{"id":185887,"date":"2019-10-04T06:30:26","date_gmt":"2019-10-03T22:30:26","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=185887"},"modified":"2019-10-04T00:15:01","modified_gmt":"2019-10-03T16:15:01","slug":"%e3%80%90%e5%b7%b2%e6%a0%a1%e7%a8%bf%e3%80%91nature-energy%e6%b0%9f%e5%8c%96%e5%8e%9f%e7%94%b2%e9%85%b8%e9%85%af%e7%94%b5%e8%a7%a3%e6%b6%b2%e5%8a%a9%e5%8a%9bsei%e4%b8%80%e4%bd%93%e5%8c%96%e5%87%8f","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=185887","title":{"rendered":"Nature Energy:\u6c1f\u5316\u539f\u7532\u9178\u916f\u7535\u89e3\u6db2\u52a9\u529bSEI\u4e00\u4f53\u5316\u51cf\u5c11\u9502\u91d1\u5c5e\u8d1f\u6781\u7684\u7c89\u5316\u548c\u635f\u8017"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n

\u8fd1\u5e74\u6765\uff0c\u5bf9\u4e8e\u9ad8\u80fd\u91cf\u5bc6\u5ea6\u7535\u6c60\u7684\u4e0d\u65ad\u8ffd\u6c42\u4f7f\u5f97\u9502(Li)\u91d1\u5c5e\u8d1f\u6781(LMA)\u518d\u6b21\u6210\u4e3a\u4e86\u7814\u7a76\u70ed\u70b9\u3002\u7136\u800c\uff0c\u7531\u4e8eLMA\u7a33\u5b9a\u6027\u9762\u4e34\u7740\u8bb8\u591a\u95ee\u9898\u9650\u5236\u4e86\u5176\u5927\u89c4\u6a21\u5e94\u7528\u3002\u9502\u91d1\u5c5e\u4e0e\u7535\u89e3\u6db2\u7684\u8fde\u7eed\u526f\u53cd\u5e94\u4f1a\u4f7f\u5f97\u9502\u91d1\u5c5e\u548c\u7535\u89e3\u6db2\u88ab\u635f\u8017\uff0c\u8fdb\u4e00\u6b65\u5f71\u54cd\u7535\u6c60\u7684\u5e93\u4f26\u6548\u7387\u548c\u5faa\u73af\u5bff\u547d\u3002\u5373\u4f7f\u5728\u5177\u6709\u9ad8\u5e93\u4ed1\u6548\u7387\u548c\u65e0\u679d\u6676\u7684\u60c5\u51b5\u4e0b\uff0cLMA\u7684\u7c89\u672b\u5316\u53ca\u5176\u5728\u957f\u671f\u5faa\u73af\u540e\u7684\u4f53\u79ef\u81a8\u80c0\u4ecd\u7136\u5e26\u6765\u5f88\u5927\u7684\u5b89\u5168\u6027\u95ee\u9898\u3002\u7531\u4e8eLi\u7684\u6210\u6838\u548c\u751f\u957f\u4e3b\u8981\u53d6\u51b3\u4e8e\u7535\u89e3\u8d28\u7684\u5316\u5b66\u6027\u8d28\uff0c\u56e0\u6b64\u5f00\u53d1\u5177\u6709\u826f\u597d\u7a33\u5b9a\u6027\u7684\u7535\u89e3\u6db2\uff08\u5728LMA\u4e0a\u5f62\u6210\u5747\u5300\uff0c\u575a\u56fa\u7684SEI\uff09\u5bf9\u4e8eLMB\u7684\u8fdb\u4e00\u6b65\u5f00\u53d1\u662f\u81f3\u5173\u91cd\u8981\u7684\u3002\u540c\u6837\uff0c\u7535\u89e3\u6db2\u5bf9\u6b63\u6781\u7684\u7a33\u5b9a\u6027\u4e5f\u5f88\u91cd\u8981\u3002\u4f8b\u5982\u4e00\u4e9b\u5bf9LMA\u8868\u73b0\u51fa\u4f18\u5f02\u7a33\u5b9a\u6027\u7684\u7535\u89e3\u6db2\u5728\u9ad8\u538b\u6b63\u6781(NCM811)\u4f53\u7cfb\u53ef\u80fd\u4e0d\u7a33\u5b9a\u3002\u56e0\u6b64\uff0c\u7406\u60f3\u7684\u7535\u89e3\u6db2\u9700\u8981\u540c\u65f6\u5728\u6b63\u8d1f\u6781\u4e0a\u5f62\u6210\u7a33\u5b9a\u7684\u7535\u6781\u754c\u9762\u3002<\/p>\n

