{"id":240121,"date":"2022-07-22T07:55:39","date_gmt":"2022-07-21T23:55:39","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=240121"},"modified":"2022-07-21T14:31:42","modified_gmt":"2022-07-21T06:31:42","slug":"%e6%b8%a4%e6%b5%b7%e5%a4%a7%e5%ad%a6%e9%84%82%e6%b6%9b%e7%a8%8b%e9%a2%96mtchem%ef%bc%9a%e8%9a%80%e5%88%bb%e6%b3%95%e6%9e%84%e5%bb%basi-o-mo%e9%94%ae%e5%a2%9e%e5%bc%bamos2-%e8%92%99%e8%84%b1%e5%9c%9f","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=240121","title":{"rendered":"\u6e24\u6d77\u5927\u5b66\u9102\u6d9b&\u7a0b\u9896MTCHEM\uff1a\u8680\u523b\u6cd5\u6784\u5efaSi-O-Mo\u952e:\u589e\u5f3aMoS2\/\u8499\u8131\u571f\u5bf9Pb2+\u7684\u9009\u62e9\u6027\u5438\u9644\u80fd\u529b"},"content":{"rendered":"

\u7814\u7a76\u80cc\u666f<\/b><\/strong><\/p>\n

\u4e8c\u786b\u5316\u94bc\uff08MoS2<\/sub>\uff09\u4f5c\u4e3a\u5178\u578b\u7684\u4e8c\u7ef4\u7eb3\u7c73\u6750\u6599\uff0c\u7531\u4e8e\u5176\u663e\u8457\u7684\u5316\u5b66\u548c\u529b\u5b66\u6027\u80fd\uff0c\u52a0\u4e0a\u5176\u8fb9\u7f18\u4e0a\u7684S\u57fa\u56e2\uff0c\u5728\u5438\u9644\u9886\u57df\u5f97\u5230\u4e86\u5e7f\u6cdb\u7684\u5e94\u7528\u3002\u6839\u636e\u8f6f\u786c\u9178\u78b1\u7406\u8bba\uff0cMoS2<\/sub>\u4e2d\u7684S\u539f\u5b50\u5bf9Pb2+<\/sup>\u5177\u6709\u8f83\u5f3a\u7684\u5438\u9644\u80fd\u529b\uff0c\u8fd9\u662f\u56e0\u4e3aS2-<\/sup>\u5bf9Pb2+<\/sup>\u7684\u7ed3\u5408\u80fd\u529b\u8fdc\u5927\u4e8e\u5176\u4ed6\u5e38\u89c1\u91cd\u91d1\u5c5e\u79bb\u5b50\u3002\u56e0\u6b64\uff0c\u901a\u5e38\u4f5c\u4e3a\u5438\u9644\u5242\u53bb\u9664\u6c34\u6eb6\u6db2\u4e2dPb2+<\/sup>\u3002\u7136\u800c\uff0c\u7531\u4e8e\u5c42\u95f4\u8303\u5fb7\u534e\u529b\u548c\u8f83\u9ad8\u7684\u8868\u9762\u80fd\uff0cMoS2<\/sub>\u7eb3\u7c73\u7247\u5f88\u5bb9\u6613\u5806\u79ef\uff0c\u5927\u5927\u964d\u4f4e\u4e86\u6d3b\u6027\u4f4d\u70b9\u7684\u66b4\u9732\u7a0b\u5ea6\uff0c\u5bfc\u81f4\u5438\u9644\u80fd\u529b\u8f83\u5dee\u3002\u76ee\u524d\uff0c2H\u76f8MoS2<\/sub>\u5df2\u88ab\u5e7f\u6cdb\u5e94\u7528\u4e8e\u6c34\u4e2d\u91cd\u91d1\u5c5e\u7684\u53bb\u9664\u3002\u7136\u800c\uff0c\u7531\u4e8e\u7535\u8377\u8f6c\u79fb\u80fd\u529b\u8f83\u5dee\uff0c\u56e0\u6b64\u53ea\u6709\u8fb9\u7f18\u7684S\u539f\u5b50\u662f\u6d3b\u8dc3\u7684\u3002\u76f8\u6bd4\u4e4b\u4e0b\uff0c1T\u76f8MoS2<\/sub>\u53ef\u4ee5\u5f15\u5165\u66f4\u591a\u7684S\u7a7a\u4f4d\uff0cS\u7a7a\u4f4d\u65e2\u662f\u7ed3\u6784\u7f3a\u9677\u53c8\u662f\u63d0\u9ad8\u5438\u9644\u80fd\u529b\u7684\u6d3b\u6027\u4f4d\u70b9\u3002\u56e0\u6b64\uff0c1T\u76f8\u7684\u751f\u6210\u5bf9\u63d0\u9ad8MoS2<\/sub>\u7684\u5438\u9644\u80fd\u529b\u5177\u6709\u91cd\u8981\u610f\u4e49\u3002<\/p>\n

