{"id":232000,"date":"2022-01-17T06:01:51","date_gmt":"2022-01-16T22:01:51","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=232000"},"modified":"2022-01-16T18:32:33","modified_gmt":"2022-01-16T10:32:33","slug":"%e6%b8%a4%e6%b5%b7%e5%a4%a7%e5%ad%a6%e9%84%82%e6%b6%9bjclp-%e9%92%bc%e7%84%b6%e7%a6%bb%e5%8e%bb%ef%bc%8c%e7%a1%ab%e4%b8%8b%e6%b4%bb%e5%8a%9b%ef%bc%9a%e4%b8%8d","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=232000","title":{"rendered":"\u6e24\u6d77\u5927\u5b66\u9102\u6d9bJCLP\uff1a \u201c\u94bc\u201d\u7136\u79bb\u53bb\uff0c\u201c\u786b\u201d\u4e0b\u6d3b\u529b\uff1a\u4e0d\u9971\u548c\u94bc\u7a7a\u4f4d\u4fee\u9970MoS2\/TiO2\u6784\u5efaZ\u578b\u5f02\u8d28\u7ed3&\u63d0\u9ad8\u7535\u5b50\u8fc1\u79fb\u7387"},"content":{"rendered":"

\u3010\u7814\u7a76\u80cc\u666f\u3011<\/strong><\/p>\n

\u8fd1\u5e74\u6765\uff0c2D\u8fc7\u6e21\u91d1\u5c5e\u786b\u5316\u7269\uff08TMDs\uff09\u6750\u6599\u5907\u53d7\u5173\u6ce8\uff0c\u5176\u4e2d\u6700\u5177\u4ee3\u8868\u6027\u7684\u662fMoS2<\/sub>\u3002\u7531\u4e8e\u5176\u53ef\u8c03\u63a7\u7684\u5e26\u9699\u3001\u8f83\u4f4e\u7684\u6210\u672c\u548c\u4e30\u5bcc\u7684\u6d3b\u6027\u8fb9\u7f18\u4f4d\u70b9\uff0c\u88ab\u5e7f\u6cdb\u5e94\u7528\u4e8e\u5149\u7535\u50ac\u5316\u3001\u7535\u6781\u6750\u6599\u53ca\u50a8\u80fd\u6750\u6599\u4e2d\u3002\u7136\u800c\uff0c\u6d3b\u6027\u4f4d\u70b9\u8fb9\u7f18\u5316\u7684\u95ee\u9898\u5c06\u5f71\u54cdMoS2<\/sub>\u7684\u50ac\u5316\u6027\u80fd\u3002\u56e0\u6b64\uff0c\u5728MoS2<\/sub>\u60f0\u6027\u886c\u5e95\u4e2d\u5f15\u5165\u7a7a\u4f4d\u7f3a\u9677\u53ef\u4ee5\u6fc0\u6d3b\u60f0\u6027\u57fa\u9762\uff0c\u66b4\u9732\u5927\u91cf\u7684\u6d3b\u6027\u4f4d\u70b9\uff0c\u63d0\u9ad8\u6750\u6599\u7684\u5149\u50ac\u5316\u6027\u80fd\u3002\u5728\u6cbb\u7406\u53d7\u6c61\u67d3\u6c34\u4f53\u7684\u5b9e\u9645\u5e94\u7528\u4e2d\u5177\u6709\u91cd\u8981\u610f\u4e49\u3002<\/p>\n

