{"id":249129,"date":"2023-03-24T06:10:35","date_gmt":"2023-03-23T22:10:35","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=249129"},"modified":"2023-03-23T14:14:53","modified_gmt":"2023-03-23T06:14:53","slug":"%e5%a6%82%e4%bd%95%e7%94%a8%e6%89%ab%e6%8f%8f%e7%94%b5%e9%95%9c%e5%ae%9e%e7%8e%b0%e7%ba%b3%e7%b1%b3%e7%ba%a7%e7%95%8c%e9%9d%a2%e8%a1%a8%e5%be%81%ef%bc%9f","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=249129","title":{"rendered":"\u5982\u4f55\u7528\u626b\u63cf\u7535\u955c\u5b9e\u73b0\u7eb3\u7c73\u7ea7\u754c\u9762\u8868\u5f81\uff1f"},"content":{"rendered":"<p>&nbsp;<\/p>\n<p><strong><b>\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n<p>\u77f3\u58a8\u70ef\/\u91d1\u5c5e\u4f53\u7cfb\u754c\u9762\u6c27\u5316\u5c42\u7684\u8868\u5f81\u5bf9\u4e8e\u7814\u7a76\u754c\u9762\u6c27\u5316\u884c\u4e3a\u4ee5\u53ca\u77f3\u58a8\u70ef\u7684\u5e72\u8f6c\u79fb\u5177\u6709\u91cd\u8981\u610f\u4e49\u3002\u7136\u800c\uff0c\u7531\u4e8e\u77f3\u58a8\u70ef\u8986\u76d6\u533a\u57df\u7684\u754c\u9762\u6c27\u5316\u5728\u7eb3\u7c73\u5c3a\u5ea6\u4e0a\u662f\u4e0d\u5747\u5300\u7684\uff0c\u56e0\u6b64\uff0c\u901a\u8fc7\u5206\u8fa8\u7387\u76f8\u5bf9\u8f83\u4f4e\u7684\u4f20\u7edf\u5149\u8c31\u6280\u672f\uff08XPS\u3001Raman\u7b49\uff09\u8fdb\u884c\u77f3\u58a8\u70ef\/\u91d1\u5c5e\u754c\u9762\u6c27\u5316\u5c42\u5728\u7eb3\u7c73\u7ea7\u5c3a\u5ea6\u7684\u5f02\u8d28\u6027\u8868\u5f81\u662f\u4e00\u9879\u975e\u5e38\u5177\u6709\u6311\u6218\u6027\u7684\u4efb\u52a1\u3002<\/p>\n<p>&nbsp;<\/p>\n<p>\u626b\u63cf\u7535\u955c\u901a\u5e38\u7528\u4e8e\u8868\u9762\u5fae\u89c2\u5f62\u8c8c\u7684\u89c2\u5bdf\u4e0e\u8868\u5f81\uff0c\u5176\u7535\u5b50\u675f\u5177\u6709\u626b\u63cf\u548c\u6210\u50cf\u7684\u80fd\u529b\uff0c\u5e76\u4e14\u80fd\u591f\u63d0\u4f9b\u7eb3\u7c73\u7ea7\u7684\u4f4d\u7f6e\u7cbe\u5ea6\u548c\u5206\u8fa8\u7387\uff0c\u80fd\u591f\u5b9e\u73b0\u5bf9\u611f\u5174\u8da3\u533a\u57df\u7684\u7eb3\u7c73\u7ea7\u5b9a\u4f4d\u8868\u5f81\u3002\u53e6\u5916\uff0c\u901a\u8fc7\u626b\u63cf\u7535\u955c\u7535\u5b50\u675f\u7684\u8f90\u7167\u53ef\u4ee5\u8bf1\u5bfc\u5c40\u90e8\u6c27\u5316\u7269\u7684\u8fd8\u539f\u3002\u6839\u636e\u626b\u63cf\u7535\u955c\u6210\u50cf\u539f\u7406\uff0c\u56fe\u50cf\u7684\u8d28\u539a\u886c\u5ea6\u5bf9\u6210\u50cf\u533a\u57df\u80fd\u591f\u5f15\u8d77\u4e8c\u6b21\u7535\u5b50\u4ea7\u7387\u53d8\u5316\u7684\u8868\u9762\u6216\u754c\u9762\u6c27\u5316\u7269\u7684\u7ec4\u6210\u548c\u539a\u5ea6\u6bd4\u8f83\u654f\u611f\u3002\u7ed3\u5408\u4ee5\u4e0a\u626b\u63cf\u7535\u955c\u7684\u7535\u5b50\u675f\u8fd8\u539f\u4e0e\u7eb3\u7c73\u7ea7\u8868\u5f81\u7684\u4f18\u52bf\uff0c\u6211\u4eec\u5efa\u7acb\u4e86\u5229\u7528\u626b\u63cf\u7535\u955c\u5b9e\u73b0\u754c\u9762\u7eb3\u7c73\u7ea7\u8868\u5f81\u7684\u65b0\u65b9\u6cd5\uff0cSEM