{"id":246660,"date":"2023-02-12T06:27:09","date_gmt":"2023-02-11T22:27:09","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=246660"},"modified":"2023-02-09T14:27:37","modified_gmt":"2023-02-09T06:27:37","slug":"afm%ef%bc%9a%e7%a2%b3%e7%82%b9%e6%8f%92%e5%b1%82mxene%e8%96%84%e8%86%9c%e7%94%b5%e6%9e%81%e6%9e%84%e5%bb%ba%e9%ab%98%e6%80%a7%e8%83%bd%e6%9f%94%e6%80%a7%e8%b6%85%e7%ba%a7%e7%94%b5%e5%ae%b9%e5%99%a8","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=246660","title":{"rendered":"AFM\uff1a\u78b3\u70b9\u63d2\u5c42MXene\u8584\u819c\u7535\u6781\u6784\u5efa\u9ad8\u6027\u80fd\u67d4\u6027\u8d85\u7ea7\u7535\u5bb9\u5668"},"content":{"rendered":"

\u4e00\u3001\u5bfc\u8bfb<\/strong><\/p>\n

\u8d85\u7ea7\u7535\u5bb9\u5668\u5177\u6709\u529f\u7387\u5bc6\u5ea6\u9ad8\u3001\u5faa\u73af\u5bff\u547d\u957f\u548c\u5feb\u901f\u5145\u653e\u7535\u7b49\u4f18\u70b9\uff0c\u662f\u4e00\u7c7b\u5177\u6709\u5e7f\u6cdb\u5e94\u7528\u524d\u666f\u7684\u7535\u5316\u5b66\u50a8\u80fd\u5668\u4ef6\u3002\u7136\u800c\uff0c\u53ef\u7a7f\u6234\u548c\u4fbf\u643a\u5f0f\u7535\u5b50\u8bbe\u5907\u7684\u5feb\u901f\u53d1\u5c55\u4e0d\u4ec5\u8981\u6c42\u50a8\u80fd\u5668\u4ef6\u5177\u6709\u4f18\u5f02\u7684\u67d4\u97e7\u6027\uff0c\u4eba\u4eec\u5bf9\u4e8e\u9ad8\u7eed\u822a\u7684\u9700\u6c42\u4e5f\u4f7f\u5f97\u50a8\u80fd\u5668\u4ef6\u9700\u8981\u5728\u5c3d\u53ef\u80fd\u5c0f\u7684\u7a7a\u95f4\u5185\u5b58\u50a8\u66f4\u591a\u7684\u7535\u8377\uff0c\u8fd9\u5c31\u5bf9\u7535\u6781\u7684\u4f53\u79ef\u6027\u80fd\u63d0\u51fa\u4e86\u66f4\u9ad8\u7684\u8981\u6c42\u3002\u7531\u4e8e\u4e8c\u7ef4\uff082D\uff09\u6750\u6599\u6613\u4e8e\u5236\u5907\u6210\u5177\u6709\u4f18\u5f02\u67d4\u97e7\u6027\u548c\u9ad8\u5806\u79ef\u5bc6\u5ea6\u7684\u81ea\u652f\u6491\u8584\u819c\u7535\u6781\uff0c\u5176\u5728\u67d4\u6027\u8d85\u7ea7\u7535\u5bb9\u5668\u4e2d\u7684\u5e94\u7528\u5f97\u5230\u4e86\u7814\u7a76\u8005\u5e7f\u6cdb\u7684\u5173\u6ce8\u3002<\/p>\n

