{"id":252981,"date":"2023-07-18T06:39:33","date_gmt":"2023-07-17T22:39:33","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=252981"},"modified":"2023-07-17T20:39:45","modified_gmt":"2023-07-17T12:39:45","slug":"%e5%8d%97%e5%bc%80%e7%8e%8b%e5%b0%8f%e9%87%8e%e8%af%be%e9%a2%98%e7%bb%84angew%ef%bc%9a%e5%9f%ba%e4%ba%8e%e9%9d%9e%e8%8b%af%e8%8a%b3%e7%83%83acepleiadylene%e7%9a%84%e6%96%b0%e5%9e%8b%e6%9c%89%e6%9c%ba","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=252981","title":{"rendered":"\u5357\u5f00\u738b\u5c0f\u91ce\u8bfe\u9898\u7ec4Angew\uff1a\u57fa\u4e8e\u975e\u82ef\u82b3\u70c3Acepleiadylene\u7684\u65b0\u578b\u6709\u673a\u534a\u5bfc\u4f53\u6750\u6599"},"content":{"rendered":"

\u975e\u82ef\u82b3\u70c3\u662f\u4e00\u7c7b\u5206\u5b50\u5185\u5177\u6709\u975e\u516d\u5143\u73af\u7ed3\u6784\u7684\u591a\u73af\u82b3\u70c3\uff0c\u5176\u72ec\u7279\u7684\u62d3\u6251\u7ed3\u6784\u8d4b\u4e88\u4e86\u5176\u4e0d\u540c\u4e8e\u7ecf\u5178\u82ef\u578b\u591a\u73af\u82b3\u70c3\u7684\u6027\u8d28\uff0c\u56e0\u6b64\u5f15\u8d77\u4e86\u5e7f\u6cdb\u7684\u5173\u6ce8\u3002\u7136\u800c\uff0c\u57fa\u4e8e\u975e\u82ef\u82b3\u70c3\u7684\u6709\u673a\u534a\u5bfc\u4f53\u6750\u6599\u4f53\u7cfb\u975e\u5e38\u6709\u9650\uff0c\u5e76\u4e14\u975e\u82ef\u82b3\u70c3\u7684\u72ec\u7279\u6027\u8d28\u4e0e\u5176\u5149\u7535\u5668\u4ef6\u6027\u80fd\u7684\u5173\u7cfb\u4ecd\u4e0d\u6e05\u6670\uff0c\u8fd9\u9650\u5236\u4e86\u975e\u82ef\u82b3\u70c3\u7c7b\u6750\u6599\u5728\u6709\u673a\u5149\u7535\u5668\u4ef6\u4e2d\u7684\u5e94\u7528\u3002<\/p>\n

Acepleiadylene (APD) \u662f\u8298\u7684\u975e\u82ef\u578b\u540c\u5206\u5f02\u6784\u4f53\uff0c\u5177\u6709\u5927\u7684\u5206\u5b50\u5076\u6781\u3001\u7a84\u7684\u5149\u5b66\u80fd\u9699\u548c\u660e\u663e\u7684\u7535\u8377\u5206\u79bb\u7279\u5f81\u3002\u8298\u4f5c\u4e3a\u7ecf\u5178\u7684\u5408\u6210\u780c\u5757\u5df2\u88ab\u5e7f\u6cdb\u7528\u4e8e\u6784\u7b51\u9ad8\u6027\u80fd\u6709\u673a\u534a\u5bfc\u4f53\u6750\u6599\uff0c\u4f46\u5176\u975e\u82ef\u578b\u540c\u5206\u5f02\u6784\u4f53APD\u8fd8\u4ece\u672a\u88ab\u5e94\u7528\u4e8e\u6709\u673a\u5149\u7535\u6750\u6599\u9886\u57df\u3002<\/p>\n

