{"id":237870,"date":"2022-06-02T05:52:44","date_gmt":"2022-06-01T21:52:44","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=237870"},"modified":"2022-06-01T15:52:50","modified_gmt":"2022-06-01T07:52:50","slug":"%e9%92%a0%e7%94%b5%e6%9c%80%e6%96%b0nat-commun-%e7%86%b5%e4%b8%8e%e6%99%b6%e9%9d%a2%e8%b0%83%e6%8e%a7%e5%8a%a9%e5%8a%9b%e9%95%bf%e5%af%bf%e5%91%bdp2%e5%9e%8b%e5%b1%82%e7%8a%b6%e6%ad%a3%e6%9e%81","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=237870","title":{"rendered":"\u94a0\u7535\u6700\u65b0Nat. Commun.: \u71b5\u4e0e\u6676\u9762\u8c03\u63a7\u52a9\u529b\u957f\u5bff\u547dP2\u578b\u5c42\u72b6\u6b63\u6781"},"content":{"rendered":"

1.<\/strong>\u3010\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u7531\u4e8e\u94a0\u5143\u7d20\u5177\u6709\u9ad8\u7684\u81ea\u7136\u4e30\u5ea6\u4ee5\u53ca\u4e0e\u9502\u76f8\u4f3c\u7684\u5316\u5b66\u6027\u8d28\uff0c\u94a0\u79bb\u5b50\u7535\u6c60\u88ab\u8ba4\u4e3a\u662f\u66ff\u4ee3\u9502\u79bb\u5b50\u7535\u6c60\u7684\u4f4e\u6210\u672c\u65b9\u6848\uff0c\u6709\u5e0c\u671b\u88ab\u5e94\u7528\u4e8e\u672a\u6765\u7684\u5927\u89c4\u6a21\u50a8\u80fd\u3002\u53d1\u5c55\u94a0\u79bb\u5b50\u7535\u6c60\u7684\u9996\u8981\u6311\u6218\u5728\u4e8e\u5f00\u53d1\u9ad8\u6027\u80fd\u548c\u4f4e\u6210\u672c\u7684\u7535\u6781\u6750\u6599\u3002\u5728\u73b0\u6709\u6b63\u6781\u6750\u6599\u4e2d\uff0cP2\u578b\u5c42\u72b6\u6c27\u5316\u7269\uff0c\u7279\u522b\u662f\u5bcc\u9530\u94a0\u6c27\u5316\u7269(Nax<\/sub>MnO2<\/sub>)\u56e0\u8f83\u9ad8\u7684\u6bd4\u5bb9\u91cf\u548c\u6027\u4ef7\u6bd4\u88ab\u8ba4\u4e3a\u662f\u6700\u5177\u5438\u5f15\u529b\u7684\u6b63\u6781\u5019\u9009\u6750\u6599\u4e4b\u4e00\u3002\u7136\u800c\uff0c\u5728\u9ad8\u7535\u538b\u72b6\u6001\u4e0b<\/strong>(<\/strong>\u5982<\/strong>4.0 V<\/strong>\u4ee5\u4e0a<\/strong>)<\/strong>\uff0c\u4e0d\u53ef\u9006\u7684\u76f8\u53d8\u548c\u9634\u79bb\u5b50\u6c27\u5316\u8fd8\u539f\u53cd\u5e94\u5f15\u8d77\u7684\u7ed3\u6784\u626d\u66f2\u548c\u9633\u79bb\u5b50\u91cd\u6392\uff0c\u4f1a\u5bfc\u81f4\u7f13\u6162\u7684\u94a0\u79bb\u5b50\u52a8\u529b\u5b66\u548c\u4e25\u91cd\u7684\u7535\u6c60\u5bb9\u91cf\u8870\u51cf\u3002<\/strong>\u503c\u5f97\u6ce8\u610f\u7684\u662f\uff0c\u79bb\u5b50\u4f20\u8f93\u52a8\u529b\u5b66\u5f88\u5927\u7a0b\u5ea6\u4e0a\u53d6\u51b3\u4e8e\u7535\u6781\u6750\u6599\u7684\u4e3b\u4f53\u7ed3\u6784\u548c\u79bb\u5b50\u6269\u6563\u901a\u9053\u3002\u7a33\u5b9a\u7684\u4e3b\u4f53\u7ed3\u6784\u53ef\u4ee5\u907f\u514d\u6676\u683c\u548c\u6269\u6563\u901a\u9053\u7684\u574d\u584c\uff0c\u6709\u5229\u4e8e\u5b9e\u73b0\u53ef\u9006\u7684\u79bb\u5b50\u5d4c\u5165\u4e0e\u8131\u51fa\u3002\u56e0\u6b64\uff0c\u63d0\u9ad8\u94a0\u7535<\/strong>P2<\/strong>\u578b\u6b63\u6781\u79bb\u5b50\u52a8\u529b\u5b66\u7684\u5173\u952e\uff0c\u5728\u4e8e\u6784\u5efa\u5177\u6709\u66f4\u591a\u79bb\u5b50\u4f20\u8f93\u901a\u9053\u7684\u7a33\u5b9a\u4e3b\u4f53\u7ed3\u6784\u3002<\/strong><\/p>\n

