{"id":220086,"date":"2021-04-07T12:00:14","date_gmt":"2021-04-07T04:00:14","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=220086"},"modified":"2021-04-07T10:29:15","modified_gmt":"2021-04-07T02:29:15","slug":"%e7%8e%8b%e6%98%a5%e7%94%9f%e6%95%99%e6%8e%88angew%ef%bc%9a%e6%b0%b4%e7%b3%bb%e9%94%8c%e7%a6%bb%e5%ad%90%e7%94%b5%e6%b1%a0%e7%9a%84%e5%9b%ba%e6%80%81%e7%94%b5%e8%a7%a3%e8%b4%a8%e7%95%8c%e9%9d%a2","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=220086","title":{"rendered":"\u738b\u6625\u751f\u6559\u6388Angew\uff1a\u6c34\u7cfb\u950c\u79bb\u5b50\u7535\u6c60\u7684\u56fa\u6001\u7535\u89e3\u8d28\u754c\u9762\u4e2d\u95f4\u76f8\u8bbe\u8ba1"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u6c34\u7cfb\u950c\u79bb\u5b50\u7535\u6c60\u5177\u6709\u8f83\u9ad8\u7684\u7406\u8bba\u6bd4\u5bb9\u91cf(820 mAh g-1<\/sup>)\uff0c\u950c\u8d44\u6e90\u4e30\u5bcc\u548c\u5b89\u5168\u6027\u9ad8\u7684\u4f18\u52bf\uff0c\u4f7f\u5176\u5728\u5927\u89c4\u6a21\u50a8\u80fd\u9886\u57df\u6709\u7740\u826f\u597d\u7684\u5e94\u7528\u524d\u666f\u3002\u7531\u4e8eZn\u7684\u8fd8\u539f\u7535\u4f4d\u6bd4\u6c22\u6790\u51fa\u53cd\u5e94(HER)\u66f4\u4f4e\uff0c\u56e0\u6b64\u5728Zn\u6c89\u79ef\/\u5265\u79bb\u8fc7\u7a0b\u4e2d\u6c34\u4f1a\u88ab\u8fd8\u539f\u4e3aH2<\/sub>\uff0c\u4e00\u65b9\u9762\u4ea7\u751f\u7684H2<\/sub>\u4f1a\u5c06\u7535\u6781\u8868\u9762\u5f62\u6210\u7684SEI\u5439\u8d70\uff1b\u53e6\u4e00\u65b9\u9762\u6c34\u8fd8\u539f\u5bfc\u81f4\u7535\u6781\/\u7535\u89e3\u6db2\u754c\u9762\u5c40\u90e8\u5448\u78b1\u6027\u73af\u5883\u3002\u78b1\u6027\u73af\u5883\u4e2d\u5f62\u6210\u591a\u5b54\u7684Zn(OH)2<\/sub>\u548cZnO\u949d\u5316\u5c42\u8150\u8680Zn\u8d1f\u6781\u8868\u9762\u3002Zn\u8d1f\u6781\u8868\u9762\u5c42\u7684\u4e0d\u5747\u5300\u5f62\u6001\u4f1a\u5bfc\u81f4Zn\u679d\u6676\u7684\u751f\u957f\uff0c\u964d\u4f4eZn\u6c89\u79ef\/\u5265\u79bb\u7684\u5e93\u4ed1\u6548\u7387\uff0c\u5e76\u5bfc\u81f4\u7535\u6c60\u5feb\u901f\u5931\u6548\u3002\u4e3a\u4e86\u89e3\u51b3\u8fd9\u4e9b\u95ee\u9898\uff0c\u8bb8\u591a\u7814\u7a76\u81f4\u529b\u4e8e\u901a\u8fc7\u5728Zn\u8868\u9762\u6d82\u8986\u65e0\u673a\u6216\u805a\u5408\u7269\u6765\u6784\u9020\u4eba\u5de5SEI\uff0