{"id":226900,"date":"2021-09-05T06:30:12","date_gmt":"2021-09-04T22:30:12","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=226900"},"modified":"2021-09-04T18:48:26","modified_gmt":"2021-09-04T10:48:26","slug":"%e6%b5%99%e6%b1%9f%e7%90%86%e5%b7%a5%e5%a4%a7%e5%ad%a6%e8%83%a1%e6%af%85%e6%95%99%e6%8e%88%e8%af%be%e9%a2%98%e7%bb%84cej-%e9%ab%98%e5%af%bc%e7%94%b5%e6%80%a7egain-%e4%b8%9d%e7%b4%a0%e5%a2%a8","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=226900","title":{"rendered":"\u6d59\u6c5f\u7406\u5de5\u5927\u5b66\u80e1\u6bc5\u6559\u6388\u8bfe\u9898\u7ec4CEJ: \u9ad8\u5bfc\u7535\u6027EGaIn \/\u4e1d\u7d20\u58a8\u6c34\u7528\u4e8e\u77f3\u58a8\u70ef3D\u9635\u5217\u7ed3\u6784MSCs"},"content":{"rendered":"

\u8fd1\u65e5, \u6d59\u6c5f\u7406\u5de5\u5927\u5b66\u80e1\u6bc5\u8bfe\u9898\u7ec4\u5728Chemical Engineering Journal\uff08\u5f71\u54cd\u56e0\u5b5013.327\uff09\u4e0a\u53d1\u8868\u4e86\u9898\u4e3a\u201cHighly Conductive EGaIn\/Silk Fibroin Ink for Graphene 3D Array Structure Micro-supercapacitors\u201d\u7684\u7814\u7a76\u5185\u5bb9\uff08DOI: 10.1016\/j.cej.2021.132084\uff09\u3002<\/p>\n

\u53d7\u7eba\u7ec7\u67d3\u6574\u9886\u57df\u4f4e\u6210\u672c\u3001\u9ad8\u901a\u91cf\u548c\u53ef\u6269\u5c55\u5370\u82b1\u5de5\u827a\u542f\u53d1\uff0c\u4f7f\u57fa\u4e8e\u7535\u5b50\u58a8\u6c34\u7684\u5e73\u7f51\u5370\u82b1\u5de5\u827a\u5728\u6539\u8fdb\u67d4\u6027\u53ef\u7a7f\u6234\u667a\u80fd\u7eba\u7ec7\u4ea7\u54c1\u7684\u6709\u9650\u5236\u9020\u65b9\u6cd5\u4e0a\u5b9e\u73b0\u53ef\u80fd\u3002\u7136\u800c\uff0c\u5f53\u524d\u5236\u5907\u7684\u67d4\u6027\u7535\u5b50\u5668\u4ef6\uff0c\u5176\u7535\u5b50\u7535\u5bfc\u7387\u548c\u79bb\u5b50\u4f20\u8f93\u63d0\u5347\u4ecd\u7136\u5b58\u5728\u6311\u6218\u3002\u7814\u7a76\u4eba\u5458\u901a\u8fc7\u63a2\u7a76\u4e1d\u7d20\uff08SF\uff09\u5bf9\u6db2\u6001\u91d1\u5c5e\u79bb\u5b50\u7684\u5438\u9644\u87af\u5408\u4f5c\u7528\u5236\u5907\u51fa\u9ad8\u7a33\u5b9a\u6027\u9553\u94df\uff08EGaIn\uff09\/ SF\u58a8\u6c34\uff0c\u8fd0\u7528\u5e73\u7f51\u5370\u82b1\u7b56\u7565\u5728\u67d4\u6027\u57fa\u6750\u4e0a\u53ef\u6269\u5c55\u5236\u5907\u56fe\u6848\u5316\u9ad8\u5bfc\u7535EGaIn\u96c6\u6d41\u5668\uff0c\u5e76\u5bf9\u5176\u5bfc\u7535\u6062\u590d\u673a\u5236\u8fdb\u884c\u89e3\u6790\u3002\u540c\u65f6\uff0c\u901a\u8fc7\u8c03\u8282\u4e1d\u7f51\u76ee\u6570\u548c\u7cbe\u51c6\u5bf9\u82b1\u5370\u5236\u77f3\u58a8\u70ef3D\u9635\u5217\u7ed3\u6784\u5fae\u578b\u8d85\u7ea7\u7535\u5bb9\u5668\uff08MSCs\uff09\u7535\u6781\uff0c\u8fdb\u4e00\u6b65\u89e3\u6790\u5176\u591a\u5411\u79bb\u5b50\u6269\u6563\u673a\u7406\u3002\u6d4b\u8bd5\u7ed3\u679c\u8868\u660e\uff0c\u6240\u5f97\u7684MSCs\u5668\u4ef6\u8868\u73b0\u51fa\u51fa\u8272\u7684\u673a\u68b0\u67d4\u6027\u3001\u96c6\u6210\u6027\u548c\u7535\u5316\u5b66\u6027\u80fd\uff0c\u8fd9\u5728\u672a\u6765\u7684\u67d4\u6027\u53ef\u7a7f\u6234\u667a\u80fd\u7eba\u7ec7\u54c1\u4e2d\u5177\u6709\u6781\u5927\u5e94\u7528\u6f5c\u529b\u3002<\/p>\n