\"\"<\/a><\/p>\n

\u3010\u6587\u7ae0\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u6e24\u6d77\u5927\u5b66\u5316\u5b66\u4e0e\u6750\u6599\u5de5\u7a0b\u5b66\u9662\u5468\u745e\u5cf0\u7855\u58eb\u7814\u7a76\u751f\u4e3a\u7b2c\u4e00\u4f5c\u8005\uff0c\u6768\u59dd\u5b9c\u526f\u6559\u6388\u548c\u9102\u6d9b\u6559\u6388\u4e3a\u901a\u8baf\u4f5c\u8005\u7684\u7814\u7a76\u6210\u679c\u300aThe defect is perfect: MoS2<\/sub>\/TiO2<\/sub> modified with unsaturated Mo vacancies to construct Z-scheme heterojunction & improve mobility of e–<\/sup>\u300b\u5728\u73af\u5883\u9886\u57df\u56fd\u9645\u8457\u540d\u671f\u520a\u300aJournal of Cleaner Production\u300b\uff08IF=9.3\uff09\u53d1\u8868\u3002\u672c\u6587\u901a\u8fc7\u4e00\u6b65\u6c34\u70ed\u6cd5\u5236\u5907\u4e86\u7f3a\u9677\u578bMoS2<\/sub>\/TiO2<\/sub>\u5149\u50ac\u5316\u5242\u5e76\u7814\u7a76\u4e86\u7f3a\u9677\u5f62\u6210\u673a\u7406\u53ca\u4e0d\u540c\u7f3a\u9677\u5ea6\u4e0b\u50ac\u5316\u5242\u5bf9\u7f57\u4e39\u660eB\uff08Rh-B\uff09\u964d\u89e3\u7684\u5f71\u54cd\u3002\u7ed3\u679c\u8868\u660e\uff0c\u5728MoS2<\/sub>\u60f0\u6027\u57fa\u9762\u5f15\u5165\u7a7a\u4f4d\u7f3a\u9677\u5c06\u66b4\u9732\u5927\u91cfMo-S\u60ac\u7a7a\u952e\uff0c\u589e\u52a0MoS2<\/sub>\u8868\u9762\u6d3b\u6027\u4f4d\u70b9\u4fc3\u8fdb\u7535\u5b50\u7684\u6355\u83b7\uff0c\u63d0\u9ad8\u5149\u751f\u7535\u5b50-\u7a7a\u7a74\u5bf9\u7684\u5206\u79bb\u7387\u3002\u6b64\u5916\uff0c\u4fdd\u7559\u4e8c\u6c27\u5316\u949b\u8f83\u5f3a\u6c27\u5316\u8fd8\u539f\u80fd\u529b\u7684\u540c\u65f6\uff0c\u589e\u5f3a\u4e86\u4e8c\u786b\u5316\u94bc\u7684\u6297\u5149\u8150\u8680\u80fd\u529b\u3002\u8fdb\u4e00\u6b65\u7a81\u51fa\u4e86MoS2<\/sub>\u4f5c\u4e3a\u52a9\u50ac\u5316\u5242\u7684\u4f18\u52bf\uff0c\u5e76\u4e3a\u5149\u50ac\u5316\u6cbb\u7406\u53d7\u6c61\u67d3\u6c34\u4f53\u63d0\u4f9b\u4e86\u53ef\u884c\u7684\u9014\u5f84\u3002<\/p>\n

\u3010\u672c\u6587\u8981\u70b9\u3011<\/strong><\/p>\n

\u8981\u70b9\u4e00:MoS2<\/sub>\/TiO2<\/sub>\u7684\u5236\u5907<\/p>\n

\"\"<\/a><\/p>\n

\u56fe1\uff1a<\/p>\n

(a)\u5236\u5907\u5149\u50ac\u5316\u5242\u5b9e\u9a8c\u6d41\u7a0b\u56fe;<\/p>\n

(b) MoS2<\/sub>\u548cMoS2<\/sub>\/TiO2<\/sub>\u7684SEM\u3001TEM\u3001EDS\u56fe\u3002(b1\u4e3a\u7eafMoS2<\/sub>\u7684SEM\u56fe\uff0cb2\u4e3a\u8d1f\u8f7d\u5728MoS2<\/sub>\u8584\u7247\u4e0a\u7684TiO2<\/sub>\u7684SEM\u56fe\uff0cb3\u4e3aMoS2<\/sub>\/TiO2<\/sub>\u7684TEM\u56fe\uff0cb4\u4e3aMoS2<\/sub>\/TiO2<\/sub>\u5728\u9ad8\u5206\u8fa8\u900f\u5c04\u7535\u955c\u4e0b\u7684\u6676\u683c\u6761\u7eb9\u56fe\uff0cEDS Mapping\u5305\u62ecMo\u3001S\u3001O\u548cTi);<\/p>\n

