{"id":216775,"date":"2021-01-27T06:20:10","date_gmt":"2021-01-26T22:20:10","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=216775"},"modified":"2021-01-26T18:20:20","modified_gmt":"2021-01-26T10:20:20","slug":"%e6%ae%b5%e9%95%b6%e9%94%8bnano-lett-%ef%bc%9a%e5%85%a8%e6%97%a0%e6%9c%ba%e5%8d%a4%e5%8c%96%e9%93%85%e9%92%99%e9%92%9b%e7%9f%bf%e8%96%84%e8%86%9c%e7%9a%84%e5%a4%a7%e9%9d%a2%e7%a7%af%e5%90%88%e6%88%90","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=216775","title":{"rendered":"\u6bb5\u9576\u950bNano Lett.\uff1a\u5168\u65e0\u673a\u5364\u5316\u94c5\u9499\u949b\u77ff\u8584\u819c\u7684\u5927\u9762\u79ef\u5408\u6210\u4e0e\u56fe\u6848\u5316\u53ca\u5176\u5f02\u8d28\u7ed3\u6784"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n

\u7532\u57fa\u94f5\u5364\u5316\u94c5\u9499\u949b\u77ff\u56e0\u5176\u5728\u5149\u4f0f\u9886\u57df\u7684\u4f18\u5f02\u6027\u80fd\u800c\u5f15\u8d77\u4e86\u5e7f\u6cdb\u7684\u7814\u7a76\u5174\u8da3\uff0c\u5355\u7247\u592a\u9633\u80fd\u7535\u6c60\u7684\u8ba4\u8bc1\u529f\u7387\u8f6c\u6362\u6548\u7387\u5728\u77ed\u77ed\u51e0\u5e74\u5185\u5c31\u8fc5\u901f\u4e0a\u5347\u523025.2%\u3002\u5c3d\u7ba1\u53d6\u5f97\u4e86\u8fd9\u4e00\u975e\u51e1\u7684\u8fdb\u5c55\uff0c\u4f20\u7edf\u7684\u6df7\u5408\u9499\u949b\u77ff\u57fa\u5668\u4ef6\u7ecf\u5e38\u53d7\u5230\u73af\u5883\u7a33\u5b9a\u6027\u5dee\u7684\u56f0\u6270\u3002\u6700\u8fd1\u7684\u7814\u7a76\u8868\u660e\uff0c\u7528\u65e0\u673a\u9633\u79bb\u5b50\u4ee3\u66ff\u6709\u673a\u9633\u79bb\u5b50\u5236\u5907\u6df7\u5408\u9633\u79bb\u5b50\u9499\u949b\u77ff\u6216\u5168\u65e0\u673a\u9499\u949b\u77ff\u53ef\u80fd\u6709\u52a9\u4e8e\u5e94\u5bf9\u8fd9\u4e00\u6311\u6218\uff0c\u5e76\u663e\u8457\u63d0\u9ad8\u7a33\u5b9a\u6027\u3002\u5c3d\u7ba1\u4eba\u4eec\u5df2\u7ecf\u4e3a\u5408\u6210\u5355\u6676\u5fae\u7ed3\u6784\u548c\u5168\u65e0\u673a\u9499\u949b\u77ff\u7684\u8fde\u7eed\u8584\u819c\u4ed8\u51fa\u4e86\u5de8\u5927\u52aa\u529b\uff0c\u4f46\u5bf9\u4e8e\u5408\u6210\u539a\u5ea6\u5728100 nm-1\u03bcm\u7684\u9ad8\u8d28\u91cf\u5355\u6676\u8584\u819c\u4ee5\u53ca\u5728\u4e0d\u540c\u4f4d\u7f6e\u5177\u6709\u4e0d\u540c\u5316\u5b66\u6210\u5206\u548c\u7535\u5b66\u6027\u80fd\u7684\u5f02\u8d28\u7ed3\u6784\u7684\u63a2\u7d22\u8981\u5c11\u5f97\u591a\uff0c\u800c\u8fd9\u5bf9\u4e8e\u63a2\u7d22\u8fd9\u7c7b\u65b0\u578b\u6750\u6599\u5177\u6709\u7279\u5b9a\u529f\u80fd\u7684\u5149\u7535\u5e94\u7528\u81f3\u5173\u91cd\u8981\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u7f8e\u56fd\u52a0\u5dde\u5927\u5b66\u6d1b\u6749\u77f6\u5206\u6821\u6bb5\u9576\u950b\u6559\u6388<\/b><\/strong>\uff08\u901a\u8baf\u4f5c\u8005\uff09<\/b><\/strong>\u56e2\u961f\u62a5\u9053\u4e86\u5927\u9762\u79ef\u751f\u957f\u7684\u5355\u6676\u5168\u65e0\u673a\u9499\u949b\u77ff\u8584\u819c\uff0c\u5e76\u57fa\u4e8e\u8be5\u8584\u819c\u8fdb\u4e00\u6b65\u5f62\u6210\u5f02\u8d28\u7ed3\u6784\u9635\u5217\u3002\u7814\u7a76\u8868\u660e\uff0c\u9ad8\u5ea6\u4e00\u81f4\u53d6\u5411\u7684CsPbBr3<\/sub>\u5fae\u6676\u7574\u53ef\u4ee5\u5f88\u5bb9\u6613\u5730\u751f\u957f\u5728\u5177\u6709\u660e\u786e\u5916\u5ef6\u5173\u7cfb\u7684\u767d\u4e91\u6bcd\u886c\u5e95\u4e0a\u3002\u5fae\u6676\u7574\u53ef\u4ee5\u8fdb\u4e00\u6b65\u6269\u5c55\u5e76\u6700\u7ec8\u5408\u5e76\u6210\u5177\u6709\u4f18\u826f\u5149\u5b66\u8d28\u91cf\u7684\u5927\u9762\u79ef\u5355\u6676CsPbBr3<\/sub>\u8584\u819c\u3002\u8fdb\u4e00\u6b65\u7814\u7a76\u53d1\u73b0\uff0c\u5229\u7528\u9009\u62e9\u6027\u9634\u79bb\u5b50\u4ea4\u6362\u5de5\u827a\uff0c\u56fe\u6848\u5316\u53ef\u4ee5\u5728\u5927\u9762\u79ef\u7684CsPbBr3<\/sub>\u8584\u819c\u4e0a\u8fdb\u884c\uff0c\u5e76\u6700\u7ec8\u9009\u62e9\u6027\u5730\u5c06CsPbBr3<\/sub>\u8f6c\u5316\u4e3aCsPbI3<\/sub>\uff0c\u4ece\u800c\u5f62\u6210\u5177\u6709\u7a7a\u95f4\u8c03\u5236\u5149\u81f4\u53d1\u5149\u548c\u8868\u89c2\u7535\u6d41\u6574\u6d41\u884c\u4e3a\u7684CsPbBr3<\/sub>-CsPbI3<\/sub>\u6a2a\u5411\u5f02\u8d28\u7ed3\u6784\u9635\u5217\u3002\u5927\u9762\u79efCsPbBr3<\/sub>\u5355\u6676\u8584\u819c\u7684\u5236\u5907\u548c\u5f02\u8d28\u7ed3\u6784\u9635\u5217\u7684\u6784\u5efa\uff0c\u4e3a\u91d1\u5c5e\u5364\u5316\u7269\u9499\u949b\u77ff\u5149\u7535\u6027\u80fd\u7684\u57fa\u7840\u7814\u7a76\u548c\u6f5c\u5728\u5e94\u7528\u5960\u5b9a\u4e86\u575a\u5b9e\u7684\u6750\u6599\u5e73\u53f0\u3002\u8be5\u6210\u679c\u4ee5\u9898\u4e3a\u201cLarge-Area Synthesis and Patterning of All-Inorganic Lead Halide Perovskite Thin Films and Heterostructures\u201d<\/b><\/strong>\u53d1\u8868\u5728\u4e86Nano Lett<\/b><\/strong>ers<\/b><\/strong>\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/b><\/strong><\/p>\n

