{"id":271648,"date":"2026-04-29T09:14:00","date_gmt":"2026-04-29T01:14:00","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=271648"},"modified":"2026-04-28T21:20:27","modified_gmt":"2026-04-28T13:20:27","slug":"%e5%8c%97%e5%b7%a5%e5%a4%a7%e5%90%b4%e7%8e%89%e9%94%8b%e3%80%81%e7%8e%8b%e9%95%bf%e9%be%99am-%e8%84%89%e5%86%b2%e7%94%b5%e8%a7%a3%e9%a9%b1%e5%8a%a8%e5%8a%a8%e6%80%81%e5%be%ae%e7%8e%af%e5%a2%83","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=271648","title":{"rendered":"\u5317\u5de5\u5927\u5434\u7389\u950b\u3001\u738b\u957f\u9f99AM-\u8109\u51b2\u7535\u89e3\u9a71\u52a8\u52a8\u6001\u5fae\u73af\u5883\u8c03\u63a7\u5b9e\u73b0\u542b\u786b\u5371\u5e9f\u9ad8\u6548\u8d44\u6e90\u5316"},"content":{"rendered":"\n
\"\"<\/figure>\n\n\n\n

\u80cc\u666f\u4ecb\u7ecd<\/strong><\/strong><\/h4>\n\n\n\n

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\u7535\u5316\u5b66\u786b\u5316\u7269\u6c27\u5316\u53cd\u5e94\uff08SOR\uff09\u53ef\u5728\u6e29\u548c\u6761\u4ef6\u4e0b\u5b9e\u73b0\u786b\u5316\u7269\u5411\u5355\u8d28\u786b\u7684\u8f6c\u5316\uff0c\u5e76\u534f\u540c\u4ea7\u6c22\u3002\u7136\u800c\uff0c\u5176\u5728\u5b9e\u9645\u5e94\u7528\u4e2d\u4ecd\u9762\u4e34\u5173\u952e\u6311\u6218\uff1a\u786b\u7269\u79cd\u4e0e\u91d1\u5c5e\u6d3b\u6027\u4f4d\u70b9\u4e4b\u95f4\u7684\u5f3a\u76f8\u4e92\u4f5c\u7528\u867d\u6709\u5229\u4e8e\u53cd\u5e94\u6d3b\u5316\uff0c\u5374\u4e0d\u53ef\u907f\u514d\u5730\u5bfc\u81f4\u8868\u9762\u786b\u6c89\u79ef\u4e0e\u50ac\u5316\u5242\u4e2d\u6bd2\u5931\u6d3b\uff1b\u540c\u65f6\uff0c\u591a\u786b\u4e2d\u95f4\u4f53\u7684\u7a33\u5b9a\u5438\u9644\u8fdb\u4e00\u6b65\u52a0\u5267\u6d3b\u6027\u4f4d\u70b9\u8986\u76d6\uff0c\u5f62\u6210\u201c\u9ad8\u6d3b\u6027\u2014\u4f4e\u7a33\u5b9a\u6027\u201d\u7684\u5185\u5728\u77db\u76fe\uff0c\u4e25\u91cd\u5236\u7ea6\u5176\u957f\u671f\u7a33\u5b9a\u8fd0\u884c\u3002<\/p>\n\n\n\n

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\u7814\u7a76\u521b\u65b0\u70b9<\/strong><\/strong><\/h4>\n\n\n\n

1. \u63d0\u51fa\u201c\u8109\u51b2\u7535\u89e3\u9a71\u52a8\u7684\u52a8\u6001\u5fae\u73af\u5883\u5de5\u7a0b\u201d\u65b0\u7b56\u7565\uff1a\u7a81\u7834\u4f20\u7edf\u6052\u7535\u4f4d\u7535\u89e3\u6a21\u5f0f\uff0c\u901a\u8fc7\u9ad8\u7535\u4f4d\/\u5f00\u8def\u7535\u4f4d\u7684\u5468\u671f\u5207\u6362\uff0c\u5b9e\u73b0\u754c\u9762\u53cd\u5e94\u73af\u5883\u7684\u52a8\u6001\u8c03\u63a7\uff0c\u4ece\u673a\u5236\u4e0a\u91cd\u6784\u53cd\u5e94\u8def\u5f84\u3002<\/p>\n\n\n\n

2. \u7834\u89e3SOR\u4e2d\u201c\u6d3b\u6027\u2014\u7a33\u5b9a\u6027\u201d\u5185\u5728\u77db\u76fe\uff1a\u5229\u7528\u8109\u51b2\u8c03\u63a7\u4fc3\u8fdb\u786b\u5728\u4f4e\u7535\u4f4d\u9636\u6bb5\u5feb\u901f\u8131\u9644\uff0c\u7834\u89e3\u50ac\u5316\u5242\u4e2d\u6bd2\u96be\u9898\uff0c\u5728\u4fdd\u6301\u9ad8\u6d3b\u6027\u7684\u540c\u65f6\u663e\u8457\u63d0\u5347\u4f53\u7cfb\u957f\u671f\u7a33\u5b9a\u6027\uff0c\u5b9e\u73b0\u4e8c\u8005\u7684\u534f\u540c\u4f18\u5316\u3002<\/p>\n\n\n\n