2.<\/strong>\u3010\u6210\u679c\u63a0\u5f71\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u534e\u4fa8\u5927\u5b66\u4ed8\u82b3\u526f\u6559\u6388\u3001\u7f8e\u56fd\u963f\u8d21\u56fd\u5bb6\u5b9e\u9a8c\u5ba4\u5f90\u6842\u826f\u3001<\/strong>Amine<\/strong>\u6559\u6388\u4e0e\u53a6\u95e8\u5927\u5b66\u5b59\u4e16\u521a\u9662\u58eb\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09\u7b49\u4eba<\/strong>\uff0c\u63d0\u51fa\u901a\u8fc7\u589e\u52a0\u71b5\u4e0e\u6d3b\u6027\u6676\u9762\u6765\u5236\u5907\u517c\u5177\u5feb\u5145\u80fd\u529b\u4e0e\u957f\u5faa\u73af\u6027\u80fd\u7684<\/strong>P2<\/strong>\u578b\u5c42\u72b6\u6c27\u5316\u7269\u6b63\u6781\u6750\u6599\u3002<\/strong>\u6240\u5236\u5907\u7684\u9ad8\u71b5\u591a\u5143\u7d20\u6b63\u6781\u6750\u6599Na0.62<\/sub>Mn0.67<\/sub>Ni0.23<\/sub>Cu0.05<\/sub>Mg0.07<\/sub>Ti0.01<\/sub>O2<\/sub> (CuMgTi-571)\u5177\u6709\u66f4\u591a\u7684{010}\u6d3b\u6027\u6676\u9762\uff0c\u53ef\u4ee5\u6709\u6548\u63d0\u9ad8\u7ed3\u6784\u548c\u70ed\u7a33\u5b9a\u6027\uff0c\u83b7\u5f97\u66f4\u5feb\u7684\u9634\u79bb\u5b50\u6c27\u5316\u8fd8\u539f\u52a8\u529b\u5b66\u3002\u76f8\u5173\u7814\u7a76\u6210\u679c\u4ee5\u201cEntropy and crystal-facet modulation of P2-type layered cathodes for long-lasting sodium-based batteries\u201d\u4e3a\u9898\u53d1\u8868\u5728Nature Communications<\/em><\/strong>\u671f\u520a\u4e0a\u3002<\/p>\n

