{"id":196425,"date":"2020-02-21T06:36:13","date_gmt":"2020-02-20T22:36:13","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=196425"},"modified":"2020-02-20T22:52:59","modified_gmt":"2020-02-20T14:52:59","slug":"%e4%b8%9c%e5%8d%8e%e5%a4%a7%e5%ad%a6%e7%bd%97%e7%bb%b4%e6%95%99%e6%8e%88advanced-science-%e5%85%b7%e6%9c%89n-n%e5%9e%8b%e5%bc%82%e8%b4%a8%e7%bb%93%e7%9a%84%e6%a0%91%e6%9e%9d%e7%8a%b6%e5%a4%9a","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=196425","title":{"rendered":"\u4e1c\u534e\u5927\u5b66\u7f57\u7ef4\u6559\u6388Adv Sci: \u5177\u6709n-n\u578b\u5f02\u8d28\u7ed3\u7684\u6811\u679d\u72b6\u591a\u7ea7\u4ecb\u5b54TiO2-SnO2\u590d\u5408\u6750\u6599\u53ca\u5176\u9ad8\u6548\u4e59\u9187\u6c14\u4f53\u4f20\u611f\u6027\u80fd\u7814\u7a76"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u57fa\u4e8e\u534a\u5bfc\u4f53\u91d1\u5c5e\u6c27\u5316\u7269\u6750\u6599\u7684\u6c14\u4f53\u4f20\u611f\u5668\u56e0\u5176\u5728\u7a7a\u6c14\u8d28\u91cf\u548c\u6c14\u4f53\u6cc4\u6f0f\u76d1\u6d4b\uff0c\u98df\u54c1\u5b89\u5168\u548c\u533b\u7597\u8bca\u65ad\u7b49\u65b9\u9762\u7684\u5e7f\u6cdb\u5e94\u7528\u800c\u5907\u53d7\u5173\u6ce8\uff0c\u4e3a\u4e86\u8fdb\u4e00\u6b65\u63d0\u5347\u6750\u6599\u7684\u6c14\u654f\u6027\u80fd\uff0c\u5408\u7406\u8bbe\u8ba1\u548c\u5408\u6210\u5177\u6709\u4e30\u5bcc\u8868\u9762\u6d3b\u6027\u4f4d\u70b9\u548c\u826f\u597d\u754c\u9762\u6027\u80fd\u7684\u7eb3\u7c73\u7ed3\u6784\u663e\u5f97\u81f3\u5173\u91cd\u8981\u3002\u6709\u5e8f\u4ecb\u5b54\u6750\u6599\u51ed\u501f\u4e92\u901a\u7684\u5b54\u9053\u7ed3\u6784\uff0c\u9ad8\u7684\u6bd4\u8868\u9762\u79ef\u548c\u8f83\u5927\u7684\u5b54\u5f84\u5c3a\u5bf8\uff0c\u6709\u5229\u4e8e\u6c14\u4f53\u5206\u5b50\u5728\u9aa8\u67b6\u4e2d\u7684\u5feb\u901f\u6269\u6563\uff0c\u5e76\u63d0\u4f9b\u5927\u91cf\u7684\u8868\u9762\u6d3b\u6027\u4f4d\u70b9\u6765\u5438\u9644\u6c14\u4f53\u5206\u5b50\uff0c\u4ece\u800c\u6709\u52a9\u4e8e\u6c14\u4f53\u4f20\u611f\u6027\u80fd\u7684\u63d0\u5347\u3002\u7136\u800c\uff0c\u4f20\u7edf\u4ecb\u5b54\u534a\u5bfc\u4f53\u91d1\u5c5e\u6c27\u5316\u7269\u6750\u6599\u7684\u5f62\u8c8c\u4e0e\u5c3a\u5bf8\u96be\u4ee5\u63a7\u5236\uff0c\u4f7f\u6750\u6599\u7684\u672c\u5f81\u4f18\u52bf\u4e0d\u80fd\u5f97\u5230\u5f7b\u5e95\u7684\u5f00\u53d1\u3002\u6b64\u5916\uff0c\u4e3a\u63d0\u5347\u6c14\u4f53\u4f20\u611f\u6750\u6599\u7684\u7075\u654f\u5ea6\u548c\u9009\u62e9\u6027\uff0c\u4fee\u9970\u7b2c\u4e8c\u7ec4\u5206\u662f\u4e00\u79cd\u5e38\u7528\u7684\u7b56\u7565\u3002\u4f46\u662f\uff0c\u5df2\u62a5\u9053\u4ecb\u5b54\u6750\u6599\u7684\u529f\u80fd\u5316\u65b9\u6cd5\u5927\u591a\u91c7\u7528\u540e\u8d1f\u8f7d\u7b56\u7565\uff0c\u6b65\u9aa4\u7e41\u6742\uff0c\u4e14\u5206\u6563\u6027\u4e0d\u4f73\u3002\u56e0\u6b64\uff0c\u5408\u6210\u5177\u6709\u5f62\u8c8c\u53ef\u63a7\uff0c\u529f\u80fd\u7ec4\u5206\u5206\u6563\u3001\u53ef\u8c03\u7684\u4ecb\u5b54\u534a\u5bfc\u4f53\u91d1\u5c5e\u6c27\u5316\u7269\u6750\u6599\u5c31\u663e\u5f97\u53ca\u91cd\u8981\u53c8\u8feb\u5207\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u4e1c\u534e\u5927\u5b66\u7ea4\u7ef4\u6750\u6599\u6539\u6027\u56fd\u5bb6\u91cd\u70b9\u5b9e\u9a8c\u5ba4\u3001\u6750\u6599\u79d1\u5b66\u4e0e\u5