EBI-RIO method\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-249130\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72470-16.png\" alt=\"\" width=\"1140\" height=\"694\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72470-16.png 1140w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72470-16-300x183.png 300w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72470-16-768x468.png 768w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72470-16-1024x623.png 1024w\" sizes=\"(max-width: 1140px) 100vw, 1140px\" \/><\/p>\n<p>&nbsp;<\/p>\n<p>&nbsp;<\/p>\n<p><strong><b>\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n<p>\u54c8\u5c14\u6ee8\u5de5\u4e1a\u5927\u5b66\u5927\u5b66\u5316\u5de5\u4e0e\u5316\u5b66\u5b66\u9662\u7684<a href=\"http:\/\/homepage.hit.edu.cn\/pages\/yanggan\">\u7518\u9633\u6559\u6388<\/a>\u548c\u6307\u5bfc\u7684\u535a\u58eb\u751f\u51af\u76fc\u76fc\uff08\u8bba\u6587\u7b2c\u4e00\u4f5c\u8005\uff09\uff0c\u91c7\u7528Zeiss\u70ed\u573a\u53d1\u5c04SEM\uff0c\u5bf9\u77f3\u58a8\u70ef\/\u94dc\u4f53\u7cfb\u7684\u754c\u9762\u6c27\u5316\u5c42\u8fdb\u884c\u4e86\u7eb3\u7c73\u7ea7\u5c3a\u5ea6\u7684\u8868\u5f81\u5206\u6790\uff0c\u901a\u8fc7\u5b9e\u9a8c\u6570\u636e\u9a8c\u8bc1\u4e86\u7535\u5b50\u675f\u8bf1\u5bfc\u7684\u754c\u9762\u6c27\u5316\u5c42\u7684\u8fd8\u539f\u4e0e\u56fe\u50cf\u886c\u5ea6\u53d8\u5316\u4e4b\u95f4\u7684\u5173\u7cfb\uff0c\u5efa\u7acb\u4e86\u7eb3\u7c73\u7ea7\u5c3a\u5ea6\u754c\u9762\u8868\u5f81\u7684\u65b0\u65b9\u6cd5\u3002<\/p>\n<p>&nbsp;<\/p>\n<p>\u4ed6\u4eec\u53d1\u73b0EBI\u8bf1\u5bfc\u7684\u754c\u9762Cu\u6c27\u5316\u7269\u7684\u539a\u5ea6\u548c\u8986\u76d6\u5ea6\u7684\u53d8\u5316\u662fSEM\u56fe\u50cf\u886c\u5ea6\u7684\u53cd\u8f6c\u6216\u53d8\u5316\u7684\u539f\u56e0\u3002\u8fd9\u662f\u7531\u4e8e\u754c\u9762\u94dc\u6c27\u5316\u7269\u7684\u539a\u5ea6\u548c\u8986\u76d6\u5ea6\u7684\u53d8\u5316\u4f1a\u5bfc\u81f4\u76f8\u5e94\u533a\u57df\u51fa\u5c04\u7684\u4e8c\u6b21\u7535\u5b50\u7684\u91cf\u53d1\u751f\u53d8\u5316\uff0c\u4ece\u800c\u5bfc\u81f4\u76f8\u5e94\u533a\u57df\u7684\u56fe\u50cf\u886c\u5ea6\u53d1\u751f\u53d8\u5316\u3002<\/p>\n<p>&nbsp;<\/p>\n<p>\u4ed6\u4eec\u8fd8\u53d1\u73b0\uff0c\u8be5\u65b9\u6cd5\u9002\u7528\u4e8e\u754c\u9762\u6c27\u5316\u5c42\u539a\u5ea6\u4e3a1-5 