{"id":208100,"date":"2020-09-10T06:34:05","date_gmt":"2020-09-09T22:34:05","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=208100"},"modified":"2020-09-09T20:34:15","modified_gmt":"2020-09-09T12:34:15","slug":"%e8%b7%9f%e7%9d%80%e9%a1%b6%e5%88%8a%e5%ad%a6%e6%b5%8b%e8%af%95%ef%bd%9c%e7%87%95%e5%b1%b1%e5%a4%a7%e5%ad%a6%e9%bb%84%e5%bb%ba%e5%ae%87%e6%95%99%e6%8e%88acs-energy-letters%ef%bc%9a%e7%94%a8etem-afm","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=208100","title":{"rendered":"\u8ddf\u7740\u9876\u520a\u5b66\u6d4b\u8bd5\uff5c\u71d5\u5c71\u5927\u5b66\u9ec4\u5efa\u5b87\u6559\u6388ACS Energy Letters\uff1a\u7528ETEM-AFM\u5e73\u53f0\u539f\u4f4d\u89c2\u5bdf\u94a0\u679d\u6676\u751f\u957f\u53ca\u540c\u6b65\u529b\u5b66\u6027\u80fd\u6d4b\u91cf"},"content":{"rendered":"<p>\u94a0\u91d1\u5c5e\u7535\u6c60\uff08SMB\uff09\u4f5c\u4e3a\u9502\u91d1\u5c5e\u7535\u6c60\uff08LMB\uff09\u7684\u66ff\u4ee3\u54c1\uff0c\u56e0\u5176\u6bd4\u5bb9\u91cf\u9ad8\u3001Na\u4f9b\u5e94\u4e30\u5bcc\u3001\u6210\u672c\u4f4e\u7b49\u4f18\u70b9\uff0c\u8fd1\u5e74\u6765\u5907\u53d7\u5173\u6ce8\u3002\u4e0eLi\u7c7b\u4f3c\uff0cNa\u4ee5\u6811\u679d\u72b6\u7684\u5f62\u5f0f\u6c89\u79ef\u5728SMB\u7535\u6c60\u4e2d\u9020\u6210\u77ed\u8def\uff0c\u963b\u788d\u4e86\u9ad8\u6027\u80fdSMB\u7535\u6c60\u7684\u53d1\u5c55\u3002\u6587\u732e\u4e2d\u5bf9Li\u679d\u6676\u751f\u957f\u6216\u6c89\u79ef\u7684\u673a\u7406\u8fdb\u884c\u4e86\u5e7f\u6cdb\u7684\u7814\u7a76\u3002\u7136\u800c\uff0c\u5bf9\u94a0\u679d\u6676\u751f\u957f\u6216\u94a0\u6c89\u79ef\u7684\u7814\u7a76\u5374\u5f88\u5c11\u3002\u76ee\u524d\u5bf9Na\u6c89\u79ef\u7684\u5149\u8c31\u5b66\u7814\u7a76\u5f88\u5c11\uff0c\u4e3b\u8981\u7814\u7a76\u7684\u662f\u5728\u7535\u89e3\u6db2\u4e2d\u5f62\u6210\u5177\u6709\u6839\u7cfb\u751f\u957f\u673a\u5236\u7684\u6811\u679d\u72b6Na\u6c89\u79ef\u3002\u6700\u8fd1\u7684\u51e0\u9879\u7814\u7a76\u90fd\u63ed\u793a\u4e86\u94a0\u662f\u5982\u4f55\u5728\u5168\u56fa\u6001SMB\u4e2d\u6c89\u79ef\u6216\u751f\u957f\u7684\u3002Fincher\u7b49\u4eba\u901a\u8fc7\u7ed3\u5408\u4f53\u538b\u7f29\u3001\u663e\u5fae\u786c\u5ea6\u548c\u7eb3\u7c73\u538b\u75d5\u8bd5\u9a8c\uff0c\u7cfb\u7edf\u5730\u7814\u7a76\u4e86\u5927\u5757Na\u5728\u5ba4\u6e29\u4e0b\u7684\u529b\u5b66\u6027\u80fd\u3002\u4ed6\u4eec\u62a5\u544a\u7684\u6768\u6c0f\u6a21\u91cf\u7ea6\u4e3a3.9 GPa\uff0c8%\u5e94\u53d8\u4e0b\u7684\u6d41\u52a8\u5e94\u529b\u57280.1 ~ 0.25 MPa\u4e4b\u95f4\u53d8\u5316\uff0c\u5e94\u53d8\u901f\u7387\u57280.01 ~ 1% s<sup>-1<\/sup>\u4e4b\u95f4\uff0c\u5fae\u786c\u5ea6\u57281.1 ~ 1.6 MPa\u4e4b\u95f4\u3002\u4ed6\u4eec\u7684\u7814\u7a76\u8868\u660e\uff0c\u94a0\u91d1\u5c5e\u975e\u5e38\u67d4\u8f6f\uff0c\u5bb9\u6613\u8815\u52a8\uff0c\u5e76\u8868\u73b0\u51fa\u660e\u663e\u7684\u5c3a\u5bf8\u6548\u5e94\u3002\u8fd9\u4e9b\u7ed3\u679c\u4e3a\u7406\u89e3\u5b8f\u89c2\u548c\u5fae\u5c3a\u5ea6\u94a0\u7684\u529b\u5b66\u884c\u4e3a\u63d0\u4f9b\u4e86\u91cd\u8981\u4f9d\u636e\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-208101 size-full\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2020\/08\/\u56fe\u72471-29.png\" alt=\"\" width=\"600\" height=\"209\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2020\/08\/\u56fe\u72471-29.