de5\u7a0b\u5b66\u9662\u7684\u7f57\u7ef4\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09\u3001\u6c5f\u839e\u6559\u6388\u3001\u535a\u58eb\u7814\u7a76\u751f\u8d75\u6d9b\uff08\u5171\u540c\u7b2c\u4e00\u4f5c\u8005\uff09\u3001\u9752\u5e74\u6559\u5e08\u90b1\u9e4f\u9e4f\uff08\u5171\u540c\u7b2c\u4e00\u4f5c\u8005\uff09\u4e0e\u590d\u65e6\u5927\u5b66\u5316\u5b66\u7cfb\u9093\u52c7\u8f89\u6559\u6388\u5408\u4f5c\uff0c\u9009\u7528SnO2<\/sub>\u7eb3\u7c73\u6676\uff08NCs,3-5 nm\uff09\u4e3a\u9521\u6e90\uff0c\u949b\u9178\u6b63\u4e01\u916f\u4e3a\u949b\u6e90\uff0c\u5b9e\u9a8c\u5ba4\u81ea\u5408\u6210\u4e24\u4eb2\u6027\u5d4c\u6bb5\u5171\u805a\u7269\u805a\u73af\u6c27\u4e59\u70f7-block<\/em>-\u805a\u82ef\u4e59\u70ef\uff08PEO-b<\/em>-PS\uff09\u4e3a\u6a21\u677f\u5242,\u5f00\u53d1\u4e86\u4e00\u79cd\u6eb6\u5242\u6325\u53d1\u8bf1\u5bfc\u53d6\u5411\u5171\u7ec4\u88c5\u7b56\u7565\uff0c\u5408\u6210\u4e86\u5177\u6709n-n\u578b\u5f02\u8d28\u7ed3\u7684\u6811\u679d\u72b6\u591a\u7ea7\u4ecb\u5b54TiO2<\/sub>-SnO2<\/sub>\u590d\u5408\u6750\u6599\uff08SHMT\uff09\u3002SnO2<\/sub>\u7eb3\u7c73\u6676\u8868\u9762\u4e30\u5bcc\u7684\u7f9f\u57fa\u4f7f\u5176\u53ef\u4ee5\u901a\u8fc7\u6c22\u952e\u548c\u6a21\u677f\u5242\u7684PEO\u6bb5\u76f8\u4e92\u4f5c\u7528\uff0c\u5e76\u901a\u8fc7\u5171\u7ec4\u88c5\u8fc7\u7a0b\u5d4c\u5165\u5230\u591a\u7ea7\u4ecb\u5b54TiO2<\/sub>\u6750\u6599\u7684\u5b54\u58c1\u4e2d\u3002\u6240\u83b7\u5f97\u7684\u591a\u7ea7\u4ecb\u5b54\u590d\u5408\u6750\u6599\u5177\u6709\u6811\u679d\u72b6\u5f62\u8c8c\uff0c\u5747\u5300\u7684\u7c92\u5f84\uff08500 nm\uff09\u548c\u53d1\u6563\u578b\u7684\u4ecb\u5b54\u5b54\u9053(9 nm)\uff0c\u5176\u6bd4\u8868\u9762\u79ef\u4ee5\u53ca\u5b54\u5bb9\u5206\u522b\u53ef\u8fbe76m2<\/sup>\/g\u548c0.11 cm3<\/sup>\/g\u3002\u5728\u8be5\u4f53\u7cfb\u4e2d\uff0c\u4e0d\u6dfb\u52a0SnO2<\/sub> \u7eb3\u7c73\u6676\u4ecd\u7136\u53ef\u4ee5\u5f97\u5230\u6811\u679d\u72b6\u7684\u591a\u7ea7\u4ecb\u5b54\u7ed3\u6784\uff08HMT\uff09\uff0c\u7b80\u5355\u7684\u6539\u53d8\u53cd\u5e94\u6761\u4ef6\uff0c\u6750\u6599\u7684\u5f62\u8c8c\u8fd8\u53ef\u4ee5\u8c03\u63a7\u4e3a\u4ecb\u5b54\u5fae\u7403\u548c\u4ecb\u5b54\u8584\u819c\u3002\u901a\u8fc7\u5bf9\u4e8e\u5408\u6210\u8fc7\u7a0b\u7684\u8ffd\u8e2a\uff0c\u7814\u7a76\u8005\u5bf9\u6750\u6599\u7684\u5f62\u6210\u673a\u7406\u8fdb\u884c\u4e86\u900f\u5f7b\u7684\u5206\u6790\u3002\u8be5\u5de5\u4f5c\u4e3a\u9ad8\u6548\u7387\u5236\u5907\u6709\u5e8f\u4ecb\u5b54\u91d1\u5c5e\u6c27\u5316\u7269\u6750\u6599\u63d0\u4f9b\u4e86\u65b0\u601d\u8def\uff0c\u51ed\u501f\u7740\u72ec\u7279\u7684\u5f62\u8c8c\u548c\u7ed3\u6784\uff0c\u57fa\u4e8eSHMT\u7684\u6c14\u4f53\u4f20\u611f\u5668\u5c55\u73b0\u51fa\u4f18\u5f02\u7684\u4e59\u9187\u6c14\u4f53\u4f20\u611f\u6027\u80fd\uff0c\u54cd\u5e94\/\u6062\u590d\u901f\u5ea6\u4ec5\u4e3a7\/5 s\uff0c\u68c0\u6d4b\u9650\u4f4e\u81f3200 ppb\u3002\u76f8\u5173\u7814\u7a76\u6210\u679c\u4ee5\u9898\u4e3a<\/strong>\u201cHierarchical Branched Mesoporous TiO2<\/sub>\u2013SnO2<\/sub> Nanocomposites with Well-defined n-n Heterojunctions for Highly Efficient Ethanol Sensing\u201d<\/strong>\u53d1\u8868\u5728<\/strong>Advanced Science<\/em><\/strong>\u4e0a\u3002<\/strong><\/p>\n

