{"id":259253,"date":"2024-04-09T06:02:46","date_gmt":"2024-04-08T22:02:46","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=259253"},"modified":"2024-04-08T11:17:05","modified_gmt":"2024-04-08T03:17:05","slug":"%e5%8d%8e%e5%8d%97%e7%90%86%e5%b7%a5%e5%9b%bd%e7%ab%8b%e9%a6%96%e5%b0%94%e5%a4%a7%e5%ad%a6acs-catalysis%ef%bc%9a%e7%94%b5%e5%8c%96%e5%ad%a6%e6%b4%bb%e5%8c%96%e8%a1%a8%e9%9d%a2%e6%b0%a7%e5%ae%9e","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=259253","title":{"rendered":"\u534e\u5357\u7406\u5de5&\u56fd\u7acb\u9996\u5c14\u5927\u5b66ACS Catalysis\uff1a\u7535\u5316\u5b66\u6d3b\u5316\u8868\u9762\u6c27\u5b9e\u73b0\u9ad8\u6548\u7684\u9ad8\u6e29\u7535\u5316\u5b66\u70f7\u70c3\u6c27\u5316\u8131\u6c22\u53cd\u5e94"},"content":{"rendered":"

\u5728\u56fa\u4f53\u6c27\u5316\u7269\u7535\u89e3\u6c60\uff08SOEC\uff09\u4e2d\u5229\u7528CO2<\/sub>\u8fd8\u539f\u4ea7\u751f\u7684\u6c27\u79bb\u5b50\u6765\u5b9e\u73b0\u70f7\u70c3\u6c27\u5316\u8131\u6c22\u53cd\u5e94\uff08ODH\uff09\u4f5c\u4e3a\u4e00\u79cd\u65e2\u80fd\u751f\u4ea7\u9ad8\u4ef7\u503c\u70ef\u70c3\uff0c\u53c8\u80fd\u5229\u7528\u6e29\u5ba4\u6c14\u4f53\u7684\u53ef\u884c\u65b9\u6cd5\uff0c\u5df2\u7ecf\u5f15\u8d77\u4e86\u5168\u4e16\u754c\u7684\u5173\u6ce8\u3002\u7136\u800c\uff0c\u70f7\u70c3\u5728SOEC\u9633\u6781\u4fa7\u53d1\u751fODH\u53cd\u5e94\u7684\u673a\u7406\u4ecd\u4e0d\u6e05\u695a\u3002\u5728\u70ed\u50ac\u5316\u9886\u57df\uff0c\u53d1\u73b0\u50ac\u5316\u5242\u8868\u9762\u7684\u6c27\u7269\u79cd\uff0c\u5982\u4e0d\u7a33\u5b9a\u6c27\u7269\u79cd\u3001\u4eb2\u7535\u6c27\uff08O–<\/sup>\u3001O2-<\/sup>\u548cO2<\/sub>2-<\/sup>\uff09\u548c\u4eb2\u6838\u6c27\uff08O2-<\/sup>\uff09\uff0c\u5728\u51b3\u5b9a\u70f7\u70c3ODH\u7684\u8f6c\u5316\u7387\u548c\u9009\u62e9\u6027\u65b9\u9762\u53d1\u6325\u7740\u5173\u952e\u4f5c\u7528\uff1b\u5bf9\u4e8eSOEC\uff0c\u7531\u4e8e\u6c27\u79bb\u5b50\u901a\u8fc7\u7535\u89e3\u8d28\u88ab\u7535\u5316\u5b66\u6cf5\u9001\u5230\u9633\u6781\u8868\u9762\uff0c\u56e0\u6b64\u7535\u6c60\u7684\u8fd0\u884c\u6761\u4ef6\u5bf9\u4e8e\u8868\u9762\u6c27\u7269\u79cd\u5177\u6709\u663e\u8457\u7684\u5f71\u54cd\u3002\u7136\u800cSOEC\u8fd0\u884c\u6761\u4ef6\u4e0b\u8868\u9762\u6c27\u7269\u79cd\u5982\u4f55\u53d1\u751f\u6f14\u5316\uff0c\u4ee5\u53ca\u8fd9\u79cd\u6f14\u5316\u662f\u5982\u4f55\u5f71\u54cdODH\u52a8\u529b\u5b66\uff0c\u76ee\u524d\u5c1a\u4e0d\u6e05\u695a\u3002<\/p>\n

