{"id":221154,"date":"2021-04-27T06:08:50","date_gmt":"2021-04-26T22:08:50","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=221154"},"modified":"2021-04-26T21:09:11","modified_gmt":"2021-04-26T13:09:11","slug":"%e9%83%ad%e7%8e%89%e5%9b%bd%e8%be%9b%e6%a3%ae-jacs%ef%bc%9a%e6%9e%84%e5%bb%ballztopan%e7%94%b5%e8%a7%a3%e8%b4%a8%ef%bc%8c%e5%ae%9e%e7%8e%b0%e9%ab%98%e6%95%88li%e4%bc%a0%e8%be%93%ef%bc%8c%e5%8a%a9","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=221154","title":{"rendered":"\u90ed\u7389\u56fd&\u8f9b\u68ee JACS\uff1a\u6784\u5efaLLZTO@PAN\u7535\u89e3\u8d28\uff0c\u5b9e\u73b0\u9ad8\u6548Li+\u4f20\u8f93\uff0c\u52a9\u529b\u9ad8\u6027\u80fdLMBs"},"content":{"rendered":"

\u3010\u80cc\u666f\u4ecb\u7ecd\u3011<\/strong><\/p>\n

\u8fd1\u4e9b\u5e74\u6765\uff0c\u4eba\u4eec\u5bf9\u9ad8\u80fd\u91cf\u7684\u5148\u8fdb\u5b58\u50a8\u8bbe\u5907\u7684\u9700\u6c42\uff0c\u4f7f\u5f97\u7531\u6db2\u4f53\u9502\u79bb\u5b50\u7535\u6c60\u53d1\u5c55\u5230\u5168\u56fa\u6001\u91d1\u5c5e\u9502\u7535\u6c60\uff08LMB\uff09\u3002\u5229\u7528\u56fa\u4f53\u7535\u89e3\u8d28\u4ee3\u66ff\u6613\u71c3\u7684\u6709\u673a\u6db2\u4f53\u7535\u89e3\u8d28\uff0c\u6709\u6548\u5730\u63d0\u9ad8\u4e86\u7535\u6c60\u7684\u5b89\u5168\u6027\u548c\u7a33\u5b9a\u6027\u3002\u5176\u4e2d\uff0c\u7acb\u65b9\u77f3\u69b4\u77f3\u578bLi7<\/sub>La3<\/sub>Zr2<\/sub>O12<\/sub>\uff08LLZO\uff09\u53ca\u5176Ta\/Ga-\u63ba\u6742\u884d\u751f\u7269\uff08Li6.4<\/sub>La3<\/sub>Zr1.4<\/sub>Ta0.6<\/sub>O12<\/sub>\uff0c\u7b80\u79f0LLZTO\uff09\u5728\u5ba4\u6e29\u4e0b\u5177\u6709\u9ad8\u7684Li+\u8f6c\u79fb\u6570\uff08t<\/em>Li<\/sub>\u22481\uff09\u548c\u79bb\u5b50\u5bfc\u7535\u6027\uff08\u03c3<\/em>Li<\/sub>\u224810-4<\/sup>-10-3<\/sup> S cm-1<\/sup>\uff09\u3001\u5bbd\u7684\u7535\u5316\u5b66\u7a97\u53e3\uff080-6 V vs Li+<\/sup>\/Li\uff09\u3001\u56fa\u6709\u7684\u4eb2Li\u6027\u7b49\u4f18\u70b9\u3002\u7814\u7a76\u53d1\u73b0\uff0c\u56fa\u4f53\u7535\u89e3\u8d28\u7684\u539a\u5ea6\u5fc5\u987b\uff1c50 \u03bcm\uff0c\u624d\u80fd\u83b7\u5f97\u6bd4\u80fd\u91cf\uff1e500 Wh kg-1<\/sup>\u7684LMB\u3002\u4f46\u662f\uff0c\u76ee\u524d\u5f88\u96be\u5e94\u7528\u4f20\u7edf\u7684\u5236\u9020\u6280\u672f\uff08\u5207\u5272\u3001\u629b\u5149\u7b49\uff09\u6765\u5236\u5907\u539a\u5ea6< 200 \u03bcm\u7684\u9676\u74f7\u6c27\u5316\u7269\u7535\u89e3\u8d28\u3002\u867d\u7136\u77f3\u69b4\u77f3\u7535\u89e3\u8d28\u7684\u5404\u5411\u540c\u6027\u526a\u5207\u6a21\u91cf\uff08\u572856-61 GPa\u8303\u56f4\u5185\uff09\u6bd4\u6291\u5236Li\u679d\u6676\u6240\u9700\u7684\u4e34\u754c\u503c\uff08\u7ea68.5 