{"id":260272,"date":"2024-05-19T06:20:40","date_gmt":"2024-05-18T22:20:40","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=260272"},"modified":"2024-05-19T00:29:45","modified_gmt":"2024-05-18T16:29:45","slug":"%e6%b1%9f%e8%8b%8f%e7%a7%91%e6%8a%80%e5%a4%a7%e5%ad%a6%e9%83%ad%e5%b3%b0-%e6%96%bd%e4%bc%9f%e9%be%99%e5%9b%a2%e9%98%9fsmall%ef%bc%9a%e5%88%a9%e7%94%a8%e5%85%b7%e6%9c%89%e4%b8%b0%e5%af%8c%e8%be%b9","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=260272","title":{"rendered":"\u6c5f\u82cf\u79d1\u6280\u5927\u5b66\u90ed\u5cf0\/\u65bd\u4f1f\u9f99\u56e2\u961fSmall\uff1a\u5229\u7528\u5177\u6709\u4e30\u5bcc\u8fb9\u7f18\u6d3b\u6027\u4f4d\u70b9\u4fee\u9970\u7684\u9ad8\u7ed3\u6676\u5ea6C3N5\u6784\u5efa\u51c6\u5747\u76f8\u5149\u50ac\u5316\u8fc7\u7a0b\u4ece\u7eaf\u6c34\u4e2d\u751f\u4ea7\u8fc7\u6c27\u5316\u6c22"},"content":{"rendered":"

\u3010\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u8fc7\u6c27\u5316\u6c22(H2<\/sub>O2<\/sub>)\u5728\u6c34\u5904\u7406\u3001\u7eb8\u6d46\u6f02\u767d\u3001\u533b\u7597\u4fdd\u5065\u548c\u98df\u54c1\u5de5\u4e1a\u7b49\u591a\u4e2a\u9886\u57df\u90fd\u8868\u73b0\u51fa\u5353\u8d8a\u7684\u529f\u6548\u3002\u7136\u800c\uff0c\u4f20\u7edf\u7684H2<\/sub>O2<\/sub>\u5408\u6210\u65b9\u6cd5\u4e3b\u8981\u4f9d\u8d56\u4e8e\u84bd\u918c\u5de5\u827a\uff0c\u5e9f\u7269\u79ef\u7d2f\u3001\u80fd\u8017\u9ad8\u548c\u53cd\u5e94\u8981\u6c42\u4e25\u683c\u7b49\u95ee\u9898\u9650\u5236\u4e86\u5176\u53ef\u6301\u7eed\u751f\u4ea7\u548c\u5e7f\u6cdb\u9002\u7528\u6027\u3002\u4e0e\u84bd\u918c\u6cd5\u76f8\u6bd4\uff0c\u5149\u50ac\u5316\u53cc\u7535\u5b50\u6c27\u8fd8\u539f\u53cd\u5e94(2e–<\/sup>@ORR) \u662f\u4e00\u79cd\u66f4\u73af\u4fdd\u3001\u66f4\u9ad8\u6548\u7684\u751f\u6210H2<\/sub>O2<\/sub>\u7684\u5408\u6210\u9014\u5f84\u3002\u5728\u8fd9\u4e00\u9886\u57df\u4e2d\uff0c\u5bcc\u6c2e\u578b\u6c2e\u5316\u78b3\uff08g-C3<\/sub>N5<\/sub>\uff09\u7531\u4e8e\u5176\u589e\u5f3a\u7684\u7535\u5b50\u4f9b\u4f53\u4f4d\u70b9\u548c\u78b1\u6027\u6c2e\u542b\u91cf\uff0c\u53d7\u5230\u4e86\u5e7f\u6cdb\u5173\u6ce8\u3002\u989d\u5916\u7684\u6c2e\u5f15\u5165g-C3<\/sub>N5<\/sub>\u7684\u4e09\u55ea\u5355\u5143\u4e2d\uff0c\u6269\u5c55\u4e86\u5176\u5171\u8f6d\u7ed3\u6784\uff0c\u63d0\u9ad8\u4e86\u70ed\u529b\u5b66\u7a33\u5b9a\u6027\u3001\u7535\u5b50\u6027\u80fd\uff0c\u5e76\u7f29\u5c0f\u4e86\u5e26\u9699\u3002\u7136\u800c\uff0c\u5feb\u901f\u8f7d\u6d41\u5b50\u590d\u5408\u3001\u4f4e2e–<\/sup>@ORR\u9009\u62e9\u6027\u3001O2<\/sub>\u5438\u9644\u80fd\u529b\u4e0d\u8db3\u4ee5\u53ca\u6d3b\u6027\u4f4d\u70b9\u7a00\u7f3a\u7b49\u95ee\u9898\u4ecd\u7136\u963b\u788d\u4e86g-C3<\/sub>N5<\/sub>\u5728\u5149\u50ac\u5316H2<\/sub>O2<\/sub>\u751f\u4ea7\u4e2d\u7684\u5e94\u7528\u3002<\/p>\n