\u6587\u7ae0\u7b80\u4ecb<\/b><\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u6e24\u6d77\u5927\u5b66\u5316\u5b66\u4e0e\u6750\u6599\u5de5\u7a0b\u5b66\u9662\u6768\u59dd\u5b9c\u526f\u6559\u6388\u4e3a\u7b2c\u4e00\u4f5c\u8005\uff0c\u7a0b\u9896\u7855\u58eb\u7814\u7a76\u751f\u4e3a\u7b2c\u4e8c\u4f5c\u8005\uff0c\u9102\u6d9b\u6559\u6388\u4e3a\u901a\u8baf\u4f5c\u8005\u7684\u7814\u7a76\u6210\u679c\u300aConstruction Si-O-Mo bond via etching method: enhancing selective adsorption capacity of MoS2<\/sub>\/montmorillonite to Pb2+<\/sup>\u300b\u5728\u56fd\u9645\u8457\u540d\u671f\u520a\u300aMaterials Today Chemistry\u300b\uff08\u4e2d\u79d1\u9662\u4e00\u533a\uff0cIF=7.613\uff09\u53d1\u8868\u3002\u672c\u6587\u63d0\u51fa\u4e86\u4e00\u79cd\u60f0\u6027\u57fa\u4f53\u8868\u9762\u6d3b\u5316\u7b56\u7565\uff0c\u5373\u5c06\u6c34\u70ed\u6cd5\u5236\u5907\u7684MoS2<\/sub>\/\u8499\u8131\u571f(MMT)\u590d\u5408\u6750\u6599\u6d78\u6ce1\u5728NaF\u6eb6\u6db2\u4e2d(F-Mt)\u3002\u5176\u4e2dNa+<\/sup>\u63d2\u5c42\u8bf1\u5bfcMoS2<\/sub>\u4e2d2H\u76f8\u8f6c\u53d8\u4e3a1T\u76f8\uff0c\u63d0\u4f9b\u5927\u91cf\u7684S\u7a7a\u4f4d\uff0c\u66b4\u9732\u51fa\u6709\u6548\u7684Mo4+<\/sup>\u3002\u540c\u65f6\uff0c\u7531\u4e8eMMT\u7ed3\u6784\u4e2d\u90e8\u5206[Si4<\/sub>O10<\/sub>]4-<\/sup>\u88abF–<\/sup>\u523b\u8680\uff0c\u81f4\u4f7f\u5176\u8868\u9762\u88ab\u6fc0\u6d3b\uff0c\u5f62\u6210Si-O-Mo\u952e\uff0c\u4fc3\u8fdb\u7535\u8377\u8f6c\u79fb\u3002\u7535\u8377\u8f6c\u79fb\u901f\u7387\u7684\u63d0\u9ad8\u4f7fMoS2<\/sub>\u4e2d\u7684S2-<\/sup>\u79ef\u7d2f\u4e86\u66f4\u591a\u7684\u8d1f\u7535\u8377\uff0c\u5927\u5927\u589e\u5f3a\u4e86\u5bf9Pb2+<\/sup>\u7684\u5438\u9644\u80fd\u529b\u3002\u6b64\u5916\uff0c\u6d3b\u5316\u60f0\u6027\u57fa\u5e95\u8868\u9762\u6982\u5ff5\u53ef\u4ee5\u63a8\u5e7f\u5230\u5176\u4ed6\u7eb3\u7c73\u6750\u6599\uff0c\u4f7f\u5176\u5728\u5438\u9644\u65b9\u9762\u53d1\u6325\u5de8\u5927\u7684\u5e94\u7528\u6f5c\u529b\u3002<\/p>\n