c\u4ee5\u5141\u8bb8Zn2+<\/sup>\u4f20\u8f93\u4f46\u963b\u6b62\u6c34\u6e17\u900f\u5230Zn\u8868\u9762\u3002\u7136\u800c\uff0c\u8fd9\u4e9b\u754c\u9762\u5c42\u5728\u5faa\u73af\u671f\u95f4\u7531\u4e8eZn\u7684\u4f53\u79ef\u53d8\u5316\u4f1a\u906d\u53d7\u7834\u574f\/\u6216\u964d\u89e3\u3002\u7531\u4e8e\u8fd9\u4e9b\u4eba\u5de5SEI\u4e0d\u80fd\u50cf\u539f\u4f4d\u5f62\u6210\u7684SEI\u4e00\u6837\u81ea\u6211\u4fee\u590d\uff0c\u56e0\u6b64\u4f1a\u9010\u6e10\u5931\u53bb\u4fdd\u62a4\u529f\u80fd\u3002\u4e00\u822c\u901a\u8fc7\u52a0\u5165\u5177\u6709\u9ad8\u8fd8\u539f\u7535\u4f4d\u7684\u6dfb\u52a0\u5242\u53ef\u89e3\u51b3\u4e0a\u8ff0\u95ee\u9898\uff0c\u4f46\u5f62\u6210\u81f4\u5bc6\u7684SEI\u5c42\u901a\u5e38\u9700\u8981\u5f88\u957f\u65f6\u95f4\uff0c\u56e0\u4e3a\u8fd9\u4e9b\u6dfb\u52a0\u5242\u4e0d\u80fd\u5feb\u901f\u6291\u5236H2<\/sub>\u7684\u6790\u51fa\u3002\u56e0\u6b64\uff0c\u4e9f\u9700\u901a\u8fc7\u7535\u89e3\u6db2\u6dfb\u52a0\u6dfb\u52a0\u5242\uff0c\u5feb\u901f\u6291\u5236H2<\/sub>\u6790\u51fa\uff0c\u540c\u65f6\u5229\u7528\u7535\u89e3\u6db2\u7ec4\u5206\u5728\u7535\u6781\u8868\u9762\u4e0a\u7684\u5206\u89e3\u6765\u5f62\u6210\u539f\u4f4dSEI\u4fdd\u62a4\u91d1\u5c5eZn\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u9a6c\u91cc\u5170\u5927\u5b66\u738b\u6625\u751f\u6559\u6388<\/strong>\u56e2\u961f\u901a\u8fc7\u54113 M Zn(OTF)2<\/sub>\u6c34\u7cfb\u7535\u89e3\u6db2\u4e2d\u6dfb\u52a020 mM Zn(NO3<\/sub>)2<\/sub>\u6dfb\u52a0\u5242(Zn(OTF)2<\/sub>– Zn(NO3<\/sub>)2<\/sub>)\uff0c\u5728Zn\u8d1f\u6781\u8868\u9762\u5316\u5b66\u5f62\u6210\u4e00\u5c42\u8584\u800c\u81f4\u5bc6\u7684Zn5<\/sub>(OH)8<\/sub>(NO3<\/sub>)2<\/sub>\u00b72H2<\/sub>O\u949d\u5316\u5c42\uff0c\u8fdb\u800c\u963b\u6b62\u6c34\u6e17\u900f\u5230Zn\u8868\u9762\u4e14\u540c\u65f6\u6709\u6548\u6291\u5236\u5728Zn\u6c89\u79ef\/\u5265\u79bb\u671f\u95f4H2<\/sub>\u7684\u6790\u51fa\u3002Zn\u4e0eZn(OTF)2<\/sub>– Zn(NO3<\/sub>)2<\/sub>\u7535\u89e3\u6db2\u63a5\u89e6\u540e\uff0c\u6c34\u5728Zn\u8868\u9762\u8fd8\u539f\uff0c\u4ea7\u751f\u5c40\u90e8\u78b1\u6027\u73af\u5883\uff0c\u5bfc\u81f4Zn\u4e0eNO3-<\/sup>\/OH–<\/sup>\u4e4b\u95f4\u7684\u70ed\u529b\u5b66\u548c\u52a8\u529b\u5b66\u4e0a\u6709\u5229