{"id":214678,"date":"2020-12-19T06:30:22","date_gmt":"2020-12-18T22:30:22","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=214678"},"modified":"2020-12-18T22:02:44","modified_gmt":"2020-12-18T14:02:44","slug":"advanced-science-rurh%e5%8f%8c%e9%87%91%e5%b1%9e%e7%ba%b3%e7%b1%b3%e7%8e%af%e9%ab%98%e6%95%88%e5%88%b6%e6%b0%a2","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=214678","title":{"rendered":"Advanced Science: RuRh\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u9ad8\u6548\u5236\u6c22"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u94c2\uff08Pt\uff09\u662f\u76ee\u524d\u5728\u6790\u6c22\u53cd\u5e94\uff08HER\uff09\u9886\u57df\u5185\u4f7f\u7528\u6700\u5e7f\u6cdb\u7684\u50ac\u5316\u5242\u3002\u7136\u800c\uff0c\u94c2\u9762\u4e34\u7740\u7a00\u7f3a\u3001\u9ad8\u6210\u672c\u95ee\u9898\u3002\u7814\u7a76\u4eba\u5458\u6b63\u5728\u63a2\u7d22\u7ecf\u6d4e\u6709\u6548\u7684\u5176\u4ed6\u50ac\u5316\u5242\u6765\u66ff\u4ee3Pt\uff0c\u5176\u4e2d\u6700\u6709\u6548\u7684\u7b56\u7565\u662f\u589e\u52a0\u975ePt\u8d35\u91d1\u5c5e\u50ac\u5316\u5242\u7684\u6d3b\u6027\u4f4d\u70b9\u3002\u5e38\u7528\u7684\u65b9\u6cd5\u6709\u5408\u91d1\u5316\u3001\u4fee\u9970\u6676\u76f8\u53ca\u5f15\u5165\u72ec\u7279\u7684\u7eb3\u7c73\u7ed3\u6784\uff08\u7eb3\u7c73\u819c\u3001\u7eb3\u7c73\u7247\/\u7eb3\u7c73\u7ebf\u3001\u591a\u5b54\/\u6742\u4ea4\u7eb3\u7c73\u6750\u6599\u7b49\uff09\u7b49\u3002\u4e8b\u5b9e\u4e0a\uff0c\u901a\u8fc7\u754c\u9762\u5de5\u7a0b\uff08\u5982\u914d\u4f53\u548c\u6676\u683c\u5e94\u53d8\u6548\u5e94\uff09\u6253\u7834\u53cc\u91d1\u5c5e\u50ac\u5316\u5242\u7684\u5bf9\u79f0\u6027\uff0c\u6539\u53d8\u53cd\u5e94\u4e2d\u95f4\u4f53\u7684\u5438\u9644\u72b6\u6001\uff0c\u53ef\u5f71\u54cd\u53cc\u91d1\u5c5e\u50ac\u5316\u5242\u7684\u6574\u4f53\u6d3b\u6027\u3002\u7136\u800c\uff0c\u5927\u591a\u6570\u65b9\u6cd5\u90fd\u53ea\u80fd\u5728\u5c40\u90e8\u533a\u57df\u8c03\u8282\u50ac\u5316\u5242\u7684\u8868\u9762\u5438\u9644\u80fd\uff0c\u800c\u4e0d\u80fd\u6574\u4f53\u8c03\u8282\u50ac\u5316\u5242\u7684\u6d3b\u6027\u4f4d\u70b9\u3002\u6b64\u5916\uff0c\u53ef\u63a7\u5408\u6210\u53cc\u91d1\u5c5e\u7eb3\u7c73\u6676\u7684\u8fc7\u7a0b\u4e2d\uff0c\u53cc\u91d1\u5c5e\u539f\u5b50\u4ea4\u66ff\u6392\u5217\u53ef\u5bfc\u81f4\u5bf9\u79f0\u6027\u7834\u7f3a\uff0c\u8fdb\u800c\u5c40\u90e8\u7535\u8377\u8fc7\u5269\uff0c\u4ece\u800c\u8fdb\u4e00\u6b65\u50ac\u5316\u6027\u80fd\u3002\u7136\u800c\uff0c\u76f8\u5173\u7684\u7814\u7a76\u62a5\u9053\u8f83\u5c11\u3002<\/p>\n