\u56fe1 \u751f\u957f\u5728\u767d\u4e91\u6bcd\u4e0a\u7684CsPbBr<\/b><\/strong>3<\/b><\/sub><\/strong>\u8584\u819c\u7684\u8868\u5f81<\/b><\/strong>\"\"<\/p>\n

(a) CsPbBr3<\/sub>\u8584\u819c\u7684\u7167\u7247\u3002<\/p>\n

(b) CsPbBr3<\/sub>\u7684XRD\u5206\u6790\uff0c\u767d\u4e91\u6bcd\u7684\u884d\u5c04\u5cf0\u7531\u2217\u6807\u8bb0\u3002<\/p>\n

(c) \u9499\u949b\u77ff\u7684EDS\u5206\u6790\u8868\u660e\uff0cCs:Pb:Br\u7684\u539f\u5b50\u6bd4\u4e3a19.7%:21.2%:59.1%\u3002\u63d2\u56fe\u4e3aEDS\u5143\u7d20\u5206\u5e03\uff0c\u663e\u793a\u6240\u6709\u5143\u7d20\u5747\u5300\u5206\u6563\u3002<\/p>\n

(d) \u592a\u9633\u5149\u76f4\u5c04\u4e0bCsPbBr3<\/sub>\u8584\u819c\u7684\u7167\u7247\u3002<\/p>\n