\u7684\u53cd\u5e94\u53d1\u751f\uff0c\u5f62\u6210\u9ad8\u7535\u5b50\u548c\u9ad8\u79bb\u5b50\u7535\u963b\u7684Zn5<\/sub>(OH)8<\/sub>(NO3<\/sub>)2<\/sub>\u00b72H2<\/sub>O\u949d\u5316\u5c42\u3002\u8be5\u949d\u5316\u5c42\u53ef\u6291\u5236\u6c34\u6e17\u900f\u5230Zn\u8868\u9762\uff0c\u4ece\u800c\u4f7f\u5f97OTF– <\/sup>\u79bb\u5b50\u5728\u950c\u8d1f\u6781\u8868\u9762\u8fd8\u539f\u5f62\u6210\u7a33\u5b9a\u7684SEI\uff1b\u540c\u65f6\u901a\u8fc7\u590d\u5206\u89e3\u53cd\u5e94\u539f\u4f4d\u8f6c\u5316\u4e3a\u6709\u5229\u4e8eZn2+<\/sup>\u4f20\u5bfc\u7684Zn5<\/sub>(CO3<\/sub>)2<\/sub>(OH)6<\/sub>\u65e0\u673a\u5c42\u3002SEI\u7531\u67d4\u6027\u7684\u6709\u673a\u7269\u4e3a\u4e3b\u7684\u5916\u5c42\u4e0e\u65e0\u673aZnF2<\/sub>\u4e3a\u4e3b\u7684\u5185\u5c42\u7ec4\u6210\u3002\u9ad8\u67d4\u97e7\u6027\u7684\u6709\u673a\u5916\u5c42\u53ef\u9632\u6b62SEI\u56e0\u4f53\u79ef\u53d8\u5316\u800c\u7834\u88c2\uff0c\u5e76\u6709\u52a9\u4e8e\u6eb6\u5242\u5316\u7684Zn\u79bb\u5b50\u8fc1\u79fb\uff1b\u5185\u5c42\u4e2d\u7684\u758f\u6c34\u6027ZnF2<\/sub>\u8fdb\u4e00\u6b65\u53bb\u9664\u4e86\u6eb6\u5242\u5316\u7684\u6c34\uff0c\u5e76\u901a\u8fc7\u9632\u6b62\u950c\u4e0e\u6c34\u76f4\u63a5\u63a5\u89e6\u800c\u6291\u5236\u4e86\u6c34\u5206\u89e3\u548cZn\u679d\u6676\u7684\u751f\u957f\u3002\u8fd9\u79cdSEI\u5728200\u5c0f\u65f6\u5185\u5c06Zn\u9540\u5c42\/\u5265\u79bbCE\u63d0\u5347\u81f399.8\uff05\u3002\u57fa\u4e8e\u8be5\u949d\u5316\u5c42\u7684Zn || MnO2\u7535\u6c60\u5177\u6709\u5341\u5206\u4f18\u5f02\u7684\u5faa\u73af\u6027\u7a33\u5b9a\u6027\uff08700\u6b21\u5faa\u73af\u4e2d\u6bcf\u4e2a\u5faa\u73af\u4ec5\u5177\u67090.005\uff05\u7684\u5bb9\u91cf\u8870\u51cf\u7387\uff09\u3002\u76f8\u5173\u7814\u7a76\u6210\u679c\u4ee5 \u201cSolid Electrolyte Interphase Design for Aqueous Zn Batteries<\/strong>\u201d\u4e3a\u9898\u53d1\u8868\u5728Angew. Chem. Int. Ed<\/strong>\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00<\/strong>Zn<\/strong>\u91d1\u5c5e\u8d1f\u6781\u8868\u9762\u6f14\u5316\u673a\u5236\u7684\u793a\u610f\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u6c34\u7cfb\u7535\u89e3\u6db2\u4e2d\u4e2d\u950c\u679d\u6676\u7684\u751f\u957f\u793a\u610f\u56fe\u3002<\/p>\n