\u5357\u5f00\u5927\u5b66\u738b\u5c0f\u91ce\u8bfe\u9898\u7ec4\u57282019\u5e74\u53d1\u5c55\u4e86\u65b0\u9896\u7684\u5408\u6210\u7b56\u7565\u5b9e\u73b0\u4e86APD\u7684\u9ad8\u6548\u514b\u7ea7\u5236\u5907\uff0c\u89e3\u51b3\u4e86\u957f\u671f\u4ee5\u6765APD\u96be\u4ee5\u5408\u6210\u7684\u95ee\u9898\uff0c\u4e3a\u63a2\u7d22\u57fa\u4e8eAPD\u7684\u65b0\u578b\u6709\u673a\u534a\u5bfc\u4f53\u6750\u6599\u4f53\u7cfb\u5960\u5b9a\u4e86\u575a\u5b9e\u7684\u5316\u5b66\u57fa\u7840 (X.-Y. Wang* et al.<\/em>, J. Am. Chem. Soc.<\/em> 2021<\/strong>, 143<\/em>, 5314\u22125318)\u3002\u8fd1\u65e5\uff0c\u8be5\u8bfe\u9898\u7ec4\u9996\u6b21\u4ee5APD\u4f5c\u4e3a\u7ed3\u6784\u57fa\u5143\uff0c\u53d1\u5c55\u4e86D-A-D\u578b\u6709\u673a\u534a\u5bfc\u4f53\u5206\u5b50APD-IID\uff0c\u901a\u8fc7\u4e0e\u57fa\u4e8e\u8298\u7684\u540c\u5206\u5f02\u6784\u4f53\u8fdb\u884c\u5bf9\u6bd4\u7814\u7a76\uff0c\u63ed\u793a\u4e86\u975e\u82ef\u578bAPD\u884d\u751f\u7269\u7684\u72ec\u7279\u6027\u8d28\u53ca\u5176\u5728\u6709\u673a\u534a\u5bfc\u4f53\u5668\u4ef6\u4e2d\u7684\u4f18\u52bf (\u56fe1)\u3002<\/p>\n

\"\"<\/p>\n

\u56fe1. \u5229\u7528APD\u7535\u8377\u5206\u79bb\u7279\u5f81\u6240\u8bbe\u8ba1\u7684D-A-D\u578b\u6709\u673a\u534a\u5bfc\u4f53\u5206\u5b50APD-IID\u53ca\u5176\u82ef\u578b\u5f02\u6784\u4f531Py-IID\u548c2Py-IID<\/p>\n

\u901a\u8fc7\u7406\u8bba\u8ba1\u7b97\uff0c\u4f5c\u8005\u53d1\u73b0\u5728APD-IID\u7684\u9759\u7535\u52bf\u5206\u5e03\u56fe (ESP) \u4e2d\uff0c\u6b63\u7535\u8377\u4e3b\u8981\u5206\u5e03\u5728APD\u7684\u4e03\u5143\u73af\u4e0a\uff0c\u800c\u8d1f\u7535\u8377\u4e3b\u8981\u5206\u5e03\u5728\u5f02\u975b\u84dd (IID) \u7247\u6bb5\u548cAPD\u7684\u4e94\u5143\u73af\u4e0a\uff0c\u5206\u5b50\u6574\u4f53\u8868\u73b0\u51fa\u660e\u663e\u7684\u7535\u8377\u5206\u79bb\u7279\u5f81 (\u56fe2)\u3002\u53e6\u5916\uff0c\u5728\u4f18\u5316\u540e\u7684\u5206\u5b50\u6784\u578b\u4e2d\uff0cAPD-IID\u7ed9\u4f53\u548c\u53d7\u4f53\u4e4b\u95f4\u7684\u78b3\u78b3\u952e\u66f4\u77ed\uff0c\u8868\u73b0\u51fa\u4e00\u5b9a\u7684\u53cc\u952e\u7279\u5f81\uff0c\u8fd9\u8868\u660eAPD-IID\u7684\u7535\u8377\u5206\u79bb\u5171\u632f\u5f0f\u5bf9\u5176\u57fa\u6001\u7535\u5b50\u7ed3\u6784\u5177\u6709\u660e\u663e\u8d21\u732e (\u56fe1)\uff0c\u6709\u5229\u4e8e\u589e\u5f3a\u5206\u5b50\u95f4\u7684\u76f8\u4e92\u4f5c\u7528\u3002\u540c\u65f6\uff0cAPD-IID\u4e2d\u7ed9\u53d7\u4f53\u4e4b\u95f4\u7684\u626d\u8f6c\u89d2\u66f4\u5c0f\uff0c\u5373\u5206\u5b50\u5177\u6709\u66f4\u5e73\u9762\u7684\u6784\u8c61\uff0c\u66f4\u6709\u5229\u4e8e\u5206\u5b50\u5728\u56fa\u6001\u4e0b\u7684\u7d27\u5bc6\u5806\u79ef\u3002<\/p>\n