(c)\u7eafMoS2<\/sub>\u548cMoS2<\/sub>\/TiO2<\/sub>\u4e0d\u540c\u7f3a\u9677\u7a0b\u5ea6\u7684FI-IR\u5149\u8c31\u3001(d) XRD\u5149\u8c31\u3001(e)\u62c9\u66fc\u5149\u8c31;(f) MoS2<\/sub>\u548cMoS2<\/sub>\/TiO2<\/sub>\u7684TGA\u56fe(\u63d2\u56fe:DTG\u56fe)\uff0c(g) DSC\u56fe\u3002<\/p>\n

\u8981\u70b9\u4e8c\uff1a\u5149\u50ac\u5316\u964d\u89e3Rh-B<\/p>\n

\"\"<\/a><\/p>\n

\u56fe2\uff1a<\/p>\n

(a)\u5149\u50ac\u5316\u53cd\u5e94\u8fc7\u7a0b\u793a\u610f\u56fe\uff1b<\/p>\n

(b)MoS2<\/sub>\/TiO2<\/sub>-0.045\u30010.09\u30010.2\u30010.3\u5728\u5149\u50ac\u5316\u53cd\u5e94\u4e2d\u5bf9Rh-B\u7684\u964d\u89e3\u7387;<\/p>\n

(c)\u4e0d\u540c\u5149\u50ac\u5316\u5242\u7684\u964d\u89e3\u901f\u7387\u5e38\u6570\uff1b<\/p>\n

(d)MoS2<\/sub>\/TiO2<\/sub>-0.09\u7684\u5438\u5149\u5ea6\u968f\u65f6\u95f4\u53d8\u5316\uff1b<\/p>\n

(e)\u548c(f)\u4e0d\u540cpH\u548c\u6295\u52a0\u91cf\u4e0bRh-B\u7684\u964d\u89e3\u7387\u3002<\/p>\n

\u8981\u70b9\u4e09\uff1a\u6750\u6599\u7f3a\u9677\u7684\u8868\u5f81<\/p>\n

\"\"<\/a><\/p>\n

\u56fe3\uff1a<\/p>\n

(a) MoS2<\/sub>\u7684\u900f\u5c04\u7535\u955c\u56fe\uff1b<\/p>\n

(b)-(d)\u4e0d\u540c\u7f3a\u9677\u5ea6\u7684MoS2<\/sub>\u548c\u7f3a\u9677\u578bMoS2<\/sub>\u7684XRD\u3001\u62c9\u66fc\u5149\u8c31\uff1b\u7eafMoS2<\/sub>\u548cMoS2<\/sub>-0.09\u7684\u7535\u5b50\u987a\u78c1\u5171\u632f\u56fe\uff1b<\/p>\n

(e)-(g) Mo3d\u3001S2p\u7684XPS\u5149\u8c31\u53caMoS2<\/sub>\uff0cMoS2<\/sub>\/TiO2<\/sub>-0.09\u603b\u8c31\u56fe\uff1b<\/p>\n

(h)-(i) O1s\u3001Ti2p\u53caMoS2<\/sub>\/TiO2<\/sub>-0.09\u7684XPS\u5149\u8c31\u3002<\/p>\n

\u8981\u70b9\u56db\uff1a\u5bc6\u5ea6\u6cdb\u51fd\u7406\u8bba\uff08DFT\uff09\u8ba1\u7b97<\/p>\n

\"\"<\/a><\/p>\n

\u56fe4\uff1a<\/p>\n

(a)\u7eafMoS2<\/sub>\u7684\u4fef\u89c6\u7ed3\u6784\u6a21\u578b\u3001\u4fa7\u89c6\u7ed3\u6784\u6a21\u578b\u3001\u80fd\u5e26\u8c31\u548cDOS\u56fe\uff1b<\/p>\n

(b)\u7f3a\u9677\u578bMoS2<\/sub>\u7684\u4fef\u89c6\u7ed3\u6784\u6a21\u578b\u3001\u4fa7\u89c6\u7ed3\u6784\u6a21\u578b\u3001\u80fd\u5e26\u8c31\u548cDOS\u56fe\uff1b<\/p>\n