\"\"<\/p>\n

3.<\/strong>\u3010\u6838\u5fc3\u521b\u65b0\u70b9\u3011<\/strong><\/p>\n

    \n
  1. \u8bbe\u8ba1\u5408\u6210\u4e86\u4e00\u7cfb\u5217\u591a\u5143\u7d20P2\u578b\u5c42\u72b6\u6b63\u6781Na0.62<\/sub>Mn0.67<\/sub>Ni0.23<\/sub>Cu0.05<\/sub>Mg0.09-2y<\/sub>Tiy<\/sub>O2<\/sub>\u3002\u901a\u8fc7\u7cfb\u7edf\u6bd4\u8f83\u7535\u5316\u5b66\u6027\u80fd\uff0c\u7814\u7a76\u5b83\u4eec\u5728\u5145\u653e\u7535\u8fc7\u7a0b\u4e2d\u7684\u76f8\u53d8\u548cNa\u79bb\u5b50\u6269\u6563\u7cfb\u6570\uff0c\u660e\u786e\u4e86\u71b5\u4e0e\u6d3b\u6027\u6676\u9762\u3001\u9634\/\u9633\u79bb\u5b50\u52a8\u529b\u5b66\u4ee5\u53caP2\u578b\u6b63\u6781\u7535\u5316\u5b66\u6027\u80fd\u4e4b\u95f4\u7684\u5173\u7cfb\u3002<\/li>\n
  2. \u4e0eNa0.62Mn0.67Ni0.37O2\u76f8\u6bd4\uff0c\u9ad8\u71b5Na0.62<\/sub>Mn0.67<\/sub>Ni0.23<\/sub>Cu0.05<\/sub>Mg0.07<\/sub>Ti0.01<\/sub>O2<\/sub> (CuMgTi-571)\u6b63\u6781\u5177\u6709\u66f4\u9ad8\u7684\u5feb\u5145\u80fd\u529b\u4e0e\u66f4\u597d\u7684\u957f\u5faa\u73af\u6027\u80fd\uff0c\u53ef\u57281.2 A g\u22121<\/sup>\uff0810 C\uff09\u5927\u7535\u6d41\u5bc6\u5ea6\u4e0b\u5faa\u73af2000\u6b21\u540e\u4ecd\u4fdd\u755975%\u7684\u7535\u6c60\u5bb9\u91cf\u3002<\/li>\n<\/ol>\n

    4.<\/strong>\u3010\u6570\u636e\u6982\u89c8\u3011<\/strong><\/p>\n

    \u56fe<\/strong>1. <\/strong>\u4f18\u5316\u7684<\/strong>P2<\/strong>\u578b\u6b63\u6781\u7ed3\u6784\u8bbe\u8ba1\u7b56\u7565<\/strong><\/p>\n

    \"\"<\/p>\n

    \u591a\u9633\u79bb\u5b50\u9ad8\u71b5\u5c42\u72b6\u6b63\u6781\u53ef\u4ee5\u63d0\u4f9b\u9ad8\u7684\u7ed3\u6784\u7a33\u5b9a\u6027\u548c\u7a33\u5b9a\u7684\u79bb\u5b50\u6269\u6563\u901a\u9053\u3002\u5c42\u72b6\u6b63\u6781\u4e2d\u9ad8\u542b\u91cf\u7684{010}\u6676\u9762\u53ef\u4ee5\u4e3a\u79bb\u5b50\u5feb\u901f\u8fc1\u79fb\u63d0\u4f9b\u66f4\u591a\u901a\u9053\u3002\u53e6\u5916\uff0c\u71b5\u7684\u53d8\u5316\u4f1a\u5f71\u54cd\u4f53\u7cfb\u548c\u6676\u9762\u7684\u80fd\u91cf\u3002<\/p>\n

    \u56fe<\/strong>2. <\/strong>\u5408\u6210\u6b63\u6781\u7684\u5c42\u95f4\u8ddd\u8868\u5f81<\/strong><\/p>\n

    \"\"<\/p>\n

    \uff08a\uff09CuMgTi-533,\uff08b\uff09CuMgTi-552,\uff08c\uff09CuMgTi-571,\uff08d\uff09NaMNO2<\/sub>\u6837\u54c1\u7684XRD\u56fe\u8c31\u53ca\u5176\u5bf9\u5e94Rietveld\u7cbe\u4fee\u56fe\u3002\uff08e\uff09\u5de6\u56fe\u4e3aP2\u578b\u5c42\u72b6\u7ed3\u6784\u7684\u5c42\u95f4\u8ddd\uff08d<\/em>o-o\uff09\u539f\u5b50\u6a21\u578b\uff0c\u53f3\u56fe\u4e3a\u6676\u683c\u53c2\u6570c<\/em>\u7684\u53d6\u503c\u548c\u4ee5\u4e0a4\u79cd\u6837\u54c1\u7684\u5c42\u95f4\u8ddd\u3002<\/p>\n

    \u56fe<\/strong>3. <\/strong>\u6b63\u6781\u7684\u7269\u7406\u5316\u5b66\u8868\u5f81<\/strong><\/p>\n

