{"id":173365,"date":"2019-04-23T11:48:24","date_gmt":"2019-04-23T03:48:24","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=173365"},"modified":"2019-04-23T10:48:37","modified_gmt":"2019-04-23T02:48:37","slug":"%e5%8d%97%e4%ba%ac%e5%b8%88%e5%a4%a7-%e5%88%98%e7%8a%87%e5%9b%a2%e9%98%9f-nano-lett-%e4%b8%8d%e5%af%b9%e7%a7%b0%e5%a4%9a%e9%87%91%e5%b1%9e%e4%bb%8b%e5%ad%94%e7%ba%b3%e7%b1%b3%e5%be%ae%e7%90%83","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=173365","title":{"rendered":"\u5357\u4eac\u5e08\u5927 \u5218\u7287\u56e2\u961f Nano Lett.: \u4e0d\u5bf9\u79f0\u591a\u91d1\u5c5e\u4ecb\u5b54\u7eb3\u7c73\u5fae\u7403\u7684\u53ef\u63a7\u5236\u5907\u548c\u7535\u50ac\u5316\u5e94\u7528"},"content":{"rendered":"

\u3010\u80cc\u666f\u4ecb\u7ecd\u3011<\/strong><\/p>\n

\u00a0 \u00a0 \u00a0 \u00a0 \u4f17\u6240\u5468\u77e5\uff0c\u5177\u6709\u5404\u5411\u5f02\u6027\u7684\u4e0d\u5bf9\u79f0\u8d35\u91d1\u5c5e\u7eb3\u7c73\u6676\u4f53\u662f\u4e00\u7c7b\u7528\u9014\u5e7f\u6cdb\u7684\u529f\u80fd\u6750\u6599\u3002\u5728\u4f17\u591a\u4e0d\u5bf9\u79f0\u7684\u7eb3\u7c73\u7ed3\u6784\u4e2d\uff0c\u7897\u72b6\u7eb3\u7c73\u5fae\u7403\u72b6\u7ed3\u6784\u5728\u7535\u50ac\u5316\u3001\u80fd\u6e90\u5b58\u50a8\u3001\u751f\u7269\u6280\u672f\u65b9\u9762\u6709\u7740\u5e7f\u6cdb\u6f5c\u5728\u7684\u5e94\u7528\u524d\u666f\u3002\u56e0\u6b64\uff0c\u901a\u8fc7\u5408\u7406\u7684\u8bbe\u8ba1\uff0c\u5728\u7897\u72b6\u7eb3\u7c73\u5fae\u7403\u4e2d\u6784\u5efa\u5206\u7ea7\u7ed3\u6784\u5c06\u8fdb\u4e00\u6b65\u63d0\u9ad8\u5176\u7535\u5316\u5b66\u8868\u9762\u79ef\u6d3b\u6027\uff0c\u4fc3\u8fdb\u7535\u5b50\u548c\u8d28\u91cf\u4f20\u9012\uff0c\u5e76\u6709\u52a9\u4e8e\u9664\u53bb\u6709\u6bd2\u7684\u50ac\u5316\u53cd\u5e94\u4e2d\u95f4\u4f53\uff0c\u4ece\u800c\u63d0\u9ad8\u76f8\u5e94\u7684\u50ac\u5316\u6027\u80fd\u3002\u5173\u4e8e\u5177\u6709\u6b64\u7c7b\u7ed3\u6784\u7279\u70b9\u7684\u65e0\u5b9a\u5f62SiO2\u548c\u78b3\u57fa\u6750\u6599\u7684\u6210\u529f\u5408\u6210\uff0c\u5df2\u8bc1\u660e\u4e86\u8fd9\u79cd\u4e0d\u5bf9\u79f0\u7897\u72b6\u4ecb\u5b54\u7eb3\u7c73\u5fae\u7403\uff08BMSs\uff09\u5728\u7535\u50ac\u5316\u3001\u6709\u673a\u50ac\u5316\u3001\u80fd\u91cf\u50a8\u5b58\u3001\u836f\u7269\u9012\u9001\u7b49\u65b9\u9762\u7684\u6027\u80fd\u5f80\u5f80\u4f18\u4e8e\u5bf9\u79f0\u7684\u4ecb\u5b54\u7eb3\u7c73\u5fae\u7403\u3002\u7136\u800c\uff0c\u76ee\u524d\u5df2\u62a5\u9053\u7684\u5408\u6210\u65b9\u6cd5\u8fd8\u6ca1\u6709\u6210\u529f\u5236\u5907\u51fa\u8d35\u91d1\u5c5e\u57fa\u7684BMSs\uff0c\u66f4\u4e0d\u7528\u8bf4\u4e0d\u5bf9\u79f0\u7684\u8d35\u91d1\u5c5e\u57fa\u7684BMSs\u3002\u5357\u4eac\u5e08\u8303\u5927\u5b66\u7684\u5218\u7287\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09\u56e2\u961f\u5f00\u53d1\u4e86\u4e00\u79cd\u5236\u5907\u4e0d\u5bf9\u79f0\u8d35\u91d1\u5c5eBMSs\u7684\u7b80\u4fbf\u5408\u6210\u65b9\u6cd5\uff0c\u6df1\u5165\u7814\u7a76\u4e86\u4e0d\u5bf9\u79f0\u4ecb\u5b54\u7ed3\u6784\u5bf9\u7535\u5316\u5b66\u50ac\u5316\u6027\u80fd\u7684\u5f71\u54cd\uff0c\u62d3\u5c55\u4e86\u8d35\u91d1\u5c5e\u7eb3\u7c73\u6750\u6599\u7684\u5408\u6210\u548c\u5e94\u7528\u9886\u57df\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u00a0 \u00a0 \u00a0 \u00a0 \u5728\u8be5\u56e2\u961f\u524d\u671f\u5173\u4e8e\u8868\u9762\u6d3b\u6027\u5242\u6a21\u677f\u5408\u6210\u4ecb\u5b54\u8d35\u91d1\u5c5e\u5408\u91d1\u7684\u7814\u7a76\u57fa\u7840\u4e0a\uff08ACS Cent. Sci. 2018<\/strong>, 4 1412; Chem. Sci. 2019<\/strong>, 10, 1986; Green Chem. 2019<\/strong>, 21, 2043\uff09\uff0c\u672c\u7814\u7a76\u62a5\u9053\u4e86\u4e00\u79cd\u7b80\u5355\u7684\u81ea\u4e0b\u800c\u4e0a\u7b56\u7565\u5e76\u6210\u529f\u5236\u5907\u51fa\u5f62\u8c8c\u5747\u4e00\u3001\u7c92\u5f84\u5c0f\u4e8e100 nm\u7684\u591a\u91d1\u5c5e\u4e0d\u5bf9\u79f0\u7897\u72b6\u4ecb\u5b54\u7eb3\u7c73\u7403\uff08BMSs\uff09\u3002\u8be5\u5408\u6210\u65b9\u6cd5\u662f\u5229\u7528\u8868\u9762\u6d3b\u6027\u5242\uff08\u53cc\u5341\u516b\u70f7\u57fa\u6c2f\u5316\u94f5\uff09\u7684\u53cc\u6a21\u677f\u4f5c\u7528\uff0c\u5e76\u63a7\u5236\u56ca\u6ce1\u8868\u9762\u4e0a\u91d1\u5c5e\u524d\u9a71\u4f53\u7684\u8fd8\u539f\u52a8\u529b\u5b66\uff0c\u5728\u56ca\u6ce1\u8868\u9762\u5f62\u6210\u4ecb\u5b54\u91d1\u5c5e\u5c9b\uff0c\u6700\u7ec8\u4e0d\u65ad\u751f\u957f\u5f62\u6210\u4e0d\u5bf9\u79f0\u7684\u4ecb\u5b54BMSs\u3002\u901a\u8fc7\u8fdb\u4e00\u6b65\u8c03\u63a7\u5408\u6210\u53c2\u6570\uff0c\u6210\u529f\u5b9e\u73b0\u4e86\u4e0d\u5bf9\u79f0\u7ed3\u6784\u7684\u6709\u6548\u63a7\u5236\uff0c\u5236\u5907\u51fa\u4e0d\u5bf9\u5bf9\u79f0\u6027\u7684BMSs\uff1b\u5e76\u5b9e\u73b0\u5bf9\u6750\u6599\u7ec4\u5206\u7684\u6709\u6548\u63a7\u5236\uff0c\u5408\u6210\u51fa\u591a\u79cd\u4e0d\u540c\u91d1\u5c5e\u7ec4\u6210\u7684BMSs\u3002\u7531\u4e8eBMSs\u5177\u6709\u7684\u72ec\u7279\u7684\u7ed3\u6784\u548c\u7ec4\u5206\u4f18\u52bf\uff0c\u5176\u5728\u7535\u50ac\u5316\u6c27\u5316\u53cd\u5e94\u4e2d\u8868\u65b0\u51fa\u6781\u597d\u7684\u7535\u50ac\u5316\u6027\u80fd\u3002\u8be5\u7814\u7a76\u4e3a\u5408\u7406\u8bbe\u8ba1\u5e76\u5408\u6210\u5177\u6709\u5206\u7ea7\u7684\u4e0d\u5bf9\u79f0\u7eb3\u7c73\u7ed3\u6784\u63d0\u4f9b\u4e86\u5168\u65b0\u7684\u601d\u8def\u548c\u542f\u53d1\u3002\u7814\u7a76\u6210\u679c\u4ee5\u9898\u4e3a\u201cAsymmetric Multimetallic Mesoporous Nanospheres<\/strong>\u201d\u53d1\u8868\u5728\u56fd\u9645\u77e5\u540d\u671f\u520aNano Letters<\/strong>\u4e0a\u3002\u5357\u4eac\u5e08\u8303\u5927\u5b66\u5316\u5b66\u4e0e\u6750\u6599\u79d1\u5b66\u5b66\u9662\u7814\u7a76\u751f\u5415\u6d69\u548c\u526f\u6559\u6388\u8bb8\u51ac\u51ac\u4e3a\u8bba\u6587\u5171\u540c\u7b2c\u4e00\u4f5c\u8005\u3002<\/strong><\/p>\n