\u56fe<\/strong>1. SHMT<\/strong>\u7684\u7ed3\u6784\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

a, b. \u4e3aSHMT\u7684SEM\u56fe\u3002<\/p>\n

c, d. \u4e3aSHMT\u7684TEM\u56fe\uff08\u63d2\u56fe\u4e3aSAED\uff09\u3002<\/p>\n

e\u4e3aSHMT\u7684HRTEM\u56fe\u3002<\/p>\n

f\u4e3aSHMT\u7684\u8d85\u8584\u5207\u7247TEM\u56fe\u3002<\/p>\n

g-j. \u4e3aSTEM\u56fe\u548c\u5143\u7d20\u5206\u5e03\u56fe\u3002<\/p>\n

\u56fe<\/strong>2. HMT<\/strong>\u7684\u7ed3\u6784\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

a, b. \u4e3aHMT\u7684SEM\u56fe\u3002<\/p>\n

c, d. \u4e3aHMT\u7684TEM\u56fe\u3002<\/p>\n

\u56fe<\/strong>3. SHMT<\/strong>\u7684\u7ec4\u5206\u548c\u6027\u8d28\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

a.SHMT\u548cHMT\u4e0d\u540c\u70ed\u5904\u7406\u9636\u6bb5\u7684XRD\u8c31\u56fe\u3002<\/p>\n

b.SHMT\u7684\u6c2e\u6c14\u5438\u9644-\u8131\u9644\u7b49\u6e29\u7ebf\u3002<\/p>\n

c.SHMT\u7684\u5b54\u5f84\u5206\u5e03\u3002<\/p>\n

d.Ti\u7684XPS\u56fe\u3002<\/p>\n

e.Sn\u7684XPS\u56fe\u3002<\/p>\n

f.O\u7684XPS\u56fe\u3002<\/p>\n

\u56fe<\/strong>4.<\/strong>\u7ec4\u88c5\u8fc7\u7a0b\u548c\u673a\u7406\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