\u4e3a\u4e86\u89e3\u51b3\u8fd9\u4e9b\u95ee\u9898\u5e76\u63d0\u9ad8g-C3<\/sub>N5<\/sub>\u7684\u5149\u50ac\u5316\u6d3b\u6027\uff0c\u7814\u7a76\u4eba\u5458\u91c7\u7528\u4e86\u4e00\u7cfb\u5217\u7b56\u7565\uff0c\u5305\u62ec\u5f02\u8d28\u7ed3\u7684\u5f62\u6210\u3001\u7ed3\u6784\u5de5\u7a0b\u3001\u5143\u7d20\u63ba\u6742\u7b49\u3002\u5176\u4e2d\uff0c\u6784\u5efa\u8d85\u8584\u7eb3\u7c73\u7247\u7ed3\u6784\u8868\u73b0\u51fa\u5c24\u4e3a\u6709\u6548\u7684\u65b9\u6cd5\u3002\u8d85\u8584g-C3<\/sub>N5<\/sub>\u7ed3\u6784\u5177\u6709\u5927\u8868\u9762\u79ef\uff0c\u4e0d\u4ec5\u7f29\u77ed\u4e86\u7535\u5b50\u7684\u6269\u6563\u8def\u5f84\uff0c\u8fd8\u4fc3\u8fdb\u4e86\u5176\u5728\u5e73\u9762\u5185\u7684\u8f6c\u79fb\uff0c\u51cf\u5c11\u4e86\u7531\u4e8e\u7535\u8377\u590d\u5408\u9020\u6210\u7684\u80fd\u91cf\u635f\u5931\u3002\u7136\u800c\uff0c\u8d85\u8584g-C3<\/sub>N5<\/sub>\u5728\u5265\u79bb\u8fc7\u7a0b\u4e2d\u5bb9\u6613\u91cd\u65b0\u805a\u96c6\uff0c\u9650\u5236\u4e86\u6d3b\u6027\u4f4d\u70b9\u7684\u63a5\u89e6\u3002\u5728\u8fd9\u79cd\u60c5\u51b5\u4e0b\uff0c\u51c6\u5747\u76f8\u7cfb\u7edf\u7531\u4e8e\u5176\u9ad8\u5206\u6563\u6027\u548c\u4eb2\u6c34\u6027\uff0c\u88ab\u8ba4\u4e3a\u662f\u589e\u52a0\u8d85\u8584\u7ed3\u6784\u4e0a\u6d3b\u6027\u4f4d\u70b9\u6570\u91cf\u7684\u6709\u6548\u7b56\u7565\u3002<\/p>\n

