{"id":176476,"date":"2019-05-30T06:30:38","date_gmt":"2019-05-29T22:30:38","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=176476"},"modified":"2019-05-29T18:42:11","modified_gmt":"2019-05-29T10:42:11","slug":"%e3%80%90%e6%a0%a1%e7%a8%bf%e6%9c%aa%e5%9b%9e%e5%a4%8d%e3%80%91%e5%8d%8e%e4%b8%9c%e7%90%86%e5%b7%a5%e5%a4%a7%e5%ad%a6%e5%8d%97%e6%98%8c%e5%a4%a7%e5%ad%a6esm%e5%85%b7%e6%9c%89mof%e8%a1%8d","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=176476","title":{"rendered":"\u534e\u4e1c\u7406\u5de5\u5927\u5b66&\u5357\u660c\u5927\u5b66ESM:\u5177\u6709MOF\u884d\u751f\u7684\u591a\u5b54Co3O4-NC\u7eb3\u7c73\u7247\u9635\u5217\u7684\u78b3\u5e03\u4f5c\u4e3a\u65e0\u679d\u6676\u9502\u91d1\u5c5e\u8d1f\u6781\u7684\u4e3b\u4f53"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n

\u9502\u91d1\u5c5e\u7531\u4e8e\u5177\u6709\u6781\u9ad8\u7684\u7406\u8bba\u6bd4\u5bb9\u91cf\u548c\u6700\u4f4e\u7684\u7535\u6781\u7535\u52bf\u88ab\u8ba4\u4e3a\u662f\u6700\u6709\u524d\u666f\u7684\u8d1f\u6781\u6750\u6599\u3002\u7136\u800c\uff0cLi\u91d1\u5c5e\u8d1f\u6781\u7684\u5b9e\u9645\u5e94\u7528\u4ecd\u9762\u4e34\u7740\u4e00\u4e9b\u6311\u6218\uff0c\u4e3b\u8981\u5305\u62ecLi\u679d\u6676\u7684\u4e0d\u65ad\u751f\u957f\uff0c\u4e0d\u7a33\u5b9a\u7684SEI\u754c\u9762\u4ee5\u53ca\u5145\u653e\u7535\u5faa\u73af\u671f\u95f4\u7684\u5de8\u5927\u7684\u4f53\u79ef\u53d8\u5316\u3002\u8fd9\u4e9b\u56fa\u6709\u7684\u7f3a\u70b9\u5c06\u4f1a\u5bfc\u81f4Li\u91d1\u5c5e\u7535\u6c60\u7684\u653e\u7535\u5bb9\u91cf\u4f4e\uff0c\u5faa\u73af\u5bff\u547d\u77ed\u548c\u5b89\u5168\u6027\u95ee\u9898\u3002\u9488\u5bf9\u4ee5\u4e0a\u8fd9\u4e9b\u95ee\u9898\uff0c\u5df2\u7ecf\u63d0\u51fa\u4e86\u8bb8\u591a\u7b56\u7565\uff0c\u4f8b\u5982\u5229\u5f00\u53d1\u7535\u89e3\u6db2\u6dfb\u52a0\u5242\u6765\u7a33\u5b9aSEI\u548c\u8bbe\u8ba1\u4eba\u5de5\u754c\u9762\u5c42\u7b49\u3002\u7136\u800c\uff0c\u8fd9\u4e9b\u4e0a\u8ff0\u7b56\u7565\u672a\u80fd\u4ece\u6839\u672c\u4e0a\u514b\u670d\u5145\u653e\u7535\u671f\u95f4\u9502\u7684\u4f53\u79ef\u53d8\u5316\u548cSEI\u4e0d\u7a33\u5b9a\u7684\u95ee\u9898\u3002\u4f7f\u75283D\u96c6\u6d41\u4f53\u4f5c\u4e3a\u9502\u91d1\u5c5e\u7684\u5bbf\u4e3b\u53ef\u80fd\u662f\u5b9e\u73b0\u9ad8\u5bb9\u91cf\u548c\u957f\u5faa\u73afLi\u91d1\u5c5e\u8d1f\u6781\u975e\u5e38\u6709\u6548\u7684\u65b9\u6cd5\u3002\u78b3\u57fa\u4e3b\u4f53\u7531\u4e8e\u8d28\u91cf\u8f7b\uff0c\u6bd4\u8868\u9762\u79ef\u5927\uff0c\u5bfc\u7535\u6027\u597d\uff0c\u5316\u5b66\u7a33\u5b9a\u548c\u4f18\u5f02\u7684\u673a\u68b0\u5f3a\u5ea6\u7b49\u7279\u6027\u53d7\u5230\u4e86\u5e7f\u6cdb\u7684\u7814\u7a76\u5173\u6ce8\u3002\u4e3a\u4e86\u907f\u514d\u5728\u9502\u9884\u5b58\u50a8\u8fc7\u7a0b\u4e2d\u5f15\u5165\u4e0d\u5e0c\u671b\u7684SEI\u6216\u7535\u89e3\u6db2\u6742\u8d28\uff0c\u6700\u8fd1\u5f00\u53d1\u4e86\u7194\u878d\u6ce8\u5165\u65b9\u6cd5\u4f5c\u4e3a\u5c06\u91d1\u5c5e\u9502\u4e0e\u78b3\u4e3b\u4f53\u7ed3\u5408\u7684\u65b0\u6280\u672f\u3002\u7136\u800c\uff0c\u7531\u4e8eLi\u7684\u4eb2\u548c\u6027\u5dee\uff0c\u5927\u591a\u6570\u78b3\u4e3b\u4f53\u4e0d\u80fd\u88ab\u7194\u878d\u7684Li\u5145\u5206\u6d78\u6da6\u3002<\/p>\n