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\"\"<\/p>\n

\u672c\u6587\u4eae\u70b9\uff1a<\/b><\/strong><\/p>\n

1<\/b><\/strong>.<\/b><\/strong>\u901a\u8fc7\u540c\u6b65\u8f90\u5c04\u8fd1\u5e38\u538b\u5149\u7535\u5b50\u8c31\/\u5438\u6536\u8c31\u7b49\u5148\u8fdb\u7684\u8c31\u5b66\u6280\u672f\uff0c\u5bf9\u7535\u5316\u5b66\u9a71\u52a8\u8868\u9762\u6d3b\u6027\u6c27\u7684\u6f14\u53d8\u8fc7\u7a0b\u8fdb\u884c\u4e86\u539f\u4f4d\u63a2\u6d4b\uff1b<\/b><\/strong><\/p>\n

2<\/b><\/strong>.<\/b><\/strong>\u5728S<\/b><\/strong>OEC<\/b><\/strong>\u4e0a\u5b9e\u73b0\u50ac\u5316\u4e59\u70f7\u6c27\u5316\u8131\u6c22\u53cd\u5e94\uff08ODH\uff09\u8f6c\u5316\u4e3a\u4e59\u70ef\u540c\u65f6\u5c06CO<\/b><\/strong>2<\/b><\/sub><\/strong>\u8fd8\u539f\u4e3a CO\uff0c\u4e59\u70ef\u4ea7\u7387\u8fbe\u52306<\/b><\/strong>6.3%<\/b><\/strong>\uff0c\u5e76\u5b9e\u73b0\u4e86\u957f\u8fbe1<\/b><\/strong>00<\/b><\/strong>h\u7684\u7a33\u5b9a\u8fd0\u884c\u3002<\/b><\/strong><\/p>\n

\u56fe\u6587\u5bfc\u8bfb\uff1a<\/b><\/strong><\/p>\n

1<\/b><\/strong>.<\/b><\/strong>\u4e0d\u540cSOEC\u8fd0\u884c\u6761\u4ef6\u4e0b\u7684ODH\u6027\u80fd<\/b><\/strong>\u3002<\/b><\/strong><\/p>\n

\u5728STCF\u5bf9\u79f0\u7535\u6c60\u4e0a\u5b9e\u73b0\u4e86\u50ac\u5316\u4e59\u70f7\u6c27\u5316\u8131\u6c22\u53cd\u5e94\uff08ODH\uff09\u8f6c\u5316\u4e3a\u4e59\u70ef\u540c\u65f6\u5c06CO2<\/sub>\u00a0\u8fd8\u539f\u4e3a CO,\u5728100\u4e2a\u5c0f\u65f6\u5185C2<\/sub>H6<\/sub>\u8f6c\u5316\u7387\uff08CC<\/sub>2<\/sub>H<\/sub>6<\/sub>\uff09\u3001C2<\/sub>H4<\/sub>\u767e\u5206\u6bd4\u548c\u9009\u62e9\u6027\uff08PC<\/sub>2<\/sub>H<\/sub>4<\/sub>\u548cSC<\/sub>2<\/sub>H<\/sub>4<\/sub>\uff09\u57fa\u672c\u4fdd\u6301\u4e0d\u53d8\u3002\u5728\u6700\u4f73\u64cd\u4f5c\u6761\u4ef6\u4e0b\uff0c\u4e59\u70ef\u4ea7\u7387\u8fbe\u523066.3%\uff0c\u8fd9\u662f\u7c7b\u4f3c\u6761\u4ef6\u4e0b\u6587\u732e\u62a5\u9053\u7684\u6700\u9ad8\u4ea7\u7387\u4e4b\u4e00\u3002<\/p>\n

\"\"<\/p>\n

\u56fe1. (a) <\/b><\/strong>SOEC \u4e2d\u5b9e\u73b0\u7535\u5316\u5b66\u6c27\u5316\u8131\u6c22\u4e0e\u4e8c\u6c27\u5316\u78b3\u7535\u89e3\u8026\u5408\u7684\u793a\u610f\u56fe\uff1b(b)<\/b><\/strong>\u00a0STCF\/LSGM\/STCF \u7535\u6c60\u7684\u7535\u6781\u4e0e\u7535\u89e3\u8d28\u754c\u9762\u7684SEM\u56fe\u50cf\uff1b(c)<\/b><\/strong>\u7535\u6d41-\u7535\u538b (I-V) \u66f2\u7ebf\uff1b(d)<\/b><\/strong>\u00a0EIS \u66f2\u7ebf\uff1b(e)<\/b><\/strong>\u4e0d\u540c\u7535\u538b\u4e0b ODH \u53cd\u5e94\u4ea7\u7269\u7684\u7ec4\u6210\uff1b(f)<\/b><\/strong>C2<\/sub>H6<\/sub>\u00a0\u8f6c\u5316\u7387\u548c C2<\/sub>H4<\/sub>\/COx<\/sub>\u9009\u62e9\u6027\uff1b(g)<\/b><\/strong>\u672c\u7814\u7a76\u4e2d\u4f7f\u7528\u4e8c\u6c27\u5316\u78b3\u4f5c\u4e3a\u6c27\u5316\u5242\u7684\u4e59\u70f7 ODH \u6027\u80fd\u4e0e\u5176\u4ed6\u62a5\u544a\u7ed3\u679c\u7684\u6bd4\u8f83\uff1b(h)<\/b><\/strong>\u00a01.2 V\u6761\u4ef6\u4e0bSOEC\u7684\u7a33\u5b9a\u8fd0\u884c\u60c5\u51b5\u3002<\/p>\n