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EBI-RIO\u65b9\u6cd5\u89e3\u51b3\u4e86\u5e38\u89c4\u8868\u5f81\u6280\u672f\u5b58\u5728\u7684\u5206\u8fa8\u7387\u4f4e\u548c\u9020\u6210\u6837\u54c1\u635f\u4f24\u7684\u95ee\u9898\uff0c\u6210\u4e3aX\u5c04\u7ebf\u5149\u7535\u5b50\u80fd\u8c31\uff08XPS\uff09\u3001\u62c9\u66fc\u663e\u5fae\u955c\u548c\u9ad8\u5206\u8fa8\u7387\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c\uff08HRTEM\uff09\u7b49\u8868\u5f81\u624b\u6bb5\u7684\u5f3a\u6709\u529b\u7684\u8f85\u52a9\u5de5\u5177\u3002<\/p>\n<p>&nbsp;<\/p>\n<p>&nbsp;<\/p>\n<p><strong><b>\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/b><\/strong><\/p>\n<p>&nbsp;<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-249131\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72471-47.png\" alt=\"\" width=\"1053\" height=\"1040\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72471-47.png 1053w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72471-47-300x296.png 300w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72471-47-768x759.png 768w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72471-47-1024x1011.png 1024w\" sizes=\"(max-width: 1053px) 100vw, 1053px\" \/><\/p>\n<p><strong>\u56fe1 <\/strong><strong>\u4e0d\u540c\u5b9e\u9a8c\u6761\u4ef6\u5904\u7406\u7684Gr\/Cu\u6837\u54c1\u76f8\u540c\u533a\u57df\u7684\u7535\u955c\u56fe\u50cf\uff0cXPS\u8c31\u53caHRTEM\u56fe\u50cf\u3002<\/strong><strong>\uff08<\/strong><strong>\u5efa\u7acb\u7535\u5b50\u675f\u8bf1\u5bfc\u7684\u8fd8\u539f\u4e0e\u56fe\u50cf\u886c\u5ea6\u4e4b\u95f4\u7684\u5173\u7cfb<\/strong><strong>\uff09<\/strong><\/p>\n<p>&nbsp;<\/p>\n<p>\uff08a-c\uff09\u7535\u5b50\u675f\u8f90\u7167\u524d\uff0c\u77f3\u58a8\u70ef\u76f8\u5bf9\u4e8e\u886c\u5e95\u8f83\u6697\uff0c\u7535\u5b50\u675f\u8f90\u7167\u540e\uff0c\u77f3\u58a8\u70ef\u76f8\u5bf9\u4e8e\u886c\u5e95\u533a\u57df\u886c\u5ea6\u53d1\u751f\u53cd\u8f6c\uff0c\u518d\u6b21\u6c27\u5316\u540e\uff0c\u77f3\u58a8\u70ef\u8986\u76d6\u533a\u57df\u91cd\u65b0\u53d8\u6697\u3002<\/p>\n<p>\uff08d-f\uff09\u5bf9\u5e94\u7684XPS\u8c31\u3002\u7535\u5b50\u675f\u8f90\u7167\u540e\uff0cCuO\u6d88\u5931\uff0c\u94dc\u4e0e\u94dc\u6c27\u5316\u7269\u5cf0\u9762\u79ef\u7684\u6bd4\u503c\u589e\u52a0\uff0c\u518d\u6b21\u6c27\u5316\u540e\uff0c\u94dc\u4e0e\u94dc\u6c27\u5316\u7269\u5cf0\u9762\u79ef\u7684\u6bd4\u503c\u4e0b\u964d\uff0c\u8bf4\u660e\u754c\u9762\u6c27\u5316\u7269\u5728\u7535\u5b50\u675f\u8f90\u7167\u540e\u88ab\u8fd8\u539f\uff0c\u518d\u6b21\u70ed\u6c27\u5316\u540e\uff0c\u94dc\u88ab\u6c27\u5316\u6210\u6c27\u5316\u4e9a\u94dc\u3002<\/p>\n<p>\uff08g-i\uff09\u5bf9\u5e94\u7684HRTEM\u56fe\u50cf\u3002\u7535\u5b50\u675f\u8f90\u7167\u540e\uff0c\u754c\u9762\u6c27\u5316\u5c42\u539a\u5ea6\u53d8\u8584\uff0c\u5e76\u4e14\u4e0d\u8fde\u7eed\uff0c\u518d\u6b21\u6c27\u5316\u540e\uff0c\u754c\u9762\u6c27\u5316\u5c42\u7684\u539a\u5ea6\u589e\u52a0\u3002<\/p>\n<p>&nbsp;<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-249132\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72472-43.png\" alt=\"\" width=\"1269\" height=\"631\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72472-43.png 