{"id":179369,"date":"2019-07-05T06:30:20","date_gmt":"2019-07-04T22:30:20","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=179369"},"modified":"2019-07-04T10:08:00","modified_gmt":"2019-07-04T02:08:00","slug":"%e6%b8%85%e5%8d%8e%e5%a4%a7%e5%ad%a6esm%e7%94%a8%e4%ba%8e%e9%ab%98%e6%80%a7%e8%83%bd%e9%94%82%e7%a6%bb%e5%ad%90%e7%94%b5%e6%b1%a0%e8%b4%9f%e6%9e%81%e7%9a%84%e8%9b%8b%e7%8a%b6%e7%bb%93%e6%9e%84","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=179369","title":{"rendered":"\u6e05\u534e\u5927\u5b66ESM:\u7528\u4e8e\u9ad8\u6027\u80fd\u9502\u79bb\u5b50\u7535\u6c60\u8d1f\u6781\u7684\u86cb\u72b6\u7ed3\u6784\u7684Si @ Si3N4 @ C\u590d\u5408\u6750\u6599"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n

Si\u7531\u4e8e\u5176\u9ad8\u7406\u8bba\u6bd4\u5bb9\u91cf\u9ad8\u3001\u542b\u91cf\u4e30\u5bcc\u3001\u6210\u672c\u4f4e\uff0c\u4f5c\u4e3a\u5546\u7528\u9502\u79bb\u5b50\u7535\u6c60\uff08LIBs\uff09\u77f3\u58a8\u8d1f\u6781\u7684\u66ff\u4ee3\u54c1\u5f15\u8d77\u4e86\u5e7f\u6cdb\u7684\u5173\u6ce8\u3002\u7136\u800c\u5728\u9502\u5316\/\u53bb\u9502\u5316\u671f\u95f4\u5267\u70c8\u7684\u4f53\u79ef\u53d8\u5316\u3002\u8fd9\u5c06\u4f1a\u5bfc\u81f4Si\u7c89\u788e\uff0cSEI\u4e0d\u7a33\u5b9a\u4ee5\u53ca\u6d3b\u6027\u7269\u8d28\u7684\u8131\u843d\uff0c\u8fd9\u4e25\u91cd\u9650\u5236\u4e86Si\u57fa\u6750\u6599\u7684\u8fdb\u4e00\u6b65\u5e94\u7528\u3002\u5df2\u7ecf\u5c1d\u8bd5\u4e86\u5404\u79cd\u7b56\u7565\u6765\u89e3\u51b3\u4e0a\u8ff0\u95ee\u9898\u3002Si\/C\u590d\u5408\u6750\u6599\u589e\u5f3a\u4e86\u6574\u4f53\u5bfc\u7535\u6027; \u7136\u800c\uff0c\u78b3\u57fa\u8d28\u7684\u754c\u9762\u7ed3\u5408\u80fd\u5f31\u548c\u673a\u68b0\u5f3a\u5ea6\u4f4e\u4e0d\u80fd\u9002\u5e94\u957f\u5faa\u73af\u671f\u95f4\u7684\u4f53\u79ef\u81a8\u80c0\u3002\u5728Si\/C\u590d\u5408\u6750\u6599\u4e2d\u6784\u9020\u7ed3\u6784\u7f13\u51b2\u5c42\u88ab\u8ba4\u4e3a\u662f\u89e3\u51b3\u8fd9\u79cd\u56f0\u5883\u7684\u53ef\u80fd\u65b9\u6848\u3002\u901a\u5e38\u9009\u62e9\u6c27\u5316\u7845\u4f5c\u4e3a\u7f13\u51b2\u6750\u6599\uff0c\u56e0\u4e3a\u5b83\u4eec\u7684\u4f53\u79ef\u53d8\u5316\u5c0f\uff0c\u7136\u800c\uff0c\u5176\u9996\u6b21\u5e93\u4f26\u6548\u7387\u4f4e\u662f\u4e00\u4e2a\u5173\u952e\u95ee\u9898\u3002\u6700\u8fd1\uff0c\u5f00\u53d1\u4e86\u6c2e\u5316\u7845\u4f5c\u4e3a\u6c27\u5316\u7845\u7684\u66ff\u4ee3\u6750\u6599\u3002 \u4e0eSiOx<\/sub>\u4e0d\u540c\uff0c\u8fd9\u79cd\u7c7b\u578b\u7684\u6750\u6599\u5728\u5faa\u73af\u671f\u95f4\u6ca1\u6709\u8868\u73b0\u51fa\u989d\u5916\u7684\u526f\u53cd\u5e94\u4f7f\u5f97ICE\u53d8\u4f4e\u3002\u5728\u6c2e\u5316\u7845\u4e2d\uff0cSi3<\/sub>N4<\/sub>\u5177\u6709\u4f18\u5f02\u7684\u7ed3\u6784\u6027\u80fd\uff0c\u5f3a\u5ea6\u8d85\u8fc71.1GPa\uff0c\u97e7\u6027\u8d85 