2.<\/b><\/strong>\u901a\u8fc7\u5148\u8fdb\u7684\u5149\u8c31\u6280\u672f\u89c2\u5bdf\u6d3b\u6027\u6c27\u7269\u79cd<\/b><\/strong><\/p>\n

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\"\"<\/p>\n

\u56fe<\/b><\/strong>2.<\/b><\/strong>\uff08a\uff09<\/b><\/strong>\u8584\u819c\u6a21\u578b\u7535\u6c60\u5728C2<\/sub>H6<\/sub>\u6c14\u6c1b\u4e2d\u8fdb\u884cAPXPS\/XAS\u539f\u4f4d\u6d4b\u8bd5\u7684\u5de5\u4f5c\u539f\u7406\u793a\u610f\u56fe\uff1bO1s\uff08b\uff09<\/b><\/strong>\u3001C1s\uff08c\uff09<\/b><\/strong>\u3001O K-edge\uff08d\uff09<\/b><\/strong>\u548cCo L-edge\u8fb9\uff08e\uff09<\/b><\/strong>\u5728 0.1 mbarO2<\/sub>\uff08\u5e95\u90e8\uff09\u548c0.1 mbarC2<\/sub>H6<\/sub>\uff08640 \u4e2d\u4e0d\u540c\u7535\u89e3\u7535\u538b\u4e0b\u7684\u9633\u6781\u8868\u9762\u5149\u8c31\uff1b\uff08f\uff09<\/b><\/strong>STCF-Ov\u3001STCF \u548c STCF-O \u7684 STCF \u9633\u6781\u8868\u9762\u5728 0 V\u30012 V \u548c 2.5 V \u4e0d\u540c\u7535\u538b\u4e0b\u7684\u6a21\u578b\u56fe\u3002<\/p>\n

\"\"<\/p>\n

\u56fe3<\/b><\/strong>.<\/b><\/strong>\uff08a\uff09<\/b><\/strong>\u8584\u819c\u6a21\u578b\u7535\u6c60\u539f\u4f4d\u62c9\u66fc\u6d4b\u91cf\u793a\u610f\u56fe\uff1b\uff08b\uff09<\/b><\/strong>700\u2103\u3001C2<\/sub>H6<\/sub>\u6c14\u6c1b\u4e0bSTCF\u8584\u819c\u9633\u6781\u7684\u62c9\u66fc\u5149\u8c31\u56fe\uff1b\uff08c<\/b><\/strong>–<\/b><\/strong>f\uff09<\/b><\/strong>550\u2103\u3001C2<\/sub>H6<\/sub>\u6c14\u6c1b\u4e0bSTCF \u7c89\u672b\u7684\u539f\u4f4d\u5085\u7acb\u53f6\u53d8\u6362\u7ea2\u5916\u5149\u8c31\u56fe<\/p>\n

3<\/b><\/strong>.<\/b><\/strong>\u901a\u8fc7\u7406\u8bba\u8ba1\u7b97\u63ed\u793a\u8868\u9762\u6c27\u7269\u79cd\u7684\u4f5c\u7528<\/b><\/strong><\/p>\n

\u5bc6\u5ea6\u6cdb\u51fd\u7406\u8bba\u8ba1\u7b97\u8fdb\u4e00\u6b65\u8868\u660e\uff0c\u5728\u7535\u5316\u5b66\u9a71\u52a8\u4e0b\uff0cSTCF \u8868\u9762\u5f62\u6210\u7684\u6d3b\u6027\u6c27\u4f7fO 2p\u80fd\u5e26\u4e2d\u5fc3\u4e0a\u79fb\uff0c\u4fc3\u8fdb\u4e86\u7535\u5b50\u8f6c\u79fb\u5e76\u589e\u5f3a\u4e86\u8868\u9762\u5438\u9644\uff0c\u4ece\u800c\u6709\u529b\u5730\u4fc3\u8fdb\u4e86\u8131\u6c22\u8fc7\u7a0b\u3002<\/p>\n