(c)MoS2<\/sub>\/TiO2<\/sub>-0.09\u7684\u7ed3\u6784\u6a21\u578b\u548cDOS\u56fe\u3002<\/p>\n

\u8981\u70b9\u4e94\uff1a\u5f02\u8d28\u7ed3\u7684\u5f62\u6210\u548c\u4f5c\u7528<\/p>\n

\"\"<\/a><\/p>\n

\u56fe5\uff1a<\/p>\n

(a)MoS2<\/sub>\/TiO2<\/sub>-0.09\u5149\u50ac\u5316\u5242\u7684TEM\u56fe\uff1b<\/p>\n

(b)\u4e0e\u5f02\u8d28\u7ed3\u76f8\u5173\u7684\u7535\u5b50\u4f20\u8f93\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

(c)-(f)MoS2<\/sub>-0.09\u3001TiO2<\/sub>\u3001MoS2<\/sub>\/TiO2<\/sub>-0.09\u7684UV-DRS\u56fe\u53caKubelka-Munk\u56fe<\/p>\n

(g)\u7eaf\u76f8\u3001\u5f02\u8d28\u7ed3\u548c\u6df7\u5408\u6001\u5149\u50ac\u5316\u5242\u5bf9Rh-B\u7684\u53bb\u9664\u7387\u3002<\/p>\n

\u8981\u70b9\u516d: \u7535\u5b50\u8fc1\u79fb\u548c\u5bff\u547d<\/p>\n

\"\"<\/a><\/p>\n

\u56fe6:<\/p>\n

(a)MoS2<\/sub>\u5c42\u95f4\u7535\u5b50\u4f20\u8f93\u8def\u5f84\u793a\u610f\u56fe\uff1b<\/p>\n

(b)\u4e09\u7535\u6781\u7535\u5316\u5b66\u5de5\u4f5c\u7ad9\u793a\u610f\u56fe\uff1b<\/p>\n

(c)MoS2<\/sub>\u3001MoS2<\/sub>\/TiO2<\/sub>-0.045\u30010.09\u30010.2\u30010.3\u7684\u7535\u5316\u5b66\u963b\u6297\u56fe\uff1b<\/p>\n

(d)MoS2<\/sub>\u3001MoS2<\/sub>\/TiO2<\/sub>-0.09\u7684\u5149\u81f4\u53d1\u5149\u5149\u8c31\uff1b<\/p>\n

(e)-(f)MoS2<\/sub>\u3001MoS2<\/sub>\/TiO2<\/sub>-0.09\u7684\u8367\u5149\u5bff\u547d\u56fe\u3002<\/p>\n

\u8981\u70b9\u4e03: Z\u578b\u5f02\u8d28\u7ed3\u7684\u50ac\u5316\u673a\u7406<\/p>\n

\"\"<\/a><\/p>\n

\u56fe7:<\/p>\n

(a)\u4e0d\u540c\u6dec\u706d\u5242\u5bf9Rh-B\u964d\u89e3\u7684\u5f71\u54cd;<\/p>\n

(b)\u3001(c)\u5149\u7167\u548c\u9ed1\u6697\u6761\u4ef6\u4e0b\u00b7O2<\/sub>–<\/sup>\u548c\u00b7OH\u7684ESR\u56fe;<\/p>\n

(d)\u5728\u6a21\u62df\u5149\u7167\u6761\u4ef6\u4e0b\u4ea7\u751f\u6d3b\u6027\u7269\u8d28\u6a21\u578b\u56fe;<\/p>\n

(e)\u7535\u8377\u8f6c\u79fb\u673a\u7406\u56fe\u3002<\/p>\n

\u8981\u70b9\u516b: \u7535\u5b50\u8fc1\u79fb\u548c\u5bff\u547d<\/p>\n

\"\"<\/a><\/p>\n

\u56fe8:<\/p>\n

(a) MT-0.09\u964d\u89e3Rh-B\u7684\u5faa\u73af\u4f7f\u7528\u6b21\u6570;<\/p>\n

(b) MT-0.09\u5149\u50ac\u5316\u53cd\u5e94\u524d\u540e\u7684XRD\u8c31\u56fe(\u9644\u56fe:MT-0.09\u5149\u50ac\u5316\u53cd\u5e94\u524d\u540e\u7684SEM\u56fe);<\/p>\n