\"\"<\/b><\/strong><\/p>\n

\u56fe\u5f62\u6458\u8981<\/b><\/strong><\/p>\n

\u00a0\"\"<\/b><\/strong><\/p>\n

\u672c\u6587\u8981\u70b9<\/b><\/strong><\/p>\n

\u8981\u70b9\u4e00: F-Mt\u7684\u5f62\u8c8c\u53ca\u7ed3\u6784\u5206\u6790<\/p>\n

\"\"<\/b><\/strong><\/p>\n

\u56fe1\uff1a<\/p>\n

(a)\u548c(c) Mt\u7684SEM\u56fe;<\/p>\n

(b)\u548c(d) F-Mt\u7684SEM\u56fe;<\/p>\n

(e)-(h) F-Mt\u7684TEM\u56fe;<\/p>\n

(i)\u548c(j)\u00a0F-Mt\u7684mapping\u548cEDS\u56fe\u3002<\/p>\n

\"\"<\/b><\/strong><\/p>\n

\u56fe2\uff1a<\/p>\n

(a) Mt\u548cF-Mt\u7684Raman\u8c31\u56fe;<\/p>\n

(b)\u548c(c) Mo\u00a03d\u548cS 2p\u7684\u9ad8\u5206\u8fa8\u7387XPS\u8c31\u56fe\uff1b<\/p>\n

(e)-(g) (2\u00d72), (3\u00d73) (4\u00d74) MoS2<\/sub>\u8d85\u80de\u7ed3\u6784\u5438\u9644Pb2+<\/sup>\u540e\u7684PDOS\u8c31\u56fe;<\/p>\n

(h)\u00a0Na+<\/sup>\u63d2\u5c42\u4f5c\u7528\u8bf1\u5bfcMoS2<\/sub>\u4e2d2H\u76f8\u8f6c\u5316\u4e3a1T\u76f8\u7684\u8fc7\u7a0b\u3002<\/p>\n

\"\"<\/b><\/strong><\/p>\n

\u56fe3\uff1a<\/p>\n

(a) O 1s\u9ad8\u5206\u8fa8\u7387XPS\u8c31\u56fe;<\/p>\n

(b) Mt\u4e0eF-Mt\u7684IR\u8c31\u56fe\uff1b<\/p>\n

(c)\u00a0NaF\u5bf9MMT\u7684\u523b\u8680\u8fc7\u7a0b\uff1b<\/p>\n

(d)\u548c(e) Mt\u4e0eF-Mt\u7684CV\u66f2\u7ebf\u548c\u963b\u6297\u66f2\u7ebf\u3002<\/p>\n

\u8981\u70b9\u4e8c\uff1aF-Mt\u5bf9Pb2+<\/sup>\u7684\u5438\u9644\u6027\u80fd\u53ca\u5438\u9644\u673a\u7406<\/p>\n

\"\" <\/p>\n

\u56fe4\uff1a<\/p>\n

(a) F-Mt\u7528\u91cf\u3001\u65f6\u95f4\u3001\u6e29\u5ea6\u548cpH\u5bf9Pb2+<\/sup>\u53bb\u9664\u6548\u679c\u7684\u5f71\u54cd\uff1b<\/p>\n

(b)\u00a0\u4e0d\u540c\u65f6\u95f4\u4e0bMt\u548cF-Mt\u5bf9Pb2+<\/sup>\u7684\u53bb\u9664\u7387;<\/p>\n

(c) \u5171\u5b58\u91d1\u5c5e\u79bb\u5b50\u5bf9F-Mt\u5438\u9644Pb2+<\/sup>\u7684\u5f71\u54cd\uff1b<\/p>\n