\u3010\u6210\u679c\u63a0\u5f71\u3011<\/strong><\/p>\n

\u8d85\u8584\u6c2e\u5316\u78b3\u5f00\u521b\u4e86\u4e00\u79cd\u4fc3\u8fdb\u6709\u6548\u7535\u8377\u5206\u79bb\u548c\u52a0\u901f\u5feb\u901f\u7535\u8377\u8fc1\u79fb\u7684\u8303\u4f8b\u3002\u7136\u800c\uff0c\u7531\u4e8e\u6c2e\u5316\u78b3\u503e\u5411\u4e8e\u91cd\u65b0\u805a\u96c6\uff0c\u79bb\u89e3\u8fc7\u7a0b\u9762\u4e34\u4e2d\u65ad\uff0c\u4ece\u800c\u963b\u788d\u4e86\u6d3b\u6027\u4f4d\u70b9\u7684\u6700\u4f73\u5229\u7528\u3002\u9488\u5bf9\u8fd9\u4e00\u8feb\u5207\u9700\u8981\uff0c\u672c\u5de5\u4f5c\u91c7\u7528\u78b1\u94be\u76d0\u8f85\u52a9\u7194\u76d0\u5408\u6210\u7684\u5408\u6210\u65b9\u6cd5\u5236\u5907\u4e86\u4e00\u79cd\u5177\u6709\u8584\u5c42\u4eb2\u6c34\u6027\u7684\u6c2e\u5316\u77f3\u58a8\u6c2e\u5316\u78b3(g-C3<\/sub>N5<\/sub>-K,K)\u5149\u50ac\u5316\u5242\uff0c\u8be5\u50ac\u5316\u5242\u4e0d\u4ec5\u63d0\u9ad8\u4e86g-C3<\/sub>N5<\/sub>\u7684\u7ed3\u6676\u7a0b\u5ea6\uff0c\u800c\u4e14\u5f15\u5165\u4e86\u5927\u91cf\u4e30\u5bcc\u7684\u8fb9\u7f18\u6d3b\u6027\u4f4d\u70b9\uff0c\u5f62\u6210\u4e86\u51c6\u5747\u76f8\u7684\u5149\u50ac\u5316\u4f53\u7cfb\u3002\u5728\u53ef\u89c1\u5149\u7167\u5c04\u4e0b\uff0c\u6539\u6027\u9ad8\u7ed3\u6676g-C3<\/sub>N5<\/sub>\u5728\u7eaf\u6c34\u4e2d\u7684H2<\/sub>O2<\/sub>\u4ea7\u7387\u8fbe\u5230151.14 \u03bcM h-1<\/sup>\u3002\u8fd9\u4e00\u7a81\u7834\u6027\u7684\u7814\u7a76\u4e3a\u521b\u65b0\u8bbe\u8ba1\u5177\u6709\u51c6\u5747\u76f8\u5149\u50ac\u5316\u7cfb\u7edf\u7684\u9ad8\u6548\u5149\u50ac\u5316\u5242\u63d0\u4f9b\u4e86\u65b0\u7684\u89c6\u89d2\u3002\u76f8\u5173\u6210\u679c\u4ee5\u201cAbundant Edge Active Sites-Modified High-Crystalline g-C3<\/sub>N5<\/sub> for Hydrogen Peroxide Production from Pure-Water via a Quasi-Homogeneous Photocatalytic Process\u201d \u4e3a\u9898\u8fd1\u65e5\u5728\u7ebf\u53d1\u8868\u4e8e\u6750\u6599\u79d1\u5b66\u9886\u57df\u56fd\u9645\u8457\u540d\u5b66\u672f\u671f\u520a\u300aSmall\u300b(https:\/\/doi.org\/10.1002\/smll.202401566)\u3002\u7855\u58eb\u751f\u6c88\u94b0\u4e3a\u672c\u6587\u7b2c\u4e00\u4f5c\u8005\u3002<\/p>\n