\"\"<\/p>\n

\u3010\u56fe\u6587\u89e3\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00\u3001\u901a\u8fc7\u5404\u5411\u5f02\u6027\u7684\u5c9b\u72b6\u751f\u957f\u8fc7\u7a0b\u6784\u5efa\u5177\u6709\u53ef\u63a7\u4e0d\u5bf9\u79f0\u7ed3\u6784\u7684BMSs<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe\u4e8c\u3001 \u4e09\u91d1\u5c5ePdAgCu\u4e0d\u5bf9\u79f0BMS-4\/8\u7684\u7ed3\u6784\u8868\u5f81<\/strong>
\n \"\"\uff08a\uff09\u4f4e\u500d\u7387TEM\u56fe\uff1b<\/p>\n

\uff08b, c\uff09\u9ad8\u500d\u7387TEM\u56fe\uff1b<\/p>\n

\uff08d\uff09\u9ad8\u5206\u8fa8\u7387TEM\u56fe\u50cf\u548c\u76f8\u5e94\u7684SAED\uff08\u63d2\u56fe\uff09\uff1b<\/p>\n

\uff08e\uff09HAADF-STEM\u56fe\u50cf\uff1b<\/p>\n

\uff08f\uff09\u76f8\u5e94\u7684\u5143\u7d20\u5206\u5e03\uff1b<\/p>\n

\uff08g\uff09\u4e0d\u540c\u89d2\u5ea6\u7684TEM\u56fe\u50cf\u548c\u76f8\u5e94\u7684\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe\u4e09\u3001\u5177\u6709\u4e0d\u540c\u4e0d\u5bf9\u79f0\u7684PdAgCu BMSs\u7684\u53ef\u63a7\u5408\u6210<\/strong>
\n \"\"\uff08a\uff09 \u5728DODAC\u6d53\u5ea6\u4e3a0.1 mg\/mL\u6761\u4ef6\u4e0b\u5408\u6210\u7684\u5bf9\u79f0\u7684HMSs\u7684TEM\u56fe\u50cf\u53ca\u5176\u7ed3\u6784\u793a\u610f\u56fe\uff1bDODAC\u6d53\u5ea6\u4e3a\uff08b\uff09 0.6\u3001\uff08c\uff090.9\u3001\uff08d\uff09 1.2\u3001\uff08e\uff09 1.5\u3001\uff08f\uff09 2.0\u3001\uff08g\uff09 2.5\u3001\uff08h\uff09 3.0 mg\/mL\u5f97\u5230\u7684\u4e0d\u540c\u4e0d\u5bf9\u79f0\u6027\u7684BMSs\u3002<\/p>\n