GPa\uff09\u9ad8\u4e00\u4e2a\u6570\u91cf\u7ea7\uff0c\u4f46\u662f\u9676\u74f7\u9897\u7c92\u6ca1\u6709\u8db3\u591f\u7684\u67d4\u6027\u6765\u9002\u5e94\u7535\u6781\u6750\u6599\u5728\u5931\u6548\u524d\u7684\u53d8\u5f62\u5e94\u53d8\u3002\u4e0d\u540c\u4e8e\u786b\u5316\u7269\u57fa\u56fa\u4f53\u7535\u89e3\u8d28\uff0c\u77f3\u69b4\u77f3\u7c89\u672b\u5728\u677e\u6563\u5806\u79ef\u7684\u6676\u754c\/\u9897\u7c92\u8fb9\u754c\u4e0d\u652f\u6301Li+<\/sup>\u7684\u5feb\u901f\u4f20\u5bfc\uff0c\u56e0\u6b64\u4ee5\u77f3\u69b4\u77f3\u7c89\u4e3a\u539f\u6599\uff0c\u91c7\u7528\u6d41\u5ef6\u7b49\u4f20\u7edf\u5de5\u827a\u5236\u5907\u9ad8\u6027\u80fd\u8584\u819c\u77f3\u69b4\u77f3\u7535\u89e3\u8d28\u4ecd\u7136\u9762\u4e34\u6311\u6218\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u4e2d\u79d1\u9662\u5316\u5b66\u7814\u7a76\u6240\u90ed\u7389\u56fd\u7814\u7a76\u5458\u548c\u8f9b\u68ee\u7814\u7a76\u5458\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09\u7b49\u4eba<\/strong>\u62a5\u9053\u4e86\u901a\u8fc7\u5c06LLZTO\u9897\u7c92\u8868\u9762\u5747\u5300\u5305\u8986\u805a\u4e19\u70ef\u8148\uff08PAN\uff09\u5c42\uff0c\u5236\u5907\u4e86\u5177\u6709\u8d85\u9ad8\u9676\u74f7\u542b\u91cf\uff0894.3 wt\uff05\uff09\u7684\u6539\u6027\u77f3\u69b4\u77f3\u7c89\uff08LLZTO@PAN\uff09\u3002\u5728\u6ca1\u6709\u9897\u7c92\u70e7\u7ed3\u6216\u65bd\u52a0\u5916\u90e8\u538b\u529b\u7684\u60c5\u51b5\u4e0b\uff0c\u5176\u8868\u73b0\u51fa\u4e86\u6709\u6548\u7684\u9897\u7c92\u95f4Li+<\/sup>\u4f20\u8f93\u3002\u5176\u4e2d\uff0c\u9676\u74f7\/\u805a\u5408\u7269\u754c\u9762\u5904\u7684\u7d27\u5bc6\u5316\u5b66\u76f8\u4e92\u4f5c\u7528\u6709\u52a9\u4e8e\u8bf1\u5bfcPAN\u7684\u90e8\u5206\u8131\u6c22\u6c30\u5316\u4f5c\u7528\uff0c\u5e76\u4e14\u751f\u6210\u4e86\u5c40\u90e8\u5171\u8f6d\u7ed3\u6784\u3002\u901a\u8fc7\u56fa\u6001\u9b54\u89d2\u65cb\u8f6c\uff08MAS\uff09\u6838\u78c1\u5171\u632f\uff08NMR\uff09\u548c\u5bc6\u5ea6\u6cdb\u51fd\u7406\u8bba\uff08DFT\uff09\u8ba1\u7b97\u53d1\u73b0\uff0c\u5171\u8f6d\u7ed3\u6784\u66f4\u5bb9\u6613\u4e0eLi\u79bb\u5b50\u76f8\u4e92\u4f5c\u7528\uff0c\u5e76\u4e14\u5728LLZTO\/PAN\u754c\u9762\u4e0a\u89e6\u53d1\u5feb\u901f\u7684Li+<\/sup>\u4ea4\u6362\uff0c\u56e0\u6b64\u5b83\u4eec\u53ef\u4f5c\u4e3a\u9676\u74f7\u9897\u7c92\u4e4b\u95f4\u7684\u8fde\u7eedLi+<\/sup>\u4f20\u5bfc\u9014\u5f84\u3002\u7531\u805a\u5408\u7269\u5305\u8986\u7684\u9676\u74f7\u9897\u7c92\u6d41\u5ef6\u5236\u5907\u7684\u8584\u819c\u7535\u89e3\u8d28\uff08\u539a\u5ea6<10 \u03bcm\uff09\u663e\u793a\u51fa\u826f\u597d\u7684\u7535\u5316\u5b66\u6027\u80fd\uff0c\u53ef\u4ee5\u5b9e\u73b0\u5bf9\u79f0Li\/Li\u7535\u6c60\u548c\u5168\u56fa\u6001LMBs\u7684\u7a33\u5b9a\u5faa\u73af\u3002\u7814\u7a76\u6210\u679c\u4ee5\u9898\u4e3a\u201cBridging Interparticle Li+<\/sup> Conduction in a Soft Ceramic Oxide Electrolyte\u201d<\/strong>\u53d1\u5e03\u5728\u56fd\u9645\u8457\u540d\u671f\u520a\u00a0JACS<\/strong>\u4e0a\u3002<\/p>\n