7.0MPa\u00a0m1\/2<\/sup>\u3002\u56e0\u6b64\uff0c\u5c06Si3<\/sub>N4<\/sub>\u5145\u5f53Si\u548cC\u4e4b\u95f4\u7684\u4e2d\u95f4\u7ed3\u6784\u7f13\u51b2\u5c42\u4ee5\u63d0\u9ad8Si\u57fa\u8d1f\u6750\u6599\u662f\u4e00\u79cd\u975e\u5e38\u6709\u524d\u666f\u7684\u7b56\u7565\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u6e05\u534e\u5927\u5b66\u9b4f\u98de\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09<\/b><\/strong>\u901a\u8fc7\u76f4\u63a5\u8868\u9762\u6c2e\u5316\u5de5\u827a\uff0c\u7136\u540e\u8fdb\u884c\u5316\u5b66\u6c14\u76f8\u6c89\u79ef\uff08CVD\uff09\u78b3\u751f\u957f\uff0c\u5236\u5907\u4e86\u7531Si\uff0cSi3<\/sub>N4<\/sub>\u548c\u9ad8\u77f3\u58a8\u5316\u78b3\u7ec4\u6210\u7684\u86cb\u72b6\u7ed3\u6784\u590d\u5408\u6750\u6599(Si@Si3<\/sub>N4<\/sub>@C)\u3002\u6240\u63d0\u51fa\u7684\u6280\u672f\u7684\u5173\u952e\u7279\u5f81\u5982\u4e0b\uff1a\u9996\u5148\uff0c\u4e0e\u524d\u4e00\u79cd\u65b9\u6cd5\u4e0d\u540c\uff0c\u9996\u5148\u91c7\u7528\u76f4\u63a5\u8868\u9762\u6c2e\u5316\u6765\u5f15\u5165\u7ed3\u6676\u81f4\u5bc6\u7684Si3<\/sub>N4<\/sub>\u5c42\uff0c\u7136\u540e\u8fdb\u884cCVD\u5de5\u827a\u4ee5\u6d82\u8986\u9ad8\u8d28\u91cf\u7684\u78b3\u5c42\u3002\u4e24\u6b65\u6c14\u56fa\u53cd\u5e94\u53ef\u4ee5\u907f\u514d\u6db2\u4f53\u4f53\u7cfb\u4e2d\u8868\u9762\u79ef\u589e\u52a0\u7684\u95ee\u9898\u3002\u6b64\u5916\uff0c\u5177\u6709\u9ad8\u5f3a\u5ea6\u548c\u97e7\u6027\u7684Si3<\/sub>N4<\/sub>\u5c42\u5145\u5f53\u7f13\u51b2\u5c42\u4ee5\u6709\u6548\u5730\u7f13\u89e3\u4f53\u79ef\u53d8\u5316\uff0c\u4ece\u800c\u4fdd\u6301\u7ed3\u6784\u7a33\u5b9a\u6027\uff0c\u5e76\u4e14\u9ad8\u8d28\u91cf\u7684\u78b3\u5c42\u6539\u5584\u4e86\u6574\u4f53\u5bfc\u7535\u6027\u3002\u7814\u7a76\u4e86Si3<\/sub>N4<\/sub>\u5c42\u5bf9\u4fc3\u8fdbLi\u6269\u6563\u7684\u5f71\u54cd\uff0c\u5e76\u63d0\u51fa\u4e86\u53ef\u80fd\u7684\u539f\u56e0\u3002\u86cb\u72b6\u7ed3\u6784\u590d\u5408\u9633\u6781\u5177\u6709\u9ad8\u5bb9\u91cf\uff0c\u4f18\u5f02\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u548c\u500d\u7387\u6027\u80fd\u548c\u9ad8\u521d\u59cb\u5e93\u4f26\u6548\u7387\u3002\u76f8\u5173\u7814\u7a76\u6210\u679c\u201cSi@Si<\/b><\/strong>3<\/b><\/sub><\/strong>N<\/b><\/strong>4<\/b><\/sub><\/strong>@C composite with egg-like structure as high-performance anode material for lithium ion batteries<\/b><\/strong>\u201d\u4e3a\u9898\u53d1\u8868\u5728Energy Storage Materials<\/b><\/strong>\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/b><\/strong><\/p>\n

