{"id":198094,"date":"2020-03-14T20:04:28","date_gmt":"2020-03-14T12:04:28","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=198094"},"modified":"2020-03-14T20:04:28","modified_gmt":"2020-03-14T12:04:28","slug":"%e4%b8%ad%e5%8d%97%e5%a4%a7%e5%ad%a6%e6%ac%a7%e6%98%9f%e4%b8%9c%e5%8c%97%e5%a4%a7%e5%ad%a6%e9%aa%86%e6%96%87%e5%bd%acacs-nano%ef%bc%9a%e5%8f%8c%e9%87%91%e5%b1%9e%e7%a1%ab%e5%8c%96%e7%89%a9sb2s3f","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=198094","title":{"rendered":"\u4e2d\u5357\u5927\u5b66\u6b27\u661f&\u4e1c\u5317\u5927\u5b66\u9a86\u6587\u5f6cACS Nano\uff1a\u53cc\u91d1\u5c5e\u786b\u5316\u7269Sb2S3@FeS2\u7a7a\u5fc3\u7eb3\u7c73\u68d2\u52a9\u529b\u9ad8\u6027\u80fd\u94a0\u79bb\u5b50\u7535\u6c60"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u94a0\u79bb\u5b50\u7535\u6c60\uff08SIBs\uff09\u7531\u4e8e\u94a0\u5143\u7d20\u50a8\u91cf\u4e30\u5bcc\u3001\u7ecf\u6d4e\u6548\u76ca\u9ad8\u548c\u9002\u5b9c\u7684\u6c27\u5316\u8fd8\u539f\u7535\u4f4d\u7b49\u4f17\u591a\u4f18\u70b9\u800c\u5907\u53d7\u77a9\u76ee\uff0c\u56e0\u800c\u4e5f\u88ab\u8ba4\u4e3a\u5728\u57fa\u4e8e\u7535\u7f51\u7684\u50a8\u80fd\u7cfb\u7edf\u4e2d\u6700\u5177\u53d1\u5c55\u524d\u666f\u3002\u5728\u957f\u671f\u7684\u7814\u7a76\u62a5\u9053\u4e2d\uff0cSIBs\u5982\u4f55\u5b9e\u73b0\u9ad8\u80fd\u91cf\u5bc6\u5ea6\u3001\u9ad8\u500d\u7387\u6027\u80fd\u548c\u4f18\u826f\u7684\u5faa\u73af\u5bff\u547d\u4ecd\u56f0\u96be\u91cd\u91cd\u3002\u56e0\u6b64\uff0c\u5bfb\u6c42\u7406\u60f3\u7684\u6d3b\u6027\u7535\u6781\u6750\u6599\u663e\u5f97\u5c24\u4e3a\u91cd\u8981\u3002\u8fc7\u6e21\u91d1\u5c5e\u6c27\u5316\u7269\u3001\u5408\u91d1\u57fa\u6750\u6599\u3001\u91d1\u5c5e\u7852\u5316\u7269\u548c\u91d1\u5c5e\u786b\u5316\u7269\u7b49\u4f17\u591a\u6750\u6599\uff0c\u7531\u4e8e\u5176\u6bd4\u5bb9\u91cf\u9ad8\u3001\u53cd\u5e94\u5e73\u53f0\u9002\u5b9c\u3001\u4ef7\u683c\u4f4e\u5ec9\u7b49\u4f18\u70b9\u88ab\u8ba4\u4e3a\u662fSIBs\u7406\u60f3\u7684\u8d1f\u6781\u6750\u6599\u3002\u5728\u8fc7\u6e21\u91d1\u5c5e\u786b\u5316\u7269\u4e2d\uff0c\u4e09\u786b\u5316\u4e8c\u9511\uff08Sb2<\/sub>S3<\/sub>\uff09\u5177\u6709\u6b63\u4ea4\u6676\u7cfb\u7684\u6676\u4f53\u7ed3\u6784\u548c\u9ad8\u8fbe954 mAh\/g\u7684\u7406\u8bba\u6bd4\u5bb9\u91cf\uff0c\u5728TMDs\u4e2d\u8131\u9896\u800c\u51fa\uff0c\u4e14\u5176Na+<\/sup>\u8131\u5d4c\u8fc7\u7a0b\u6d89\u53ca\u5230\u8f6c\u5316\u548c\u5408\u91d1\u5316\u53cd\u5e94\u7684\u4e24\u79cd\u673a\u5236\u3002\u7136\u800c\uff0c\u57fa\u4e8eSb2<\/sub>S3<\/sub>\u7684\u8d1f\u6781\u6750\u6599\u5b58\u5728\u4e00\u4e9b\u7f3a\u70b9\uff0c\u5176\u56fa\u6709\u7684\u4f4e\u7535\u5bfc\u7387\u5bb9\u6613\u5bfc\u81f4\u8f83\u5927\u7684\u963b\u6297\u548c\u8f83\u5dee\u7684\u500d\u7387\u6027\u80fd\uff1b\u540c\u65f6\uff0c\u8f6c\u5316\u548c\u8fdb\u4e00\u6b65\u5408\u91d1\u5316\u53cd\u5e94\u8fc7\u7a0b\u4e2d\u5f15\u8d77\u7684\u5de8\u5927\u4f53\u79ef\u81a8\u80c0\u4f1a\u4e0d\u53ef\u907f\u514d\u5730\u4ea7\u751f\u8f83\u5927\u7684\u673a\u68b0\u5185\u5e94\u529b\uff0c\u4ece\u800c\u81f4\u4f7f\u7eb3\u7c73\u9897\u7c92\u7c89\u788e\u548c\u805a\u96c6\uff0c\u91d1\u5c5eSb0<\/sup>\u548cNa2<\/sub>S\u4e4b\u95f4\u7684\u6d3b\u6027\u53cd\u5e94\u754c\u9762\u5927\u5927\u964d\u4f4e\uff0c\u5bfc\u81f4\u7535\u5316\u5b66\u53cd\u5e94\u7684\u53ef\u9006\u6027\u8f83\u5dee\uff0c\u957f\u671f\u5faa\u73af\u7684\u5bb9\u91cf\u4fdd\u6301\u7387\u4f4e\u4e0b\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb<\/strong>\u3011<\/p>\n