\"\"<\/p>\n

\u3010\u56fe\u6587\u89e3\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00\u3001LLZTO@PAN\u7684\u5fae\u89c2\u7ed3\u6784<\/strong>
\n \"\"\uff08a\uff09\u6ca1\u6709\u805a\u5408\u7269\u5305\u8986\u5c42\u548c\u9502\u76d0\u7684LLZTO\u9897\u7c92\u7684TEM\u56fe\u50cf\uff1b<\/p>\n

\uff08b\uff09\u901a\u8fc7PAN\u5305\u8986\u5c42\u8fde\u63a5\u7684LLZTO@PAN\u9897\u7c92\u7684TEM\u56fe\u50cf\uff1b<\/p>\n

\uff08c\uff09LLZTO@PAN\u9897\u7c92\u7684TEM\u56fe\u50cf\uff1b<\/p>\n

\uff08d\uff09\u4eceLLZTO@PAN\u9897\u7c92\u7684\u8fb9\u7f18\u83b7\u53d6\u7684\u9ad8\u5206\u8fa8\u7387\u51b7\u51bbTEM\u56fe\u50cf\u3002<\/p>\n

\u56fe\u4e8c\u3001LLZTO@PAN\u4e2d\u7684\u5316\u5b66\u53cd\u5e94\u673a\u7406<\/strong>
\n \"\"\uff08a\uff09LLZTO\u3001LLZTO@PAN\u548c\u7145\u70e7\u7684LLZTO@PAN\u7684\u5149\u5b66\u56fe\u50cf\uff08\u57281000 \u00b0C\uff09<\/p>\n

\uff08b-c\uff09LLZTO\u3001PAN\u548cLLZTO@PAN\u7684XRD\u56fe\u3001FTIR\u5149\u8c31\uff0c\u03bd<\/em>C-H<\/sub>=2939 cm-1<\/sup>\u3001\u03bd<\/em>CN<\/sub>=2245 cm-1<\/sup>\uff1b<\/p>\n

\uff08d\uff09LLZTO@PAN\u7684XPS C 1s\u8c31\uff1b<\/p>\n

\uff08e\uff09PAN\u548c\u5177\u6709\u4e0d\u540c\u91cfLLZTO\u7684PAN\u76841<\/sup>H NMR\u8c31\uff1b<\/p>\n