\u8fd1\u5e74\u6765\uff0c\u63d0\u51fa\u4e86\u901a\u8fc7\u9ad8\u76d0\u6d53\u5ea6\u7535\u89e3\u8d28(HCE)\u4ee5\u51cf\u5c11\u6e38\u79bb\u6eb6\u5242\u5206\u5b50\u7684\u6570\u91cf\u548c\u6539\u53d8Li+<\/sup>\u6eb6\u5242\u5316\u7ed3\u6784\u6765\u7a33\u5b9a\u9ad8\u538b\u6b63\u6781\u548cLMA\u3002\u867d\u7136\u8fd9\u4e9b\u65b9\u6cd5\u5927\u5927\u63d0\u9ad8\u4e86LMA\u7684\u7a33\u5b9a\u6027\u5e76\u5ef6\u957f\u4e86\u9502\u91d1\u5c5e\u7535\u6c60(LMBs)\u7684\u5faa\u73af\u5bff\u547d\uff0c\u4f46\u662f\u5728\u957f\u671f\u5faa\u73af\u540e\u4ecd\u7136\u89c2\u5bdf\u5230LMA\u7684\u539a\u5ea6\u589e\u52a0\u548c\u7535\u6781\u7c89\u5316\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u7f8e\u56fd\u897f\u5317\u592a\u5e73\u6d0b\u56fd\u5bb6\u5b9e\u9a8c\u5ba4\uff08PNNL\uff09\u7684\u66f9\u971e\u535a\u58eb\uff08\u7b2c\u4e00\u4f5c\u8005\uff09\uff0c\u5f20\u7ee7\u5149\u535a\u58eb<\/b><\/strong>\u548c\u8bb8\u6b66\u535a\u58eb\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/b><\/strong>\u63d0\u51fa\u4e86\u4e00\u7c7b\u7528\u4e8e\u51cf\u5c11\u9502\u91d1\u5c5e\u8d1f\u6781\u635f\u8017\u548c\u7c89\u5316\u7684\u6c1f\u5316\u539f\u7532\u9178\u916f\u7c7b\u7535\u89e3\u6db2\u3002\u4f5c\u8005\u4ee5TFEO\u4e3a\u4f8b\uff0c\u7814\u7a76\u4e86\u5176\u5bf9\u7535\u6c60\u6b63\u8d1f\u6781\u7684\u7a33\u5b9a\u6027\u548c\u5faa\u73af\u6027\u80fd\u7684\u5f71\u54cd\u3002TFEO\u7684\u6cb8\u70b9\u4e3a145\u00b0C\uff0c\u8fd9\u4f7f\u5f97\u7535\u6c60\u53ef\u4ee5\u5728\u9ad8\u6e29\u4e0b\u5e94\u7528\u3002TFEO\u4e0d\u542b\u4efb\u4f55\u4e0e\u9502\u91d1\u5c5e\u4ea7\u751f\u526f\u53cd\u5e94\u7684\u57fa\u56e2, \u63d0\u9ad8\u4e86\u5176\u5bf9\u9502\u91d1\u5c5e\u7684\u7a33\u5b9a\u6027\u3002\u4e0e\u5176\u4ed6\u5178\u578b\u6eb6\u5242\u76f8\u6bd4\uff0c\u5b83\u5177\u6709\u975e\u5e38\u4f4e\u7684HOMO\u80fd\u91cf\u503c\uff0c\u8be5\u7279\u6027\u5927\u5927\u63d0\u9ad8\u4e86\u5176\u9ad8\u538b\u7a33\u5b9a\u6027\u3002\u540c\u65f6\uff0c\u5176\u4f4e\u7c98\u5ea6\u7279\u6027\u4f7f\u5176\u6210\u4e3a\u4f18\u5f02\u7684\u7535\u89e3\u8d28\u52a9\u6eb6\u5242\u3002\u57fa\u4e8eTFEO\u7684\u7535\u89e3\u6db2\u7684\u663e\u8457\u4f18\u70b9\u662f\u53ef\u4ee5\u5f62\u6210\u975e\u5e38\u5747\u5300\uff0c\u4e00\u4f53\u5316\u7684SEI\uff0c\u8fd9\u80fd\u591f\u5927\u5927\u51cf\u5c11LMA\u5728\u957f\u5faa\u73af\u671f\u95f4\u7684\u635f\u8017\u548c\u7c89\u5316\u3002\u6b64\u5916\u5728\u9ad8\u538b\u6b63\u6781\u4e00\u4fa7\uff0c\u8fd9\u79cd\u7535\u89e3\u6db2\u53ef\u4ee5\u6291\u5236\u6b63\u6781\u7ed3\u6784\u7684\u76f8\u53d8\u3002\u76f8\u5173\u7814\u7a76\u6210\u679c\u4ee5\u201cMonolithic solid<\/b><\/strong>\u2013<\/b><\/strong>electrolyte interphases formed in fluorinated orthoformate-based electrolytes minimize Li depletion and pulverization<\/b><\/strong>\u201d\u4e3a\u9898\u53d1\u8868\u5728\u8fd1\u671f\u7684Nature Energy<\/b><\/strong>\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/b><\/strong><\/p>\n