1269w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72472-43-300x149.png 300w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72472-43-768x382.png 768w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2023\/03\/\u56fe\u72472-43-1024x509.png 1024w\" sizes=\"(max-width: 1269px) 100vw, 1269px\" \/><\/p>\n<p><strong>\u56fe2 SEM RBI-RIO\u65b9\u6cd5\u7684\u4f18\u52bf\u2014\u5b9e\u73b0\u591a\u5c3a\u5ea6\u8f90\u7167\u8303\u56f4\u7684\u754c\u9762\u8868\u5f81<\/strong><\/p>\n<p>&nbsp;<\/p>\n<p>\u5982\u56fe\u6240\u793a\uff0c\u5206\u522b\u4e3aGr\/Cu\u6837\u54c1\u4e0d\u540c\u5c3a\u5bf8\u7535\u5b50\u675f\u8f90\u7167\u8303\u56f4\u5185\u4e0d\u540c\u8f90\u7167\u65f6\u95f4\u7684SEM\u56fe\u50cf\u3002\uff08a\uff0950 \u00b5m\u00d737.5 \u00b5m\uff1b\uff08b\uff0920 \u00b5m\u00d715 \u00b5m\uff1b\uff08c\uff095 \u00b5m \u00d73.75 \u00b5m\uff1b\uff08d\uff09\u5bbd\u5ea6\u4e3a500 nm\u7684HIT\u6807\u8bb0\uff1b\uff08e\uff09\u5c3a\u5bf8\u4e3a2.5 \u00b5m\u00d7200 nm\u533a\u57df\u3002\u52a0\u901f\u7535\u538b\uff1a5 kV\uff0c\u5de5\u4f5c\u8ddd\u79bb: 7 mm\u3002\u901a\u8fc7\u8f90\u7167\u4e0d\u540c\u5c3a\u5bf8\u7684\u533a\u57df\uff0c\u5b9e\u73b0\u5728\u79d2\u5230\u5206\u949f\u7684\u65f6\u95f4\u5c3a\u5ea6\u8303\u56f4\u5185\u5bf9\u51e0\u5341\u5fae\u7c73\u5230200 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RBI-RIO\u65b9\u6cd5\u7684\u4f18\u52bf\u2014\u5b9e\u73b0\u7eb3\u7c73\u7ea7\u7684\u5fae\u5c0f\u533a\u57df\u5f02\u8d28\u6027\u754c\u9762\u6c27\u5316\u7684\u8868\u5f81<\/strong><\/p>\n<p>&nbsp;<\/p>\n<p>\u5982\u56fe\u6240\u793a\u4e3aGr\/Cu\u6837\u54c1\u5728EBI\u524d\u540e\u7684SEM\u56fe\u50cf\u3002I\uff1aEBI\u540e\u886c\u5ea6\u53cd\u8f6c\u7684\u533a\u57df\u3002II\uff1aEBI\u540e\u6ca1\u6709\u53cd\u8f6c\u7684\u533a\u57df\u3002III\uff1a \u95f4\u8ddd&lt;100 nm\u7684\u5c0f\u533a\u57df\u3002IV\uff1aEBI\u540e\u51fa\u73b0\u886c\u5ea6\u53cd\u8f6c\u7684\u7a84\u6761\u7eb9\u3002V\uff1aEBI\u540e\u51fa\u73b0\u886c\u5ea6\u53cd\u8f6c\u7684\u8f83\u5927\u533a\u57df\u3002<\/p>\n<p>\u7531\u4e8eEBI-RIO\u65b9\u6cd5\u5bf9Gr\/Cu\u754c\u9762\u6c27\u5316\u5c42\u7684\u539a\u5ea6\u8f83\u654f\u611f\uff0c\u56e0\u6b64\uff0c\u4e0d\u540c\u7a0b\u5c40\u90e8\u886c\u5ea6\u7684\u53d8\u5316\u5b9e\u9645\u4e0a\u53cd\u6620\u4e86\u5f02\u8d28\u7684\u754c\u9762\u6c27\u5316\u3002\u901a\u8fc7\u8f90\u7167\u540e\u4e0d\u540c\u7a0b\u5ea6\u7684\u886c\u5ea6\u53cd\u8f6c\uff0c\u5b9e\u73b0\u5728\u4e9a100 nm\u7a7a\u95f4\u5206\u8fa8\u7387\u4e0b\u5bf9\u7eb3\u7c73\u7ea7\u533a\u57df\u7684\u5f02\u8d28\u6027\u754c\u9762\u6c27\u5316\u7684\u8868\u5f81\u3002<\/p>\n<p>&nbsp;<\/p>\n<p><strong><b>\u3010\u5c0f\u7ed3\u3011<\/b><\/strong><\/p>\n<p>\u8be5\u5de5\u4f5c\u5229\u7528SEM 