{"id":170829,"date":"2019-03-27T11:44:46","date_gmt":"2019-03-27T03:44:46","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=170829"},"modified":"2019-03-26T22:45:00","modified_gmt":"2019-03-26T14:45:00","slug":"%e9%99%88%e5%bf%a0%e4%bc%9fadv-energy-mater-%e7%bc%ba%e9%99%b7%e5%92%8c%e5%bd%a2%e8%b2%8c%e8%b0%83%e6%8e%a7%e7%ad%96%e7%95%a5%e5%8d%8f%e5%90%8c%e5%a2%9e%e5%bc%ba%e9%94%82%e7%a1%ab%e7%94%b5","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=170829","title":{"rendered":"\u9648\u5fe0\u4f1fAdv. Energy Mater. : \u7f3a\u9677\u548c\u5f62\u8c8c\u8c03\u63a7\u7b56\u7565\u534f\u540c\u589e\u5f3a\u9502\u786b\u7535\u6c60\u6027\u80fd"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\n \u9502-\u786b(Li-S)\u7535\u6c60\u56e0\u5176\u4e2d\u95f4\u4f53\u591a\u786b\u5316\u9502(LPS)\u7684\u6eb6\u89e3\u548c\u7a7f\u68ad\u884c\u4e3a\u4ee5\u53ca\u5faa\u73af\u8fc7\u7a0b\u4e2d\u4f53\u79ef\u81a8\u80c0\u6548\u5e94\u4e25\u91cd\u9650\u5236\u4e86\u5176\u5546\u4e1a\u5316\u7684\u5e94\u7528\u3002Co3<\/sub>O4<\/sub>\u7531\u4e8e\u5176\u8f83\u9ad8\u7684\u7535\u5316\u5b66\u7a33\u5b9a\u6027\u4ee5\u53ca\u8f83\u5f3a\u7684LPS\u5438\u9644\u6548\u679c\u5728\u4f5c\u4e3a\u786b\u5bbf\u4e3b\u6750\u6599\u65f6\u5177\u6709\u5e7f\u6cdb\u7684\u5e94\u7528\u524d\u666f\u3002\u7136\u800c\uff0cCo3<\/sub>O4<\/sub>\u9897\u7c92\u56e0\u5176\u76f8\u5bf9\u8f83\u5dee\u7684\u7535\u5b50\u3001\u79bb\u5b50\u4f20\u8f93\u80fd\u529b\u4ee5\u53ca\u4f4e\u50ac\u5316\u6d3b\u6027\u6781\u5927\u5730\u963b\u788d\u4e86\u5176\u8fdb\u4e00\u6b65\u5e94\u7528\u3002\u7f3a\u9677\u5de5\u7a0b\u548c\u5f62\u8c8c\u8c03\u63a7\u7684\u5f15\u5165\u662f\u6539\u5584\u4e0a\u8ff0\u95ee\u9898\u7684\u6709\u6548\u7b56\u7565\u3002\u79bb\u5b50\u7f3a\u9677\u80fd\u591f\u8c03\u63a7\u7535\u5b50\u7ed3\u6784\uff0c\u4ece\u800c\u6539\u5584\u7535\u5b50\u4f20\u8f93\u80fd\u529b\uff0c\u6b64\u5916\u5f62\u6210\u7684\u7f3a\u4f4d\u5177\u6709\u5f88\u5f3a\u7684LPS\u5438\u9644\u80fd\u529b\u5e76\u63d0\u9ad8\u50ac\u5316\u6d3b\u6027\u3002\u53e6\u5916\uff0c\u5f62\u8c8c\u8c03\u63a7\u53ef\u901a\u8fc7\u7f29\u77edLPS\u6269\u6563\u9014\u5f84\u4ee5\u53ca\u63d0\u4f9b\u826f\u597d\u7684\u79bb\u5b50\/\u7535\u5b50\u4f20\u5bfc\u80fd\u529b\u5bf9\u786b\u7684\u6c27\u5316\u8fd8\u539f\u52a8\u529b\u5b66\u884c\u4e3a\u4ea7\u751f\u91cd\u8981\u5f71\u54cd\u3002\u7136\u800c\uff0c\u6709\u5173\u7f3a\u9677\u548c\u5f62\u8c8c\u8c03\u63a7\u6765\u534f\u540c\u6539\u5584\u9502\u786b\u7535\u6c60\u7684\u7535\u5316\u5b66\u884c\u4e3a\u7684\u7814\u7a76\u5be5\u5be5\u65e0\u51e0\uff0c\u56e0\u6b64\u5168\u9762\u4e86\u89e3\u5f62\u8c8c\u8c03\u63a7\u548c\u7f3a\u9677\u5de5\u7a0b\u7684\u534f\u540c\u4f5c\u7528\u5c06\u6709\u52a9\u4e8e\u8bbe\u8ba1\u9ad8\u6027\u80fdLi-S\u7535\u6c60\u4e2d\u7684\u591a\u529f\u80fd\u786b\u5bbf\u4e3b\u6750\u6599\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\n \u8fd1\u65e5\uff0c\u52a0\u62ff\u5927\u6ed1\u94c1\u5362\u5927\u5b66\u9648\u5fe0\u4f1f\u6559\u6388(\u901a\u8baf\u4f5c\u8005)\u7b49<\/strong>\u5229\u7528\u7f3a\u9677\u5de5\u7a0b\u548c\u5f62\u8c8c\u8c03\u63a7\u7684\u534f\u540c\u7b56\u7565\u8bbe\u8ba1\u4e86\u9ad8\u5ea6\u65e0\u5e8f\u7684\u5c16\u6676\u77f3NiCo2<\/sub>O4-x<\/sub>\u7f3a\u9677\u6c27\u5316\u7269\u53cc\u58f3\u5fae\u7403(NCO-HS)\uff0c\u5176\u53ef\u4f5c\u4e3a\u591a\u529f\u80fd\u7684\u786b\u5bbf\u4e3b\u6750\u6599\uff0c\u5e76\u5728Adv. Energy Mater.<\/strong>\u4e0a\u53d1\u8868\u4e86\u9898\u4e3a\u201cSynergistic Engineering of Defects and Architecture in Binary Metal Chalcogenide toward Fast and Reliable Lithium\u2013Sulfur Batteries<\/strong>\u201d\u7684\u7814\u7a76\u8bba\u6587\uff0c\u6587\u7ae0\u7684\u7b2c\u4e00\u4f5c\u8005\u4e3a\u7f57\u4e39\u535a\u58eb\u548c\u674e\u9ad8\u7136\u535a\u58eb\u3002\u539f\u4f4d\u5f15\u5165\u7684\u954d\u79bb\u5b50\u63ba\u6742\u548c\u4ea7\u751f\u7684\u6c27\u7f3a\u9677\u8d4b\u4e88\u4e86NCO-HS\u663e\u8457\u589e\u5f3a\u7684\u7535\u5b50\u4f20\u5bfc\u6027\u548c\u4f18\u5f02\u7684\u591a\u786b\u5316\u7269\u5438\u9644\u6027\u3002\u540c\u65f6\uff0c\u7cbe\u7ec6\u7684\u7eb3\u7c73\u7ed3\u6784\u63d0\u4f9b\u4e86\u4e30\u5bcc\u7684\u6d3b\u6027\u754c\u9762\u548c\u66f4\u77ed\u7684\u79bb\u5b50\u6269\u6563\u8def\u5f84\u4ee5\u5b9e\u73b0\u9ad8\u6548\u7684\u786b\u7684\u7535\u5316\u5b66\u884c\u4e3a\u3002\u57fa\u4e8e\u7f3a\u9677\u548c\u5f62\u8c8c\u8c03\u63a7\u7684\u534f\u540c\u6548\u5e94\uff0c\u786b\u590d\u5408\u7535\u6781\u5728\u9ad8\u8fbe5 C\u65f6\u5177\u6709\u4f18\u5f02\u7684\u500d\u7387\u6027\u80fd\uff0c\u5728800\u6b21\u5faa\u73af\u540e\u5177\u6709\u826f\u597d\u7684\u7a33\u5b9a\u6027\uff0c\u5e76\u4e14\u5728\u9ad8\u786b\u8d1f\u8f7d\u91cf\u4e0b\u4ecd\u5177\u67096.3 mAh\u00b7cm-2<\/sup>\u7684\u9762\u79ef\u5bb9\u91cf\u3002\u5229\u7528\u534f\u540c\u6548\u5e94\u8bbe\u8ba1\u9ad8\u5bfc\u7535\u6027\u548c\u5438\u9644\u6027\u591a\u529f\u80fd\u786b\u4e3b\u4f53\u4e3a\u5b9e\u73b0\u4f18\u5f02\u7684Li-S\u7535\u6c60\u6027\u80fd\u63d0\u4f9b\u4e86\u4fdd\u969c\uff0c\u4e5f\u4e3a\u5176\u4ed6\u7535\u5316\u5b66\u9886\u57df\u7684\u5e94\u7528 (\u4f8b\u5982\u7535\u50ac\u5316\u548c\u8d85\u7ea7\u7535\u5bb9\u5668) \u4e2d\u7f3a\u9677\u8bbe\u8ba1\u4e0e\u5f62\u8c8c\u8c03\u63a7\u7684\u534f\u540c\u4f5c\u7528\u7684\u7814\u7a76\u94fa\u5e73\u4e86\u9053\u8def\u3002<\/p>\n