    \"\"<\/p>\n

    \uff08a\uff09CuMgTi-533,\uff08b\uff09CuMgTi-552,\uff08c\uff09CuMgTi-571,\uff08d\uff09NaMNO2<\/sub>\u6837\u54c1\u7684SEM\u56fe\u50cf\u3002\uff08e\uff09CuMgTi-571\u7684HAADF-STEM\u56fe\u50cf\u548c\u5176\u4e2d\u76f8\u5e94\u7684Na, Mn, Ni, Cu, Mg, Ti\u5143\u7d20\u5206\u5e03\u56fe\u3002\uff08f\uff09CuMgTi-571\u7684\u9009\u533a\u7535\u5b50\u884d\u5c04\u56fe\u50cf\u3002\uff08g\uff09\u5177\u67096\u4e2a{010}\u6676\u9762\u548c2\u4e2a{001}\u6676\u9762\u7684\u5fae\u7c92\u793a\u610f\u56fe\uff0c\u53f3\u56fe\u4e3a{010}\u6676\u9762\u7684\u8868\u9762\u539f\u5b50\u5206\u5e03\u3002\uff08h\uff09CuMgTi-533, CuMgTi-552, CuMgTi-571, NaMNO2<\/sub>\u6837\u54c1{010}\u6676\u9762\u7684\u542b\u91cf\u548c\u6784\u578b\u71b5\u3002<\/p>\n

    \u56fe<\/strong>4. Na0.62<\/sub>Mn0.67<\/sub>Ni0.23<\/sub>Cu0.05<\/sub>Mg0.09-2y<\/sub>Tiy<\/sub>O2<\/sub><\/strong>\u548c<\/strong>NaMNO2<\/sub><\/strong>\u6b63\u6781\u7684\u5faa\u73af\u548c\u500d\u7387\u6027\u80fd<\/strong><\/p>\n

    \"\"<\/p>\n

    \uff08a\uff09CuMgTi-571\u4e0e\uff08b\uff09NaMNO2<\/sub>\u57280.1 C\uff0812 mA g-1<\/sup>\uff092.0-4.3 V\u7535\u538b\u8303\u56f4\u5185\u7684\u5145\u653e\u7535\u66f2\u7ebf\u3002\uff08c\uff09CuMgTi-571\u4e0eNaMNO2<\/sub>\u57280.1 C\uff0812 mA g-1<\/sup>\uff09\u7684100\u6b21\u5faa\u73af\u6027\u80fd\u3002\uff08d\uff09Na0.62<\/sub>Mn0.6<\/sub>7Ni0.23<\/sub>Cu0.05<\/sub>Mg0.09-2y<\/sub>Tiy<\/sub>O2<\/sub>\u4e0eNaMNO2<\/sub>\u4ece0.1 C\u523010 C\uff081 C=120 mA g-1<\/sup>\uff09\u7684\u500d\u7387\u6027\u80fd\u3002\u5faa\u73af\u4e0e\u500d\u7387\u6d4b\u8bd5\u5747\u572825\u2103\u4e0b\uff0c\u4ee5\u91d1\u5c5eNa\u4e3a\u8d1f\u6781\u7ec4\u88c5\u6263\u5f0f\u7535\u6c60\u8fdb\u884c\u3002<\/p>\n

    \u56fe<\/strong>5. Na0.62<\/sub>Mn0.67<\/sub>Ni0.23<\/sub>Cu0.05<\/sub>Mg0.09-2y<\/sub>Tiy<\/sub>O2<\/sub><\/strong>\u548c<\/strong>NaMNO2<\/sub><\/strong>\u6b63\u6781\u7684\u957f\u5faa\u73af\u6027\u80fd\u3002<\/strong><\/p>\n