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\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/b><\/strong><\/p>\n

\u56fe\u4e00<\/b><\/strong>CFC\/Co-NC @ Li<\/b><\/strong>\u8d1f\u6781\u7684\u5236\u5907\u6d41\u7a0b\u56fe\u53ca\u5176\u5f62\u8c8c\u8868\u5f81\"\"<\/b><\/strong><\/p>\n

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\uff08h\uff09CFC\/Co3<\/sub>O4<\/sub>-NC\u7684SEM\u5143\u7d20\u6620\u5c04\u56fe\u50cf\u3002<\/p>\n

\u56fe\u4e8c<\/b><\/strong>CFC\/Co<\/b><\/strong>3<\/b><\/sub><\/strong>O<\/b><\/strong>4<\/b><\/sub><\/strong>-NC<\/b><\/strong>\u7684\u6210\u5206\u8868\u5f81<\/b><\/strong><\/p>\n

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\"\"<\/p>\n

\uff08a\uff09CFC\uff0cCFC\/Co3<\/sub>O4<\/sub>-NC\u548cCFC\/Co3O4-NC @ Li\u7684XRD\u56fe\u3002<\/p>\n

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\u56fe\u4e09<\/b><\/strong>CFC\/Co<\/b><\/strong>3<\/b><\/sub><\/strong>O<\/b><\/strong>4<\/b><\/sub><\/strong>-NC<\/b><\/strong>\u7684\u7194\u878d\u9502\u8fc7\u7a0b<\/b><\/strong><\/p>\n

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\uff08a\uff09CFC\/Co3<\/sub>O4<\/sub>-NC\u7194\u878dLi\u8fc7\u7a0b\u7684\u5149\u5b66\u7167\u7247\u3002<\/p>\n

\uff08b\uff09\u7194\u878dLi\u70ed\u704c\u6ce8\u8fc7\u7a0b\u7684\u793a\u610f\u56fe\u3002<\/p>\n

\uff08c\uff09CFC\/Co-NC @ Li\u590d\u5408\u6750\u6599\u7684SEM\u56fe\u50cf\u3002<\/p>\n

\uff08d-e\uff09\u901a\u8fc7\u6d78\u5165\u4e59\u9187\u6eb6\u6db2\u4e2d\u9664\u53bbLi\u91d1\u5c5e\u540e\u7684CFC\/Co-NC @ Li\u7684SEM\u56fe\u50cf\u3002<\/p>\n

\u56fe\u56db<\/b><\/strong>CFC\/Co-NC @ Li\u590d\u5408\u7535\u6781\u7684\u9502\u6c89\u79ef\/\u5265\u79bb\u5f62\u8c8c\u6f14\u53d8<\/b><\/strong><\/p>\n