a-d. \u949b\u6e90\u548cPEO-b<\/em>-PS\u7ec4\u88c5\u8fc7\u7a0b\u7684TEM\u56fe\u3002<\/p>\n

e-h. \u9521\u6e90\u3001\u949b\u6e90\u548cPEO-b<\/em>-PS\u5171\u7ec4\u88c5\u8fc7\u7a0b\u7684TEM\u56fe\u3002<\/p>\n

i.\u80f6\u675f\u7ec4\u88c5\u8fc7\u7a0b\u673a\u7406\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe<\/strong>5. SHMT<\/strong>\u6c14\u654f\u6027\u80fd\u6d4b\u8bd5<\/strong><\/p>\n

\"\"<\/p>\n

SHMT\uff0cHMT\u548cSnO2<\/sub> NCs\u7684\u6e29\u5ea6\u9009\u62e9\u6027\u3002<\/p>\n

b, c. SHMT\uff0cHMT\u548cSnO2<\/sub> NCs \u5bf9\u4e59\u9187\u4e0d\u540c\u6d53\u5ea6\u4e0b\u7684\u54cd\u5e94\u503c\u3002<\/p>\n

d.SHMT\u5bf950 ppm\u548c400 ppm\u4e59\u9187\u7684\u54cd\u5e94\/\u6062\u590d\u66f2\u7ebf\u3002<\/p>\n

e.SHMT\u4f20\u611f\u5668\u7684\u6c14\u4f53\u9009\u62e9\u6027\u3002<\/p>\n

f.\u91d1\u5c5e\u6c27\u5316\u7269\u57fa\u6c14\u654f\u6750\u6599\u7684\u6027\u80fd\u5bf9\u6bd4\u56fe\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u7814\u7a76\u56e2\u961f\u53d1\u5c55\u4e86\u4e00\u79cd\u65b0\u578b\u6eb6\u5242\u6325\u53d1\u8bf1\u5bfc\u53d6\u5411\u5171\u7ec4\u88c5\u7b56\u7565\uff0c\u6784\u5efa\u4e86\u5177\u6709n-n\u578b\u5f02\u8d28\u7ed3\u7684\u6811\u679d\u72b6\u591a\u7ea7\u4ecb\u5b54TiO2<\/sub>-SnO2<\/sub>\u590d\u5408\u6750\u6599\u3002\u8be5\u6750\u6599\u5de8\u5927\u7684\u6bd4\u8868\u9762\u79ef\u63d0\u4f9b\u4e86\u5145\u8db3\u7684\u8868\u9762\u6d3b\u6027\u4f4d\u70b9\uff0c\u8f83\u5927\u7684\u4ecb\u5b54\u5b54\u5f84\u6709\u5229\u4e8e\u6c14\u4f53\u5206\u5b50\u7684\u5728\u5438\u9644\u548c\u8131\u9644\u8fc7\u7a0b\u4e2d\u7684\u5feb\u901f\u4f20\u8f93\uff0c\u9ad8\u5ea6\u7ed3\u6676\u7684\u9aa8\u67b6\u4fdd\u8bc1\u4e86\u7ed3\u6784\u7684\u7a33\u5b9a\u6027\uff0c\u6811\u679d\u72b6\u7684\u7ed3\u6784\u6709\u5229\u4e8e\u7535\u5b50\u5728\u5f84\u5411\u7684\u4f20\u9012\u3002\u6b64\u5916\uff0c\u4e30\u5bcc\u7684n-n\u578b\u5f02\u8d28\u7ed3\u4e5f\u8fdb\u4e00\u6b65\u63d0\u5347\u4e86\u6750\u6599\u7684\u6c14\u4f53\u4f20\u611f\u6027\u80fd\u3002\u8fd9\u79cd\u4ece\u7ec4\u5206\uff0c\u7ed3\u6784\u548c\u5f62\u8c8c\u4e0a\u7684\u534f\u540c\u4f5c\u7528\uff0c\u4e3a\u8bbe\u8ba1\u548c\u5408\u6210\u5177\u6709\u72ec\u7279\u7eb3\u7c73\u7ed3\u6784\u7684\u6c14\u4f53\u4f20\u611f\u6750\u6599\u63d0\u4f9b\u4e86\u65b0\u601d\u8def\u3002\u540c\u65f6\uff0c\u672c\u6587\u63d0\u51fa\u7684\u5408\u6210\u7b56\u7565\u6709\u671b\u63a8\u5e7f\u5230\u5176\u4ed6\u7ec4\u5206\u6709\u5e8f\u4ecb\u5b54\u91d1\u5c5e\u6c27\u5316\u7269\u6750\u6599\u7684\u5408\u6210\u4e2d\u3002<\/p>\n