\u5728\u4f17\u591a\u76842D\u6750\u6599\u4e2d\uff0cMXenes\u5177\u6709\u7c7b\u91d1\u5c5e\u7684\u5bfc\u7535\u6027\u3001\u9ad8\u5bc6\u5ea6\u3001\u4e30\u5bcc\u7684\u8868\u9762\u5316\u5b66\u6d3b\u6027\u3001\u67d4\u97e7\u6027\u597d\u548c\u673a\u68b0\u5f3a\u5ea6\u9ad8\u7b49\u7279\u6027\uff0c\u662f\u50a8\u80fd\u3001\u50ac\u5316\u3001\u4f20\u611f\u3001\u7535\u78c1\u5c4f\u853d\u7b49\u9886\u57df\u7684\u70ed\u95e8\u6750\u6599\u3002Ti3<\/sub>C2<\/sub>Tx<\/sub> MXene\u7531\u4e8e\u6027\u8d28\u8f83\u4e3a\u7a33\u5b9a\u3001\u5408\u6210\u76f8\u5bf9\u6210\u719f\uff0c\u662f\u7814\u7a76\u6700\u4e3a\u5e7f\u6cdb\u7684MXene\uff0c\u5176\u7528\u4e8e\u8d85\u7ea7\u7535\u5bb9\u5668\u67d4\u6027\u7535\u6781\u6750\u6599\u7684\u62a5\u9053\u5c42\u51fa\u4e0d\u7a77\u3002\u7136\u800c\uff0c\u4e8c\u7ef4\u6750\u6599\u5c42\u95f4\u5f3a\u7684\u8303\u5fb7\u534e\u529b\u5bfc\u81f4MXene\u5b58\u5728\u4e25\u91cd\u7684\u7247\u5c42\u5806\u53e0\uff0c\u8fd9\u4e00\u73b0\u8c61\u5728\u4e8c\u7ef4\u7247\u5c42\u6709\u5e8f\u6392\u5217\u7684\u819c\u7535\u6781\u4e2d\u5c24\u4e3a\u4e25\u91cd\uff0c\u4f7f\u5f97\u79bb\u5b50\u4f20\u8f93\u9014\u5f84\u5ef6\u957f\uff0c\u964d\u4f4e\u79bb\u5b50\u53ef\u53ca\u7684\u6d3b\u6027\u8868\u9762\u8868\uff0c\u6700\u7ec8MXene\u819c\u7684\u7535\u5316\u5b66\u6027\u80fd\u4e0d\u5c3d\u5982\u4eba\u610f\u3002<\/p>\n

\u5c06\u5bc6\u96c6\u5806\u53e0\u7684MXene\u8584\u819c\u8f6c\u53d8\u4e3a\u4e09\u7ef4\uff083D\uff09\u591a\u5b54\u7ed3\u6784\uff0c\u53ef\u4ee5\u6709\u6548\u5730\u6291\u5236MXene\u7247\u5c42\u7684\u5806\u53e0\u73b0\u8c61\uff0c\u66b4\u9732\u5176\u6d3b\u6027\u6bd4\u8868\u9762\uff0c\u4fc3\u8fdb\u79bb\u5b50\/\u7535\u5b50\u5728\u7535\u6781\u754c\u9762\u7684\u4f20\u8f93\u3002\u76ee\u524d\uff0c3D MXene\u8584\u819c\u7684\u5236\u5907\u65b9\u6cd5\u53ea\u8981\u5305\u62ec\u6a21\u677f\u6cd5\u3001\u5316\u5b66\u7ec4\u88c5\u3001\u9aa8\u67b6\u6cd5\u7b49\u3002\u77f3\u58a8\u70ef\u3001\u78b3\u7eb3\u7c73\u7ba1\u3001\u7eb3\u7c73\u78b3\u7ea4\u7ef4\u3001\u548c\u805a\u5408\u7269\u7b49\u4f4e\u7ef4\u7eb3\u7c73\u6750\u6599\u53ef\u4ee5\u8d77\u5230\u201c\u5c42\u95f4\u95f4\u9694\u7269\u201d\u7684\u4f5c\u7528\uff0c\u5f15\u5165\u5230MXene\u5c42\u95f4\u540e\u53ef\u4ee5\u589e\u52a0\u5176\u5c42\u95f4\u8ddd\uff0c\u4e5f\u53ef\u4ee5\u6709\u6548\u964d\u4f4eMXene\u8584\u819c\u5c42\u95f4\u518d\u5806\u79ef\u3002\u7136\u800c\uff0c\u4e09\u7ef4\u7ed3\u6784\u7684\u6784\u7b51\u867d\u7136\u53ef\u4ee5\u6539\u5584MXene\u7684\u7535\u5316\u5b66\u6027\u80fd\uff0c\u4f46\u662f\u4e0d\u53ef\u907f\u514d\u5730\u964d\u4f4e\u4e86MXene\u819c\u7684\u5bc6\u5ea6\uff0c\u5f71\u54cd\u5176\u4f53\u79ef\u6027\u80fd\u3002<\/p>\n