\u8fd1\u671f\uff0c\u4e2d\u5357\u5927\u5b66\u6b27\u661f\u526f\u6559\u6388<\/strong>\u548c\u4e1c\u5317\u5927\u5b66\u9a86\u6587\u5f6c\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u7b49\u4eba\u5229\u7528\u4e24\u6b65\u6eb6\u5242\u70ed\u6cd5\u6210\u529f\u5236\u5907\u4e86\u9576\u5d4c\u5728\u6c2e\u63ba\u6742\u77f3\u58a8\u70ef\u57fa\u4f53\u4e2d\u7684Sb2<\/sub>S3<\/sub>@FeS2<\/sub>\u7a7a\u5fc3\u7eb3\u7c73\u68d2\uff08SFS\/C\uff09\u5206\u7ea7\u590d\u5408\u7ed3\u6784\uff0c\u5e76\u5c06\u5176\u7528\u4f5c\u94a0\u79bb\u5b50\u7535\u6c60\u8d1f\u6781\u6750\u6599\u3002\u4e8c\u5143\u91d1\u5c5e\u786b\u5316\u7269\u4e0d\u540c\u7ec4\u5206\u4e4b\u95f4\u7684\u5f02\u8d28\u754c\u9762\u4e0d\u4ec5\u8bf1\u5bfc\u4ea7\u751f\u4e86\u5185\u5efa\u7535\u573a\uff0c\u52a0\u5feb\u4e86Na+<\/sup>\u6269\u6563\u901f\u5ea6\u548c\u754c\u9762\u7535\u8377\u8f6c\u79fb\uff0c\u800c\u4e14\u8fd8\u4e3a\u7535\u5316\u5b66\u53cd\u5e94\u589e\u52a0\u4e86\u6d3b\u6027\u4f4d\u70b9\u3002\u6b64\u5916\uff0cSb2<\/sub>S3<\/sub>@FeS2<\/sub>\u7a7a\u5fc3\u7eb3\u7c73\u68d2\u9576\u5d4c\u5728N-\u63ba\u6742\u77f3\u58a8\u70ef\u57fa\u4f53\u4e2d\u7684\u5206\u7ea7\u590d\u5408\u7ed3\u6784\uff0c\u53ef\u4ee5\u7f13\u89e3\u5145\u653e\u7535\u5faa\u73af\u6240\u5e26\u6765\u7684\u4f53\u79ef\u81a8\u80c0\uff0c\u786e\u4fdd\u8f83\u5927\u7684\u53cd\u5411\u5bb9\u91cf\u3002\u96c6\u7a7a\u5fc3\u5206\u7ea7\u7eb3\u7c73\u7ed3\u6784\u3001\u5f02\u8d28\u6676\u4f53\u548c\u5f02\u8d28\u7ed3\u8bf1\u5bfc\u534f\u540c\u8026\u5408\u6548\u5e94\u7b49\u4f17\u591a\u4f18\u70b9\u4e8e\u4e00\u8eab\u7684SFS\/C\u590d\u5408\u6750\u6599\uff0c\u5176\u8868\u73b0\u51fa\u4e86\u4f18\u5f02\u7684Na+<\/sup>\u5b58\u50a8\u6027\u80fd\u3002\u57285 A\/g\u7684\u7535\u6d41\u5bc6\u5ea6\u4e0b\uff0cSFS\/C\u7684\u53ef\u9006\u6bd4\u5bb9\u91cf\u4e3a534.8 mAh\/g\uff0c\u4e141000\u6b21\u5145\u653e\u7535\u5faa\u73af\u540e\u7684\u6bd4\u5bb9\u91cf\u4fdd\u6301\u7387\u4e3a85.7 %\uff0c\u800c\u4e14\u572810 A\/g\u7684\u8d85\u9ad8\u500d\u7387\u4e0b\uff0c\u5176\u6bd4\u5bb9\u91cf\u53ef\u8fbe537.9 mAh\/g\u3002\u8be5\u9879\u7814\u7a76\u4ee5\u9898\u4e3a\u201cBimetallic Sulfide Sb2<\/sub>S3<\/sub>@FeS2<\/sub> Hollow Nanorods as High-Performance Anode Materials for Sodium-Ion Batteries<\/strong>\u201d\u53d1\u8868\u5728ACS Nano<\/strong>\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb<\/strong>\u3011<\/p>\n