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\u56fe<\/b><\/strong>\u4e94\u5bf9\u79f0\u7535\u6c60\u7684\u7535\u5316\u5b66\u6027\u80fd<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff0cc\uff09\u9502\u7247\u548cCFC\/Co-NC @ Li\u5728\u7ebd\u6263\u5bf9\u79f0\u7535\u6c60\u4e2d\u7684\u6052\u6d41\u5145\u653e\u7535\u7535\u538b\u548c\u65f6\u95f4\u66f2\u7ebf\uff0c\u7535\u6d41\u5bc6\u5ea6\u4e3a(a)1 mA cm-2<\/sup>\uff0c(b)3 mA cm-2<\/sup>\u548c(c)5 mA cm-2<\/sup>\u3002<\/p>\n

\uff08d\uff09\u9502\u7247\u548cCFC\/Co-NC @ Li\u5728\u7ebd\u6263\u5bf9\u79f0\u7535\u6c60\u4e2d\u7684\u6052\u6d41\u5145\u653e\u7535\u7535\u538b\u548c\u65f6\u95f4\u66f2\u7ebf<\/p>\n

\u7535\u6d41\u5bc6\u5ea6\u4e3a5 mA cm-2<\/sup>\uff0c\u6c89\u79ef\/\u5265\u79bb\u91cf\u4e3a10 mAh cm-2<\/sup>\u3002<\/p>\n

\u56fe<\/b><\/strong>\u516d<\/b><\/strong>CFC\/Co-NC @ Li\u7684\u53cd\u5e94\u52a8\u529b\u5b66<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\u00a0<\/b><\/strong>\uff08a\uff0cb\uff09\u5faa\u73af\u4e4b\u524d\u548c\u5faa\u73af10\u5708\u4e4b\u540e\u9502\u7247\u548cCFC\/Co-NC @ Li\u5bf9\u79f0\u7535\u6c60\u7684EIS\u56fe\u3002<\/p>\n

\uff08c\uff09CFC\/Co3<\/sub>O4<\/sub>-NC\u4e0eCu\u7b94\u4e0a\u6c89\u79ef\u7684\u5e93\u4ed1\u6548\u7387\u3002<\/p>\n

\uff08d\uff09\u9502\u7247\u548cCFC\/Co-NC @ Li\u7535\u6781\u4e0e\u7535\u89e3\u6db2\u7684\u6da6\u6e7f\u89d2\u6d4b\u8bd5\u3002<\/p>\n

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\"\"<\/p>\n

\uff08a\uff091C\u7684\u7535\u6d41\u5bc6\u5ea6\u4e0bCF\/Co-NC @ Li | LFP\u548cLi | LFP\u7535\u6c60\u7684\u5145\u653e\u7535\u66f2\u7ebf\u3002<\/p>\n

\uff08b\uff09CFC\/Co-NC @ Li | LFP\u548cLi | LFP\u7535\u6c60\u7684\u5faa\u73af\u6027\u80fd\u3002<\/p>\n

\uff08c\uff0cd\uff09CFC\/Co-NC @ Li | S\u548cLi | S\u7535\u6c60\u7684\u5faa\u73af\u6027\u80fd\u548c\u500d\u7387\u6027\u80fd\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/b><\/strong><\/p>\n

\u603b\u4e4b\uff0c\u672c\u6587\u6784\u5efa\u4e86\u4e00\u79cd\u5728\u78b3\u5e03\u7531MOF\u884d\u751f\u7684Co3<\/sub>O4<\/sub>\u5d4c\u5165\u548c\u6c2e\u63ba\u6742\u7684\u591a\u5b54\u78b3\u7eb3\u7c73\u7247\u9635(CFC\/Co3<\/sub>O4<\/sub>-NC)\u4f5c\u4e3a\u7194\u878d\u9502\u7684\u4e3b\u4f53\uff0c\u7528\u4e8e\u65e0\u679d\u6676\u7684Li\u91d1\u5c5e\u9633\u6781\u3002\u7531\u4e8e\u5d4c\u5165\u7684Co3<\/sub>O4<\/sub>\u4e0e\u7194\u878dLi\u7684\u5316\u5b66\u53cd\u5e94\u6027\uff0c\u6c2e\u63ba\u6742\u5242\u7684\u4eb2\u55dc\u6027\u548c\u591a\u5b54\u7ed3\u6784\u7684\u6bdb\u7ec6\u7ba1\u529b\uff0c<\/p>\n