\uff08f-h\uff09DMSO\u548cLLZTO\/DMSO\u6df7\u5408\u7269\u7684FTIR\u5149\u8c31\uff0c\u03bd<\/em>S=O<\/sub>\u22481039 cm-1<\/sup>, 1<\/sup>H NMR\u8c31\u548c13<\/sup>C NMR\u8c31\u3002<\/p>\n

\u56fe\u4e09\u3001LLZTO@PAN\u7684\u7535\u5316\u5b66\u548c\u7269\u7406\u6027\u8d28<\/strong>
\n \"\"\uff08a\uff09LLZTO@PAN\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684Arrhenius\u66f2\u7ebf\uff1b<\/p>\n

\uff08b\uff09LLZTO@PAN\u56fa\u4f53\u7535\u89e3\u8d28\u7684\u7535\u5316\u5b66\u7a97\u53e3\uff1b<\/p>\n

\uff08c\uff09\u5177\u6709LLZTO@PAN\u56fa\u4f53\u7535\u89e3\u8d28\u7684\u5bf9\u79f0Li\/Li\u7535\u6c60\u7684\u8ba1\u65f6\u7535\u6d41\u5206\u6790\u66f2\u7ebf\u3002<\/p>\n

\uff08d\uff09\u7eafPAN\u548cLLZTO@PAN\u7684DSC\u66f2\u7ebf\u3002<\/p>\n

\u56fe\u56db\u3001LLZTO@PAN\u4e0a\u7684\u56fa\u6001MAS NMR\u6d4b\u91cf<\/strong>
\n \"\"\uff08a\uff09298\u548c333 K \u76841D\u5355\u8109\u51b21<\/sup>H MAS NMR\u8c31\uff1b<\/p>\n

\uff08b\uff09298\u548c333 K\u76847<\/sup>Li HPDEC-MAS NMR\u8c31\uff1b<\/p>\n

\uff08c-d\uff09298 K\u548c333 K\u65f6\u76842D 7<\/sup>Li-1<\/sup>H HETCOR\u8c31\uff1b<\/p>\n

\uff08e-f\uff09\u5728298 K\u548c333 K\u5904\u76842D 7<\/sup>Li-7<\/sup>Li\u4ea4\u6362\u8c31\u3002<\/p>\n

\u56fe\u4e94\u3001Li\u79bb\u5b50\u4f20\u8f93\u673a\u7406<\/strong>
\n \"\"\uff08a\uff09LLZTO@PAN\u56fa\u4f53\u7535\u89e3\u8d28\u4e2d\u9897\u7c92\u95f4Li+<\/sup>\u4f20\u8f93\u793a\u610f\u56fe\u3002<\/p>\n

\uff08b-c\uff09\u5728LLZTO\/d-PAN\u548cLLZTO\/PAN\u7684\u5f02\u8d28\u754c\u9762\u4e0a\u8ba1\u7b97\u7684CDD\uff1b<\/p>\n

\uff08d-f\uff09\u901a\u8fc7\u9676\u74f7\/\u805a\u5408\u7269\u754c\u9762\u7684\u4e0d\u540cLi+<\/sup>\u4f20\u8f93\u673a\u5236\u7684\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe\u516d\u3001\u6d41\u5ef6\u5236\u5907\u8584\u819c\u7535\u89e3\u8d28<\/strong>
\n \"\"\uff08a\uff09\u56fa\u6001\u7535\u6c60\u7ec4\u88c5\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08b\uff09\u56fa\u6001\u7535\u6c60\u622a\u9762SEM\u56fe\u50cf\uff1b<\/p>\n

\uff08c-j\uff09EDS\u8c31\u56fe\uff1b<\/p>\n

\uff08h\uff09\u5339\u914dLFP\u6b63\u6781\u7684\u56fa\u6001\u7535\u6c60\u7684\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

\uff08i\uff09\u5faa\u73af\u8fc7\u7a0b\u4e2d\u7684\u653e\u7535\u6bd4\u5bb9\u91cf\uff1b<\/p>\n