\u00a0<\/strong><\/p>\n

\u4e8c\u3001\u6210\u679c\u63a0\u5f71<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u5317\u4eac\u5316\u5de5\u5927\u5b66\u5f90\u658c\u6559\u6388\u56e2\u961f\u63d0\u51fa\u4e86\u4e00\u79cd\u201c\u51dd\u80f6\u81f4\u5bc6\u5316-\u78b3\u70b9\u63d2\u5c42\u201d\u7b56\u7565\uff0c\u901a\u8fc7\u6d77\u85fb\u9178\u9499\u5728\u4e8c\u7ef4MXene\u5c42\u95f4\u7684\u51dd\u80f6\u5316\u53ca\u540e\u7eed\u70ad\u5316\u5904\u7406\uff0c\u5236\u5907\u5177\u6709\u9ad8\u79bb\u5b50\u53ef\u53ca\u7684\u6d3b\u6027\u8868\u9762\u548c\u9ad8\u5bc6\u5ea6\u7684\u67d4\u6027MXene\u8584\u819c\u7535\u6781\u3002\u5728\u51dd\u80f6\u5316\u8fc7\u7a0b\u4e2d\uff0cMXene\u5c42\u95f4\u7684\u6d77\u85fb\u9178\u94a0\u4e0e\u9499\u79bb\u5b50\u4ea4\u8054\u5f62\u6210\u6d77\u85fb\u9178\u9499\u6c34\u51dd\u80f6\uff08CA\uff09\uff0c\u968f\u540e\u5728\u84b8\u53d1\u5e72\u71e5\u8fc7\u7a0b\u4e2d\u6bdb\u7ec6\u7ba1\u4f5c\u7528\u529b\u53ef\u4ee5\u8bf1\u5bfcMXene\/CA\u6c34\u51dd\u80f6\u819c\u8868\u73b0\u51fa\u8f83\u9ad8\u7684\u5806\u79ef\u5bc6\u5ea6\uff084.0 g cm-3<\/sup>\uff09\u3002\u968f\u540e\u7ecf\u9ad8\u6e29\u5904\u7406\u4f7f\u5f97CA\u5f62\u6210\u884d\u751f\u78b3\u70b9\u5d4c\u5165\u5230MXene\u5c42\u95f4\uff0c\u4f7f\u5f97MXene\/CAC\u8584\u819c\u8868\u73b0\u51fa3.3 g cm-3<\/sup>\u7684\u9ad8\u5806\u79ef\u5bc6\u5ea6\u548c13.7 \u00c5\u7684\u5927\u5c42\u95f4\u8ddd\u3002MXene\/CAC\u8584\u819c\u57281 A g-1<\/sup>\u8d28\u91cf\u6bd4\u7535\u5bb9\u548c\u4f53\u79ef\u6bd4\u7535\u5bb9\u5206\u522b\u8fbe\u5230372.6 F g-1<\/sup>\u548c1244.6 F cm-3<\/sup>\uff0c\u5373\u4f7f\u7535\u6d41\u5bc6\u5ea6\u8fbe\u52301000 A g-1<\/sup>\u65f6\uff0c\u5176\u4ecd\u7136\u4fdd\u6301662.5 F cm-3<\/sup>\u7684\u4f53\u79ef\u6bd4\u7535\u5bb9\uff0c\u5177\u6709\u4f18\u5f02\u7684\u4f53\u79ef\u6027\u80fd\u548c\u500d\u7387\u6027\u80fd\u3002MXene\/CAC\u8584\u819c\u8fd8\u5177\u6709\u826f\u597d\u7684\u5faa\u73af\u7a33\u5b9a\u6027\uff0c\u57283\u4e07\u6b21\u5faa\u73af\u540e\u7684\u7535\u5bb9\u4fdd\u7559\u7387\u8fbe\u523093.5%\u3002\u6b64\u5916\uff0c\u572810.0 mg cm-2<\/sup>\u7684\u8d85\u9ad8\u9762\u8f7d\u91cf\u4e0b\uff0cMXene\/CAC\u8584\u819c\u57281 A g-1<\/sup>\u65f6\u4e5f\u5b9e\u73b0\u4e86912.1 F cm-3<\/sup>\u7684\u4f53\u79ef\u6bd4\u7535\u5bb9\u3002\u5f53\u7ec4\u88c5\u6210\u5168\u56fa\u6001\u5bf9\u79f0\u8d85\u7ea7\u7535\u5bb9\u5668\u65f6\uff0c\u6700\u5927\u4f53\u79ef\u80fd\u91cf\u5bc6\u5ea6\u53ef\u4ee5\u8fbe\u523027.2 Wh L-1<\/sup>\uff0c\u4e14\u5728\u4e0d\u540c\u5f2f\u66f2\u7a0b\u5ea6\u53ca\u4e32\u5e76\u8054\u72b6\u6001\u4e0b\u5747\u5c55\u73b0\u51fa\u4f18\u5f02\u7684\u6027\u80fd\u3002\u76f8\u5173\u7814\u7a76\u5de5\u4f5c\u4ee5\u201cFlexible Carbon Dots-Intercalated MXene Film Electrode with Outstanding Volumetric Performance for Supercapacitors<\/strong>\u201d\u4e3a\u9898\u53d1\u8868\u5728\u56fd\u9645\u77e5\u540d\u671f\u520aAdvanced Functional Materials<\/em>\u4e0a\u3002<\/p>\n