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nm\u5c3a\u5ea6\u7a7a\u95f4\u5206\u8fa8\u7387\u4e0b\u5bf9Gr\/Cu\u975e\u5747\u5300\u754c\u9762\u6c27\u5316\u7684\u8868\u5f81\u3002<\/p>\n<p>&nbsp;<\/p>\n<p>\u672c\u5de5\u4f5c\u5efa\u7acb\u7684\u65b0\u65b9\u6cd5\uff08EBI-RIO\u65b9\u6cd5\uff09\u4e5f\u9002\u7528\u4e8e\u5176\u4ed62D\u6750\u6599\u548c\u5668\u4ef6\u754c\u9762\u6c27\u5316\u7684\u7eb3\u7c73\u7ea7\u8868\u5f81\uff0c\u800c\u4e14\u6709\u5229\u4e8e\u7814\u7a76\u754c\u9762\u6c27\u5316\u5bf9\u77f3\u58a8\u70ef\u8f6c\u79fb\u7684\u5f71\u54cd\uff0c\u4ee5\u53ca\u4e8c\u7ef4\u6750\u6599\u548c\u886c\u5e95\u4e4b\u95f4\u7eb3\u7c73\u5c3a\u5ea6\u7684\u7a7a\u95f4\u9650\u57df\u5316\u5b66\u53cd\u5e94\u3002<\/p>\n<p>&nbsp;<\/p>\n<p>\u8be5\u7814\u7a76\u5f97\u5230\u4e86\u56fd\u5bb6\u81ea\u7136\u79d1\u5b66\u57fa\u91d1\u91cd\u70b9\u9879\u76ee\u3001\u56fd\u5bb6\u91cd\u70b9\u7814\u53d1\u8ba1\u5212\u9879\u76ee\u3001\u9ed1\u9f99\u6c5f\u7701\u91cd\u5927\u79d1\u6280\u62db\u6807\u8ba1\u5212\u9879\u76ee\u7684\u8d44\u52a9\u3002<\/p>\n<p>&nbsp;<\/p>\n<p>\u7518\u9633\u6559\u6388<\/p>\n<p>\u7518\u9633\uff0c\u54c8\u5c14\u6ee8\u5de5\u4e1a\u5927\u5b66\uff0c\u65b0\u80fd\u6e90\u6750\u6599\u548c\u5668\u4ef6\u7cfb\u6559\u6388\uff0c\u535a\u5bfc\uff0c\u82f1\u56fd\u7687\u5bb6\u5316\u5b66\u5b66\u58eb\uff0c\u66fe\u4efb\u54c8\u5c14\u6ee8\u5de5\u4e1a\u5927\u5b66\u80fd\u6e90\u5316\u5de5\u7cfb\u4e3b\u4efb\u3002\u53d1\u8868\u8fc7\u00a070 \u591a\u7bc7 SCI \u8bba\u6587\uff0c\u66fe\u83b7 Frans Habraken \u6700\u4f73\u8bba\u6587\u5956\uff0c\u5e76\u5728\u591a\u5bb6\u56fd\u9645\u671f\u520a\u62c5\u4efb\u7f16\u59d4\u3002\u4e2d\u56fd\u5316\u5de5\u5b66\u4f1a\u5316\u5de5\u65b0\u6750\u6599\u59d4\u5458\u4f1a\u7406\u4e8b\uff0c\u56fd\u9645\u534a\u5bfc\u4f53\u4ea7\u4e1a\u534f\u4f1a\uff08SEMI\uff09\u4e2d\u56fd\u5316\u5408\u7269\u534a\u5bfc\u4f53\u6807\u51c6\u6280\u672f\u59d4\u5458\u4f1a\u6838\u5fc3\u59d4\u5458\uff0c\u56fd\u9645\u884d\u5c04\u6570\u636e\u59d4\u5458\u4f1a\uff08ICDD\uff09\u59d4\u5458\u3002<\/p>\n<p>&nbsp;<\/p>\n<p>&nbsp;<\/p>\n<p>\u3010\u6587\u732e\u94fe\u63a5\u3011\uff1aPanpan Feng, et al,\u00a0Nanoscale characterization of the heterogeneous interfacial oxidation layer of graphene\/Cu based on a SEM electron beam induced reduction effect, Physical Chemistry Chemical Physics, 2023, DOI:\u00a010.1039\/D2CP05809J.<\/p>\n<p><a href=\"https:\/\/pubs.rsc.org\/en\/content\/articlehtml\/2023\/cp\/d2cp05809j\"><u>https:\/\/pubs.rsc.org\/en\/content\/articlehtml\/2023\/cp\/d2cp05809j<\/u><\/a><\/p>\n<p>\u672c\u6587\u7531\u4f5c\u8005\u4f9b\u7a3f<\/p>\n","protected":false},"excerpt":{"rendered":"<p>&nbsp; \u3010\u5f15\u8a00\u3011 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