(d) \u5ba4\u6e29\u4e0b\u8d2e\u5b5860 d\u540eF-Mt\u5bf9Pb2+<\/sup>\u7684\u5438\u9644\u6027\u80fd\u6bd4\u8f83\uff1b<\/p>\n

(e) Pb2+<\/sup>\u53bb\u9664\u7387\u6807\u51c6\u5316\u6548\u5e94\u5e15\u7d2f\u6258\u56fe:(A) F-Mt\u6295\u52a0\u91cf,\u00a0(B)\u65f6\u95f4, (C)\u6e29\u5ea6, (D) pH;<\/p>\n

(f)\u00a0\u5438\u9644\u6b63\u6001\u56fe;<\/p>\n

(g) \u5f71\u54cdPb2+<\/sup>\u53bb\u9664\u7387\u7684\u4e3b\u8981\u56e0\u7d20\u56fe;<\/p>\n

(h) \u5f71\u54cdPb2+<\/sup>\u53bb\u9664\u7387\u7684\u76f8\u4e92\u4f5c\u7528\u6548\u5e94\u56fe\u3002<\/p>\n

\"\"<\/p>\n

\u56fe5\uff1a<\/p>\n

(a) F-Mt\u5438\u9644Pb2+<\/sup>\u7684\u5faa\u73af\u4f7f\u7528\u5bff\u547d;<\/p>\n

(b) F-Mt\u6bcf\u6b21\u5438\u9644-\u89e3\u5438\u5faa\u73af\u540e\u5bf9\u5e94\u7684SEM\u56fe\u3002<\/p>\n

\"\"<\/p>\n

\u56fe6\uff1a<\/p>\n

(a) F-Mt\u5438\u9644Pb2+<\/sup>\u524d\u540e\u7684XRD\u8c31\u56fe;<\/p>\n

(b)\u548c(c)\u00a0F-Mt\u5438\u9644Pb2+<\/sup>\u540e\u7684SEM\u56fe;<\/p>\n

(d)\u548c(e) F-Mt\u5438\u9644Pb2+<\/sup>\u540e\u7684mapping\u548cEDS\u56fe\uff1b<\/p>\n

(f)-(h)\u00a0O 1s,\u00a0S 2p\u548cPb 4f\u7684\u9ad8\u5206\u8fa8\u7387XPS\u8c31\u56fe\u3002<\/p>\n

\"\"<\/p>\n

\u56fe7\uff1a<\/p>\n

(a)\u548c(b) MoS2<\/sub>\u548cD-MoS2<\/sub>\u7684\u80fd\u5e26\u7ed3\u6784\u56fe;<\/p>\n

(c)\u548c(d) MoS2<\/sub>\u548cD-MoS2<\/sub>\u5438\u9644Pb2+<\/sup>\u540e\u7684PDOS\u56fe\u3002<\/p>\n

\u7ed3\u8bba<\/b><\/strong><\/p>\n

\u672c\u7814\u7a76\u901a\u8fc7\u6c34\u70ed\u6cd5\u5c06MoS2<\/sub>\u539f\u4f4d\u751f\u957f\u5728MMT\u8868\u9762\uff0c\u7136\u540e\u5c06\u5176\u6d78\u6ce1\u5728NaF\u6eb6\u6db2\u4e2d\u3002\u5f97\u5230\u7684F-Mt\u53ef\u4ee5\u6709\u6548\u5730\u89e3\u51b3MoS2<\/sub>\u7eb3\u7c73\u7247\u6613\u5806\u79ef\u548c\u758f\u6c34\u6027\u7684\u95ee\u9898\u3002\u6b64\u5916\uff0cNaF\u4e2d\u4e0d\u4ec5Na+<\/sup>\u8d77\u5230\u63d2\u5c42\u4f5c\u7528\uff0cF–<\/sup>\u8fd8\u53c2\u4e0e\u523b\u8680\u4f5c\u7528\uff0c\u6709\u6548\u63d0\u9ad8\u8fb9\u7f18\u6d3b\u6027\u4f4d\u70b9\u7684\u53ef\u7528\u6027\uff0c\u5e76\u4fc3\u8fdbF-Mt\u4e2dSi-O-Mo\u952e\u7684\u5f62\u6210\u3002Si-O-Mo\u952e\u7684\u751f\u6210\u52a0\u901f\u4e86MoS2<\/sub>\u4e0eMMT\u4e4b\u95f4\u7684\u7535\u8377\u8f6c\u79fb\u901f\u7387\uff0c\u6709\u52a9\u4e8e\u589e\u5f3aS2-<\/sup>\u7684\u8d1f\u7535\u8377\u5bc6\u5ea6\u8fdb\u800c\u589e\u5f3a\u5bf9Pb2+<\/sup>\u7684\u5438\u9644\u80fd\u529b\u3002<\/p>\n