\u56fe\u4e00<\/strong>\u00a0 SFS\/C <\/strong>\u590d\u5408\u6750\u6599\u7684\u5408\u6210\u8def\u5f84\u53ca\u5f62\u8c8c\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a) SFS\/C\u590d\u5408\u6750\u6599\u7684\u5408\u6210\u8def\u5f84\u793a\u610f\u56fe\uff1b<\/p>\n

(b-h) \u5206\u522b\u4e3aSFS\/C\u7684SEM\u3001TEM\u3001HRTEM\u3001SAED\u53caEDS\u5143\u7d20\u5206\u5e03\u56fe\u50cf\u3002<\/p>\n

\u56fe\u4e8c<\/strong>\u00a0 SFS\/C<\/strong>\u7684<\/strong>XRD<\/strong>\u53ca<\/strong>XPS<\/strong>\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a-c) SFS\/C\u7684XRD\u3001\u62c9\u66fc\u5149\u8c31\u548cN2<\/sub>\u5438\u8131\u9644\u66f2\u7ebf\uff1b<\/p>\n

(d) Sb2<\/sub>S3<\/sub>\u3001 SFS\u548cSFS\/C\u7684Sb 3d XPS\u80fd\u8c31\u56fe\uff1b<\/p>\n

(e, f) SFS\/C\u7684C 1s\u548cN 1s XPS\u80fd\u8c31\u56fe\u3002<\/p>\n

\u56fe\u4e09<\/strong> \u00a0SFS\/C<\/strong>\u590d\u5408\u6750\u6599\u7684\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

(a) SFS\/C\u57280.1 mV\/s\u7684\u626b\u63cf\u901f\u7387\u4e0b\uff0c0.1~3.0 V\u8303\u56f4\u5185\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

(b) \u57280.1 A\/g\u7684\u7535\u6d41\u5bc6\u5ea6\u4e0b\uff0cSFS\/C\u521d\u59cb3\u6b21\u5faa\u73af\u7684\u6052\u6d41\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

(c) Sb2<\/sub>S3<\/sub>\u3001 SFS\u548cSFS\/C\u5728\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u500d\u7387\u6027\u80fd\uff1b<\/p>\n

(d) SFS\/C\u7535\u6781\u5728\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

(e) SFS\/C\u7535\u6781\u4e0e\u5176\u4ed6\u7528\u4e8eSIBs\u7684Sb2<\/sub>S3<\/sub>\u57fa\u8d1f\u6781\u6027\u80fd\u5bf9\u6bd4\u56fe\uff1b<\/p>\n

(f, g) Sb2<\/sub>S3<\/sub>\u3001 SFS\u548cSFS\/C\u57281 A\/g\u548c5 A\/g\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u5faa\u73af\u6027\u80fd\u3002<\/p>\n