\u3010\u56fe\u6587\u7b80\u4ecb\u3011<\/strong>
\n \u56fe1 NCO-HS\u7684\u5408\u6210<\/strong><\/p>\n

\"\"<\/p>\n

NCO-HS\u5408\u6210\u8fc7\u7a0b\u4e2d\u5f62\u8c8c\u53d8\u5316\u7684\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe2 NCO-HS\u7684\u5f62\u8c8c\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

A) CMF\u7684SEM\u56fe\u50cf\uff1b
\n B,C) NCO-HS\u7684SEM\u56fe\u50cf\uff1b
\n D) NCO-HS\u7684SHIM\u56fe\u50cf\uff1b
\n E) NCO-HS\u7684HRTEM\u56fe\u50cf\uff1b
\n F) NCO-HS\u7684FFT\u56fe\u50cf\uff1b
\n G) NCO-HS\u7684STEM\u56fe\u50cf
\n H-J) NCO-HS\u7684\u5143\u7d20\u5206\u5e03\u56fe\u50cf\u3002<\/p>\n

\u56fe3 NCO-HS\u7684\u7ed3\u6784\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

A) NCO-HS\u548cCo3<\/sub>O4<\/sub>-HS\u7684XRD\u56fe\u8c31\uff0c\u5185\u63d2\u4e3a(220)\u548c(311)\u9762\u7684\u5c40\u90e8\u653e\u5927\uff1b
\n B) NCO-HS\u7684\u9ad8\u5206\u8fa8Ni 2p\u548cCo 2p XPS\u5149\u8c31\uff1b
\n C) NCO-HS\u7684\u9ad8\u5206\u8fa8O 1s XPS\u5149\u8c31\uff1b
\n D) NCO-HS\u548cCo3<\/sub>O4<\/sub>-HS\u7684O K\u8fb9\u548cCo L2,3\u8fb9\u7684ELNES\u5149\u8c31\uff1b
\n E) NCO-HS\u548cCo3<\/sub>O4<\/sub>-HS\u7684EPR\u56fe\u8c31\uff1b
\n F) NCO-HS\u4e0a\u7f3a\u9677\u90e8\u4f4d\u7684TEM\u56fe\u50cf\u3002<\/p>\n

\u56fe4 NCO-HS\u7684LPS\u5438\u9644\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

A) Co3<\/sub>O4<\/sub>-NPs\u3001Co3<\/sub>O4<\/sub>-HS\u548cNCO-HS\u5438\u9644LPS\u6eb6\u6db2\u540e\u7684\u7d2b\u5916-\u53ef\u89c1\u5149\u8c31\u548c\u5149\u5b66\u56fe\u50cf\uff1b
\n B) \u4e0d\u540c\u5438\u9644\u5242\u7684\u591a\u786b\u5316\u7269\u5438\u9644\u80fd\u529b\uff1b
\n C) \u539f\u59cbLi2<\/sub>S6<\/sub>\u3001Co3<\/sub>O4<\/sub>-HS\/LPS\u548cNCO-HS\/LPS\u7684S 2p XPS\u5149\u8c31\u3002<\/p>\n