\"\"<\/p>\n

\u4e09\u3001\u6838\u5fc3\u521b\u65b0\u70b9<\/strong><\/p>\n

\u672c\u7814\u7a76\u901a\u8fc7\u201c\u51dd\u80f6\u81f4\u5bc6\u5316-\u78b3\u70b9\u63d2\u5c42\u201d\u7b56\u7565\uff0c\u6784\u7b51\u4e86\u4e00\u79cd\u517c\u5177\u9ad8\u79bb\u5b50\u53ef\u53ca\u7684\u6d3b\u6027\u8868\u9762\u548c\u9ad8\u5bc6\u5ea6\u7684\u8d85\u7ea7\u7535\u5bb9\u5668MXene\u819c\u7535\u6781\uff08MXene\/CAC\uff09\u3002MXene\/CAC\u819c\u5177\u6709\u9ad8\u7684\u4f53\u79ef\u6bd4\u5bb9\u91cf\u3001\u4f18\u5f02\u7684\u500d\u7387\u6027\u80fd\u548c\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u672c\u7814\u7a76\u4e3a\u6784\u5efa\u9ad8\u4f53\u79ef\u6027\u80fd\u7684MXene\u8584\u819c\u7535\u6781\u63d0\u4f9b\u4e86\u4e00\u79cd\u7b80\u5355\u800c\u6709\u6548\u7684\u7b56\u7565\u3002<\/p>\n

\u56db\u3001\u6570\u636e\u6982\u89c8<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe1 a) MXene\/CAC\u8584\u819c\u5236\u5907\u793a\u610f\u56fe\u3002b,c) \u663e\u793ai) MXene\/CA-5%\u6c34\u51dd\u80f6\u548cii) MXene\/CA-5%\u8584\u819c\u7684\u5f62\u8c8c\u3001\u67d4\u97e7\u6027\u548c\u53ef\u89c4\u6a21\u5316\u5236\u5907\u7684\u6570\u7801\u7167\u7247\u3002d) p-MXene\u3001a-MXene\u548cMXene\/CAC\u8584\u819c\u7684\u7535\u5bfc\u7387(n = 10)\u3002\u00a9 2022 John Wiley & Sons, Inc.<\/strong><\/p>\n