\"\"<\/p>\n

\u3010\u56fe\u6587\u89e3\u6790\u3011<\/strong><\/p>\n

1.\u5408\u6210\u673a\u7406<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>1.<\/strong> \u78b1\u6027\u94be\u76d0\u8f85\u52a9\u56fa\u4f53\u76d0\u7ed3\u6676\u5408\u6210g-C3<\/sub>N5<\/sub>-K,K\u5149\u50ac\u5316\u5242\u7684\u793a\u610f\u56fe\u3002<\/p>\n

2.<\/strong>\u5f62\u8c8c\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>2.<\/strong> g-C3<\/sub>N5<\/sub>\u3001g-C3<\/sub>N5<\/sub>-K\u548cg-C3<\/sub>N5<\/sub>-K,K\u7684 (a-c) TEM\uff0c(d-f) AFM\u548c(g-i) HRTEM\u56fe\u50cf\uff1b(j)g-C3<\/sub>N5<\/sub>-K,K\u7684HAADF\u548cEDS\u5143\u7d20\u6620\u5c04\u56fe\u50cf\u3002<\/p>\n

3.<\/strong>\u7ed3\u6784\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>3.<\/strong> g-C3<\/sub>N5<\/sub>\u3001g-C3<\/sub>N5<\/sub>-K\u548cg-C3<\/sub>N5<\/sub>-K,K\u7684\uff08a, b\uff09XRD\u8c31\u56fe\uff0c\uff08c\uff09FT-IR\u5149\u8c31\uff0c\uff08d, e\uff09XPS\u6d4b\u91cf\u5149\u8c31\uff1b\uff08f\uff09K 2p\uff0c\uff08g\uff09C 1s\uff0c\uff08h\uff09N 1s\u548c\uff08i\uff09O 1s\u7684\u9ad8\u5206\u8fa8\u7387XPS\u5149\u8c31\u3002<\/p>\n

4.\u4eb2\u6c34\u6027\u548c\u5206\u6563\u6027\u6d4b\u8bd5<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>4<\/strong>.\uff08a\uff09g-C3<\/sub>N5<\/sub>\u3001\uff08b) g-C3<\/sub>N5<\/sub>-K\u548c\uff08c\uff09g-C3<\/sub>N5<\/sub>-K,K\u7684\u5438\u9644-\u89e3\u5438\u7b49\u6e29\u7ebf\uff1b\uff08d\uff09g-C3<\/sub>N5<\/sub>\u3001\uff08e\uff09g-C3<\/sub>N5<\/sub>-K\u548c\uff08f\uff09g-C3<\/sub>N5<\/sub>-K,K\u7684\u63a5\u89e6\u89d2\u6d4b\u8bd5\uff1b\uff08g\uff09\u5c06\u5236\u5907\u7684\u6837\u54c1\u5206\u6563\u5728\u53bb\u79bb\u5b50\u6c34\u4e2d14\u5929\u7684\u7167\u7247\uff1bg-C3<\/sub>N5<\/sub>\u3001g-C3<\/sub>N5<\/sub>-K\u548cg-C3<\/sub>N5<\/sub>-K,K\u7684\uff08h\uff09Zeta\u7535\u4f4d\u548c\uff08i\uff09\u7eb3\u7c73\u9897\u7c92\u6c89\u964d\u66f2\u7ebf\u3002<\/p>\n

