{"id":228371,"date":"2021-10-18T06:19:00","date_gmt":"2021-10-17T22:19:00","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=228371"},"modified":"2021-10-17T21:19:12","modified_gmt":"2021-10-17T13:19:12","slug":"%e6%9a%a8%e5%8d%97%e5%a4%a7%e5%ad%a6advanced-science%ef%bc%9a%e4%b8%80%e7%a7%8d%e5%b5%8c%e5%85%a52d-3d%e5%bc%82%e8%b4%a8%e7%bb%93%e6%9e%84%e7%9a%84%e9%ab%98%e6%80%a7%e8%83%bdfa%e5%90%88%e9%87%91","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=228371","title":{"rendered":"\u66a8\u5357\u5927\u5b66Advanced\u00a0Science\uff1a\u4e00\u79cd\u5d4c\u51652D\/3D\u5f02\u8d28\u7ed3\u6784\u7684\u9ad8\u6027\u80fdFA\u5408\u91d1\u5316\u67d4\u6027\u9499\u949b\u77ff\u592a\u9633\u80fd\u7535\u6c60\uff0c\u5176\u6548\u7387\u53ef\u8fbe20%\u4ee5\u4e0a"},"content":{"rendered":"<p>\u8fd1\u5e74\u6765\uff0c\u6709\u673a-\u65e0\u673a\u6742\u5316\u9499\u949b\u77ff\u56e0\u5176\u9ad8\u8f7d\u6d41\u5b50\u8fc1\u79fb\u7387\u3001\u9ad8\u5438\u6536\u7cfb\u6570\u3001\u957f\u6269\u6563\u957f\u5ea6\u548c\u4f4e\u6fc0\u5b50\u7ed3\u5408\u80fd\u7b49\u5f15\u4eba\u5165\u80dc\u7684\u7279\u6027\u800c\u5728\u5149\u4f0f\u5e94\u7528\u4e2d\u5f15\u8d77\u4e86\u6781\u5927\u7684\u5173\u6ce8\u3002\u9499\u949b\u77ff\u592a\u9633\u80fd\u7535\u6c60 (PSC) \u7684\u6700\u9ad8\u529f\u7387\u8f6c\u6362\u6548\u7387 (PCE) \u5df2\u8fbe\u5230 25.5% \u7684\u9ad8\u6c34\u5e73\u3002PSC \u7684\u4e00\u4e2a\u503c\u5f97\u6ce8\u610f\u7684\u4f18\u70b9\u662f\u5b83\u4eec\u53ef\u4ee5\u5728\u4f4e\u6e29\u4e0b\u8fdb\u884c\u6eb6\u6db2\u5904\u7406\uff0c\u8fd9\u5bf9\u4e8e\u5236\u9020\u67d4\u6027\u8bbe\u5907\u7279\u522b\u6709\u7528\u3002\u67d4\u6027\u9499\u949b\u77ff\u592a\u9633\u80fd\u7535\u6c60(f-PSC)\u56e0\u5176\u5728\u6d88\u8d39\u7c7b\u7535\u5b50\u8bbe\u5907\u4e2d\u7684\u5de8\u5927\u5e94\u7528\u6f5c\u529b\u800c\u53d7\u5230\u8d8a\u6765\u8d8a\u591a\u7684\u5173\u6ce8\u3002\u5728\u805a\u5408\u7269\u57fa\u7247\u7c97\u7cd9\u8868\u9762\u6c89\u79ef\u65e0\u9488\u5b54\u3001\u5747\u5300\u3001\u65e0\u7f3a\u9677\u7684\u9499\u949b\u77ff\u8584\u819c\u662f\u5b9e\u73b0\u9ad8\u6027\u80fd\u5668\u4ef6\u7684\u5173\u952e\u3002<\/p>\n<p>\u6765\u81ea\u66a8\u5357\u5927\u5b66\u7684\u9ea6\u8000\u534e\u6559\u6388\u548c\u90ed\u98de\u7814\u7a76\u5458\u9996\u6b21\u4f7f\u7528\u4e86\u4e00\u79cd\u6eb6\u5242\u5de5\u7a0b\u6765\u8c03\u6574\u7528\u4e00\u6b65\u6cd5\u53f6\u7247\u6d82\u8986\