\u7814\u7a76\u8868\u660e\uff0c\u948c\uff08Ru\uff09\u8868\u73b0\u51fa\u4e0ePt\u7c7b\u4f3c\u7684\u6c22\u952e\u80fd\uff0c\u4f46\u4ef7\u683c\u6bd4\u53ea\u6709\u4e0d\u5230Pt\u7684\u5341\u5206\u4e4b\u4e00\uff0c\u4f7fRu\u6210\u4e3a\u7406\u60f3\u7684\u975ePt\u6790\u6c22\u50ac\u5316\u5242\u4e4b\u4e00\u3002\u7136\u800c\uff0cRu\u5728\u78b1\u6027\u4ecb\u8d28\u4e2d\u7684\u6c34\u89e3\u80fd\u529b\u5f31\u3002\u8fd1\u5e74\u6765\u7814\u7a76\u8868\u660e\uff0c\u8868\u9762\u7f3a\u9677\u5de5\u7a0b\u548c\u5408\u91d1\u5316\u53ef\u4ee5\u6709\u6548\u5730\u8bf1\u5bfc\u7535\u5b50\u4eceRu\u5185\u90e8\u8f6c\u79fb\u5230\u8868\u9762\uff0c\u66b4\u9732\u51fa\u66f4\u591a\u7684\u6d3b\u6027\u4f4d\u70b9\u3002\u6b64\u5916\uff0c\u4e0eRu\u6216\u94d1\uff08Rh\uff09\u5355\u91d1\u5c5e\u76f8\u6bd4\uff0c\u5728\u5404\u5411\u5f02\u6027\u7eb3\u7c73\u6676\u4e2d\uff0c\u5927\u591a\u6570Ru (Rh)\u57fa\u5408\u91d1\u5728\u6676\u754c\uff08GBs\uff09\u4e0a\u5b58\u5728\u626d\u66f2\u7684\u51e0\u4f55\u6784\u578b\uff0c\u6709\u5229\u4e8e\u7535\u50ac\u5316\u6d3b\u6027\u7684\u63d0\u9ad8\u3002\u540c\u65f6\uff0c\u8584\u7247\u72b6\u7ed3\u6784\u4f7f\u91d1\u5c5e\u5408\u91d1\u5177\u6709\u8f83\u5927\u7684\u7535\u5316\u5b66\u6d3b\u6027\u8868\u9762\u79ef\u548c\u8f83\u9ad8\u7684\u539f\u5b50\u5229\u7528\u7387\uff0c\u53ef\u8fdb\u4e00\u6b65\u50ac\u5316\u6027\u80fd\uff0c\u63d0\u9ad8\u6750\u6599\u7684\u8d28\u91cf\u6d3b\u6027\u3002\u867d\u7136Ru (Rh)\u57fa\u5408\u91d1\u7eb3\u7c73\u6676\u50ac\u5316\u5242\u5df2\u7ecf\u53d6\u5f97\u4e86\u4e00\u4e9b\u8fdb\u5c55\uff0c\u4f46\u7531\u4e8e\u7eb3\u7c73\u6676\u6676\u7c92\u8f83\u5927\uff0c\u800c\u4e14\u5176\u5149\u6ed1\u7684\u8868\u9762\u4e5f\u9650\u5236\u4e86\u6d3b\u6027\u4f4d\u70b9\u7684\u6570\u91cf\uff0c\u8868\u9762GBs\u7f3a\u9677\u4e5f\u963b\u788d\u4e86\u5176\u7a33\u5b9a\u6027\u3002\u56e0\u6b64\uff0c\u4f18\u5316Ru (Rh)\u57fa\u5408\u91d1\u8584\u7247\u72b6\u7ed3\u6784\u7684\u8868\u9762\u7f3a\u9677\u7ed3\u6784\uff0c\u7a33\u5b9a\u4e24\u4e2a\u76f8\u90bb\u5355\u4f53\u7684\u914d\u4f4d\u6548\u5e94\uff0c\u5bf9\u4e8e\u9ad8\u6027\u80fd\u50ac\u5316\u5242\u7684\u5236\u5907\u5177\u6709\u91cd\u8981\u610f\u4e49\u3002<\/p>\n