\u56fe\u4e00.<\/b><\/strong>\u00a0<\/b><\/strong>\u9502\u8d1f\u6781\u4e0a\u7684<\/b><\/strong>SEI<\/b><\/strong>\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\u00a0\uff08a-c\uff09\u4e0d\u540c\u5c3a\u5ea6\u4e0bTEM\u7f51\u683c\u4e0a\u7684Cryo-EM\u56fe\u50cf\u3002<\/p>\n

\uff08d\uff09\u57281M LiFSI\/DME-TFEO\uff08\u6469\u5c14\u6bd41.2:3\uff09\u7535\u89e3\u6db2\u4e2d\u6c89\u79ef\u7684Li\u4e0a\u89c2\u5bdf\u5230\u7684\u5355\u5c42SEI\u7ed3\u6784\u7684\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe\u4e8c.<\/b><\/strong>\u00a0<\/b><\/strong>\u4e0d\u540c\u7535\u89e3\u6db2\u4e2d\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u7535\u5316\u5b66\u7a33\u5b9a\u7a97\u53e3<\/p>\n

\uff08b\uff09\u5e93\u4f26\u6548\u7387<\/p>\n

\uff08c\uff09\u5728Li-Li\u5bf9\u79f0\u7535\u6c60\u6d4b\u8bd5\u7684\u7535\u538b\u65f6\u95f4\u66f2\u7ebf\u3002<\/p>\n

\uff08d\uff09Li || NMC811\u7535\u6c60\u7684\u5faa\u73af\u6027\u80fd\u5bf9\u6bd4<\/p>\n

\uff08e\uff0cf\uff09Li || NMC811\u7535\u6c60\u7684\u500d\u7387\u6027\u80fd\u5bf9\u6bd4<\/p>\n

\u56fe\u4e09. <\/b><\/strong>Li || NMC811<\/b><\/strong>\u7535\u6c60\u5728<\/b><\/strong>100<\/b><\/strong>\u4e2a\u5faa\u73af\u540e\u7684<\/b><\/strong>Li<\/b><\/strong>\u635f\u8017\u548c\u4f53\u79ef\u81a8\u80c0<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\uff08a-c\uff09\u00a0Li-\u91d1\u5c5e\u7535\u6781\u5728\u4e09\u79cd\u7535\u89e3\u6db2\u4e2d\u7684\u6a2a\u622a\u9762SEM\u56fe\u50cf<\/p>\n

\uff08d\uff09\u57281M LiFSI\/DME-TFEO\u4e2d100\u4e2a\u5faa\u73af\u540eLi\u635f\u5931\u91cf\u3002<\/p>\n

\uff08e\uff09Li || NMC811\u7535\u6c60100\u6b21\u5faa\u73af\u540eLi\u635f\u5931\u548c\u76f8\u5e94\u539a\u5ea6\uff08\u4f53\u79ef\uff09\u81a8\u80c0\u7684\u793a\u610f\u56fe<\/p>\n

\u56fe\u56db.<\/b><\/strong>100<\/b><\/strong>\u6b21\u5faa\u73af\u4e4b\u540e\u7684<\/b><\/strong>Li<\/b><\/strong>\u8868\u9762\u7684<\/b><\/strong>XPS<\/b><\/strong>\u6d4b\u8bd5<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\uff08a-c\uff09\u5728\u4e09\u79cd\u7535\u89e3\u6db2\u4e2d\u5faa\u73af100\u6b21\u540e\u7684Li\u8d1f\u6781SEI\u7684C 1s\u8c31<\/p>\n

\uff08d\uff09P\u00a02p\u8c31<\/p>\n

\uff08e\uff0cf\uff09S 2p\u8c31<\/p>\n

\uff08g-i\uff09100\u6b21\u5faa\u73af\u540eLi\u8d1f\u6781\u8868\u9762SEI\u5728\u4e0d\u540c\u6e85\u5c04\u6df1\u5ea6\u7684\u5143\u7d20\u542b\u91cf<\/p>\n