u5236\u5907\u7684\u9499\u949b\u77ff\u578bFA\u5408\u91d1\u8584\u819c\u7684\u6676\u4f53\u5f62\u8c8c\u3002\u7ed3\u679c\u53d1\u73b0\uff0c\u4f7f\u7528\u4e8c\u5143\u6eb6\u5242DMF\uff1aNMP\u800c\u4e0d\u662f\u4f20\u7edf\u7684DMF\uff1aDMSO\uff0c\u53ef\u4ee5\u5728\u521a\u6027\u548c\u67d4\u6027\u886c\u5e95\u4e0a\u6c89\u79ef\u81f4\u5bc6\u3001\u5747\u5300\u7684\u9499\u949b\u77ff\u578bFA\u5408\u91d1\u5316\u8584\u819c\u3002\u4f5c\u4e3a\u51b3\u5b9a\u6027\u7684\u4e00\u6b65\uff0c\u901a\u8fc7\u52a0\u5165\u5c11\u91cf\u76844-\u80cd\u57fa\u4e01\u9178(GBA)\u539f\u4f4d\u5f62\u6210\u4e86\u5d4c\u5165\u578b2D\/3D\u9499\u949b\u77ff\u5f02\u8d28\u7ed3\u6784\u3002\u76f8\u5e94\u5730\uff0c\u7531\u4e8e\u975e\u8f90\u5c04\u590d\u5408\u53d7\u5230\u660e\u663e\u6291\u5236\uff0c\u5149\u7535\u538b\u5347\u9ad8\u4e86100 mV\uff0c\u6700\u7ec8\u4f7f\u5f97\u521a\u6027\u886c\u5e95\u548c\u67d4\u6027\u886c\u5e95\u4e0a\u7684\u5149\u4f0f\u6548\u7387\u5206\u522b\u8fbe\u523021.45%\u548c20.16%\u3002\u540c\u65f6\uff0c\u7531\u4e8e\u5d4c\u51652D\u76f8\u7684\u5b58\u5728\uff0c\u63d0\u9ad8\u4e86\u67d4\u6027\u5668\u4ef6\u7684\u673a\u68b0\u7a33\u5065\u6027\u3002\u7814\u7a76\u7ed3\u679c\u5f3a\u8c03\u4e86\u5f62\u8c8c\u63a7\u5236\u548c\u7f3a\u9677\u949d\u5316\u5728\u5236\u5907\u9ad8\u6027\u80fd\u67d4\u6027\u9499\u949b\u77ff\u578b\u67d4\u6027\u9499\u949b\u77ff\u5668\u4ef6\u4e2d\u7684\u91cd\u8981\u6027\u3002\u76f8\u5173\u5de5\u4f5c\u4ee5\u9898\u4e3a\u201cAn Embedding 2D\/3D Heterostructure Enables High-Performance FA-Alloyed Flexible Perovskite Solar Cells with Efficiency over 20%\u201d\u7684\u7814\u7a76\u6027\u6587\u7ae0\u5728\u300aAdvanced\u00a0Science\u300b\u4e0a\u53d1\u8868\u3002<\/p>\n<p>\u94fe\u63a5\uff1ahttps:\/\/doi.org\/10.1002\/advs.202101856<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-228372\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72471-3.png\" alt=\"\" width=\"600\" height=\"296\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72471-3.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72471-3-300x148.