\u56fe\u56db<\/strong>\u00a0 SFS\/C<\/strong>\u7684\u539f\u4f4d<\/strong>XRD<\/strong>\u53ca\u975e\u539f\u4f4d<\/strong>HRTEM<\/strong>\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a) SFS\/C\u7535\u6781\u5728\u521d\u59cb\u94a0\u5316\u548c\u53bb\u94a0\u5316\u5faa\u73af\u4e2d\uff0c\u76f8\u5bf9\u4e8e\u5145\u653e\u7535\u66f2\u7ebf\u7684XRD\u7b49\u9ad8\u7ebf\u56fe\uff1b<\/p>\n

(b-c) \u57280.8 V\u548c0.1 V\u7684\u94a0\u5316\u72b6\u6001\u4e0b\uff0cSFS\/C\u7684\u975e\u539f\u4f4dHRTEM\u53caSAED\u56fe\u50cf\uff1b<\/p>\n

(d-e) \u57281.4 V\u548c3.0 V\u7684\u53bb\u94a0\u5316\u72b6\u6001\u4e0b\uff0cSFS\/C\u7684\u975e\u539f\u4f4dHRTEM\u53caSAED\u56fe\u50cf\u3002<\/p>\n

\u56fe\u4e94<\/strong>\u00a0 SFS\/C<\/strong>\u4f18\u5f02\u500d\u7387\u6027\u80fd\u4e2d\u7684\u7535\u5bb9\u8d21\u732e\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

(a) SFS\/C\u57280.2 ~ 10.0 mV\/s\u626b\u63cf\u901f\u7387\u4e0b\uff0cSFS\/C\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

(b) \u5728\u7279\u5b9a\u5cf0\u503c\u901f\u7387\u4e0b\uff0clog i vs log v\u7684\u5173\u7cfb\u66f2\u7ebf\uff1b<\/p>\n

(c) \u57281.0 mV\/s\u4e0b\uff0cCV\u66f2\u7ebf\u4e2d\u7684\u7535\u5bb9\u8d21\u732e\uff1b<\/p>\n

(d) \u4e0d\u540c\u626b\u63cf\u901f\u7387\u4e0b\uff0cSFS\/C\u7535\u6781\u7684\u7535\u5bb9\u8d21\u732e\u6bd4\u4f8b\u67f1\u72b6\u56fe\u5bf9\u6bd4\uff1b<\/p>\n

(e, f) Sb2<\/sub>S3<\/sub>\u3001 SFS\u548cSFS\/C\u7684\u80fd\u594e\u65af\u7279\u66f2\u7ebf\u53caZ\u2019\u548c\u03c9-1\/2<\/sup>\u7684\u7ebf\u6027\u5173\u7cfb\u66f2\u7ebf\u3002<\/p>\n

\u56fe\u516d<\/strong>\u00a0 DFT<\/strong>\u8ba1\u7b97\u6a21\u62df\u7ed3\u679c\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

(a-e) \u8ba1\u7b97\u7684TDOS\u3001\u754c\u9762\u5904\u7684\u7535\u5b50\u5bc6\u5ea6\u5dee\u5206\u56fe\u4ee5\u53ca\u5728\u6700\u7a33\u5b9a\u7684\u5438\u9644\u6784\u578b\u4e0bNa2<\/sub>S\u7684\u7ed3\u5408\u80fd\uff1aSFS\/C\uff08a, c, e\uff09, Sb2<\/sub>S3<\/sub>\uff08b, d, e\uff09\uff1b<\/p>\n

(f) \u957f\u671f\u5145\u653e\u7535\u5faa\u73af\u540e\uff0cSb2<\/sub>S3<\/sub>\u3001 SFS\u548cSFS\/C\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

(g, h) \u57280.5 A\/g\u7684\u7535\u6d41\u5bc6\u5ea6\u4e0b\uff0cSFS\/C\u7ecf\u8fc7100\u6b21\u5145\u653e\u7535\u5faa\u73af\u540e\u7684TEM\u53caEDS\u5143\u7d20\u5206\u5e03\u56fe\u50cf\u3002<\/p>\n

\u3010\u5c0f\u7ed3<\/strong>\u3011<\/p>\n

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\u539f\u6587\u94fe\u63a5\uff1a<\/strong>Bimetallic Sulfide Sb2<\/sub>S3<\/sub>@FeS2<\/sub> Hollow Nanorods as High-Performance Anode Materials for Sodium-Ion Batteries<\/a> (ACS Nano<\/em>, 2020, DOI: 10.1021\/acsnano.0c00020)<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba \u6df1\u6d77\u4e07\u91cc \u4f9b\u7a3f\u3002<\/p>\n

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