\u3010\u901a\u8baf\u4f5c\u8005\u4ecb\u7ecd\u3011<\/strong><\/p>\n

\u7f57\u7ef4\uff0c\u535a\u58eb\uff0c\u4e1c\u534e\u5927\u5b66\u6559\u6388\u3001\u535a\u58eb\u751f\u5bfc\u5e08\uff0c\u5165\u9009\u201c\u56fd\u5bb6\u4f18\u79c0\u9752\u5e74\u79d1\u5b66\u57fa\u91d1\u201d\u3001\u201c\u4e0a\u6d77\u5e02\u9752\u5e74\u79d1\u6280\u542f\u660e\u661f\u201d\u3001\u201c\u4e0a\u6d77\u5e02\u9752\u5e74\u62d4\u5c16\u4eba\u624d\u201d\u3002\u4e3b\u8981\u4ece\u4e8b\u9ad8\u6d3b\u6027\u4ecb\u5b54\u6750\u6599\u7684\u7ed3\u6784\u8c03\u63a7\u4e0e\u5176\u5728\u4f4e\u6e29\u70e7\u7ed3\u3001\u6c14\u4f53\u4f20\u611f\u548c\u80fd\u91cf\u50a8\u5b58\u4e0e\u8f6c\u5316\u7b49\u9886\u57df\u7684\u7814\u7a76\u5de5\u4f5c\u3002\u4e3b\u6301\u56fd\u5bb6\u81ea\u7136\u79d1\u5b66\u57fa\u91d1\u3001\u4e0a\u6d77\u5e02\u201c\u79d1\u6280\u521b\u65b0\u884c\u52a8\u8ba1\u5212\u201d\u3001\u4e1c\u534e\u5927\u5b66\u201c\u52b1\u5fd7\u8ba1\u5212\u201d\u7b49\u9879\u76ee\uff0c\u201c\u529f\u80fd\u4ecb\u5b54\u65e0\u673a\u975e\u91d1\u5c5e\u6750\u6599\u7684\u8bbe\u8ba1\u5408\u6210\u4e0e\u5e94\u7528\u201d\u83b7\u6559\u80b2\u90e8\u81ea\u7136\u79d1\u5b66\u4e8c\u7b49\u5956\uff08\u7b2c3\u5b8c\u6210\u4eba\uff09\u3002\u4ee5\u7b2c\u4e00\u6216\u901a\u8baf\u4f5c\u8005\u5728\u201cAdv. Mater.\u201d\u3001\u201cJ. Am. Chem. Soc.\u201d\u3001\u201cAdv. Energy Mater.\u201d\u3001\u201cAdv. Funct. Mater.\u201d\u3001\u201cAngew. Chem. Int. Ed.\u201d\u7b49\u9ad8\u6c34\u5e73\u671f\u520a\u53d1\u8868\u591a\u7bc7\u8bba\u6587\u3002\u76ee\u524d\u4efb\u62c5\u4efb\u201cChinese Chemical Letters\u201d\u671f\u520a\u9752\u5e74\u7f16\u59d4\u3001\u201c\u4e2d\u56fd\u6750\u6599\u7814\u7a76\u5b66\u4f1a\u9752\u5e74\u5de5\u4f5c\u59d4\u5458\u4f1a\u201d\u548c\u201c\u4e2d\u56fd\u7845\u9178\u76d0\u5b66\u4f1a\u9752\u5e74\u5de5\u4f5c\u59d4\u5458\u4f1a\u201d\u7406\u4e8b\u7b49\u804c\u52a1\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1aHierarchical Branched Mesoporous TiO2<\/sub>\u2013SnO2<\/sub> Nanocomposites with Well-defined n-n Heterojunctions for Highly Efficient Ethanol Sensing\uff08Adv. Sci. 2019, 6<\/em>, 1902008, DOI: 10.1002\/advs.201902008\uff09<\/p>\n

https:\/\/onlinelibrary.wiley.com\/doi\/full\/10.1002\/advs.201902008<\/a><\/p>\n","protected":false},"excerpt":{"rendered":"

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