\u56fe\u56db\u3001\u5408\u6210\u65b9\u6cd5\u7684\u666e\u9002\u6027<\/strong>
\n \"\"\uff08a, c, e, g\uff09TEM\u56fe\u50cf\uff1b
\n \uff08b, d, f, h\uff09HAADF-STEM\u56fe\u50cf\u548c\u76f8\u5e94\u7684\u5143\u7d20\u5206\u5e03\uff0c\u5176\u4e2d\uff08a, b\uff09\u53cc\u91d1\u5c5ePdAg BMSs\u3001\uff08c, d\uff09\u4e09\u91d1\u5c5ePdPtAg BMSs\uff0c\uff08e\uff0cf\uff09\u56db\u91d1\u5c5ePdPtAgCu BMSs\u4ee5\u53ca\uff08g, h\uff09\u56db\u91d1\u5c5ePdAgCuFe BMSs\u3002<\/p>\n

\u56fe\u4e94\u3001\u4e0d\u5bf9\u79f0PdAgCu BMSs\u7684\u7535\u50ac\u5316\u6027\u80fd<\/strong>
\n \"\"\uff08a\uff09\u57281.0 M KOH\u4e2d\u6536\u96c6\u7684PdAgCu BMSs\u3001HMSs\u548cMSs\u4ee5\u53caPdAg BMSs\u548cPdB\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

\uff08b\uff09PdAgCu BMSs\u548cMSs\u4e0ePdAg BMSs\u7684CO\u5438\u8131\u9644\u66f2\u7ebf\uff1b<\/p>\n

\uff08c\uff09\u57281.0 M KOH\u548c1.0 M\u4e59\u9187\u4e2d\u5f97\u5230\u7684PdAgCu BMSs\u3001HMSs\u548cMSs\u4ee5\u53caPdAg BMSs\u548cPdB\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

\uff08d\uff09\u57281.0 M KOH\u548c1.0 M\u4e59\u9187\u4e2d\u5f97\u5230\u7684PdAgCu BMSs\u3001HMSs\u548cMSs\u4ee5\u53caPdAg BMSs\u548cPdB\u7684\u603b\u7684\u8d28\u91cf\u6d3b\u6027\uff1b<\/p>\n

\uff08e\uff09\u57281.0 M KOH\u548c1.0 M\u4e59\u9187\u4e2d\u5f97\u5230\u7684PdAgCu BMSs\u3001HMSs\u548cMSs\u4ee5\u53caPdAg BMSs\u548cPdB\u7684\u8d77\u59cb\u7535\u4f4d\u548cIf<\/sub><\/em>\/Ib<\/sub><\/em>\u503c\uff1b<\/p>\n