\u4f5c\u8005\u7b80\u4ecb<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\u901a\u8baf\u4f5c\u8005 \u9102\u6d9b\uff1a<\/strong>\u535a\u58eb\uff0c\u6559\u6388\uff0c\u6e24\u6d77\u5927\u5b66\u73af\u5883\u5de5\u7a0b\u4e13\u4e1a\u5e26\u5934\u4eba\uff0c\u7855\u58eb\u7814\u7a76\u751f\u5bfc\u5e08\u3002\u8fbd\u5b81\u7701\u6bdb\u76ae\u7eff\u8272\u5236\u9020\u4ea7\u4e1a\u6280\u672f\u521b\u65b0\u6218\u7565\u8054\u76df\u7406\u4e8b\u957f\uff0c\u6e24\u6d77\u5927\u5b66\u73af\u5883\u7814\u7a76\u9662\u526f\u9662\u957f\uff0c\u9526\u5dde\u5e02\u91d1\u5c5e\u6750\u6599\u4ea7\u4e1a\u521b\u65b0\u8054\u76df\u4e13\u5bb6\u59d4\u5458\uff0c\u6e24\u6d77\u5927\u5b66\u73af\u4fdd\u4ea7\u4e1a\u6280\u672f\u7814\u7a76\u6240\u6240\u957f\u3002\u7814\u7a76\u5174\u8da3\uff1a\u5316\u5de5\u6e05\u6d01\u751f\u4ea7\u5de5\u827a\uff0c\u571f\u58e4\u4e0e\u6c34\u6c61\u67d3\u4fee\u590d\u6280\u672f\u3001\u4f4e\u78b3\u51cf\u78b3\u5de5\u827a\u6280\u672f\u5f00\u53d1\u53ca\u949b\u57fa\u529f\u80fd\u6750\u6599\u7684\u5236\u5907\u5de5\u827a\u53ca\u5e94\u7528\u3002\u5728ACS Appl Mater Interfaces<\/em>\uff0cJ<\/em>\u00a0H<\/em>aza<\/em>rd Mater<\/em>\uff0c<\/em>Sep Purif Technol<\/em>\uff0c<\/em>J CLEAN PROD<\/em>\uff0c<\/em>Mater. Today Che<\/em>m\uff0c <\/em>J. Environ. Chem. Eng<\/em>\u7b49\u56fd\u9645\u8457\u540d\u671f\u520a\u4e0a\u4ee5\u7b2c\u4e00\/\u901a\u8baf\u4f5c\u8005\u53d1\u8868SCI\u6536\u5f55\u8bba\u658725\u7bc7\uff0c\u4e3b\u630124\u9879\u79d1\u7814\u9879\u76ee\uff0c\u4ee5\u7b2c\u4e00\u53d1\u660e\u4eba\u83b7\u5f97\u6388\u6743\u53d1\u660e\u4e13\u522913\u9879\uff0c\u5355\u9879\u4e13\u5229\u8f6c\u5316\u989d\u5ea6\u8d85100\u4e07\uff0c\u8fd1\u4e09\u5e74\u79d1\u6280\u6210\u679c\u8f6c\u5316\u5408\u540c\u91d1\u989d623\u4e07\u3002<\/p>\n