\"\"<\/p>\n

\u56fe2. \u4f18\u5316\u7684\u5206\u5b50\u6784\u578b\u548c\u9759\u7535\u52bf\u5206\u5e03\u56fe<\/p>\n

\u968f\u540e\uff0c\u4f5c\u8005\u5bf9\u4e09\u4e2a\u5206\u5b50\u5728\u56fa\u6001\u4e0b\u7684\u805a\u96c6\u884c\u4e3a\u8fdb\u884c\u4e86\u8868\u5f81 (\u56fe3)\u3002\u4e09\u4e2a\u5206\u5b50\u5728\u805a\u7532\u57fa\u4e19\u70ef\u9178\u7532\u916f (PMMA) \u57fa\u8d28\u4e2d\u7684\u5438\u6536\u5149\u8c31\u8868\u660e\uff0c\u968f\u7740\u5206\u5b50\u5728PMMA\u57fa\u8d28\u4e2d\u7684\u6d53\u5ea6\u589e\u52a0\uff0cAPD-IID\u7684\u805a\u96c6\u4fe1\u53f7\u5cf0\u8868\u73b0\u51fa\u660e\u663e\u589e\u5f3a\uff0c\u800c1Py-IID\u548c2Py-IID\u5728\u8584\u819c\u6001\u4e0b\u6ca1\u6709\u51fa\u73b0\u660e\u663e\u7684\u805a\u96c6\u5cf0\uff0c\u8fd9\u8bf4\u660eAPD-IID\u5728\u56fa\u6001\u4e0b\u5177\u6709\u66f4\u5f3a\u7684\u805a\u96c6\u8d8b\u52bf\u3002\u4ece\u4e09\u4e2a\u5206\u5b50\u7684\u8584\u819c\u4e8c\u7ef4\u63a0\u5165\u5c04\u5e7f\u89d2X\u5c04\u7ebf\u6563\u5c04 (2D-GIWAXS) \u56fe\u53ef\u4ee5\u770b\u51fa\uff0cAPD-IID\u8584\u819c\u8868\u73b0\u51fa\u6e05\u6670\u7684\u884d\u5c04\u70b9\uff0c\u800c1Py-IID\u8868\u73b0\u51fa\u884d\u5c04\u73af\uff0c2Py-IID\u8868\u73b0\u51fa\u884d\u5c04\u5f27\uff0c\u8fd9\u8bf4\u660eAPD-IID\u5728\u56fa\u6001\u4e0b\u7684\u5806\u79ef\u66f4\u4e3a\u6709\u5e8f\u3002\u8fd9\u4e9b\u7ed3\u679c\u8868\u660eAPD-IID\u5177\u6709\u66f4\u5f3a\u7684\u5206\u5b50\u95f4\u4f5c\u7528\u529b\uff0c\u56e0\u800c\u5728\u56fa\u6001\u4e0b\u5206\u5b50\u5806\u79ef\u66f4\u52a0\u7d27\u5bc6\u6709\u5e8f\uff0c\u8fd9\u6709\u5229\u4e8e\u7535\u8377\u7684\u9ad8\u6548\u4f20\u8f93\u3002<\/p>\n

\"\"<\/p>\n

\u56fe3. APD-IID\uff0c1Py-IID\uff0c\u548c2Py-IID\u7684\u805a\u96c6\u884c\u4e3a\u7814\u7a76<\/p>\n

\u4f5c\u8005\u57fa\u4e8e\u4e09\u4e2a\u5206\u5b50\u6784\u7b51\u4e86\u5e95\u6805\u9876\u7535\u6781\u7ed3\u6784\u7684\u6709\u673a\u573a\u6548\u5e94\u6676\u4f53\u7ba1\u5668\u4ef6\uff0c\u5e76\u5bf9\u5176\u7535\u5b66\u6027\u80fd\u8fdb\u884c\u4e86\u7814\u7a76 (\u56fe4)\u3002\u901a\u8fc7\u5bf9\u9000\u706b\u6e29\u5ea6\u7684\u4f18\u5316\uff0c\u4f5c\u8005\u53d1\u73b0APD-IID\u5728120 \u00b0C\u7684\u9000\u706b\u6e29\u5ea6\u4e0b\u53ef\u4ee5\u8868\u73b0\u51fa0.20 cm2<\/sup> V-1<\/sup> s-1<\/sup>\u7684\u6700\u9ad8\u7a7a\u7a74\u8fc1\u79fb\u7387\uff0c\u8fd9\u6bd4\u5176\u82ef\u578b\u540c\u5206\u5f02\u6784\u4f53\u7684\u6700\u9ad8\u8fc1\u79fb\u7387\u9ad8\u51fa\u4e00\u5230\u4e24\u4e2a\u6570\u91cf\u7ea7 (1Py-IID: 7.53 \u00d7 10-3<\/sup> cm2<\/sup> V-1<\/sup> s-1<\/sup>; 2Py-IID: 4.74 \u00d7 10-2<\/sup> cm2<\/sup> V-1<\/sup> s-1<\/sup>)\u3002<\/p>\n