\u56fe\u4e00<\/b><\/strong>Si@Si<\/b><\/strong>3<\/b><\/sub><\/strong>N<\/b><\/strong>4<\/b><\/sub><\/strong>@C\u7684<\/b><\/strong>\u5236\u5907\u793a\u610f\u56fe\u53ca\u5f62\u8c8c\u8868\u5f81<\/b><\/strong><\/p>\n

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\uff08b-c\uff09SEM\u548cHR-TEM\u56fe\u50cf\uff0c\u3002<\/p>\n

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\u56fe\u4e8c<\/b><\/strong>Si@Si<\/b><\/strong>3<\/b><\/sub><\/strong>N<\/b><\/strong>4<\/b><\/sub><\/strong>@C\u7684\u9ad8\u500d\u7387TEM\u56fe\u50cf\u548cFFT<\/b><\/strong><\/p>\n

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 <\/p>\n

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\uff08b\uff09Si @Si@Si3<\/sub>N4<\/sub>@C\u590d\u5408\u6750\u6599\u7684\u62c9\u66fc\u5149\u8c31\u3002<\/p>\n

\uff08c\uff09Si\u548cSi@Si3<\/sub>N4<\/sub>@C\u590d\u5408\u6750\u6599\u7684TGA\u66f2\u7ebf\u3002<\/p>\n

\uff08d\uff09Si\u548cSi@Si3<\/sub>N4<\/sub>@C\u590d\u5408\u6750\u6599\u7684\u6c2e\u5438\u9644\/\u89e3\u5438\u7b49\u6e29\u66f2\u7ebf\u3002<\/p>\n

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\uff08b\uff09Si @ Si3N4 @ C\u590d\u5408\u6750\u6599\u7684\u5404\u4e2a\u5faa\u73af\u5708\u6570\u4e0b\u7684\u6bd4\u5bb9\u91cf-\u7535\u538b\u66f2\u7ebf\u3002<\/p>\n

\uff08c\uff09\u57280.5C\u7684\u7535\u6d41\u5bc6\u5ea6\u4e0b\u8fdb\u884c200\u6b21\u5faa\u73af\u540e\uff0c\u4e0d\u540cSi3<\/sub>N4<\/sub>\u542b\u91cf\u590d\u5408\u6750\u6599\u5728200\u6b21\u5faa\u73af\uff08\u76f8\u5bf9\u4e8e\u7b2c\u4e8c\u6b21\u653e\u7535\uff09\u540e\u7684\u7b2c\u4e00\u6b21\u653e\u7535\u5bb9\u91cf\u548c\u4fdd\u6301\u7387\u3002<\/p>\n

\uff08d-e\uff09Si @ C\u548cSi @ Si3<\/sub>N4<\/sub>\u00a0@ C\u590d\u5408\u6750\u6599\u7684\u500d\u7387\u6027\u80fd\u3002<\/p>\n

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\uff08d-f\uff09 EIS\u8c31\u56fe\u4ee5\u53ca\u963b\u6297\u548c\u03c9–<\/sup>1\/2<\/sup>\u7684\u7ebf\u6027\u62df\u5408\u548c\u76f8\u5e94\u7684\u8868\u9762\u6269\u6563\u7cfb\u6570\u6bd4\u8f83\u3002<\/p>\n

\uff08g\uff09\u4e0d\u540c\u626b\u63cf\u901f\u7387\u4e0b\u7684CV\u66f2\u7ebf\u3002<\/p>\n

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\uff08i\uff09\u4e0d\u540c\u626b\u901f\u4e0b\u7684\u8d5d\u7535\u5bb9\u8d21\u732e\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/b><\/strong><\/p>\n