\u3010\u7814\u7a76\u8fdb\u5c55\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u5357\u4eac\u6653\u5e84\u5b66\u9662\u7684\u5218\u82cf\u8389\u6559\u6388\u548c\u6b66\u6c49\u7406\u5de5\u5927\u5b66\u6728\u58eb\u6625\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u5728advanced science<\/strong>\u4e0a\u53d1\u8868\u4e86\u4e00\u7bc7\u9898\u76ee\u4e3a\u201cRuRh Bimetallene Nanoring as High-efficiency pH-Universal Catalyst for Hydrogen Evolution Reaction\u201d\u7684\u6587\u7ae0\u3002\u8be5\u7814\u7a76\u5408\u6210\u4e86\u5177\u6709\u4e30\u5bcc\u7ed3\u6784\u7f3a\u9677\u7684RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\uff0c\u5e76\u5728-0.05 V\u548c-0.07 V\u4e0b\u8868\u73b0\u51fa\u8f83\u9ad8\u7684\u8d28\u91cf\u6d3b\u6027\u3002\u540c\u65f6\uff0c\u5728\u9178\u6027\u4ecb\u8d28\u4e2d\uff0c\u5373\u4f7f\u7ecf\u8fc73\u4e07\u4e2a\u7535\u4f4d\u5faa\u73af\uff0c\u5b83\u4ecd\u80fd\u4fdd\u6301\u7a33\u5b9a\u7684\u4ea7\u6c22\u53cd\u5e94\u3002\u6b64\u5916\uff0cRuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u5728\u78b1\u6027\u548c\u4e2d\u6027\u4ecb\u8d28\u4e2d\u5747\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u6d3b\u6027\uff0c\u4f18\u4e8ePt\u50ac\u5316\u5242\u548c\u5176\u4ed6\u62a5\u9053\u7684HER\u50ac\u5316\u5242\u3002\u7ed3\u5408\u5b9e\u9a8c\u6570\u636e\u5206\u6790\u548c\u5bc6\u5ea6\u6cdb\u51fd\u7406\u8bba\u8ba1\u7b97\u8868\u660e\uff0c\u5bf9\u79f0\u6027\u7834\u7f3a\u7684\u754c\u9762\u6548\u5e94\u548c\u8868\u9762\u7f3a\u9677\u5de5\u7a0b\u4e0d\u4ec5\u53ef\u4ee5\u524a\u5f31\u6c22\u539f\u5b50\u7684\u5438\u9644\u5f3a\u5ea6\uff0c\u800c\u4e14\u8fd8\u4fc3\u8fdb\u7535\u5b50\u7684\u8f6c\u79fb\u548c\u53cd\u5e94\u7269\u7684\u5438\u9644\uff0c\u8fdb\u4e00\u6b65\u63d0\u9ad8\u50ac\u5316\u6d3b\u6027\u3002<\/p>\n

\u3010\u56fe\u6587\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u56fe<\/strong>1<\/strong><\/p>\n

\"\"<\/p>\n

a) RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u50ac\u5316\u5242\u5408\u6210\u8fc7\u7a0b\u793a\u610f\u56fe\uff1b<\/p>\n

b) RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u7684HAADF-STEM\u56fe\uff1b<\/p>\n

c-e) RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u7684TEM\u56fe\uff1b<\/p>\n

f)\u5355\u4e2aRuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u7684mapping\u56fe\uff1b<\/p>\n

g) RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u7684XRD\u56fe\uff1b<\/p>\n

h, j) Ru 3p\u548cRh 3d RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u7684\u9ad8\u5206\u8fa8\u7387XPS\u5149\u8c31\u3002<\/p>\n

\u56fe<\/strong>2 <\/strong>\u50ac\u5316\u6027\u80fd\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

a, d, f) RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u3001Ru\u3001Rh\u548c\u5546\u7528Pt\u5728 0.5 M H2<\/sub>SO4<\/sub>\u30011.0 M KOH\u548c1.0 M PBS\u4e2d\u7684\u7ebf\u6027\u626b\u63cf\u56fe\uff1b<\/p>\n

b, e, g) RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u3001Ru\u3001Rh\u548c\u5546\u7528Pt\u5728 0.5 M H2<\/sub>SO4<\/sub>\u30011.0 M KOH\u548c1.0 M PBS\u4e2d\u7684\u5854\u83f2\u5c14\u659c\u7387\u56fe\uff1b<\/p>\n

c) RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u3001Ru\u3001Rh\u548c\u5546\u7528Pt\u5728\u8fc7\u7535\u4f4d\u4e3a50 mV\u548c70 mV\u4e0b\u8d35\u91d1\u5c5e\u7684\u8d28\u91cf\u6d3b\u6027\uff1b<\/p>\n

h, i) RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u5728 0.5 M H2<\/sub>SO4<\/sub>\u548c1.0 M KOH\u4e0b\u7684\u7a33\u5b9a\u6027\u6d4b\u8bd5\u3002\u00a0<\/strong><\/p>\n