\"\"<\/p>\n

\u67d4\u6027\u53ef\u7a7f\u6234\u7535\u5b50\u4ea7\u54c1\u7684\u53d1\u5c55\u4f7f\u5f97\u4eba\u4eec\u5bf9\u5fae\u578b\u50a8\u80fd\u5668\u4ef6\u7684\u7ed3\u6784\u521b\u65b0\u3001\u6027\u80fd\u63d0\u5347\u548c\u5236\u9020\u6280\u672f\u4f18\u5316\u7b49\u65b9\u9762\u7684\u9700\u6c42\u589e\u52a0\u3002\u8fd1\u5e74\u6765\uff0c\u5fae\u578b\u8d85\u7ea7\u7535\u5bb9\u5668(MSCs)\u56e0\u5176\u7247\u4e0a\u96c6\u6210\u6027\u3001\u9ad8\u529f\u7387\u5bc6\u5ea6\u3001\u53ef\u5feb\u901f\u5145\u653e\u7535\u548c\u5faa\u73af\u4f7f\u7528\u5bff\u547d\u957f\u7b49\u7279\u70b9\u800c\u53d7\u5230\u5e7f\u6cdb\u5173\u6ce8\u3002\u7136\u800c\uff0c\u4f20\u7edf\u7ed3\u6784\u5fae\u578bMSCs\u5177\u6709\u521a\u6027\u5f3a\u3001\u4f53\u79ef\u5927\u3001\u8d28\u91cf\u91cd\u7b49\u7279\u70b9\uff0c\u96be\u4ee5\u96c6\u6210\u5230\u67d4\u6027\u53ef\u7a7f\u6234\u50a8\u80fd\u4f53\u7cfb\u4e2d\uff0c\u9650\u5236\u4e86\u5b83\u4eec\u7684\u5b9e\u9645\u5e94\u7528\u3002\u76ee\u524d\uff0c\u5e73\u9762\u53c9\u6307\u578bMSCs\u56e0\u5176\u4f18\u5f02\u7684\u67d4\u6027\u548c\u53ef\u7a7f\u6234\u6027\u80fd\u800c\u88ab\u5e7f\u6cdb\u7814\u7a76\uff0c\u4f46\u5176\u4ecd\u7136\u9762\u4e34\u4e00\u4e9b\u6311\u6218\uff0c\u4f8b\u5982\u53ef\u6269\u5c55\u6027\u6709\u9650\uff0c\u79bb\u5b50\u6269\u6563\u7387\u4f4e\u548c\u7535\u5b50\u4f20\u5bfc\u6027\u8f83\u5dee\u3002<\/p>\n

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Fig. 1. a) Preparation process and chelation mechanism of EGaIn \/SF ink. b) Optical microscope Photo of EGaIn\/SF ink. c) SEM image and size distribution graph. d) TEM image. e) Viscosity plotted as a function of shear rates of as-formulated optimal ink. f) Fourier infrared spectrum of EGaIn\/SF ink, SF and PEO. g) Zeta potential of the EGaIn\/SF ink and pure SF solution.<\/p>\n