(e) (d)\u4e2d\u865a\u7ebf\u5708\u6807\u51fa\u7684PL\u5149\u8c31\u3002<\/p>\n

(f) CsPbBr3<\/sub>\u7684\u65f6\u95f4\u5206\u8fa8\u5149\u81f4\u53d1\u5149\uff0c\u62df\u5408\u5f97\u5230\u5177\u6709\u4e24\u79cd\u6210\u5206\u7684\u5bff\u547d\u8870\u51cf\uff0c\u5206\u522b\u5bf9\u5e9414.8 ns\u7684\u77ed\u5bff\u547d\u548c170.2 ns\u7684\u957f\u5bff\u547d\u3002<\/p>\n

\u56fe2 CsPbBr<\/b><\/strong>3<\/b><\/sub><\/strong>\u8584\u819c\u5728\u767d\u4e91\u6bcd\u4e0a\u7684\u751f\u957f\u8fc7\u7a0b<\/b><\/strong>\"\"<\/p>\n

\uff08a\uff09\u751f\u957f15min\u540e\u5f97\u5230\u7684\u5206\u79bb\u6392\u5217\u7684\u8584\u7247\uff0c\u63d2\u56fe\u4e3a\u76f8\u5e94\u7684PL\u56fe\u50cf\u3002<\/p>\n

\uff08b\uff09\u751f\u957f30min\u540e\u5f97\u5230\u7684\u672a\u5b8c\u6210\u7684\u8584\u819c\uff0c\u5206\u79bb\u7684\u8584\u7247\u76f8\u4e92\u6269\u5c55\u5408\u5e76\uff0c\u8986\u76d6\u6574\u4e2a\u533a\u57df\uff0c\u663e\u793a\u7684\u6761\u7eb9\u4e3a\u672a\u586b\u6ee1\u7684\u6c9f\u69fd\uff0c\u63d2\u56fe\u4e3a\u76f8\u5e94\u7684PL\u56fe\u50cf\u3002<\/p>\n

\uff08c\uff09\u751f\u957f60min\u540e\u5b8c\u6210\u8584\u819c\uff0c\u6c9f\u69fd\u88ab\u586b\u6ee1\u5e76\u5f62\u6210\u5149\u6ed1\u65e0\u9488\u5b54\u7684\u8868\u9762\uff0c\u63d2\u56fe\u4e3a\u76f8\u5e94\u7684PL\u56fe\u50cf;<\/p>\n

\uff08d\uff09\u5206\u79bb\u7684\u8584\u7247(15min\u751f\u957f)\u7684AFM\u56fe\u50cf\uff0c\u63d2\u56fe\u663e\u793a\u4e86\u8584\u7247\u7684\u539a\u5ea6\u4e3a196 nm\u3002<\/p>\n

\uff08e\uff09\u672a\u5b8c\u6210\u8584\u819c(30min\u751f\u957f)\u8fb9\u7f18\u7684AFM\u56fe\u50cf\uff0c\u63d2\u56fe\u663e\u793a\u539a\u5ea6\u4e3a428 nm\u3002<\/p>\n

\uff08f\uff09\u5b8c\u6210\u7684\u8584\u819c(60min\u751f\u957f)\u8fb9\u7f18\u7684AFM\u56fe\u50cf\uff0c\u63d2\u56fe\u663e\u793a\u539a\u5ea6\u4e3a1062 nm\u3002<\/p>\n

\u56fe3 \u901a\u8fc7TEM\u8868\u5f81\u786e\u5b9aCsPbBr<\/b><\/strong>3<\/b><\/sub><\/strong>\u8584\u819c\u4e0e\u767d\u4e91\u6bcd\u7684\u5916\u5ef6\u5173\u7cfb<\/b><\/strong>\"\"<\/p>\n

(a) TEM\u8868\u5f81\u7684\u9762\u5185\u6837\u54c1(\u7ea2\u8272\u65b9\u6846)\u548c\u9762\u5916\u6837\u54c1(\u9ec4\u8272\u65b9\u6846)\u5236\u5907\u793a\u610f\u56fe\u3002<\/p>\n

(b) \u9762\u5185\u6837\u54c1\u7684\u4f4e\u653e\u5927\u500d\u6570TEM\u56fe\u50cf\u3002<\/p>\n

(c) CsPbBr3<\/sub>\u8584\u7247\u95f4\u6c9f\u69fd\u5185\u767d\u4e91\u6bcd\u7684\u7535\u5b50\u884d\u5c04\u56fe\u3002<\/p>\n

(d) \u5047\u60f3\u7684CsPbBr3<\/sub>\u5728\u767d\u4e91\u6bcd\u4e0a\u7684\u4e0d\u76f8\u79f0\u5916\u5ef6\u5173\u7cfb\uff0cCsPbBr3<\/sub>\/\u767d\u4e91\u6bcd\u7684\u6676\u4f53\u7ed3\u6784\u56fe\u4e2d\u7bad\u5934\u5206\u522b\u6807\u8bb0[100]\u548c[010]\u6676\u5411\u3002<\/p>\n