\uff08b\uff09ZnF2<\/sub>-Zn5<\/sub>(CO3<\/sub>)2<\/sub>(OH)6<\/sub>\u6709\u673aSEI\u7684\u5f62\u6210\u673a\u7406\u3002<\/p>\n

\u56fe\u4e8c<\/strong>Zn<\/strong>\u8d1f\u6781\u7684\u7535\u5316\u5b66\u6027\u80fd\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u5e26\u6709Zn(OTF)2<\/sub>– Zn(NO3<\/sub>)2<\/sub>\u7535\u89e3\u6db2\u7684Zn || Ti\u7535\u6c60\u7684CV\u66f2\u7ebf\u3002<\/p>\n

\uff08b\uff09\u6052\u7535\u6d41\u4e0bZn\u6c89\u79ef\/\u5265\u79bb\u7684\u65f6\u95f4-\u7535\u538b\u66f2\u7ebf\u3002<\/p>\n

\uff08c\uff09\u4f7f\u7528\u6c14\u76f8\u8272\u8c31\u4eea\u539f\u4f4d\u68c0\u6d4b\u6c22\u6c14\u6790\u51fa\u7684\u88c5\u7f6e\u793a\u610f\u56fe\u3002<\/p>\n

\uff08d\uff0ce\uff09\u4f7f\u7528Zn(OTF)2<\/sub>– Zn(NO3<\/sub>)2<\/sub>\u548cZn(OTF)2<\/sub>\u7535\u89e3\u6db2\u4eceZn || Zn\u7535\u6c60\u91ca\u653e\u7684\u6c22\u6c14\u7684\u5cf0\u503c\u3002<\/p>\n

\uff08f\uff09\u5bf9\u79f0\u7535\u6c60\u5faa\u73af\u671f\u95f4\u7684\u963b\u6297\u53d8\u5316\u3002<\/p>\n

\uff08f\uff09\u4e0d\u540c\u7535\u89e3\u6db2\u7684\u950c\u6c89\u79ef\/\u5265\u79bb\u7684\u5e93\u4f26\u6548\u7387\u3002<\/p>\n

\u56fe\u4e09\u950c\u8d1f\u6781\u5bf9\u79f0\u7535\u6c60\u5faa\u73af\u540e\u7684\u5f62\u8c8c\u548c\u539a\u5ea6\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe\u56db<\/strong>SEI<\/strong>\u5c42\u7684\u7ec4\u6210\u6210\u5206\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a-c\uff09SEI\u5728\u4e0d\u540c\u6e85\u5c04\u65f6\u95f4\u4e0b\u7684XPS\u80fd\u8c31\u3002<\/p>\n

\uff08d\uff09Zn(OTF)2<\/sub>– Zn(NO3<\/sub>)2<\/sub>\u7535\u89e3\u8d28\u4e2d\u8fdb\u884c50\u6b21\u6c89\u79ef\/\u5265\u79bb\u540e\uff0cZn\u8d1f\u6781SEI\u7684\u5143\u7d20\u7ec4\u6210\u3002<\/p>\n

\uff08e\uff0cf\uff09\u4f7f\u7528\u9762\u79ef\u4e3a5\u03bcm\u00d75\u03bcm\u7684Ga+<\/sup>\u79bb\u5b50\u675f\u5bf9SEI\u8fdb\u884c\u98de\u884c\u65f6\u95f4\u4e8c\u6b21\u79bb\u5b50\u8d28\u8c31\uff08TOF-SIMS\uff09\u5206\u6790\u3002<\/p>\n

\u56fe\u4e94\u57fa\u4e8e<\/strong>Zn(OTF)2<\/sub>– Zn(NO3<\/sub>)2<\/sub><\/strong>\u548c<\/strong>Zn(OTF)2<\/sub><\/strong>\u7535\u89e3\u8d28\u7684<\/strong>Zn || MnO2<\/sub><\/strong>\u7535\u6c60\u7684\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u626b\u63cf\u901f\u5ea6\u4e3a0.1 mV\/s\u7684Zn || MnO2<\/sub>\u5168\u7535\u6c60\u7684CV\u66f2\u7ebf\u3002<\/p>\n

\uff08b\uff09\u57fa\u4e8eZn(OTF)2<\/sub>– Zn(NO3<\/sub>)2<\/sub>\u7535\u89e3\u6db2\u7684\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u5145\u653e\u7535\u66f2\u7ebf<\/p>\n