\u56fe5 NCO-HS\u7684\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

A) S@NCO-HS\u3001S@Co3<\/sub>O4<\/sub>-HS\u548cS@Co3<\/sub>O4<\/sub>-NPs\u7535\u6781\u57280.2 C\u65f6\u7684\u6052\u7535\u6d41\u5145-\u653e\u7535\u66f2\u7ebf\uff1b
\n B) \u626b\u901f\u4e3a0.1mV\u00b7s-1<\/sup>\u65f6\uff0cS@NCO-HS\u3001S@Co3<\/sub>O4<\/sub>-HS\u548cS@Co3<\/sub>O4<\/sub>-NPs\u7535\u6781\u7684CV\u66f2\u7ebf\uff1b
\n C) S@NCO-HS\u3001S@Co3<\/sub>O4<\/sub>-HS\u548cS@Co3<\/sub>O4<\/sub>-NPs\u7535\u6781\u7684\u500d\u7387\u6027\u80fd\uff1b
\n D) S@NCO-HS\u3001S@Co3<\/sub>O4<\/sub>-HS\u548cS@Co3<\/sub>O4<\/sub>-NPs\u7535\u6781\u57280.2 C\u7684\u5faa\u73af\u6027\u80fd\uff1b
\n E) \u57280.2 C\u7684\u957f\u671f\u5faa\u73af\u4e2d\uff0cS@NCO-HS\u7535\u6781\u7684\u6bd4\u5bb9\u91cf\u548c\u5e93\u4ed1\u6548\u7387\u3002<\/p>\n

\u56fe6 NCO-HS\u7684\u7535\u5b50\u548c\u79bb\u5b50\u4f20\u8f93<\/strong><\/p>\n

\"\"<\/p>\n

A) S@NCO-HS\u7684Li+<\/sup>\u6269\u6563\u793a\u610f\u56fe\uff1b
\n B) S@NCO-HS\u3001S@Co3<\/sub>O4<\/sub>-HS\u548cS@Co3<\/sub>O4<\/sub>-NPs\u7535\u6781\u7684PITT\u66f2\u7ebf\uff0c\u663e\u793a\u51fa\u5145-\u653e\u7535\u8fc7\u7a0b\u4e2d\u4e0a\u8ff0\u7535\u6781\u7684Li+<\/sup>\u6269\u6563\u7cfb\u6570\uff1b
\n C) NCO-HS\u3001Co3<\/sub>O4<\/sub>-HS\u548cCo3<\/sub>O4<\/sub>-NPs\u53ca\u5176\u786b\u590d\u5408\u7269\u7684\u7535\u5bfc\u7387\uff1b
\n D) S@NCO-HS\u3001S@Co3<\/sub>O4<\/sub>-HS\u548cS@Co3<\/sub>O4<\/sub>-NPs\u7535\u6781\u7684EIS\u56fe\u8c31\u3002<\/p>\n

\u56fe7 NCO-HS\u7684\u5b9e\u9645\u5e94\u7528\u63a2\u7d22<\/strong><\/p>\n

\"\"<\/p>\n

A) \u786b\u8d1f\u8f7d\u91cf\u4e3a5.5 mg\u00b7cm-2<\/sup>\u7684S@NCO-HS\u7535\u6781\u5728\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u5145-\u653e\u7535\u66f2\u7ebf\uff1b
\n B) \u786b\u8d1f\u8f7d\u91cf\u4e3a5.5 mg\u00b7cm-2<\/sup>\u7684S@NCO-HS\u7535\u6781\u7684\u901f\u7387\u6027\u80fd\uff1b
\n C) \u57280.2 C\u7535\u6d41\u4e0b\uff0cS@NCO-HS\u7535\u6781\u7684\u5faa\u73af\u6027\u80fd\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\n \u7efc\u4e0a\u6240\u8ff0\uff0c\u4f5c\u8005\u5229\u7528\u4e00\u79cd\u7b80\u4fbf\u7684\u534f\u540c\u7b56\u7565\u5408\u6210\u4e86\u5177\u6709\u4e30\u5bcc\u79bb\u5b50\u7f3a\u9677\u7684NCO-HS\u3002\u6240\u5f97NCO-HS\u5177\u6709\u72ec\u7279\u7684\u53cc\u58f3\u4e2d\u7a7a\u7ed3\u6784\u548c\u591a\u7ea7\u5b54\u5206\u5e03\uff0c\u6709\u5229\u4e8e\u5747\u5300\u7684\u786b\u5206\u5e03\u3001\u5feb\u901f\u7684\u79bb\u5b50\u8f6c\u79fb\u548c\u826f\u597d\u7684\u7269\u7406\u56fa\u786b\u4f5c\u7528\u3002\u7f3a\u9677\u5c16\u6676\u77f3NCO-HS\u5728Co3<\/sub>O4<\/sub>-HS\u57fa\u5e95\u4e2d\u5177\u6709\u4e30\u5bcc\u7684Ni2+\u53d6\u4ee3\uff0c\u540c\u65f6Ni2+<\/sup>\u5728\u66ff\u6362\u516b\u9762\u4f53\u4f4d\u70b9\u7684Co3+<\/sup>\u540e\u4ea7\u751f\u4e86\u5927\u91cf\u7684\u6c27\u7a7a\u4f4d\uff0c\u4f7f\u5f97NCO-HS\u7684\u79bb\u5b50\/\u7535\u5b50\u4f20\u5bfc\u6027\u4ee5\u53ca\u4e0e\u786b\u7684\u5316\u5b66\u76f8\u4e92\u4f5c\u7528\u663e\u8457\u589e\u5f3a\uff0c\u6709\u52a9\u4e8e\u63d0\u9ad8Li-S\u7684\u52a8\u529b\u5b66\u884c\u4e3a\u3002\u5f97\u76ca\u4e8e\u4e0a\u8ff0\u4f18\u52bf\uff0cS@NCO-HS\u5b9e\u73b0\u4e86\u5728800\u6b21\u5faa\u73af\u4e2d\u6bcf\u54680.045%\u7684\u6700\u4f4e\u5bb9\u91cf\u8870\u51cf\u7387\uff0c\u5e76\u5177\u6709\u9ad8\u8fbe5 C\u7684\u4f18\u5f02\u7684\u500d\u7387\u6027\u80fd\u548c6.3 mAh\u00b7cm-2<\/sup>\u7684\u9ad8\u9762\u79ef\u5bb9\u91cf\u3002<\/p>\n