\u56fe<\/strong>3 <\/strong>\u50ac\u5316\u6027\u80fd\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

a, c) \u57280.5 M H2<\/sub>SO4<\/sub>\u548c1.0 M KOH\u6eb6\u6db2\u4e2d\uff0c\u5404\u79cd\u626b\u63cf\u901f\u7387\u7684\u5faa\u73af\u4f0f\u5b89\u56fe\uff1b<\/p>\n

b, d) a, c\u56fe\u4e2d\u7684\u63d0\u53d6\u7684\u6570\u636e\u66f2\u7ebf\uff1b<\/p>\n

e, f) Ru\u548cRh\u5206\u522b\u57280.5 M H2<\/sub>SO4<\/sub>\u548c1.0 M KOH\u4e2d\u7684\u7535\u5316\u5b66\u963b\u6297\u8c31\u3002<\/p>\n

\u56fe<\/strong>4 <\/strong>\u7406\u8bba\u8ba1\u7b97<\/strong><\/p>\n

\"\"<\/p>\n

a, b) \u6c22\u5438\u9644\u7684\u81ea\u7531\u80fd\u56fe\u548c\u6c34\u89e3\u79bb\u80fd\uff1b<\/p>\n

c) \u6c34\u5206\u89e3\u7684\u6d3b\u5316\u80fd\u3002<\/p>\n

\u56fe<\/strong>5<\/strong>\u7406\u8bba\u8ba1\u7b97<\/strong><\/p>\n

\"\"<\/p>\n

a) RuRh2<\/sub>\u7684\u539f\u5b50\u6784\u578b\uff1b<\/p>\n

b, c) RuRh2<\/sub>\u8868\u9762Ru\u4f4d\u70b9\u548cRh\u4f4d\u70b9\u7684\u7535\u8377\u5bc6\u5ea6\u5dee\uff1b<\/p>\n

d-g) RuRh2<\/sub>\/Rh\uff08\u4e0e\u6676\u683c\u5e94\u53d8\u6548\u5e94\u76f8\u5173\uff09\u4f4d\u70b9\uff0cRuRh2<\/sub>\/Ru\uff08\u4e0e\u6676\u683c\u5e94\u53d8\u6548\u5e94\u76f8\u5173\uff09\u4f4d\u70b9\uff0cRuRh2<\/sub>\/Ru\u548cRuRh2<\/sub>\/Rh\u8868\u9762\u7684\u6001\u5bc6\u5ea6\u5206\u6790\uff1b<\/p>\n