\uff08c\uff09\u4e0d\u540c\u7535\u89e3\u6db2\u7684\u5728\u7535\u6d41\u5bc6\u5ea6\u4e3a10C\u4e0b\u7684\u957f\u5faa\u73af\u6027\u80fd\u5bf9\u6bd4<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u603b\u4e4b\uff0c\u672c\u6587\u901a\u8fc7\u5c06NO3-<\/sup>\u6dfb\u52a0\u5242\u5f15\u5165\u4f4e\u6d53\u5ea6Zn(OTF)2<\/sub>\u6c34\u7cfb\u7535\u89e3\u8d28\u4e2d\uff0c\u4ee5\u5316\u5b66\u65b9\u5f0f\u5f62\u6210\u7edd\u7f18\u949d\u5316\u5c42\uff0c\u4ece\u800c\u6291\u5236\u4e86\u6c34\u7684\u5206\u89e3\u3002\u7136\u540e\uff0c\u7edd\u7f18\u949d\u5316\u5c42\u5728\u6700\u521dZn\u6c89\u79ef\/\u5265\u79bb\u671f\u95f4\u8f6c\u5316\u4e3a\u5177\u6709Zn2+<\/sup>\u4f20\u5bfc\u6027\u7684SEI\uff0c\u540c\u65f6\u6291\u5236\u4e86\u6c22\u6c14\u7684\u6790\u51fa\u3002\u5728\u957f\u5faa\u73af\u4e2d\uff0cNO3<\/sub>–<\/sup>\u6dfb\u52a0\u5242\u5728\u4fc3\u8fdbSEI\u7684\u5f62\u6210\u548c\u7535\u5316\u5b66\u7a33\u5b9a\u6027\u65b9\u9762\u8d77\u7740\u4e24\u4e2a\u5173\u952e\u4f5c\u7528\uff1a\uff081\uff09\u4e0e\u6c34\u7cfb\u7535\u89e3\u6db2\u4e2d\u7684\u950c\u9633\u6781\u63a5\u89e6\u65f6\uff0cNO3<\/sub>–<\/sup>\u5f62\u6210\u7535\u7edd\u7f18\u548c\u79bb\u5b50\u7edd\u7f18\u7684Zn5<\/sub>(OH)8<\/sub>(NO3<\/sub>)2<\/sub>\u00b72H2<\/sub>O\u949d\u5316\u5c42\uff0c\u53ef\u4ee5\u6709\u6548\u5730\u5728Zn\u8868\u9762\u6784\u5efa\u65e0\u6c34\u73af\u5883\uff0c\u5e76\u907f\u514dSEI\u7ec4\u5206\u6d41\u5931\uff1b\uff082\uff09\u5728\u950c\u6c89\u79ef\/\u5265\u79bb\u8fc7\u7a0b\u4e2d\uff0cZn5<\/sub>(OH)8<\/sub>(NO3<\/sub>)2<\/sub>\u00b72H2<\/sub>O\u949d\u5316\u5c42\u8f6c\u53d8\u4e3a\u7535\u5b50\u7edd\u7f18\u4f46\u5177\u6709\u79bb\u5b50\u5bfc\u7535\u6027\u7684Zn5<\/sub>(CO3<\/sub>)2<\/sub>(OH)6<\/sub>\uff0c\u540c\u65f6\u6eb6\u5242\u5316\u7684NO3<\/sub>–<\/sup>\u4fc3\u8fdbOTF-\u7684\u5206\u89e3\u4e3a\u6c1f\u5316SEI\u3002\u6c1f\u5316SEI\u4fdd\u62a4\u7684Zn\u8d1f\u6781\u53ef\u5b9e\u73b099.8\uff05\u7684\u53ef\u9006\u4e14\u65e0\u679d\u6676\u7684Zn\u6c89\u79ef\/\u5265\u79bb\u6548\u7387\uff0c\u57fa\u4e8e\u8be5Zn\u8d1f\u6781\u7684Zn||MnO2<\/sub>\u7535\u6c60\u5b9e\u73b0\u4e86168 Wh\u00b7kg-1<\/sup>\u7684\u9ad8\u80fd\u91cf\u5bc6\u5ea6\uff08\u57fa\u4e8e\u9634\u6781\u548c\u9633\u6781\u8d28\u91cf\uff09\uff0c\u5e76\u572810 C\u4e0b\u5faa\u73af700\u6b21\u540e\u4ecd\u4fdd\u6301\u521d\u59cb\u5bb9\u91cf\u768496.5\uff05\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>\u201c<\/strong>Solid Electrolyte Interphase Design for Aqueous Zn Batteries<\/strong><\/a>\u201d(Angew. Chem. Int. Ed. DOI:<\/strong> 10.1002\/ange.202103390)<\/strong><\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u5fae\u89c2\u4e16\u754c\u7f16\u8bd1\u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u6574\u7406\u7f16\u8f91\u3002<\/p>\n

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