\u7535\u5b50\u90ae\u7bb1\uff1aetao@bhu.edu.cn<\/a><\/p>\n

\u00a0\"\"
\n<\/b><\/strong><\/p>\n

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\u7535\u5b50\u90ae\u7bb1\uff1a1335157666@qq.com<\/u><\/a><\/p>\n

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\u7b2c\u4e00\u4f5c\u8005 \u6768\u59dd\u5b9c\uff1a<\/strong>\u6e24\u6d77\u5927\u5b66\u73af\u5883\u5de5\u7a0b\u4e13\u4e1a\u526f\u6559\u6388\uff0c\u7855\u58eb\u751f\u5bfc\u5e08\u3002\u7814\u7a76\u5174\u8da3\uff1a\u571f\u58e4\u4fee\u590d\u6280\u672f\u548c\u56fa\u4f53\u5e9f\u7269\u8d44\u6e90\u5316\u3002\u5728J<\/em>\u00a0H<\/em>aza<\/em>rd Mater<\/em>\uff0c<\/em>J CLEAN PROD<\/em>\uff0cACS Appl Mater Interfaces\uff0cSep Purif Technol\uff0c<\/em>Mater. Today Che<\/em>m\uff0c<\/em>J. Alloys Compd<\/em>\u7b49\u56fd\u9645\u8457\u540d\u671f\u520a\u4e0a\u4ee5\u7b2c\u4e00\/\u901a\u8baf\u4f5c\u8005\u53d1\u8868SCI\u6536\u5f55\u8bba\u658716\u7bc7\uff0c\u62c5\u4efb\u300aJournal of Alloys and Compounds<\/em>\u300b\uff0c\u300aJournal of Cleaner Production<\/em>\u300b\uff0c\u300aJournal of Polymers and the Environment<\/em>\u300b\u7b49SCI\u77e5\u540d\u671f\u520a\u5ba1\u7a3f\u4eba\u3002<\/p>\n

\u7535\u5b50\u90ae\u7bb1\uff1ayangshuyi@bhu.edu.cn<\/p>\n

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\u7b2c\u4e8c\u4f5c\u8005<\/strong>\u00a0<\/strong>\u7a0b\u9896\uff1a<\/strong>\u6e24\u6d77\u5927\u5b66\u5316\u5b66\u5de5\u827a\u4e13\u4e1a\u7855\u58eb\u7814\u7a76\u751f\u3002\u7814\u7a76\u5174\u8da3\uff1a\u91cd\u91d1\u5c5e\u571f\u58e4\u4fee\u590d\u548c\u6c34\u4f53\u4e2d\u91cd\u91d1\u5c5e\u7684\u6df1\u5ea6\u53bb\u9664\u3002\u76ee\u524d\u5728Mater. Today Che<\/em>m\uff0c<\/em>J. Environ. Chem. Eng\uff0cInorg Chem. Commun<\/em>\u671f\u520a\u4e0a\u53d1\u8868SCI\u6536\u5f55\u8bba\u65874\u7bc7\uff0c\u4e3b\u6301\u6e24\u6d77\u5927\u5b66\u7814\u7a76\u751f\u521b\u65b0\u57fa\u91d1\u9879\u76ee1\u9879\uff0c\u6388\u6743\u53d1\u660e\u4e13\u52291\u9879\u3002<\/p>\n

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\u6587\u7ae0\u4fe1\u606f <\/b><\/strong><\/p>\n

S.\u00a0Yang,Y. Cheng, T. E*, Y. Wang,L. Liu, Y. Li**, D. Wang, J. Qian, Construction Si\u2013O\u2013Mo bond via etching method: enhancing selective adsorption capacity of MoS2<\/sub>\/montmorillonite to Pb2+<\/sup>. Materials Today Chemistry<\/i><\/em><\/strong>\u00a02022, 26 101056.\u00a0https:\/\/doi.org\/10.1016\/j.mtchem.2022.101056<\/a><\/p>\n

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