(e) CsPbBr3<\/sub>\/\u767d\u4e91\u6bcd\u5207\u7247\u7684HRTEM\u56fe\u50cf\u3002<\/p>\n

(f) CsPbBr3<\/sub>\u4e0e\u767d\u4e91\u6bcd\u5bf9\u5e94\u7684\u7535\u5b50\u884d\u5c04\uff0c\u8868\u660eCsPbBr3<\/sub>\u7684[001]\u4e0e\u767d\u4e91\u6bcd\u7684[001]\u5e73\u884c\u3002<\/p>\n

\u56fe4 \u9009\u62e9\u6027\u9634\u79bb\u5b50\u4ea4\u6362\u6cd5\u5236\u5907CsPbBr<\/b><\/strong>3<\/b><\/sub><\/strong>-CsPbI<\/b><\/strong>3<\/b><\/sub><\/strong>\u6a2a\u5411\u5f02\u8d28\u7ed3\u9635\u5217<\/b><\/strong>\"\"<\/p>\n

(a-d)\u9009\u62e9\u6027\u9634\u79bb\u5b50\u4ea4\u6362\u8fc7\u7a0b\u793a\u610f\u56fe\u3002\u751f\u957f\u7684\u8584\u819c\u88ab\u6d82\u4e0aPMMA(a)\uff0c\u7136\u540e\u901a\u8fc7\u7535\u5b50\u675f\u66dd\u5149(b)\u548c\u663e\u5f71\u5de5\u827a(c)\u00a0\u6253\u5f00\u7a97\u53e3\uff0c\u5e76\u5728\u6eb6\u6db2\u4e2d\u8fdb\u884c\u9634\u79bb\u5b50\u4ea4\u6362(d)\u3002<\/p>\n

(e)\u901a\u8fc7\u533a\u57df\u9009\u62e9\u6027\u9634\u79bb\u5b50\u4ea4\u6362\u83b7\u5f97\u7684\u68cb\u76d8\u72b6\u56fe\u6848\u7167\u7247\u3002<\/p>\n

(f)CsPbBr3<\/sub>-CsPbI3<\/sub>\u5f02\u8d28\u7ed3\u7684\u68cb\u76d8\u72b6\u56fe\u6848\u7684PL\u56fe\u50cf\u3002<\/p>\n

(g)\u5206\u522b\u4ece\u539f\u8584\u819c\u548c\u9634\u79bb\u5b50\u4ea4\u6362\u540e\u7684\u8584\u819c\u63d0\u53d6\u7684PL\u3002<\/p>\n

(h)\u5728CsPbBr3<\/sub>\u8584\u819c\u4e0a\u6c89\u79ef\u7684Au\u7535\u6781\u7684\u7167\u7247\u3002<\/p>\n

(i)\u7531PMMA\u5c42\u8986\u76d6\u7684\u7535\u6781\u5bf9\u7684\u7167\u7247\uff0c\u6bcf\u95f4\u9694\u4e00\u4e2a\u7535\u6781\u90fd\u6709\u4e00\u4e2a\u7535\u6781\u53ca\u5176\u5468\u56f4\u533a\u57df\u66b4\u9732\u51fa\u6765\uff0c\u66b4\u9732\u533a\u57df\u8fdb\u884c\u9634\u79bb\u5b50\u4ea4\u6362\uff0c\u5f62\u6210CsPbBr3<\/sub>-CsPbI3<\/sub>\u5f02\u8d28\u7ed3\u5668\u4ef6\u3002<\/p>\n

(j) \u6d4b\u8bd5\u8868\u9762\uff0c\u5728\u9634\u79bb\u5b50\u4ea4\u6362\u5f62\u6210CsPbBr3<\/sub>-CsPbI3<\/sub>\u5f02\u8d28\u7ed3\u6784\u4e4b\u524dI-V(\u7eff\u7ebf)\u662f\u5bf9\u79f0\u7684\uff0c\u4e4b\u540e(\u7ea2\u7ebf)\u5219\u5177\u6709\u6574\u6d41\u884c\u4e3a\u3002\u63d2\u56fe\u663e\u793a\u4e86\u9634\u79bb\u5b50\u4ea4\u6362\u540e\u5f02\u8d28\u7ed3\u6784\u7684PL\u56fe\u50cf\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/b><\/strong><\/p>\n

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\u00a0<\/b><\/strong>\u6587\u732e\u94fe\u63a5<\/b><\/strong>\uff1aLarge-Area Synthesis and Patterning of All-Inorganic Lead Halide Perovskite Thin Films and Heterostructures<\/u><\/a>\uff08Nano Lett., 2021, DOI:10.1021\/acs.nanolett.0c04594\uff09<\/p>\n

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