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2020\/08\/\u56fe\u72471-29-300x105.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u8fd1\u65e5\uff0c\u71d5\u5c71\u5927\u5b66<strong><b>\u9ec4\u5efa\u5b87<\/b><\/strong>\u6559\u6388\u56e2\u961f\u4ee5\u201cIn situ observation of sodium dendrite growth and concurrent\u00a0mechanical property measurements using an ETEM-AFM platform\u201d\u4e3a\u9898\u5728<em><i>ACS Energy Lett.<\/i><\/em>\u671f\u520a\u4e0a\u53d1\u8868\u91cd\u8981\u7814\u7a76\u6210\u679c\u3002\u8be5\u56e2\u961f\u5229\u7528\u73af\u5883\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c-\u539f\u5b50\u529b\u663e\u5fae\u955c\u5e73\u53f0\u4e0e\u673a\u68b0\u6027\u80fd\u6d4b\u91cf\u540c\u65f6\u5bf9\u94a0\u679d\u6676\u751f\u957f\u7684\u5b9e\u65f6\u7279\u5f81\u8fdb\u884c\u8868\u5f81\u3002\u539f\u4f4d\u7535\u9540\u4ea7\u751f\u7684\u94a0\u6c89\u79ef\u4e0e\u8584\u7684Na<sub>2<\/sub>CO<sub>3<\/sub>\u8868\u9762\u5c42\u7a33\u5b9a\u3002\u8fd9\u4e9b\u94a0\u679d\u6676\u7684\u7279\u5f81\u5c3a\u5bf8\u4e3a\u51e0\u767e\u7eb3\u7c73\uff0c\u5448\u73b0\u51fa\u4e0d\u540c\u7684\u5f62\u6001\uff0c\u5305\u62ec\u7eb3\u7c73\u68d2\u3001\u591a\u9762\u4f53\u7eb3\u7c73\u6676\u548c\u7eb3\u7c73\u7403\u3002\u539f\u4f4d\u529b\u5b66\u6d4b\u8bd5\u8868\u660e\uff0c\u8868\u9762\u6709Na<sub>2<\/sub>CO<sub>3<\/sub>\u7684Na\u679d\u6676\u7684\u6297\u538b\u5f3a\u5ea6\u548c\u62c9\u4f38\u5f3a\u5ea6\u572836 MPa\uff5e203 MPa\u4ee5\u4e0a\uff0c\u8fdc\u5927\u4e8eNa\u91d1\u5c5e\u3002\u5728\u8fc7\u7535\u4f4d\u548c\u673a\u68b0\u7ea6\u675f\u8054\u5408\u4f5c\u7528\u4e0b\uff0c\u94a0\u679d\u6676\u7684\u539f\u4f4d\u751f\u957f\u53ef\u4ee5\u4ea7\u751f\u9ad8\u7684\u5e94\u529b\u3002\u8fd9\u4e9b\u7ed3\u679c\u4e3aNa\u679d\u6676\u7684\u7535\u5316\u5b66\u548c\u529b\u5b66\u884c\u4e3a\u63d0\u4f9b\u4e86\u65b0\u7684\u57fa\u7840\u6570\u636e\uff0c\u5bf9Na\u91d1\u5c5e\u7535\u6c60\u5411\u5b9e\u9645\u50a8\u80fd\u5e94\u7528\u7684\u53d1\u5c55\u5177\u6709\u4e00\u5b9a\u7684\u6307\u5bfc\u610f\u4e49\u3002<\/p>\n<p>\u76ee\u524d\u4e3a\u6b62\uff0c\u7531\u4e8e\u5236\u5907\u9002\u5408\u4e8e\u7eb3\u7c73\u529b\u5b66\u6d4b\u8bd5\u7684\u6837\u54c1\u7684\u6280\u672f\u56f0\u96be\uff0c\u76ee\u524d\u8fd8\u6ca1\u6709\u5bf9\u56fa\u4f53\u7535\u89e3\u8d28\u754c\u9762\uff08SEI\uff09\u7a33\u5b9a\u7684\u7eb3\u7c73\u7ea7Na\u9540\u5c42\u7684\u751f\u957f\u548c\u529b\u5b66\u884c\u4e3a\u8fdb\u884c\u76f4\u63a5\u8868\u5f81\u3002\u8fd9\