5.\u5149\u50ac\u5316\u6027\u80fd\u6d4b\u8bd5<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>5.<\/strong>\uff08a\uff09\u5149\u50ac\u5316\u8fc7\u6c27\u5316\u6c22\u751f\u6210\u548c\uff08b\uff09g-C3<\/sub>N5<\/sub>\u3001g-C3<\/sub>N5<\/sub>-K\u548cg-C3<\/sub>N5<\/sub>-K,K\u7684\u8fc7\u6c27\u5316\u6c22\u751f\u6210\u901f\u7387\uff1b\uff08c\uff09\u5236\u5907\u6837\u54c1\u8fc7\u6c27\u5316\u6c22\u7684\u751f\u6210\u901f\u7387\u5e38\u6570\uff08Kf<\/sub>\uff09\u548c\u5206\u89e3\u901f\u7387\u5e38\u6570\uff08Kd<\/sub>\uff09\uff1bg-C3<\/sub>N5<\/sub>-K,K\u5728\uff08d\uff09\u4e0d\u540c\u6761\u4ef6\u548c\uff08e\uff09\u4e0d\u540c\u5355\u8272\u6ce2\u957f\u4e0b\u7684\u5149\u50ac\u5316\u8fc7\u6c27\u5316\u6c22\u751f\u4ea7\u6027\u80fd\u3002\uff08f\uff09\u5728g-C3<\/sub>N5<\/sub>-K,K\u4e0a\u8fdb\u884c\u5149\u50ac\u5316\u8fc7\u6c27\u5316\u6c22\u751f\u4ea7\u7684\u5faa\u73af\u8fd0\u884c\uff1b\uff08g\uff09\u5149\u50ac\u5316\u8fc7\u6c27\u5316\u6c22\u751f\u4ea7\u6027\u80fd\u4e0e\u76ee\u524d\u6700\u5148\u8fdb\u7684\u5149\u50ac\u5316\u5242\u7684\u6bd4\u8f83\u3002g-C3<\/sub>N5<\/sub>-K,K\u5728\uff08h\uff09\u6674\u5929\u3001\uff08i\uff09\u591a\u4e91\u548c\uff08j\uff09\u96e8\u5929\u7b49\u4e0d\u540c\u5929\u6c14\u6761\u4ef6\u4e0b\u7684\u5149\u50ac\u5316\u8fc7\u6c27\u5316\u6c22\u751f\u6210\u66f2\u7ebf\u3002<\/p>\n

6.\u80fd\u5e26\u7ed3\u6784<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>6.<\/strong> \uff08a\uff09\u7d2b\u5916-\u53ef\u89c1DRS\u5149\u8c31\uff1b\uff08b\uff09\u8f6c\u6362\u540e\u7684Kubelka-Munk\u51fd\u6570\u4e0e\u5149\u5b50\u80fd\u91cf\u7684\u5bf9\u5e94\u56fe\uff1b\uff08c\uff09g-C3<\/sub>N5<\/sub>\u3001g-C3<\/sub>N5<\/sub>-K\u548cg-C3<\/sub>N5<\/sub>-K,K\u7684VB-XPS\u5149\u8c31\uff1bg-C3<\/sub>N5<\/sub>\u3001g-C3<\/sub>N5<\/sub>-K\u548cg-C3<\/sub>N5<\/sub>-K,K\u7684\uff08d-f\uff09\u7ed3\u6784\u548c\uff08g-i\uff09DOS\u3002<\/p>\n