    \"\"<\/p>\n

    \uff08a\uff09CuMgTi-571\u4e0e\uff08b\uff09NaMNO2<\/sub>\u57281 C\uff08120 mA g-1<\/sup>\uff092.0-4.3 V\u7535\u538b\u8303\u56f4\u5185\u7684\u5145\u653e\u7535\u66f2\u7ebf\u3002\uff08c\uff09CuMgTi-571\u4e0eNaMNO2<\/sub>\u57281 C\uff08120 mA g-1<\/sup>\uff09\u7684500\u6b21\u5faa\u73af\u6027\u80fd\u3002\uff08d\uff09CuMgTi-571\u4e0eNaMNO2<\/sub>\u572810 C\uff08120 mA g-1<\/sup>\uff09\u9ad8\u500d\u7387\u4e0b\u7684\u957f\u5faa\u73af\u6027\u80fd\u3002\u957f\u5faa\u73af\u6d4b\u8bd5\u572825\u2103\u4e0b\uff0c\u4ee5\u91d1\u5c5eNa\u4e3a\u8d1f\u6781\u7ec4\u88c5\u6263\u5f0f\u7535\u6c60\u8fdb\u884c\u3002\uff08c, d\uff09\u4e2d\u7684\u7a7a\u5fc3\u5706\u548c\u5b9e\u5fc3\u5706\u5206\u522b\u4ee3\u8868\u5145\u7535\u548c\u653e\u7535\u5bb9\u91cf\u3002<\/p>\n

    \u00a0<\/strong>\u56fe<\/strong>6. <\/strong>\u4e0d\u540c\u6b63\u6781\u6750\u6599<\/strong>Na<\/strong>\u79bb\u5b50\u6269\u6563\u7cfb\u6570\u7684\u7814\u7a76<\/strong><\/p>\n

    \"\"<\/p>\n

    \u00a0<\/strong>\u5145\u653e\u7535\u8fc7\u7a0b\u4e2d\uff08a\uff09CuMgTi-571\u4e0e\uff08b\uff09NaMNO2<\/sub>\u7684GITT\u66f2\u7ebf\u548c\u76f8\u5e94\u7684Na\u79bb\u5b50\u6269\u6563\u7cfb\u6570\u3002\uff08c-f\uff09\u5728\u4e0d\u540c\u7535\u538b\u8303\u56f4\u5185CuMgTi-571\u4e0eNaMNO2<\/sub>\u7684\u5e73\u5747Na\u79bb\u5b50\u6269\u6563\u7cfb\u6570\u3002GITT\u6d4b\u8bd5\u572825\u2103\u4e0b\uff0c\u4ee5\u91d1\u5c5eNa\u4e3a\u8d1f\u6781\u7ec4\u88c5\u6263\u5f0f\u7535\u6c60\u8fdb\u884c\u3002<\/p>\n

    \u56fe<\/strong>7. 25\u2103<\/strong>\u4e0b\u6263\u5f0f\u7535\u6c60\u539f\u4f4d<\/strong>HEXRD<\/strong>\u8868\u5f81<\/strong><\/p>\n

    \"\"<\/p>\n

    CuMgTi-571\u6b63\u6781\u57282.0-4.3 V\u7535\u538b\u8303\u56f4\u5185\u539f\u4f4dHEXRD\u7684\uff08a\uff09\u7011\u5e03\u70b9\u56fe\u4e0e\uff08b\uff09\u8f6e\u5ed3\u70b9\u56fe\u3002\uff08c\uff09\u5145\u653e\u7535\u8fc7\u7a0b\u4e2d\u7535\u6c60\u53c2\u6570\u548c\u7535\u6c60\u4f53\u79ef\u7684\u53d8\u5316\u3002<\/p>\n

    \u56fe<\/strong>8. <\/strong>\u6b63\u6781\u6750\u6599\u7684\u7ed3\u6784\u4e0e\u5f62\u8c8c\u7814\u7a76<\/strong><\/p>\n

    \"\"<\/p>\n

    \u8131\u94a0\u72b6\u6001\u4e0bCuMgTi-571\u4e0eNaMNO2<\/sub> 5 \u00b0C min\u22121<\/sup>\u4ece30 \u00b0C\u52a0\u70ed\u5230450 \u00b0C\u8fc7\u7a0b\u4e2d\u7684\uff08a\uff09\u8f6e\u5ed3\u70b9\u56fe\u4e0e\uff08b\uff09\u7011\u5e03\u70b9\u56fe\uff0c\u52a0\u70ed\u6d4b\u8bd5\u6837\u54c1\u4e3a\u5145\u7535\u81f34.2 V\u65f6\u6b63\u6781\u7247\u4e0a\u522e\u53d6\u7684\u8131\u94a0\u72b6\u6001\u6b63\u6781\u7c89\u672b\u3002<\/p>\n

    5.<\/strong>\u3010\u6210\u679c\u542f\u793a\u3011<\/strong><\/p>\n

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