u6837\u7684\u8868\u5f81\u5bf9\u4e8e\u7406\u89e3Na\u679d\u6676\u548c\u76f8\u5173SEI\u5728\u5faa\u73af\u8fc7\u7a0b\u4e2d\u7684\u7535\u5316\u5b66\u673a\u68b0\u54cd\u5e94\u662f\u5fc5\u4e0d\u53ef\u5c11\u7684\uff0c\u4ece\u800c\u51cf\u7f13\u94a0\u679d\u6676\u5411\u9ad8\u6027\u80fdSMB\u7684\u53d1\u5c55\u3002\u5728\u8fd9\u91cc\uff0c\u4f5c\u8005\u521b\u5efa\u4e86\u4e00\u79cd\u65b0\u9896\u7684\u5168\u56fa\u6001\u7535\u5316\u5b66\u88c5\u7f6e\uff0c\u5305\u62ec\u4e00\u4e2aNa\u91d1\u5c5e\u9633\u6781\u3001\u4e00\u4e2aNa<sub>2<\/sub>CO<sub>3<\/sub>\u7535\u89e3\u8d28\u548c\u78b3\u7eb3\u7c73\u7ba1\u9634\u6781\u76f8\u8fde\u7684\u539f\u5b50\u529b\u663e\u5fae\u955c(AFM)\uff0c\u5b83\u662f\u5728\u4e8c\u6c27\u5316\u78b3\u6c14\u6c1b\u4e2d\u7578\u53d8\u7ea0\u6b63\u73af\u5883\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c(ETEM,\u56fe1a-d)\u4e2d\u64cd\u4f5c\u3002\u8fd9\u79cd\u7535\u5316\u5b66\u88c5\u7f6e\uff08\u7b80\u79f0ETEMAFM\uff09\u4e0d\u4ec5\u53ef\u4ee5\u5bf9Na\u7684\u7535\u5316\u5b66\u9540\u5c42\u8fdb\u884c\u539f\u4f4d\u89c2\u5bdf\uff0c\u800c\u4e14\u8fd8\u53ef\u4ee5\u5b9e\u65f6\u6d4b\u91cf\u7eb3\u7c73\u7ea7Na\u7684\u673a\u68b0\u6027\u80fd\uff0c\u4ece\u800c\u6709\u52a9\u4e8eNa<sub>2<\/sub>CO<sub>3<\/sub>\u8868\u9762\u5c42\u7a33\u5b9a\u7684Na\u6c89\u79ef\u540c\u65f6\u8fdb\u884c\u7535\u5316\u5b66\u673a\u68b0\u7279\u5f81\u63cf\u8ff0\u3002<\/p>\n<p><strong><b>\u56fe1. \u7528\u4e8e<\/b><\/strong><strong><b>Na\u679d\u6676\u539f\u4f4d\u7814\u7a76\u7684ETEM-AFM\u88c5\u7f6e\u793a\u610f\u56fe<\/b><\/strong><strong><b>\u4ee5\u53ca\u5176\u8868\u5f81<\/b><\/strong><strong><b>\u3002<\/b><\/strong><\/p>\n<p><strong><b><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-208102 size-full\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2020\/08\/\u56fe\u72472-28.png\" alt=\"\" width=\"600\" height=\"781\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2020\/08\/\u56fe\u72472-28.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2020\/08\/\u56fe\u72472-28-230x300.png 230w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/b><\/strong><\/p>\n<p>\u4f5c\u8005\u5728\u5b9e\u9a8c\u4e2d\u7684\u5927\u591a\u6570Na\u679d\u6676\u6cbf[001]\u65b9\u5411\u751f\u957f\uff08\u56fe2a-h\uff09\uff0c\u5c11\u6570\u679d\u6676\u6cbf[110]\uff08\u56fe2i-j\uff09\u548c[112]\uff08\u56fe2k-l\uff09\u751f\u957f\u3002\u8fd9\u4e9b\u7ed3\u679c\u8868\u660e\uff0c\u91c7\u7528\u73b0\u6709\u7684\u7535\u5316\u5b66\u7535\u9540\u65b9\u6cd5\u53ef\u4ee5\u5f88\u5bb9\u6613\u5730\u4ea7\u751fNa\u679d\u6676\u3002\u5916\u52a0\u7535\u538b\u662f\u63a7\u5236\u6c89\u79efNa\u679d\u6676\u5f62\u8c8c\u7684\u4e00\u4e2a\u91cd\u8981\u53c2\u6570\u3002\u5982\u56fe2m-t\u6240\u793a\uff0c\u4e00\u4e2a\u5c0f\u7684\u591a\u9762Na\u7eb3\u7c73\u6676\u4f53\u751f\u957f\u5728\u4e00\u4e2a\u5927\u7684\u591a\u9762Na\u7eb3\u7c73\u6676\u4f53\u4e0a\uff08\u56fe2m-o\uff09\u3002\u5f53\u5728CNT\u548cNa\u91d1\u5c5e\u4e4b\u95f4\u65bd\u52a0\u9ad8\u7684\u5916\u504f\u538b\uff08-5.0 