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p><strong><b>\u901a\u8fc7\u6eb6\u5242\u5de5\u7a0b\u4f18\u5316<\/b><\/strong><strong><b>\u00a0FA \u5408\u91d1\u9499\u949b\u77ff\u7684\u5f62\u6001<\/b><\/strong><\/p>\n<p>\u4f17\u6240\u5468\u77e5\uff0c\u9499\u949b\u77ff\u8584\u819c\u7684\u5f62\u6001\u3001\u7ed3\u6676\u5ea6\u548c\u6676\u7c92\u5c3a\u5bf8\u4e0e\u00a0PSC \u7684\u5149\u4f0f\u6027\u80fd\u5bc6\u5207\u76f8\u5173\u3002\u672c\u6587\u53d1\u73b0\uff0c\u4f7f\u7528\u4f20\u7edf\u7684 DMF:DMSO \u4e8c\u5143\u6eb6\u5242\uff0c\u901a\u8fc7\u771f\u7a7a\u8f85\u52a9\u522e\u5200\u6d82\u5c42\u65e0\u6cd5\u5728\u521a\u6027\u548c\u67d4\u6027\u57fa\u677f\u4e0a\u751f\u4ea7\u51fa\u5408\u683c\u7684\u542b FA \u6df7\u5408\u9633\u79bb\u5b50\u9499\u949b\u77ff\u5c42\u3002\u5982\u56fe 1a\u6240\u793a\uff0c\u5728\u7531\u4f53\u79ef\u6bd4\u4e3a\u00a04:1 \u7684 DMF:DMSO \u5904\u7406\u7684\u9499\u949b\u77ff\u8584\u819c\u4e2d\u89c2\u5bdf\u5230\u5177\u6709\u5927\u91cf\u9488\u5b54\u7684\u5c0f\u6676\u7c92\u3002\u901a\u8fc7\u4f7f\u7528\u00a0DMF:NMP \u6eb6\u5242\u53ef\u4ee5\u51cf\u6162\u7ed3\u6676\u901f\u5ea6\uff0c\u4ece\u800c\u5f62\u6210\u81f4\u5bc6\u4e14\u5747\u5300\u7684 FA \u5408\u91d1\u9499\u949b\u77ff\u8584\u819c\u3002\u5982\u56fe 1b\u6240\u793a\uff0c\u901a\u8fc7\u4f7f\u7528\u4e0d\u540c\u4f53\u79ef\u6bd4\u7684 DMF:NMP\u4e8c\u5143\u6eb6\u5242\uff0c\u53ef\u4ee5\u5f88\u5bb9\u6613\u5730\u83b7\u5f97\u5177\u6709\u5927\u6676\u7c92\u7684\u81f4\u5bc6\u65e0\u9488\u5b54\u9499\u949b\u77ff\u8584\u819c\u3002\u56fe 1c\u663e\u793a\u4e86\u5177\u6709\u4e0d\u540c\u6eb6\u5242\u4f53\u7cfb\u7684\u76f8\u5e94\u5200\u7247\u6d82\u5c42 FA \u5408\u91d1\u9499\u949b\u77ff\u8584\u819c\u7684 X \u5c04\u7ebf\u884d\u5c04 (XRD) \u5149\u8c31\u3002\u4e0e\u7531 DMF:DMSO \u6c89\u79ef\u7684\u8584\u819c\u76f8\u6bd4\uff0c\u7531 DMF:NMP \u4e8c\u5143\u6eb6\u5242\u52a0\u5de5\u7684\u9499\u949b\u77ff\u8584\u819c\u8868\u73b0\u51fa\u66f4\u5f3a\u7684 (110) \u884d\u5c04\u5cf0\u548c\u66f4\u7a84\u7684\u534a\u5cf0\u5bbd\uff0c\u8bc1\u660e\u57fa\u4e8e DMF:NMP \u7684\u9499\u949b\u77ff\u7684\u7ed3\u6676\u5ea6\u663e\u7740\u589e\u5f3a\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-228373\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72472-3.png\" alt=\"\" width=\"600\" height=\"456\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72472-3.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72472-3-300x228.