\uff08f\uff09PdAgCu BMSs\u3001HMSs\u548cMSs\u4ee5\u53caPdAg BMSs\u548cPdB\u5728\u7532\u9187\u3001\u4e19\u4e09\u9187\u548c\u7532\u9178\u7684\u7535\u89e3\u6c27\u5316\u4e2d\u7684\u8d28\u91cf\u6d3b\u6027\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u7efc\u4e0a\u6240\u8ff0\uff0c\u4f5c\u8005\u5229\u7528\u7279\u5b9a\u8868\u9762\u6d3b\u6027\u5242\u7684\u53cc\u6a21\u677f\u6548\u5e94\uff0c\u5e76\u5408\u7406\u8c03\u63a7\u91d1\u5c5e\u524d\u9a71\u4f53\u7684\u8fd8\u539f\u52a8\u529b\u5b66\uff0c\u9996\u6b21\u6210\u529f\u5408\u6210\u4e86\u5355\u5206\u6563\u3001\u9ad8\u5ea6\u5747\u5300\u7684\u5c0f\u4e8e100 nm\u7684\u591a\u91d1\u5c5e\u4e0d\u5bf9\u79f0BMSs\u3002\u4e09\u91d1\u5c5eBMSs\u7684\u7ed3\u6784\u4e0d\u5bf9\u79f0\u6027\u53ef\u4ee5\u901a\u8fc7\u53cd\u5e94\u6761\u4ef6\u7cbe\u786e\u5f97\u4ee5\u63a7\u5236\uff0c\u5b9e\u73b07\/8\u52301\/8\u7684BMSs\u7eb3\u7c73\u5fae\u7403\u7684\u5236\u5907\u3002\u540c\u65f6\uff0c\u4e0d\u5bf9\u79f0BMSs\u5177\u6709\u826f\u597d\u7684\u4ecb\u5b54\u7ed3\u6784\u548c\u53ef\u8c03\u7684\u5143\u7d20\u7ec4\u6210\u3002\u4f5c\u8005\u901a\u8fc7\u201c\u4e00\u9505\u6cd5\u201d\u5728\u5ba4\u6e29\u4e0b\u5feb\u901f\u5236\u5907\u591a\u91d1\u5c5e\u4e0d\u5bf9\u79f0BMSs\uff0c\u5e76\u4e14\u53ef\u4ee5\u5b9e\u73b0\u514b\u7ea7\u7684\u5236\u5907\u3002\u6b64\u5916\uff0c\u5747\u5300\u7684BMSs\u5177\u6709\u826f\u597d\u7684\u7ed3\u6784\u548c\u7ec4\u5206\u4f18\u52bf\uff0c\u53ef\u534f\u540c\u589e\u5f3a\u50ac\u5316\u52a8\u529b\u5b66\u3002PdAgCu BMSs\u5bf9\u6bd4\u5546\u7528PdB\u50ac\u5316\u5242\u8868\u73b0\u51fa\u975e\u5e38\u9ad8\u7684AOR\u6027\u80fd\u3002\u76f8\u4fe1\u8fd9\u79cd\u591a\u91d1\u5c5e\u4e0d\u5bf9\u79f0BMSs\u7684\u53d1\u73b0\u53ef\u4ee5\u4fc3\u8fdb\u66f4\u590d\u6742\u7684\u4e0d\u5bf9\u79f0\u7eb3\u7c73\u7ed3\u6784\u7684\u53d1\u5c55\uff0c\u4fc3\u8fdb\u6b64\u7c7b\u7eb3\u7c73\u7ed3\u6784\u5728\u80fd\u6e90\u76f8\u5173\u9886\u57df\u7684\u6df1\u5165\u5e7f\u6cdb\u5e94\u7528\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1aAsymmetric Multimetallic Mesoporous Nanospheres<\/a><\/strong>\u00a0\uff08Nano Lett., 2019<\/strong>, DOI: 10.1021\/acs.nanolett.9b01223\uff09<\/p>\n

\u901a\u8baf\u4f5c\u8005\u7b80\u4ecb<\/strong><\/p>\n

\u5218\u7287\u535a\u58eb\uff0c2017\u5e74\u53d7\u8058\u6c5f\u82cf\u7279\u8058\u6559\u6388\u52a0\u5165\u5357\u4eac\u5e08\u8303\u5927\u5b66\uff0c\u4e3b\u8981\u4ece\u4e8b\u7eb3\u7c73\u5408\u6210\u548c\u50ac\u5316\u76f8\u5173\u7814\u7a76<\/strong>\u3002\u8fd1\u5e74\u6765\uff0c\u5218\u7287\u56e2\u961f\u53d1\u5c55\u4e86\u4e00\u79cd\u8868\u9762\u6d3b\u6027\u5242\u6a21\u677f\u5bfc\u5411\u5408\u6210\u65b9\u6cd5\uff0c\u5b9e\u73b0\u4e86\u591a\u79cd\u591a\u7ef4\u5ea6\u8d35\u91d1\u5c5e\u5408\u91d1\u50ac\u5316\u5242\u7684\u7406\u6027\u5408\u6210\uff0c\u76f8\u5173\u7ed3\u679c\u53d1\u8868\u5728ACS Cent. Sci.\u3001Nano Lett.\u3001Chem. Sci.\u7b49\u671f\u520a<\/strong>\uff1b<\/p>\n

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