\"\"<\/p>\n

\u56fe4.\uff08a\uff09<\/b><\/strong>\u4e0d\u540c\u7535\u538b\u4e0b\u8868\u9762\u6c27\u7269\u79cd\u7684\u6a21\u578b\uff08\u5206\u522b\u547d\u540d\u4e3aSTCF-OV<\/sub>\u3001STCF\u3001STCF\uff09\uff1b\uff08b\uff09<\/b><\/strong>\u6c27\u7269\u79cd\u7684\u6570\u76ee\u968f\u7740\u65bd\u52a0\u7535\u538b\u7684\u5347\u9ad8\u800c\u589e\u52a0\uff0c\u4fc3\u8fdb\u4e86\u4e59\u70f7\u6d3b\u5316\u548c\u4e59\u70f7\u7684\u6df1\u5ea6\u6c27\u5316\uff1b\uff08c\uff09<\/b><\/strong>\u4e59\u70f7ODH\u53cd\u5e94\u5728STCF-OV<\/sub>\u3001STCF\u548cSTCF\u4e0a\u7684\u81ea\u7531\u80fd\u56fe;\uff08d\uff09<\/b><\/strong>\u7b2c\u4e00\u8131\u6c22\u80fd (\u2206G1<\/sub>) \u548c\u4e59\u70ef\u89e3\u5438\u81ea\u7531\u80fd\u4e0e\u4e59\u70ef\u8131\u6c22\u81ea\u7531\u80fd\u4e4b\u5dee\uff08\u2206Gdesorption <\/sub>– \u2206G3<\/sub>\uff09<\/p>\n

\"\"<\/p>\n

\u56fe5.<\/b><\/strong>\u00a0\u4e0d\u540c\u6a21\u578b\u7cfb\u7edf\u4e2d\uff08a\uff09<\/b><\/strong>H*\u548cC2<\/sub>H5<\/sub>*\u7684\u5438\u9644\u80fd\uff1b\uff08b\uff09<\/b><\/strong>\u6295\u5f71\u6001\u5bc6\u5ea6\uff08PDOS\uff09\u5206\u6790\uff1b\uff08c\uff09<\/b><\/strong>C2<\/sub>H5<\/sub>*\u5438\u9644\u524d\u540e\u6c27\u7684\u7535\u8377\u5dee\u4e0eC2<\/sub>H5<\/sub>*\u5438\u9644\u80fd\u4e4b\u95f4\u7684\u5173\u7cfb\uff1b\uff08d\uff09<\/b><\/strong>Ti-O\u952e\u7684-COHP\u81f3\u8d39\u7c73\u80fd\u7ea7\u7684\u79ef\u5206\uff1b<\/p>\n

\uff08e\uff09<\/b><\/strong>\u6c27\u7a7a\u4f4d\u5f62\u6210\u80fd\uff1b\uff08f\uff09<\/b><\/strong>STCF\u548cSTCF-O\u7cfb\u7edf\u4e0aH2<\/sub>O\u5f62\u6210\u548c\u89e3\u5438\u7684\u81ea\u7531\u80fd\u56fe<\/p>\n

\u76f8\u5173\u7814\u7a76\u4ee5\u201cElectrochemical Activation of Surface Oxygen for Efficient Oxidative Dehydrogenation Reaction at Elevated Temperatures<\/b><\/strong>\u201d\u4e3a\u9898\uff0c\u53d1\u8868\u5728ACS Catalysis <\/i><\/b><\/em><\/strong>(DOI:\u00a010.1021\/acscatal.3c04731)\u4e0a\u3002<\/p>\n

\u7b2c\u4e00\u4f5c\u8005\uff1a\u5b59\u7fd4\u3001Heejae Yang\u3001\u9648\u5954\u9a70<\/p>\n

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\u534e\u5357\u7406\u5de5\u5927\u5b66\u9648\u71d5<\/b><\/strong>\u6559\u6388\u3001\u9996\u5c14\u5927\u5b66Jeong Woo Han<\/b><\/strong>\u6559\u6388\u4e3a\u5171\u540c\u901a\u8baf\u4f5c\u8005\u3002<\/p>\n

\u6587\u7ae0\u94fe\u63a5\uff1ahttps:\/\/pubs.acs.org\/doi\/10.1021\/acscatal.3c04731\u00a0<\/p>\n

\u9648\u71d5\u6559\u6388\u4ecb\u7ecd\uff1a<\/p>\n

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Jeongwoo Han\u6559\u6388\u4ecb\u7ecd\uff1a<\/p>\n

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