\u4ece\u8695\u8327\u4e2d\u63d0\u53d6\u51faSF\uff0c\u4f7f\u5176\u6c34\u6eb6\u6db2\u4e0eEGaIn\u5728\u8d85\u58f0\u8f85\u52a9\u4e0b\u914d\u4f4d\u87af\u5408\uff0c\u5f97\u5230\u7a33\u5b9aEGaIn\/SF\u58a8\u6c34\uff08\u56fe1a\uff09\u3002\u5728SF\u5b58\u5728\u4e0b\uff0c\u7531\u8d85\u58f0\u7a7a\u5316\uff08390 W\uff09\u4ea7\u751f\u7684\u5927\u7684\u632f\u8361\u526a\u5207\u529b\u4f7f\u5f97EGaIn\u5927\u6db2\u6ef4\u572830min\u788e\u5316\u6210\u5c0f\u6db2\u6ef4\uff08\u56fe1b\uff09\uff0c\u79bb\u5fc3\u6e05\u6d17\u540e\u83b7\u5f97\u76f4\u5f84\u5c0f\u4e8e1.2\u03bcm\u7684\u6838\u58f3\u7ed3\u6784EGaIn \/ SF\u9897\u7c92\uff08\u56fe1c\uff09\u3002\u58a8\u6c34\u6d41\u53d8\u6027\u7a81\u51fa\uff0c\u8868\u73b0\u4e3a\u5178\u578b\u975e\u725b\u987f\u6d41\u4f53\uff0c\u5177\u6709\u526a\u5207\u7a00\u5316\uff08\u5047\u5851\u6027\uff09\u7279\u5f81\uff08\u56fe1e\uff09\u3002SF\u4e2d\u4e1d\u6c28\u9178(Ser)\u542b\u6709\u4e30\u5bcc\u7684\u6781\u6027\u57fa\u56e2\uff0c\u662f\u4eb2\u6c34\u6027\u57fa\u56e2\u7684\u4e3b\u8981\u6765\u6e90\uff0c\u4e0eGa3+<\/sup>\u914d\u4f4d\u87af\u5408\u524d\u540e\uff0cSF\u7a7a\u95f4\u6784\u578b\u53d1\u751f\u53d8\u5316\uff0c\u6c34\u6eb6\u6db2\u4e2dSF\u5206\u5b50\u4e3b\u8981\u4ee5\u65e0\u89c4\u7ebf\u56e2\u6784\u8c61\u5b58\u5728\uff0c\u5f62\u6210\u914d\u5408\u7269\u540e\u8f6c\u53d8\u4e3a\u03b2-\u6298\u53e0\u6784\u8c61\u548c\u5c11\u91cf\u65e0\u89c4\u7ebf\u5708\u6784\u8c61\uff0cSF\u7a7a\u95f4\u6784\u8c61\u7684\u8f6c\u53d8\u4f7f\u5f97\u7ed3\u6784\u66f4\u52a0\u548c\u8c10\uff0c\u4e14\u6240\u5236\u5907\u7684EGaIn \/ SF\u58a8\u6c34\u4e5f\u66f4\u52a0\u7a33\u5b9a\u3002<\/p>\n

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Fig. 2. a) Screen printing of EGaIn conductive layer. Screen printing different symmetrical patterns b) Interdigital in-parallel pattern, c) School emblem symmetrical pattern, and d) Chinese knot symmetrical pattern. SEM and cross-sectional SEM images of EGaIn\/SF layer (insets) e) before evaporation induction, f) before mechanical sintering, and g) after surface self-heal. h) Schematic illustrating of EGaIn layer conductivity recovery.<\/p>\n

EGaIn\/SF\u6cb9\u58a8\u53ef\u901a\u8fc7\u4e0d\u540c\u65b9\u6cd5\u5728\u4e0d\u540c\u7684\u57fa\u6750\u4e0a\u5f62\u6210\u56fe\u6848\u3002\u6587\u4e2d\u91c7\u7528\u5e73\u7f51\u5370\u82b1\u7b56\u7565\u5728\u5c3c\u9f99\u819c\u4e0a\u5236\u5907\u51fa\u7684\u5bf9\u79f0\u56fe\u6848\u5145\u5206\u5c55\u793a\u4e86\u5176\u53ef\u6269\u5c55\u6027\u3001\u56fe\u6848\u591a\u6837\u5316\u548c\u7f8e\u5b66\u7279\u6027(\u56fe2a-d)\u3002\u6709\u8da3\u7684\u662f\uff0c\u7814\u7a76\u8005\u53d1\u73b0\u5370\u5236\u7684\u56fe\u6848\u5177\u6709\u81ea\u52a8\u5206\u5c42\u7279\u6027\uff0c\u4e14\u5206\u5c42\u540e\u7684\u9876\u90e8SF\u7edd\u7f18\u5c42\u6613\u88ab\u53bb\u9664\uff0c\u66b4\u9732\u51fa\u6c89\u79ef\u5728\u5e95\u90e8\u7684\u5149\u4eae\u5bfc\u7535EGaIn\u5c42\u3002\u6b64\u73b0\u8c61\u79f0\u4e3aEGaIn\u5c42\u7684\u5bfc\u7535\u6062\u590d\u73b0\u8c61\uff0c\u5305\u62ec\u91cd\u529b\u6c89\u79ef\u3001\u84b8\u53d1\u8bf1\u5bfc\u3001\u673a\u68b0\u70e7\u7ed3\u548cEGaIn\u8868\u9762\u81ea\u6108\u5408(\u56fe2h)\u3002SEM\u548c\u6a2a\u65ad\u9762SEM\u56fe(\u56fe2e-g)\u663e\u793a\u4e86\u81ea\u52a8\u5206\u5c42\u73b0\u8c61\u7684\u52a8\u6001\u5f62\u8c8c\u53d8\u5316\uff0c\u84b8\u53d1\u8bf1\u5bfc\u524d\uff0c\u673a\u68b0\u70e7\u7ed3\u524d\uff08\u56fe2e\uff0cf\uff09\u548cEGaIn\u81ea\u6108\u5408\u540e\uff08\u56fe2g\uff09\u7684\u5370\u82b1\u56fe\u6848\u6e05\u695a\u5730\u8bf4\u660e\u4e86EGaIn\u5c42\u5bfc\u7535\u6027\u6062\u590d\u7684\u610f\u4e49\u548c\u5f71\u54cd\u3002<\/p>\n