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u56fe1.FA\u5408\u91d1\u5316\u9499\u949b\u77ff\u8584\u819c\u5728\u4e24\u79cd\u6eb6\u5242\u4f53\u7cfb\u4e2d\u7684\u626b\u63cf\u7535\u955c\u56fe\u50cf<\/p>\n<p><strong>\u539f\u4f4d\u5f62\u6210\u5d4c\u5165\u7684\u00a02D\/3D \u5f02\u8d28\u7ed3\u6784<\/strong><\/p>\n<p>\u5c3d\u7ba1\u901a\u8fc7\u4f7f\u7528\u4e8c\u5143\u6eb6\u5242\u00a0DMF:NMP \u663e\u7740\u6539\u5584\u4e86 FA \u5408\u91d1 PSC \u7684\u5149\u4f0f\u6027\u80fd\uff0c\u4f46\u6ce8\u610f\u5230\u5b58\u5728\u8f83\u5927\u7684\u5149\u7535\u538b\u4e0d\u8db3\uff08E g &#8211; V OC = 0.52 eV\uff09\uff0c\u8fd9\u662f\u9650\u5236\u7684\u4e3b\u8981\u56e0\u7d20\u8bbe\u5907\u6548\u7387\u3002\u4e3a\u6b64\uff0c\u672c\u6587\u52a0\u5165\u4e86\u5c11\u91cf\u80cd\u884d\u751f\u7269 GBA\uff08\u56fe 2a)\uff0c\u7528\u4ee5\u5236\u5907\u00a02D\/3D \u9499\u949b\u77ff\u8584\u819c\u3002\u9009\u62e9 GBA \u4f5c\u4e3a\u4e8c\u7ef4\u9499\u949b\u77ff\u7684\u5927\u4f53\u79ef\u6709\u673a\u9633\u79bb\u5b50\u4e3b\u8981\u662f\u57fa\u4e8e GBA \u4e2d\u4e09\u4e2a\u6c2e\u539f\u5b50\u7684\u5b58\u5728\u80fd\u591f\u901a\u8fc7\u5728\u6c2e\u7684\u7535\u5b50\u5b64\u5bf9\u4e0e\u6b20\u914d\u4f4d\u91d1\u5c5e\u4e4b\u95f4\u5f62\u6210\u5f3a\u952e\u6765\u949d\u5316\u6df1\u80fd\u7ea7\u53cd\u4f4d\u7f3a\u9677\u9633\u79bb\u5b50\u3002\u56fe\u00a02b\u663e\u793a\u4e86\u6dfb\u52a0\u548c\u4e0d\u6dfb\u52a0 GBA \u7684 FA \u5408\u91d1\u9499\u949b\u77ff\u8584\u819c\u7684 XRD \u8c31\u3002\u53ef\u4ee5\u770b\u51fa\uff0c\u672a\u63ba\u6742\u7684\u9499\u949b\u77ff\u8584\u819c\u5177\u6709\u6807\u51c6\u7684\u03b1\u76f8\uff0c\u6ca1\u6709\u68c0\u6d4b\u5230\u516d\u65b9\u9ec4\u8272\u76f8\uff08\u03b4\u76f8\uff09\u3002\u6dfb\u52a0\u5c11\u91cf\u00a0GBA (1 mg mL<sup>-1<\/sup>\u00a0)\uff0c\u5728 2 \u03b8\u5904\u51fa\u73b0\u4e00\u4e2a\u65b0\u7684\u5f31\u5cf0= 8.04\u00b0 \uff0c\u8fd9\u53ef\u4ee5\u5f52\u56e0\u4e8e\u4e8c\u7ef4\u9499\u949b\u77ff\u76f8\u7684\u5f62\u6210\u3002\u76f8\u5e94\u7684 SEM \u56fe\u50cf\u8bc1\u660e\u4e86\u4e00\u4e9b\u5177\u6709\u4e0d\u89c4\u5219\u5f62\u72b6\u7684\u65b0\u76f8\u5d4c\u5165\u6676\u754c\uff08\u56fe 2c\uff09\u3002\u53e6\u5916\uff0c\u5982\u56fe2d\u6240\u793a\uff0c\u5728\u4e24\u4e2a\u9499\u949b\u77ff\u8584\u819c\u4e2d\u89c2\u5bdf\u5230q<sub>\u00a0z<\/sub>\u00a0&gt;1 A <sup>-1<\/sup>\u5904\u7684\u51e0\u4e2a\u4e3b\u8981\u884d\u5c04\u73af\uff0c\u8868\u660e\u9499\u949b\u77ff\u6676\u4f53\u4ee5\u968f\u673a\u65b9\u5411\u53d6\u5411\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-228374\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72473-3.png\" alt=\"\" width=\"600\" height=\"235\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72473-3.