\u591a\u5b54Co3<\/sub>O4<\/sub>-NC\u7eb3\u7c73\u7247\u9635\u5217\u53ef\u4ee5\u6539\u5584CFC\u7684Li\u6d78\u6da6\u884c\u4e3a\uff0c\u786e\u4fdd\u7194\u878dLi\u7684\u5feb\u901f\u6ce8\u5165\u3002CFC\/Co3<\/sub>O4<\/sub>-NC\u7684\u7eb3\u7c73\u8584\u7247\u9635\u5217\u6846\u67b6\u5728\u7194\u878d\u9502\u671f\u95f4\u5f97\u5230\u4e86\u5f88\u597d\u7684\u4fdd\u6301\uff0c\u8fd8\u52a0\u5feb\u4e86Li\u5728\u6c89\u79ef\/\u5265\u79bb\u8fc7\u7a0b\u4e2d\u7684\u7535\u5b50\u548c\u79bb\u5b50\u4f20\u8f93\u3002\u5177\u6709\u9ad8\u6bd4\u8868\u9762\u79ef\u548c\u673a\u68b0\u5f3a\u5ea6\u7684CFC\/Co3<\/sub>O4<\/sub>-NC\u4e3b\u4f53\u53ef\u4ee5\u964d\u4f4e\u5c40\u90e8\u7535\u6d41\u5bc6\u5ea6\u548c\u7f13\u51b2\u4f53\u79ef\u53d8\u5316\uff0c\u4ece\u800c\u5728\u5faa\u73af\u671f\u95f4\u6291\u5236Li\u679d\u6676\u7684\u751f\u957f\u3002\u56e0\u6b64\uff0cCFC\/Co-NC @ Li\u590d\u5408\u8d1f\u6781\u5177\u6709\u4f18\u5f02\u7684\u7535\u5316\u5b66\u6027\u80fd\uff0c\u8fc7\u7535\u4f4d\u4f4e\uff08\u57281 mA cm-2<\/sup>\u4e0b<18 mV\uff09\uff0c\u5faa\u73af\u5bff\u547d\u9ad8\u8fbe1000 h\u548c\u9ad8\u5e93\u4ed1\u6548\u7387\uff08100\u6b21\u5faa\u73af\u540e\u4e3a98.4\uff05\uff09\u3002\u5f53\u4e0eLiFePO4\u6216\u786b\u6b63\u6781\u914d\u5bf9\u65f6\uff0cCFC\/Co-NC @ Li\u7535\u6781\u8868\u73b0\u51fa\u9ad8\u6bd4\u5bb9\u91cf\uff0c\u5faa\u73af\u7a33\u5b9a\u6027\u548c\u500d\u7387\u6027\u80fd\u3002\u8be5\u7814\u7a76\u4e3a\u5b9e\u73b0\u9ad8\u5faa\u73af\u7a33\u5b9a\u6027\u548c\u5b89\u9ad8\u5168\u6027\u7684Li\u91d1\u5c5e\u8d1f\u6781\u5f00\u8f9f\u4e86\u4e00\u6761\u65b0\u9014\u5f84\uff0c\u5e76\u4e3a\u5176\u4ed6MOFs\u6750\u6599\u5e94\u7528\u4e8e\u9ad8\u6027\u80fd\u78b1\u91d1\u5c5e\u8d1f\u6781\u63d0\u4f9b\u4e86\u53c2\u8003\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/b><\/strong>\u201c<\/b><\/strong>MOF-derived porous Co<\/b><\/strong>3<\/b><\/sub><\/strong>O<\/b><\/strong>4<\/b><\/sub><\/strong>-NC nanoflake arrays on carbon fiber cloth as stable hosts for dendrite-free Li metal anodes<\/b><\/strong><\/a><\/b>\u201d<\/b><\/strong><\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u5fae\u89c2\u4e16\u754c\u7f16\u8bd1\u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u6574\u7406\u7f16\u8f91\u3002<\/p>\n

\u6b22\u8fce\u5927\u5bb6\u5230\u6750\u6599\u4eba\u5ba3\u4f20\u79d1\u6280\u6210\u679c\u5e76\u5bf9\u6587\u732e\u8fdb\u884c\u6df1\u5165\u89e3\u8bfb\uff0c\u6295\u7a3f\u90ae\u7bb1tougao@cailiaoren.com\u3002<\/p>\n

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