7.\u5236\u5907\u5149\u50ac\u5316\u5242\u7684\u8868\u9762\u7535\u573a\u4e0e\u8f7d\u6d41\u5b50\u52a8\u529b\u5b66\u7814\u7a76<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>7.<\/strong>\uff08a\uff09g-C3<\/sub>N5<\/sub>\u548c\uff08b\uff09g-C3<\/sub>N5<\/sub>-K,K\u7684\u8868\u9762\u7535\u4f4d\uff1b\u7531\u5f00\u5c14\u6587\u63a2\u9488\u529b\u663e\u5fae\u955c\uff08KPFM\uff09\u5206\u6790\u5f97\u5230\uff08c\uff09g-C3<\/sub>N5<\/sub>\u548cg-C3<\/sub>N5<\/sub>-K,K\u7684\u5185\u7f6e\u7535\u573a\u5f3a\u5ea6\u548czeta\u7535\u52bf\uff1b\u5728350 nm\u6fc0\u53d1\u4e0b\u7684TA\u5149\u8c31\u89c2\u5bdf\u5230\u7684\uff08d\uff0cg\uff09\u4e8c\u7ef4\u4f2a\u8272\u56fe\u548c\uff08e\uff0ch\uff09\u77ac\u6001\u6f2b\u53cd\u5c04\u5149\u8c31\uff1b\uff08f\uff09g-C3<\/sub>N5<\/sub>\u548c\uff08i\uff09g-C3<\/sub>N5<\/sub>-K,K\u7684\u4e8c\u6b21\u5206\u8fa8TA\u52a8\u529b\u5b66\u548c\u76f8\u5e94\u7684\u62df\u5408\u7ed3\u679c\uff1b\uff08j\uff09\u9759\u7535\u52bf\uff08ESP\uff09\u7535\u8377\u5bc6\u5ea6\u5206\u5e03\uff1b\uff08k\uff09\u4f18\u5316\u540e\u7684g-C3<\/sub>N5<\/sub>\u3001g-C3<\/sub>N5<\/sub>-K\u548cg-C3<\/sub>N5<\/sub>-K,K\u7684LUMO\u548cHOMO\u7684\u7535\u5b50\u7ed3\u6784\u3002<\/p>\n

8.\u7406\u8bba\u8ba1\u7b97<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe8.\uff08a\uff09g-C3<\/sub>N5<\/sub>\u3001g-C3<\/sub>N5<\/sub>-K\u548cg-C3<\/sub>N5<\/sub>-K,K\u7684O2<\/sub>\u5438\u9644\u5409\u5e03\u65af\u81ea\u7531\u80fd\uff08Eads\uff09\uff1b\uff08b\uff09g-C3<\/sub>N5<\/sub>\u3001g-C3<\/sub>N5<\/sub>-K\u548cg-C3<\/sub>N5<\/sub>-K,K\u7684\u6e29\u5ea6\u7f16\u7a0bO2<\/sub>\u89e3\u5438\uff08TPD-O2<\/sub>\uff09\u66f2\u7ebf\uff1b\uff08c\uff09g-C3<\/sub>N5<\/sub>\u3001g-C3<\/sub>N5<\/sub>-K\u548cg-C3<\/sub>N5<\/sub>-K,K\u7684\u8d85\u6c27\u81ea\u7531\u57fa\u7535\u5b50\u81ea\u65cb\u5171\u632f\uff08ESR\uff09\u4fe1\u53f7\uff1b\u4e0d\u540c\u6fc0\u53d1\u6001\u4e0b\u7684\uff08d\uff09C3<\/sub>N5<\/sub>-K\u3001\uff08e\uff09g-C3<\/sub>N5<\/sub>-K\u548c\uff08f\uff09g-C3<\/sub>N5<\/sub>-K,K\u7684\u7535\u5b50\u7a7a\u7a74\u5206\u5e03\uff1b\uff08g\uff0ch\uff09g-C3<\/sub>N5<\/sub>-K,K\u5728\u7eaf\u6c34\u4e2d\u5149\u50ac\u5316\u8fc7\u6c27\u5316\u6c22\u751f\u6210\u8fc7\u7a0b\u4e2d\u7684\u539f\u4f4dFT-IR\u5149\u8c31\u3002<\/p>\n

\u3010\u6587\u732e\u4fe1\u606f\u3011<\/strong><\/p>\n

Yu Shen, Rui Xu, Pengnian Shan, Shunhong Zhang, Lei Sun, Haijiao Xie, Feng Guo,* Chunsheng Li,* and Weilong Shi*, Abundant Edge Active Sites-Modified High-Crystalline g-C3N5 for Hydrogen Peroxide Production from Pure-Water via a Quasi-Homogeneous Photocatalytic Process, Small 2024, 2401566.<\/p>\n

\u5168\u6587\u94fe\u63a5\uff1ahttps:\/\/doi.org\/10.1002\/smll.202401566<\/a><\/p>\n

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