(c) Rh-B\u53ef\u80fd\u7684\u964d\u89e3\u9014\u5f84\u3002<\/p>\n

\u7ed3\u8bba<\/strong><\/p>\n

\u672c\u7814\u7a76\u901a\u8fc7\u5f15\u5165\u7a7a\u4f4d\u7f3a\u9677\u4fee\u9970MoS2<\/sub>\u60f0\u6027\u57fa\u9762\u589e\u52a0\u6d3b\u6027\u4f4d\u70b9\u6765\u63d0\u9ad8\u5176\u5149\u50ac\u5316\u6027\u80fd\u3002\u540c\u65f6\uff0c\u6784\u5efa\u5f02\u8d28\u7ed3\u6539\u5584\u4e86\u7535\u5b50\u8fc1\u79fb\u8def\u5f84\uff0c\u6709\u6548\u63d0\u9ad8\u4e86\u7535\u5b50-\u7a7a\u7a74\u5bf9\u7684\u5206\u79bb\uff0c\u5ef6\u957f\u4e86\u5149\u751f\u8f7d\u6d41\u5b50\u7684\u54cd\u5e94\u65f6\u95f4\u3002\u56e0\u6b64\uff0c\u901a\u8fc7\u5f15\u5165\u7f3a\u9677\u4fee\u9970MoS2 <\/sub>\u60f0\u6027\u57fa\u9762\u505a\u52a9\u50ac\u5316\u5242\u6709\u671b\u6269\u5c55\u534a\u5bfc\u4f53\u5149\u50ac\u5316\u6750\u6599\u5728\u73af\u5883\u4fee\u590d\u4e2d\u7684\u8bbe\u8ba1\u548c\u5e94\u7528\u3002<\/p>\n

\u4f5c\u8005\u7b80\u4ecb<\/strong><\/p>\n

\"\"<\/a><\/p>\n

\u901a\u8baf\u4f5c\u8005<\/strong> \u9102\u6d9b\uff1a<\/strong>\u535a\u58eb\uff0c\u6559\u6388\uff0c\u6e24\u6d77\u5927\u5b66\u73af\u5883\u5de5\u7a0b\u4e13\u4e1a\u5e26\u5934\u4eba\uff0c\u7855\u58eb\u7814\u7a76\u751f\u5bfc\u5e08\u3002\u8fbd\u5b81\u7701\u6bdb\u76ae\u7eff\u8272\u5236\u9020\u4ea7\u4e1a\u6280\u672f\u521b\u65b0\u6218\u7565\u8054\u76df\u7406\u4e8b\u957f\uff0c\u9526\u5dde\u5e02\u91d1\u5c5e\u6750\u6599\u4ea7\u4e1a\u521b\u65b0\u8054\u76df\u4e13\u5bb6\u59d4\u5458\uff0c\u6e24\u6d77\u5927\u5b66\u73af\u4fdd\u4ea7\u4e1a\u6280\u672f\u7814\u7a76\u6240\u6240\u957f\u3002\u7814\u7a76\u5174\u8da3\uff1a\u5316\u5de5\u6e05\u6d01\u751f\u4ea7\u5de5\u827a\uff0c\u571f\u58e4\u4e0e\u6c34\u6c61\u67d3\u4fee\u590d\u6280\u672f\u3001\u4f4e\u78b3\u51cf\u78b3\u5de5\u827a\u6280\u672f\u5f00\u53d1\u53ca\u949b\u57fa\u529f\u80fd\u6750\u6599\u7684\u5236\u5907\u5de5\u827a\u53ca\u5e94\u7528\u3002\u5728ACS Appl Mater Interfaces<\/em>\uff0cJ Hazard Mater<\/em>\uff0c<\/em>Sep Purif Technol<\/em>\uff0c<\/em>J CLEAN PROD<\/em> \uff0c<\/em>J. Environ. Chem. Eng<\/em>\u7b49\u56fd\u9645\u8457\u540d\u671f\u520a\u4e0a\u4ee5\u7b2c\u4e00\/\u901a\u8baf\u4f5c\u8005\u53d1\u8868SCI\u6536\u5f55\u8bba\u658722\u7bc7\uff0c\u4e3b\u630124\u9879\u79d1\u7814\u9879\u76ee\uff0c\u4ee5\u7b2c\u4e00\u53d1\u660e\u4eba\u83b7\u5f97\u6388\u6743\u53d1\u660e\u4e13\u522913\u9879\uff0c\u5355\u9879\u4e13\u5229\u8f6c\u5316\u989d\u5ea6\u8d85100\u4e07\uff0c\u8fd1\u4e09\u5e74\u79d1\u6280\u6210\u679c\u8f6c\u5316\u5408\u540c\u91d1\u989d623\u4e07\u3002<\/p>\n