V\uff09\u65f6\uff0c\u679d\u6676\u4e3b\u8981\u6cbf\u4e00\u4e2a\u65b9\u5411\uff08\u56fe2o\u4e2d\u7684\u767d\u8272\u7bad\u5934\u6240\u793a\uff09\u9ad8\u901f\u751f\u957f\uff0c\u5448\u73b0\u51fa\u7ec6\u957f\u7684\u679d\u6676\u5f62\u6001\u3002\u5f53\u65bd\u52a0-1.0\u6216-0.5 V\u7684\u4f4e\u7535\u4f4d\u65f6\uff0c\u679d\u6676\u4ee5\u7f13\u6162\u7684\u901f\u5ea6\u5411\u5404\u4e2a\u65b9\u5411\u751f\u957f\uff08\u56fe2q\u4e2d\u7684\u767d\u8272\u7bad\u5934\uff09\u3002\u5f53\u7535\u4f4d\u518d\u6b21\u5347\u9ad8\u5230-3.5 V\u65f6\uff0cNa\u679d\u6676\u6cbf\u4e00\u4e2a\u65b9\u5411\uff08\u56fe2s\u4e2d\u7684\u767d\u8272\u7bad\u5934\uff09\u8f6c\u53d8\u4e3a\u4f18\u52bf\u751f\u957f\uff0c\u8868\u660e\u751f\u957f\u6a21\u5f0f\u53ef\u4ee5\u7531\u7535\u538b\u63a7\u5236\u3002<\/p>\n<p><strong><b>\u56fe2<\/b><\/strong><strong><b>.<\/b><\/strong><strong><b>\u00a0\u65f6\u95f4\u63a8\u79fb\u7684<\/b><\/strong><strong><b>TEM\u56fe\u50cf\u663e\u793a\u4e86\u94a0\u679d\u6676\u751f\u957f<\/b><\/strong><strong><b>\u7684\u8fc7\u7a0b\u3002<\/b><\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-208103 size-full\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2020\/08\/\u56fe\u72473-28.png\" alt=\"\" width=\"600\" height=\"673\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2020\/08\/\u56fe\u72473-28.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2020\/08\/\u56fe\u72473-28-267x300.png 267w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u4f5c\u8005\u5bf9\u6c89\u79ef\u7684Na\u679d\u6676\u8fdb\u884c\u539f\u4f4d\u538b\u7f29\u6216\u62c9\u4f38\u52a0\u8f7d\u4ee5\u6d4b\u91cf\u5176\u529b\u5b66\u6027\u80fd\u3002\u56fe3\u663e\u793a\u4e86Na\u6811\u7a81\u7684\u539f\u4f4d\u538b\u7f29\u3002\u968f\u7740Na\u91d1\u5c5e\u7535\u6781\u5c06\u6811\u7a81\u5411\u4e0a\u63a8\uff0cAFM\u60ac\u81c2\u4e5f\u968f\u4e4b\u5411\u4e0a\u79fb\u52a8(\u56fe3a)\u3002\u7531\u4e8eAFM\u60ac\u81c2\u6881\u7684\u529b\u5e38\u6570k\u5df2\u7ecf\u5df2\u77e5\uff0c\u4e14\u7531AFM\u60ac\u81c2\u6881\u7684\u4f4d\u79fb\u53ef\u77e5, \u65bd\u52a0\u5728AFM\u60ac\u81c2\u4e0a\u7684\u529b(F)\u53ef\u4ee5\u4ece\u80e1\u514b\u5b9a\u5f8b\u8ba1\u7b97F = k\u00d7\u0394X, 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srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2020\/08\/\u56fe\u72474-24.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2020\/08\/\u56fe\u72474-24-259x300.png 259w\" sizes=\"(max-width: 600px) 100vw, 600px\" 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property measurements using an ETEM-AFM platform,\u00a0<strong><em><b><i>ACS Energy Lett. <\/i><\/b><\/em><\/strong>2020. 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