\u56fe\u4e94.<\/b><\/strong>\u00a0NMC811<\/b><\/strong>\u6b63\u6781\u5728\u4e09\u79cd\u7535\u89e3\u6db2\u4e2d\u5faa\u73af\u4e4b\u540e\u7684\u8868\u5f81<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\uff08a-c\uff09\u5728\u4e09\u79cd\u7535\u89e3\u6db2\u4e2d\u5faa\u73af\u540e\u7684\u6b63\u6781CEI\u5728\u4e0d\u540c\u6e85\u5c04\u6df1\u5ea6\u7684\u5143\u7d20\u542b\u91cf<\/p>\n

\uff08d-i\uff09\u9ad8\u89d2\u73af\u5f62\u6697\u573a(HAADF)\u548c\u73af\u5f62\u4eae\u573a(ABF)\u626b\u63cf\u900f\u5c04\u663e\u5fae\u955c\u7684\u7167\u7247<\/p>\n

\uff08j-k\uff09100\u6b21\u5faa\u73af\u540e\u6b63\u6781\u8868\u9762CEI\u7684Mn\u548c Ni\u542b\u91cf<\/p>\n

\uff08l-m\uff09100\u6b21\u5faa\u73af\u540eLi\u8d1f\u6781\u8868\u9762SEI\u7684Mn\u548c Ni\u542b\u91cf<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/b><\/strong><\/p>\n

\u4f5c\u8005\u63d0\u51fa\u4e86\u4e00\u7c7b\u7528\u4e8eLMB\u7535\u89e3\u6db2\u7684\u6c1f\u5316\u539f\u7532\u9178\u916f\u6eb6\u5242\u3002\u57fa\u4e8eTFEO\u7684\u7535\u89e3\u6db2\u53ef\u4ee5\u5728LMA\u4e0a\u5f62\u6210\u9ad8\u5ea6\u5747\u5300\u7684\u65e0\u5b9a\u5f62\u548c\u4e00\u4f53\u5316SEI\u5c42\uff0c\u800c\u4e0d\u662f\u5148\u524d\u62a5\u9053\u7684\u9576\u5d4c\u6216\u591a\u5c42\u578bSEI\u7ed3\u6784\u3002\u8be5SEI\u5c42\u5bcc\u542b\u65e0\u673a\u7269\u8d28\uff0c\u53ef\u4ee5\u6291\u5236\u9502\u679d\u6676\u7684\u751f\u957f\u4e14\u5177\u6709\u5f88\u9ad8\u7684\u5e93\u4f26\u6548\u7387\u3002\u901a\u8fc7\u4e0e\u5728NMC811\u6b63\u6781\u5f62\u6210\u7684CEI\u4e00\u8d77\u534f\u540c\u4f5c\u7528\uff0c\u8be5\u7535\u89e3\u6db2\u663e\u8457\u63d0\u9ad8\u4e86Li || NMC811\u7535\u6c60\u7684\u957f\u5faa\u73af\u7a33\u5b9a\u6027\u5e76\u51cf\u5c11\u4e86LMA\u7684\u7c89\u5316\uff0c\u8fd9\u662fLMBs\u5b9e\u9645\u5e94\u7528\u7684\u4e3b\u8981\u969c\u788d\u4e4b\u4e00\u3002\u6b64\u5916\uff0cLi || NMC811\u7535\u6c60\u8fd8\u5177\u6709\u4f18\u5f02\u7684\u500d\u7387\u6027\u80fd\uff0c\u53ef\u4ee5\u57284C(~6 mA cm-2<\/sup>)\u7684\u500d\u7387\u8fdb\u884c\u5145\u653e\u7535\u3002\u4ee5\u4e0a\u8fd9\u4e9b\u7ed3\u679c\u8868\u660e\uff0c\u6c1f\u5316\u539f\u7532\u9178\u916f\u662f\u4e00\u7c7b\u975e\u5e38\u6709\u524d\u666f\u7684\u9ad8\u7535\u538b\u9502\u91d1\u5c5e\u7535\u6c60\u7535\u89e3\u6db2\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/b><\/strong>\u201c<\/b><\/strong>Monolithic solid<\/b><\/u><\/strong>\u2013<\/b><\/u><\/strong>electrolyte interphases formed in fluorinated orthoformate-based electrolytes minimize Li depletion and pulverization<\/b><\/u><\/strong><\/a>\u201d(Nature Energy<\/b><\/strong>, 2019,<\/b><\/strong>\u00a0<\/b><\/strong>4<\/b><\/strong>(<\/b><\/strong>9<\/b><\/strong>), <\/b><\/strong>796-805.<\/b><\/strong>\u00a0DOI.10.1038\/s41560-019-0464-5)<\/b><\/strong><\/p>\n