\"\"<\/p>\n

\u56fe4. APD-IID\u4e0e\u5176\u82ef\u578b\u540c\u5206\u5f02\u6784\u4f53 (1Py-IID\u548c2Py-IID) \u7684\u7535\u8377\u4f20\u8f93\u6027\u80fd\u5bf9\u6bd4\u7814\u7a76<\/p>\n

\u7efc\u4e0a\u6240\u8ff0\uff0c\u8be5\u5de5\u4f5c\u9996\u6b21\u5c06\u975e\u82ef\u82b3\u70c3APD\u4f5c\u4e3a\u7ed3\u6784\u57fa\u5143\u5e94\u7528\u4e8e\u65b0\u578b\u6709\u673a\u534a\u5bfc\u4f53\u6750\u6599\u7684\u521b\u5236\uff0c\u5e76\u901a\u8fc7\u4e0e\u5176\u82ef\u578b\u540c\u5206\u5f02\u6784\u4f53\u7684\u76f4\u63a5\u5bf9\u6bd4\uff0c\u63ed\u793a\u4e86\u5176\u72ec\u7279\u7684\u7535\u8377\u5206\u79bb\u7279\u5f81\u4e0e\u5728\u534a\u5bfc\u4f53\u5668\u4ef6\u4e2d\u7684\u4f18\u52bf\u3002\u8fd9\u4e00\u5de5\u4f5c\u4e0d\u4ec5\u8bc1\u660e\u4e86\u975e\u82ef\u82b3\u70c3\u7c7b\u5206\u5b50\u5728\u6709\u673a\u534a\u5bfc\u4f53\u6750\u6599\u4e2d\u7684\u5de8\u5927\u6f5c\u529b\uff0c\u4e5f\u4e3a\u65b0\u578b\u6709\u673a\u534a\u5bfc\u4f53\u6750\u6599\u7684\u53d1\u5c55\u5f00\u8f9f\u4e86\u65b0\u4f53\u7cfb\u4e0e\u65b0\u673a\u9047\u3002<\/p>\n

\u8fd9\u4e00\u6210\u679c\u8fd1\u671f\u53d1\u8868\u5728Angew<\/em><\/strong>. Chem<\/em>. Int<\/em>. Ed<\/em>.<\/strong>\u4e0a\uff0c\u6587\u7ae0\u7684\u901a\u8baf\u4f5c\u8005\u662f\u5357\u5f00\u5927\u5b66\u738b\u5c0f\u91ce\u7814\u7a76\u5458<\/strong>\u3002\u7b2c\u4e00\u4f5c\u8005\u662f\u5357\u5f00\u5927\u5b66\u535a\u58eb\u7814\u7a76\u751f\u5085\u6797\u4e0e\u5218\u9e4f\u624d\u535a\u58eb\uff0c\u8be5\u5de5\u4f5c\u5f97\u5230\u4e86\u9752\u5c9b\u79d1\u6280\u5927\u5b66\u95eb\u5bff\u79d1\u6559\u6388\u8bfe\u9898\u7ec4\u5728\u90e8\u5206\u8868\u5f81\u5b9e\u9a8c\u4e0a\u7684\u5e2e\u52a9\uff0c\u4ee5\u53ca\u57fa\u91d1\u59d4\u3001\u79d1\u6280\u90e8\u53ca\u4e2d\u592e\u9ad8\u6821\u57fa\u672c\u79d1\u7814\u4e1a\u52a1\u8d39\u7684\u7ecf\u8d39\u652f\u6301\u3002<\/p>\n

\u8bba\u6587\u4fe1\u606f\uff1a<\/strong><\/p>\n

Unravelling the Superiority of Nonbenzenoid Acepleiadylene as a Building Block for Organic Semiconducting Materials<\/p>\n