h, i) RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u3001Ru\u3001Rh\u548c\u5546\u7528Pt\u7684\u6c34\u89e3\u79bb\u80fd\u548c\u6c22\u5438\u9644\u80fd\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u7efc\u4e0a\u6240\u8ff0\uff0c\u57fa\u4e8e\u5b9e\u9a8c\u6570\u636e\u5206\u6790\u548c\u5bc6\u5ea6\u6cdb\u51fd\u7406\u8bba\u7684\u8ba1\u7b97\u7ed3\u679c\u8868\u660e\uff0c\u7531\u5bf9\u79f0\u6027\u7834\u7f3a\u5bfc\u81f4\u7684\u6676\u683c\u5e94\u53d8\u6548\u5e94\u3001\u5408\u91d1\u6548\u5e94\u548c\u91cf\u5b50\u5c3a\u5bf8\u6548\u5e94\u5171\u540c\u4fc3\u6210\u7684\u8d85\u8584\u7eb3\u7c73\u73af\u53ef\u6709\u6548\u8c03\u8282\u6750\u6599\u7684\u7535\u5b50\u7ed3\u6784\u3002\u8fd9\u9879\u5de5\u4f5c\u901a\u8fc7\u7cbe\u51c6\u6784\u5efa\u5177\u6709\u5f3aH+<\/sup>\/H2<\/sub>O\u5438\u9644\u6027\u3001\u4f4e\u6c34\u79bb\u89e3\u52bf\u5792\u548c\u51e0\u4e4e\u96f6H*\u7ed3\u5408\u80fd\u7684\u7f3a\u9677\u754c\u9762\u7ed3\u6784\uff0c\u7814\u5236\u51fa\u4e86\u4e00\u79cd\u5bbdpH\u8303\u56f4\u5185\u8c03\u8282HER\u6d3b\u6027\u7684\u9ad8\u6548\u53cc\u91d1\u5c5e\u50ac\u5316\u5242\u3002\u8bbe\u8ba1\u7684RuRh2<\/sub>\u53cc\u91d1\u5c5e\u7eb3\u7c73\u73af\u50ac\u5316\u5242\u5177\u6709\u8d85\u4f4e\u8d77\u59cb\u7535\u4f4d\u3001\u9ad8\u50ac\u5316\u6d3b\u6027\u548c\u5728\u5168pH\u8303\u56f4\u5185\u7684\u4f18\u5f02\u7a33\u5b9a\u6027\u3002\u672c\u9879\u7814\u7a76\u8bc1\u660e\u4e86\u7f3a\u9677\u754c\u9762\u5de5\u7a0b\u53ef\u4ee5\u6781\u5927\u63d0\u9ad8\u50ac\u5316\u6027\u80fd\uff0c\u4e3a\u4eca\u540e\u9ad8\u6548\u6790\u6c22\u50ac\u5316\u5242\u7684\u8bbe\u8ba1\u4e0e\u6784\u7b51\u63d0\u4f9b\u4e86\u79d1\u5b66\u6307\u5bfc\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5<\/strong>:<\/strong> RuRh Bimetallene Nanoring as High-efficiency pH-Universal Catalyst for Hydrogen Evolution Reaction<\/a>, 2020, advanced science, doi: 10.1002\/advs.202002341<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u5218\u4e8e\u91d1\u7f16\u8bd1\u4f9b\u7a3f\u3002\u6b22\u8fce\u5927\u5bb6\u5230\u6750\u6599\u4eba\u5ba3\u4f20\u79d1\u6280\u6210\u679c\u5e76\u5bf9\u6587\u732e\u8fdb\u884c\u6df1\u5165\u89e3\u8bfb\uff0c\u6295\u7a3f\u90ae\u7bb1tougao@cailiaoren.com\u3002<\/p>\n

\u6750\u6599\u4eba\u6295\u7a3f\u4ee5\u53ca\u5185\u5bb9\u5408\u4f5c\u53ef\u52a0\u7f16\u8f91\u5fae\u4fe1\uff1acailiaokefu \u3002<\/p>\n

\u56e2\u961f\u4ecb\u7ecd<\/strong><\/p>\n

\u5218\u82cf\u8389\u6559\u6388\uff1a2014\u5e74\u516d\u6708\u83b7\u5f97\u5357\u4eac\u5e08\u8303\u5927\u5b66\u7406\u5b66\u535a\u58eb\u5b66\u4f4d\uff0c\u540c\u5e74\u8fdb\u5165\u5357\u4eac\u6653\u5e84\u5b66\u9662\u4efb\u6559\uff0c2019\u5e74\u81f32020\u5e74\uff0c\u5728\u6b66\u6c49\u7406\u5de5\u5927\u5b66\u6728\u58eb\u6625\u6559\u6388\u6750\u6599\u590d\u5408\u65b0\u6280\u672f\u56fd\u5bb6\u91cd\u70b9\u5b9e\u9a8c\u5ba4\u8fdb\u884c\u4e3a\u671f\u4e00\u5e74\u7684\u5b66\u672f\u8bbf\u95ee\u7814\u7a76\u3002\u4e3b\u8981\u4ece\u4e8b\u65b0\u80fd\u6e90\u6750\u6599\u3001\u71c3\u6599\u7535\u6c60\u5173\u952e\u6750\u6599\u3001\u7535\u5316\u5b66\u50ac\u5316\u5242\u7b49\u76f8\u5173\u9886\u57df\u7684\u7814\u7a76\u3002\u4ee5\u901a\u8baf\u4f5c\u8005\u6216\u7b2c\u4e00\u4f5c\u8005\u5728J. Am. Chem. Soc.\u3001Nano Energy\u3001J. Mater. Chem. A\u3001Appl. Catal. B-Environ.\u7b49\u56fd\u9645\u671f\u520a\u53d1\u8868SCI\u6838\u5fc3\u8bba\u658740\u4f59\u7bc7\u3002<\/p>\n

 <\/p>\n

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