\u603b\u4e4b\uff0c\u672c\u6587\u901a\u8fc7\u4e24\u6b65\u6c14\u56fa\u53cd\u5e94\u6210\u529f\u5730\u5236\u5907\u4e86\u4e00\u79cd\u86cb\u72b6\u7ed3\u6784Si @ Si3<\/sub>N4<\/sub>\u00a0@C\u590d\u5408\u6750\u6599\uff0c\u7528\u4e8e\u9502\u79bb\u5b50\u7535\u6c60\u7684\u9ad8\u6027\u80fd\u8d1f\u6781\u3002\u7eb3\u7c73Si\u82af\u663e\u793a\u51fa\u9ad8\u5bb9\u91cf\u3002\u9ad8\u5f3a\u5ea6\u548c\u575a\u97e7\u7684Si3<\/sub>N4<\/sub>\u00a0\u4e2d\u95f4\u5c42\u5145\u5f53\u7ed3\u6784\u7f13\u51b2\u5c42\uff0c\u5e76\u4e14\u4f5c\u4e3aLi+<\/sup>\u5bfc\u5c42\u9002\u5e94\u4f53\u79ef\u53d8\u5316\u5e76\u4fc3\u8fdb\u79bb\u5b50\u4f20\u8f93\u3002\u9ad8\u5ea6\u77f3\u58a8\u5316\u7684\u78b3\u58f3\u589e\u5f3a\u4e86\u6574\u4f53\u5bfc\u7535\u6027\u3002\u86cb\u72b6\u7ed3\u6784\u590d\u5408\u6750\u6599\u7684\u9996\u6b21\u653e\u7535\u5bb9\u91cf\u4e3a3093.8 mAh g\u00a0-1<\/sup>\uff0cICE\u4e3a91.51\uff05\uff0c\u57280.5C\u7684\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7ecf200\u6b21\u5faa\u73af\u540e\u5bb9\u91cf\u4e3a2071.7 mAh g\u00a0-1<\/sup>\uff0c\u5bb9\u91cf\u4fdd\u6301\u7387\u9ad8\u4e8e80%\u3002\u7cfb\u7edf\u5730\u7814\u7a76\u4e86Si3<\/sub>N4<\/sub>\u5c42\u5728\u7535\u5316\u5b66\u53cd\u5e94\u4e2d\u7684\u4f5c\u7528\uff0c\u53d1\u73b0\u5177\u6709\u4f18\u5f02\u673a\u68b0\u6027\u80fd\u7684Si3<\/sub>N4<\/sub>\u5c42\u80fd\u591f\u9632\u6b62\u7535\u6781\u7684\u7c89\u788e\u4ee5\u4fdd\u6301\u7ed3\u6784\u5b8c\u6574\u6027\u3002\u6b64\u5916\uff0cSi3<\/sub>N4<\/sub>\u5c42\u7684\u5f15\u5165\uff0c\u6539\u5584\u4e86Li+<\/sup>\u4f20\u8f93\uff0c\u5176\u539f\u56e0\u88ab\u8ba4\u4e3a\u662f\u5177\u6709\u4f18\u5f02\u673a\u68b0\u6027\u80fd\u7684Si3<\/sub>N4<\/sub>\u5c42\uff0c\u5176\u80fd\u591f\u5728\u7535\u5316\u5b66\u53cd\u5e94\u671f\u95f4\u4fdd\u6301\u66f4\u9ad8\u7684\u7ed3\u6784\u7a33\u5b9a\u6027\uff0c\u4ece\u800c\u4ea7\u751f\u66f4\u7a33\u5b9a\u548c\u66f4\u8584\u7684SEI\u5c42\uff0c\u4ece\u800c\u964d\u4f4e\u6574\u4f53\u7535\u963b\u3002Si3<\/sub>N4<\/sub>\u5c42\u7684\u5f15\u5165\u53ef\u4ee5\u4fc3\u8fdb\u7535\u6781\u4e2d\u7684\u79bb\u5b50\u6269\u6563\u5e76\u6539\u5584\u86cb\u72b6\u7ed3\u6784\u590d\u5408\u6750\u6599\u7684\u52a8\u529b\u5b66\u884c\u4e3a\u3002\u8fd9\u9879\u5de5\u4f5c\u4e3a\u4e0b\u4e00\u4ee3\u9ad8\u6027\u80fd\u9502\u79bb\u5b50\u7535\u6c60\u63d0\u4f9b\u4e86\u4e00\u79cd\u7b80\u5355\u6709\u6548\u7684\u8d1f\u6781\u6750\u6599\u5236\u5907\u65b9\u6cd5\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/b><\/strong>\u201c<\/b><\/strong>Si@Si3N4@C composite with egg-like structure as high-performance anode<\/b><\/u><\/strong>\u00a0<\/b><\/u><\/strong>material for lithium ion batteries<\/b><\/u><\/strong><\/a>\u201d<\/b><\/strong>(DOI:10.1016\/j.ensm.2019.06.031)<\/b><\/strong><\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4ebaCYM\u7f16\u8bd1\u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u6574\u7406\u7f16\u8f91\u3002<\/p>\n

\u6b22\u8fce\u5927\u5bb6\u5230\u6750\u6599\u4eba\u5ba3\u4f20\u79d1\u6280\u6210\u679c\u5e76\u5bf9\u6587\u732e\u8fdb\u884c\u6df1\u5165\u89e3\u8bfb\uff0c\u6295\u7a3f\u90ae\u7bb1tougao@cailiaoren.com\u3002<\/p>\n

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 <\/p>\n","protected":false},"excerpt":{"rendered":"

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