\u7535\u5b50\u90ae\u7bb1\uff1aetao@bhu.edu.cn<\/p>\n

\"\"<\/a><\/p>\n

\u901a\u8baf\u4f5c\u8005<\/strong> \u6768\u59dd\u5b9c\uff1a<\/strong>\u6e24\u6d77\u5927\u5b66\u73af\u5883\u5de5\u7a0b\u4e13\u4e1a\u526f\u6559\u6388\uff0c\u7855\u58eb\u751f\u5bfc\u5e08\u3002\u7814\u7a76\u5174\u8da3\uff1a\u571f\u58e4\u4fee\u590d\u6280\u672f\u548c\u56fa\u4f53\u5e9f\u7269\u8d44\u6e90\u5316\u3002\u5728J Hazard Mater<\/em>\uff0c<\/em>J CLEAN PROD<\/em>\uff0c<\/em>ACS Appl Mater Interfaces, Sep Purif Technol<\/em>\uff0c<\/em> J. Alloys Compd<\/em>\u7b49\u56fd\u9645\u8457\u540d\u671f\u520a\u4e0a\u4ee5\u7b2c\u4e00\/\u901a\u8baf\u4f5c\u8005\u53d1\u8868SCI\u6536\u5f55\u8bba\u658714\u7bc7\uff0c\u62c5\u4efb\u300aJournal of Alloys and Compounds<\/em>\u300b\uff0c\u300aJournal of Cleaner Production<\/em>\u300b\uff0c\u300aJournal of Polymers and the Environment<\/em>\u300b\u7b49SCI\u77e5\u540d\u671f\u520a\u5ba1\u7a3f\u4eba\u3002<\/p>\n

\u7535\u5b50\u90ae\u7bb1\uff1ayangshuyi@bhu.edu.cn<\/p>\n

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\u7b2c\u4e00\u4f5c\u8005<\/strong> \u5468\u745e\u5cf0\uff1a<\/strong>\u6e24\u6d77\u5927\u5b66\u5316\u5b66\u5de5\u827a\u4e13\u4e1a\u7855\u58eb\u7814\u7a76\u751f\u3002\u7814\u7a76\u5174\u8da3\uff1a\u5149\u50ac\u5316\u9ad8\u7ea7\u6c27\u5316\u6280\u672f\u3002\u76ee\u524d\u5728J Solid State Chem.\u548cJ. Clean. Prod.\u671f\u520a\u4e0a\u53d1\u8868SCI\u6536\u5f55\u8bba\u6587\u51712\u7bc7\u3002<\/p>\n

\u7535\u5b50\u90ae\u7bb1\uff1a864554129@qq.com<\/p>\n

\u6587\u7ae0\u4fe1\u606f<\/strong><\/p>\n

Zhou, S. Yang*, T. E*,L. Liu, J. Qian, The defect is perfect: MoS2<\/sub>\/TiO2<\/sub> modified with unsaturated Mo vacancies to construct Z-scheme heterojunction & improve mobility of e–<\/sup>, Journal of Cleaner Production, Journal of Cleaner Production.<\/em><\/strong>DOI: 10.1016\/j.jclepro.2022.130511<\/p>\n

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