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72473-3-300x118.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u56fe2.a)GBA\u5206\u5b50\u5f0f(\u4e0a)\u548c\u7403\u68d2\u6a21\u578b(\u4e0b)\uff1bb)\u4e0d\u540c\u6d53\u5ea6GBA(mg mL<sup>\u2212<\/sup><sup>1<\/sup>)\u524d\u9a71\u4f53\u6eb6\u6db2\u5236\u5907\u7684\u9499\u949b\u77ff\u8584\u819c\u7684x\u5c04\u7ebf\u884d\u5c04\u5149\u8c31\uff1bc)\u73bb\u7483\u886c\u5e95\u4e0a\u4e0d\u540c\u6d53\u5ea6GBA\u524d\u9a71\u4f53\u6eb6\u6db2\u5236\u5907\u7684\u9499\u949b\u77ff\u8584\u819c\u7684\u626b\u63cf\u7535\u955c\u56fe\u50cf\uff1b(d)\u53c2\u8003\u6837\u54c1FA<sub>0.7<\/sub>MA<sub>0.25<\/sub>Cs<sub>0.05<\/sub>Pb(I<sub>0.93<\/sub>Br<sub>0.07<\/sub>)<sub>3<\/sub>\u7684GIWAXS\u56fe\u50cf\uff1be)\u542b2 mg mL<sup>\u2212<\/sup><sup>1<\/sup>GbA\u7684\u9499\u949b\u77ff\u8584\u819c\u7684GIWAXS\u56fe\u50cf.<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-228375\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72474-3.png\" alt=\"\" width=\"600\" height=\"326\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72474-3.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72474-3-300x163.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u56fe3.a)\u6ca1\u6709\u548c\u67091mgmL<sup>\u2212<\/sup><sup>1<\/sup>\u00a0GBA\u65f6\u8868\u73b0\u6700\u597d\u7684PSCs\u7684J-V\u66f2\u7ebf\u3002b)\u6027\u80fd\u6700\u4f73\u76842D\/3D\u9499\u949b\u77ff\u592a\u9633\u80fd\u7535\u6c60\u7684EQE\u8c31\u3002c)2D\/3D\u9499\u949b\u77ff\u592a\u9633\u80fd\u7535\u6c60\u7684\u7a33\u6001PCE\u548cJ<sub>SC<\/sub>\u3002d)\u53c2\u8003\u548c2D\/3D PSC\u7684PCE\u76f4\u65b9\u56fe\u3002(e)\u5927\u9762\u79ef(1cm<sup>2<\/sup>)\u9499\u949b\u77ff\u578b2D\/3D\u592a\u9633\u7535\u6c60\u7684J-V\u66f2\u7ebf\u3002f)\u50a8\u5b58\u5728N<sub>2<\/sub>\u624b\u5957\u76d2\u4e2d\u7684\u672a\u5c01\u88c5PSC\u7684\u7a33\u5b9a\u6027\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-228376\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72475-3.png\" alt=\"\" width=\"600\" height=\"334\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72475-3.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2021\/10\/\u56fe\u72475-3-300x167.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" 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