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Fig. 3. a) TEM image of physical exfoliation graphene sheet. b) Dynamic viscosity of graphene ink at variable shear rate (0-120s-1<\/sup>). c) Cross-sectional SEM image. d) SEM image. e) Magnified SEM image showing stacking of graphene sheets. f) Elemental distribution mapping. g) 3D height profile of graphene array structure measured by 3D stylus profiler. h) Schematic of multi-directional ions diffusion mechanism.<\/p>\n

\u91c7\u7528\u7269\u7406\u6cd5\u5265\u79bb\u76842D\u77f3\u58a8\u70ef\u83b7\u5f97\u7684\u5177\u6709\u4f18\u5f02\u6d41\u53d8\u6027(35.63 mPa\u00b7s)\u7684\u975e\u725b\u987f\u6d41\u4f53\u7535\u6781\u58a8\u6c34\uff0c\u53ef\u4fdd\u8bc1\u826f\u597d\u7684\u5370\u5236\u8d28\u91cf\uff08\u56fe3a,b\uff09\u3002\u8fdb\u4e00\u6b65\u901a\u8fc7\u8c03\u6574\u4e1d\u7f51\u76ee\u6570\uff08250\u3001150\u3001100\u548c80\u76ee\uff09\uff0c\u83b7\u5f97\u77f3\u58a8\u70ef3D\u9635\u5217\u7ed3\u6784\u53c9\u6307\u578b\u7535\u6781\uff08\u56fe3c-g\uff09\u3002\u6b643D\u9635\u5217\u7ed3\u6784\u5c55\u73b0\u51fa\u5178\u578b\u7684\u591a\u5411\u79bb\u5b50\u4f20\u8f93\u6548\u5e94\uff08\u56fe3h\uff09\uff0c\u53ef\u6709\u6548\u589e\u52a0\u7535\u89e3\u8d28\u79bb\u5b50\u4f20\u8f93\u8def\u5f84\uff0c\u4f7f\u6d3b\u6027\u7269\u8d28\u6700\u5927\u5316\uff1b\u77f3\u58a8\u70ef\u7247\u4e0e\u7247\u4e4b\u95f4\u7684\u5f00\u653e\u7a7a\u95f4\u8fdb\u4e00\u6b65\u7f29\u77ed\u79bb\u5b50\u6269\u6563\u8def\u5f84\u6765\u4fc3\u8fdb\u79bb\u5b50\u4f20\u8f93\uff0c\u589e\u52a0\u7535\u6781\u4e0e\u7535\u89e3\u8d28\u63a5\u89e6\u9762\u79ef\uff0c\u4ece\u800c\u8fdb\u4e00\u6b65\u6539\u5584\u5668\u4ef6\u6027\u80fd\uff1b\u540c\u65f6\uff0c\u53c9\u6307\u7ed3\u6784\u672c\u8eab\u5177\u6709\u6709\u6548\u9632\u6b62\u7535\u6781\u77ed\u8def\u548c\u9519\u4f4d\u7684\u7279\u70b9\u3002\u53c9\u6307\u6784\u578b\u548c3D\u9635\u5217\u7ed3\u6784\u7684\u534f\u540c\u6548\u5e94\u4e3a\u63d0\u9ad8\u80fd\u91cf\u5b58\u50a8\u8bbe\u5907\u6027\u80fd\u63d0\u4f9b\u53ef\u80fd\u3002<\/p>\n