\u76f8\u5173\u6587\u732e\uff1a<\/b><\/strong>\u00a0<\/b><\/strong><\/p>\n

    \n
  1. \u201cHigh-voltage lithium metal batteries enabled by localized high concentration electrolytes\u201d, Shuru Chen, Jianming Zheng, Donghai Mei, Kee Sung Han, Mark H. Engelhard, Wengao Zhao, Wu Xu, Jun Liu, Ji-Guang Zhang*, Advanced Materials<\/i><\/em>2018, 30<\/b><\/strong>, 1706102.<\/li>\n<\/ol>\n

     <\/p>\n

      \n
    1. “High-Efficiency Lithium Metal Batteries with Fire-Retardant Electrolytes,” \u00a0Shuru Chen,<\/a>Jianming Zheng,<\/a>\u00a0Xiaodi Ren,<\/a>\u00a0Mark H. Engelhard<\/a>, Chaojiang Niu,<\/a>\u00a0Hongkyung Lee,<\/a>\u00a0Wu Xu, <\/a>Jie, Xiao,<\/a>\u00a0Jun Liu, <\/a>Ji-Guang Zhang<\/a>*, Joule<\/i><\/em>\u00a02018, 2<\/b><\/strong>, \u00a01548-1558.<\/li>\n<\/ol>\n

       <\/p>\n

        \n
      1. \u201cHigh performance silicon anodes enabled by nonflammable localized high concentration electrolytes,\u201d Haiping Jia, Lianfeng Zou, Peiyuan Gao, Cao Xia, Wengao Zhao, Yang He, Mark H. Engelhard, Sarah D. Burton, Hui Wang, \u00a0Xiaodi Ren, Qiuyan Li, Ran Yi, Xin Zhang, Chongmin Wang, \u00a0Zhijie Xu, Xiaolin Li, Jiguang Zhang*, Wu Xu*, Advanced Energy Materials<\/i><\/em>2019, 9<\/b><\/strong>, 1900784.<\/li>\n<\/ol>\n

         <\/p>\n

          \n
        1. \u201cEnabling High-Voltage Lithium-Metal Batteries under Practical Conditions\u201d, Xiaodi Ren, Lianfeng Zou, Xia Cao, Mark H. Engelhard, Wen Liu, Sarah D. Burton, Hongkyung Lee, Chaojiang Niu, Bethany E. Matthews, Zihua Zhu, Chongmin Wang, Bruce W. Arey, Jie Xiao, Jun Liu, Ji-Guang Zhang,* Wu Xu,* \u00a0Joule<\/i><\/em>2019, 3<\/b><\/strong>, 1662\u20131676.<\/li>\n<\/ol>\n

           <\/p>\n

            \n
          1. \u201cLocalized High-Concentration Sulfone Electrolytes for High-Efficiency Lithium-Metal Batteries<\/a>\u201d, Xiaodi Ren, Shuru Chen, Hongkyung Lee, Donghai Mei, Mark H. Engelhard, Sarah D. Burton, Wengao Zhao, Jianming Zheng, Qiuyan Li, Michael S. Ding, Marshall Schroeder, Judith Alvarado, Kang Xu, Y. Shirley Meng, Jun Liu, Ji-Guang Zhang*, Wu Xu*, Chem<\/i><\/em>2018, 4<\/b><\/strong>, 1877-1892.<\/li>\n<\/ol>\n

             <\/p>\n

              \n
            1. “A Localized High-Concentration Electrolyte with Optimized Solvents and Lithium Difluoro(oxalate)borate Additive for Stable Lithium Metal Batteries”, Lu Yu, Shuru Chen, Hongkyung Lee, Linchao Zhang, Mark H. Engelhard, Qiuyan Li, Shuhong Jiao, Jun Liu, Wu Xu*, Ji-Guang Zhang*, ACS Energy Letters<\/i><\/em>2018, 3<\/b><\/strong>, 2059-2067.<\/li>\n<\/ol>\n

               <\/p>\n

                \n
              1. \u201cExtremely Stable Sodium Metal Batteries Enabled by Localized High Concentration Electrolytes\u201d, Jianming Zheng, Shuru Chen, Wengao Zhao, Junhua Song, Mark H. Engelhard, Ji-Guang Zhang*, ACS Energy Letters<\/i><\/em>2018, 3<\/b><\/strong>, 315\u2212321.<\/li>\n<\/ol>\n

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