53ca\u5185\u5bb9\u5408\u4f5c\u53ef\u52a0\u7f16\u8f91\u5fae\u4fe1\uff1acailiaorenVIP.<\/p>\n

\u00a0<\/b><\/strong><\/p>\n","protected":false},"excerpt":{"rendered":"

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