Lin Fu\u2020<\/sup>, Pengcai Liu\u2020<\/sup>, Rui Xue, Xiao-Yu Tang, Jiawen Cao, Ze-Fan Yao, Yuchao Liu, Shouke Yan, and Xiao-Ye Wang*<\/p>\n

Angew<\/em>. Chem<\/em>. Int<\/em>. Ed<\/em>. 2023,<\/strong> e202306509.<\/p>\n

\u6587\u7ae0\u94fe\u63a5\uff1ahttps:\/\/onlinelibrary.wiley.com\/doi\/10.1002\/anie.202306509<\/p>\n

\u4f5c\u8005\u7b80\u4ecb<\/strong><\/p>\n

\"\"<\/p>\n

\u738b\u5c0f\u91ce\uff0c\u5357\u5f00\u5927\u5b66\u5316\u5b66\u5b66\u9662\u7279\u8058\u7814\u7a76\u5458\u3001\u535a\u58eb\u751f\u5bfc\u5e08\u3001\u72ec\u7acb\u8bfe\u9898\u7ec4\u7ec4\u957f\uff08PI\uff09\uff0c\u66fe\u83b7\u5fb7\u56fd\u6d2a\u5821\u57fa\u91d1\uff0c\u5165\u9009\u56fd\u5bb6\u201c\u56db\u9752\u201d\u4eba\u624d\u8ba1\u5212\u30022009\u5e74\u672c\u79d1\u6bd5\u4e1a\u4e8e\u5357\u5f00\u5927\u5b66\uff1b2014\u5e74\u535a\u58eb\u6bd5\u4e1a\u4e8e\u5317\u4eac\u5927\u5b66\uff08\u5bfc\u5e08\uff1a\u88f4\u575a\u6559\u6388\uff09\uff1b2014\u81f32019\u5e74\u5728\u5fb7\u56fd\u9a6c\u666e\u9ad8\u5206\u5b50\u6240\u4ece\u4e8b\u535a\u58eb\u540e\u7814\u7a76\uff08\u5bfc\u5e08\uff1aKlaus M\u00fcllen\u6559\u6388\uff09\u30022019\u5e74\u52a0\u5165\u5357\u5f00\u5927\u5b66\u5316\u5b66\u5b66\u9662\uff0c\u4f9d\u6258\u5143\u7d20\u6709\u673a\u5316\u5b66\u56fd\u5bb6\u91cd\u70b9\u5b9e\u9a8c\u5ba4\u72ec\u7acb\u5f00\u5c55\u7814\u7a76\u5de5\u4f5c\u3002\u957f\u671f\u4ece\u4e8b\u65b0\u578b\u6709\u673a\u5171\u8f6d\u5206\u5b50\u6750\u6599\u7684\u8bbe\u8ba1\u5408\u6210\u53ca\u529f\u80fd\u5668\u4ef6\u7814\u7a76\uff0c\u7279\u522b\u662f\u56f4\u7ed5\u787c\u6742\u7a20\u73af\u5171\u8f6d\u4f53\u7cfb\u7684\u7cbe\u51c6\u6784\u7b51\u4e0e\u5149\u7535\u8fc7\u7a0b\u8c03\u63a7\u95ee\u9898\uff0c\u53d6\u5f97\u4e86\u7cfb\u5217\u7814\u7a76\u6210\u679c\u3002\u5df2\u5728\u56fd\u9645\u9ad8\u6c34\u5e73\u5b66\u672f\u671f\u520a\u4e0a\u53d1\u8868\u8bba\u658780\u4f59\u7bc7\uff0c\u88ab\u5f15\u75285200\u4f59\u6b21\uff0c\u4ee5\u7b2c\u4e00\/\u901a\u8baf\u4f5c\u8005\u53d1\u8868\u8bba\u658730\u4f59\u7bc7\uff0c\u5305\u62ecNat. Rev. Chem.<\/em>\uff081\u7bc7\uff09\u3001Nat. Commun<\/em>.\uff083\u7bc7\uff09\u3001J. Am. Chem. Soc<\/em>.\uff088\u7bc7\uff09\u3001Angew. Chem. Int. Ed.<\/em>\uff088\u7bc7\uff09\u3001Acc. Chem. Res<\/em>.\uff081\u7bc7\uff09\u7b49\u3002<\/p>\n

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