\u3010\u901a\u8baf\u4f5c\u8005\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u9648\u5fe0\u4f1f<\/strong>\uff0c\u52a0\u62ff\u5927\u6ed1\u94c1\u5362\u5927\u5b66<\/span>(University of Waterloo)\u5316\u5b66\u5de5\u7a0b\u7cfb\u6559\u6388\uff0c\u52a0\u62ff\u5927\u56fd\u5bb6\u9996\u5e2d\u79d1\u5b66\u5bb6<\/span>(CRC-Tier 1),\u00a0\u56fd\u9645\u7535\u5316\u5b66\u80fd\u6e90\u79d1\u5b66\u9662\u526f\u4e3b\u5e2d\uff0c\u52a0\u62ff\u5927\u5de5\u7a0b\u9662\u9662\u58eb\uff0c\u52a0\u62ff\u5927\u7687\u5bb6\u79d1\u5b66\u9662\u9752\u5e74\u9662\u58eb\u3002\u9648\u5fe0\u4f1f\u9662\u58eb\u5e26\u9886\u4e00\u652f\u7ea6<\/span>70\u4eba\u7684\u7814\u7a76\u56e2\u961f\u5e38\u5e74\u81f4\u529b\u4e8e\u71c3\u6599\u7535\u6c60\uff0c\u91d1\u5c5e\u7a7a\u6c14\u7535\u6c60\uff0c\u9502\u79bb\u5b50\u7535\u6c60\uff0c\u9502\u786b\u7535\u6c60\uff0c\u9502\u7845\u7535\u6c60\uff0c\u6db2\u6d41\u7535\u6c60\u7b49\u50a8\u80fd\u5668\u4ef6\u7684\u7814\u53d1\u548c\u4ea7\u4e1a\u5316\u3002\u8fd1\u5e74\u6765\u5df2\u5728<\/span>Nature Energy, Nature Nanotechnology, Nature Communication, Angewandte Chemie International Edition, Advanced Materials, Energy & Environmental Science, ACS Nano\u7b49\u56fd\u9645\u9876\u7ea7\u671f\u520a\u53d1\u8868\u8bba\u6587<\/span>240\u4f59\u7bc7\u3002\u76ee\u524d\u4e3a\u6b62\uff0c\u6587\u7ae0\u5df2\u5f15\u7528\u6b21\u6570\u8fbe<\/span>19000\u4f59\u6b21<\/span>, H-index\u00a0\u6307\u6570\u4e3a<\/span>69\uff0c\u5e76\u62c5\u4efb<\/span>ACS Applied & Material Interfaces\u526f\u4e3b\u7f16\u3002<\/span><\/p>\n

\u6587\u732e\u94fe\u63a5\uff1aSynergistic Engineering of Defects and Architecture in Binary Metal Chalcogenide toward Fast and Reliable Lithium\u2013Sulfur Batteries<\/a> <\/strong>(Adv. Energy Mater.<\/strong>, 2019, DOI: 10.1002\/aenm.201900228)<\/p>\n

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