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Fig. 4. a) Schematic diagram of screen-printing 3D array structure MSCs. b) CV curves at 100 mV s\u22121 of MSCs-X (X = 250, 150, 100, and 80) printed with different screen meshes. c) GCD profiles for MSCs-X at current density 25 \u00b5A cm-2<\/sup>. d) Nyquist plots. e) Long-term cycling stability of MSCs-X. f) Ragone plots of MSCs-100 compared with other MSCs fabricated by different methods.<\/p>\n

\u57fa\u4e8eEGaIn\u5bfc\u7535\u5c42\u548c\u77f3\u58a8\u70ef3D\u9635\u5217\u7ed3\u6784\u5236\u5907\u7684\u5e73\u9762\u67d4\u6027\u53c9\u6307\u578b\u77f3\u58a8\u70efMSCs(\u56fe4a)\uff0c\u8bc1\u5b9e\u4e86\u4e0a\u8ff0\u6750\u6599\u548c\u7ed3\u6784\u5bf9\u5668\u4ef6\u50a8\u80fd\u6027\u80fd\u7684\u5f71\u54cd\u3002\u5bf9\u6bd4\u53d1\u73b0\uff0c3D\u9635\u5217\u7ed3\u6784\u8d8a\u89c4\u6574\uff0c\u79bb\u5b50\u6269\u6563\u52a8\u529b\u5b66\u6539\u5584\u8d8a\u660e\u663e\uff0c100\u76ee\u4e1d\u7f51\u5370\u5236\u7684MSCs(MSCs-100)\u5177\u6709\u7a81\u51fa\u7535\u5316\u5b66\u6027\u80fd(\u56fe4b-d)\uff0c\u5176\u572825\u03bcA cm-2<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u5177\u670935.72 mF cm-2<\/sup>(10.26 F cm-3<\/sup>)\u9762\u79ef\u7535\u5bb9(\u4f53\u79ef\u7535\u5bb9)\uff0c\u5728CMC\/Na2<\/sub>SO4<\/sub>\u4e2d\u6027\u51dd\u80f6\u7535\u89e3\u8d28\u4e2d\u5faa\u73af6600\u6b21\u4ecd\u5177\u670996%\u5bb9\u91cf\u4fdd\u7559\u7387(\u56fe4e)\uff0c\u5f53\u529f\u7387\u5bc6\u5ea6\u4e3a41.59 mW cm\u2212<\/sup>2<\/sup>\u65f6\uff0c\u5176\u9762\u80fd\u91cf\u5bc6\u5ea6\u8fbe3.17 \u03bcW Wh cm\u2212<\/sup>2<\/sup>(\u56fe4f)\uff0c\u9ad8\u4e8e\u5927\u591a\u6570\u62a5\u9053\u7684\u91c7\u7528\u4e0d\u540c\u65b9\u6cd5\u5236\u5907\u7684MSCs\u3002<\/p>\n

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\u6587\u7ae0\u94fe\u63a5\uff1a<\/strong>https:\/\/doi.org\/10.1016\/j.cej.2021.132084<\/a><\/p>\n","protected":false},"excerpt":{"rendered":"

\u8fd1\u65e5, \u6d59\u6c5f\u7406\u5de5\u5927\u5b66\u80e1\u6bc5\u8bfe\u9898\u7ec4\u5728Chemical Engineering Journal\uff08\u5f71\u54cd\u56e0\u5b5013.327\uff09\u4e0a\u53d1\u8868\u4e86\u9898\u4e3a\u201cHighly Conductive…<\/p>\n","protected":false},"author":11454,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[215],"tags":[],"class_list":["post-226900","post","type-post","status-publish","format-standard","hentry","category-jiedu"],"_links":{"self":[{"href":"http:\/\/www.cailiaoniu.com\/index.php?rest_route=\/wp\/v2\/posts\/226900"}],"collection":[{"href":"http:\/\/www.cailiaoniu.com\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"http:\/\/www.cailiaoniu.com\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"http:\/\/www.cailiaoniu.com\/index.php?rest_route=\/wp\/v2\/users\/11454"}],"replies":[{"embeddable":true,"href":"http:\/\/www.cailiaoniu.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=226900"}],"version-history":[{"count":1,"href":"http:\/\/www.cailiaoniu.com\/index.php?rest_route=\/wp\/v2\/posts\/226900\/revisions"}],"predecessor-version":[{"id":226906,"href":"http:\/\/www.cailiaoniu.com\/index.php?rest_route=\/wp\/v2\/posts\/226900\/revisions\/226906"}],"wp:attachment":[{"href":"http:\/\/www.cailiaoniu.com\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=226900"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"http:\/\/www.cailiaoniu.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=226900"},{"taxonomy":"post_tag","embeddable":true,"href":"http:\/\/www.cailiaoniu.com\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=226900"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}