\uff08j\uff09\u500d\u7387\u6027\u80fd\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u7efc\u4e0a\u6240\u8ff0\uff0c\u4f5c\u8005\u62a5\u9053\u4e86\u4e00\u79cd\u5177\u6709\u7c92\u5b50\u95f4Li+<\/sup>\u4f20\u5bfc\u6027\u7684\u805a\u5408\u7269\u5305\u8986\u9676\u74f7\u6c27\u5316\u7269\u7c89\u672b\u53ca\u5176\u5728\u5168\u56fa\u6001\u91d1\u5c5e\u9502\u7535\u6c60\u4e2d\u901a\u8fc7\u6d41\u5ef6\u6cd5\u5236\u5907\u8584\u819c\u56fa\u4f53\u7535\u89e3\u8d28\u7684\u5e94\u7528\u3002\u6839\u636essNMR\u6570\u636e\u548cDFT\u8ba1\u7b97\uff0c\u5728\u77f3\u69b4\u77f3\u9897\u7c92\u8868\u9762\u5f62\u6210\u5747\u5300\u7684PAN\u7eb3\u7c73\u5305\u8986\u5c42\uff0c\u540c\u65f6\u4f34\u968f\u7740\u805a\u5408\u7269\u4e3b\u94fe\u7684\u8131\u6c22\u548c\u5c40\u90e8\u5171\u8f6d\u7ed3\u6784\u7684\u4ea7\u751f\uff0c\u6709\u5229\u4e8e\u7c92\u5b50\u95f4Li+<\/sup>\u7684\u4f20\u8f93\u3002LLZTO@PAN\u56fa\u4f53\u7535\u89e3\u8d28\u5728\u5de5\u4f5c\u6e29\u5ea6\u4e0b\u5177\u6709\u8db3\u591f\u7684\u79bb\u5b50\u5bfc\u7535\u6027\uff081.1\u00d7104<\/sup> S cm-1<\/sup>\uff09\u3001\u8f83\u5bbd\u7684\u7535\u5316\u5b66\u7a97\u53e3\uff08\u8d85\u8fc74.35 V vs Li+<\/sup>\/Li\uff09\u548c\u8f83\u9ad8\u7684Li+<\/sup>\u8fc1\u79fb\u6570\uff080.66\uff09\uff0c\u53ef\u4ee5\u7528\u6d41\u5ef6\u6cd5\u5236\u5907\u539a\u5ea6<10 \u03bcm\u7684\u8584\u819c\uff0c\u4ee5\u6ee1\u8db3\u5236\u9020\u9ad8\u6bd4\u80fd\u56fa\u6001\u7535\u6c60\u7684\u8981\u6c42\u3002\u4e0e\u8be5\u8584\u819c\u7535\u89e3\u8d28\u7ec4\u88c5\u7684\u56fa\u6001Li\/Li\u5bf9\u79f0\u7535\u6c60\u548c\u91d1\u5c5e\u9502\u7535\u6c60\u8868\u73b0\u51fa\u7a33\u5b9a\u7684\u5faa\u73af\u6027\u80fd\u3002\u603b\u4e4b\uff0c\u8be5\u5de5\u4f5c\u63a2\u7a76\u4e86\u9676\u74f7-\u805a\u5408\u7269\u590d\u5408\u7535\u89e3\u8d28\u4e2d\u6709\u5173Li+<\/sup>\u4f20\u5bfc\u7684\u57fa\u672c\u673a\u7406\uff0c\u5e76\u4e3a\u56fa\u4f53\u7535\u89e3\u8d28\u548c\u91d1\u5c5e\u9502\u7535\u6c60\u7684\u7535\u6781\/\u7535\u89e3\u8d28\u754c\u9762\u7684\u5408\u7406\u8bbe\u8ba1\u63d0\u4f9b\u4e86\u601d\u8def\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1aBridging Interparticle Li+ Conduction in a Soft Ceramic Oxide Electrolyte<\/a><\/strong>. J. Am. Chem. Soc.<\/em>, 2021<\/strong>, 143, 15, 5717\u20135726.<\/p>\n

\u901a\u8baf\u4f5c\u8005\u7b80\u4ecb<\/strong><\/p>\n

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