\u00a0\"\"<\/strong><\/p>\n

\u56fe2 a,b) p-MXene\u548cc,d) MXene\/CAC-5%\u8584\u819c\u7684\u622a\u9762SEM\u56fe\u50cf\u3002e) MXene\/CAC-5%\u7c89\u672b\u7684TEM\u548cf) HRTEM\u56fe\u50cf\uff0c\u56fe2e\u7684\u63d2\u56fe\u663e\u793a\u4e86\u78b3\u70b9(n = 100)\u7684\u7c92\u5f84\u76f4\u65b9\u56fe\u3002g) MXene\/CAC-5%\u8584\u819c\u7684SEM\u56fe\u50cf\uff0c\u5bf9\u5e94\u7684EDS\u6620\u5c04\u663e\u793aTi\u3001Ca\u3001Na\u5143\u7d20\u7684\u5206\u5e03\u3002p-MXene\u3001a-MXene\u3001MXene\/CA\u548cMXene\/CAC-5%\u8584\u819c\u7684h)\u819c\u5bc6\u5ea6(n = 8)\uff0ci) XRD\u8c31\u56fe\uff0cj) N2<\/sub>\u5438\u9644-\u8131\u9644\u7b49\u6e29\u7ebf\u548c(k)\u5b54\u5f84\u5206\u5e03\u56fe\u3002\u00a9 2022 John Wiley & Sons, Inc.<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe3 MXene\/CAC\u3001a-MXene\u548cp-MXene\u8584\u819c\u7535\u6781\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002p-MXene\u3001a-MXene\u548cMXene\/CAC\u8584\u819ca) 20mV s-1<\/sup>\u65f6\u7684CV\u66f2\u7ebf\uff0cc)\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u8d28\u91cf\u6bd4\u7535\u5bb9\uff0ce)\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u4f53\u79ef\u6bd4\u7535\u5bb9\uff0cf) Nyquist\u56fe\u3002MXene\/CAC-5%\u8584\u819c\u7684b) 5 ~ 10000 mV s-1<\/sup>\u626b\u63cf\u901f\u7387\u4e0b\u7684CV\u66f2\u7ebf\uff0cd) 1 ~ 10 A g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u5145\u653e\u7535\u66f2\u7ebf\uff0cg) 10 A g-1<\/sup>\u65f6\u7684\u957f\u5faa\u73af\u6027\u80fd\u3002\u63d2\u56fe\u663e\u793a\u4e86MXene\/CAC-5%\u8584\u819c\u521d\u59cb\u3001\u4e2d\u95f4\u548c\u6700\u540e\u4e94\u4e2a\u5faa\u73af\u7684\u5145\u653e\u7535\u66f2\u7ebf\u3002\u00a9 2022 John Wiley & Sons, Inc.<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe4 MXene\/CAC-5%\u5728\u9762\u8f7d\u91cf\u4e3a1.2 ~ 10.0 mg cm-2<\/sup>\u4e0b\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002a) 20mV s-1<\/sup>\u65f6\u7684CV\u66f2\u7ebf\uff0c\u7535\u6d41\u5bc6\u5ea6\u4ece1\u5230100 A g-1<\/sup>\u65f6\u7684b)\u8d28\u91cf\u6bd4\u7535\u5bb9\uff0cc)\u4f53\u79ef\u6bd4\u7535\u5bb9\u548cd)\u9762\u79ef\u6bd4\u7535\u5bb9\u3002\u00a9 2022 John Wiley & Sons, Inc.<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe5 \u57fa\u4e8eMXene\/CAC-5%\u819c\u7684ASSC\u7684\u7ed3\u6784\u548c\u7535\u5316\u5b66\u6027\u80fd\u3002a) ASSC\u7ed3\u6784\u7684\u793a\u610f\u56fe\uff0cb)\u76f8\u5e94\u7684\u6570\u7801\u7167\u7247\u3002c)\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684CV\u66f2\u7ebf\uff0cd)\u500d\u7387\u6027\u80fd\uff0ce) 10 A g-1<\/sup>\u65f6\u7684\u5faa\u73af\u6027\u80fd\uff0cf) MXene\/CAC-5% ASSC\u7684Ragone\u56fe\u3002\u57280\u00b0\u300145\u00b0\u300190\u00b0\u548c180\u00b0\u5f2f\u66f2\u89d2\u5ea6\u4e0b\u7684g)\u6570\u7801\u7167\u7247\u548ch) CV\u66f2\u7ebf\u3002\u4e24\u4e2aMXene\/ CAC-5% ASSC\u5728\u4e32\u8054\u548c\u5e76\u8054\u72b6\u6001\u4e0b\u7684i) 20mV s-1<\/sup>\u65f6\u7684CV\u66f2\u7ebf\u548cj) GCD\u66f2\u7ebf\u3002\u00a9 2022 John Wiley & Sons, Inc.<\/strong><\/p>\n

\u4e94\u3001\u6210\u679c\u542f\u793a<\/strong><\/p>\n

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 <\/p>\n

\u539f\u6587\u8be6\u60c5\uff1ahttps:\/\/doi.org\/10.1002\/adfm.202209918<\/p>\n

\u672c\u6587\u7531\u96fe\u8d77\u4f9b\u7a3f\u3002<\/p>\n

 <\/p>\n","protected":false},"excerpt":{"rendered":"

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