3. \u6784\u5efa\u201c\u50ac\u5316\u5242\u8bbe\u8ba1\u2014\u53cd\u5e94\u8fc7\u7a0b\u8c03\u63a7\u201d\u534f\u540c\u4f18\u5316\uff1a\u901a\u8fc7Sc\u63ba\u6742NiFe-LDH\u8c03\u63a7\u5173\u952e\u4e2d\u95f4\u4f53\u5438\u9644\u80fd\uff0c\u8026\u5408\u8109\u51b2\u7535\u89e3\uff0c\u9996\u6b21\u5b9e\u73b0\u6750\u6599\u5c42\u9762\u4e0e\u8fd0\u884c\u7b56\u7565\u7684\u534f\u540c\u8bbe\u8ba1\u3002<\/p>\n\n\n\n

4. \u5b9e\u73b0\u9ad8\u6548\u3001\u4f4e\u80fd\u8017\u7684\u786b\u5316\u7269\u8d44\u6e90\u5316\u8f6c\u5316\u4f53\u7cfb\uff1a\u5728\u6e29\u548c\u6761\u4ef6\u4e0b\u5b9e\u73b0\u786b\u5316\u7269\u5411\u5355\u8d28\u786b\u7684\u9ad8\u6548\u8f6c\u5316\uff0899.8%\u6548\u7387\u3001>500 h\u7a33\u5b9a\u8fd0\u884c\uff09\uff0c\u5e76\u8026\u5408\u9ad8\u7eaf\u6c22\u6c14\u751f\u6210\uff0c\u51cf\u6c61\u964d\u78b3\u589e\u503c\u3002<\/p>\n\n\n\n

5. \u6253\u901a\u542b\u786b\u77ff\u7269\u53ca\u590d\u5408\u56fa\u5e9f\u7684\u8d44\u6e90\u95ed\u73af\u8def\u5f84\uff1a\u63d0\u51fa\u201c\u542b\u786b\u5e9f\u5f03\u7269\u2192\u9ad8\u7eaf\u786b+\u6c22\u6c14\u201d\u7684\u9ad8\u503c\u8f6c\u5316\u8def\u7ebf\uff0c\u9a8c\u8bc1\u4e86\u4f53\u7cfb\u5728\u590d\u6742\u5de5\u51b5\u4e0b\u7684\u7a33\u5b9a\u6027\uff0c\u6784\u5efa\u4e86\u201c\u6c61\u67d3\u6cbb\u7406\u2014\u8d44\u6e90\u518d\u751f\u2014\u80fd\u6e90\u56de\u7528\u201d\u95ed\u73af\u5faa\u73af\u7ecf\u6d4e\u4f53\u7cfb\u3002<\/p>\n\n\n\n

\u56fe\u6587\u89e3\u6790<\/strong><\/strong><\/h1>\n\n\n\n
\"\"<\/figure>\n\n\n\n

\u56fe1. (a) Comparison of various anodic reactions with water electrolysis; (b) The reduction rate in energy efficiency compared to OER; (c) The subdivided cost of the entire process for SOR at the given electricity price of US$0.03 per\/kWh; (d) Levelized cost of co-productions hydrogen and sulfur via SOR, as a function of current density and electricity cost.<\/p>\n\n\n\n

\"\"<\/figure>\n\n\n\n

\u56fe2. (a) TEM image; (b) AC HAADF-STEM image of Sc-NiFe LDH and the corresponding elemental mappings; (c) HRTEM; (d) Normalized Sc K-edge XANES and (e) Fourier transform of the EXAFS spectra of Sc-NiFe-LDH and the references (Sc foil, Sc2<\/sub>O3<\/sub>); (f) Normalized Fe K-edge XANES and (g) Fourier transform of the EXAFS spectra of Sc-NiFe-LDH and the references (Fe foil, Fe2<\/sub>O3<\/sub>, NiFe-LDH); (h) WT-EXAFS contour plots of the Sc2<\/sub>O3<\/sub>, NiFe-LDH, Sc-NiFe-LDH; (i) Model of Sc-NiFe-LDH; DFT calculated adsorption energies (j) S2-<\/sup>; (k) S8<\/sub>; (l) The projected density of states (PDOS).<\/p>\n\n\n\n

\"\"<\/figure>\n\n\n\n

\u56fe3. (a) LSV curves of SOR for Sc-NiFe-LDH and control electrodes. (b) Nyquist plots at various potentials; (c) CV curves of Sc-NiFe-LDH in 1 M KOH with and without 0.5 M Na2<\/sub>S; (d) LSV curves of Sc-NiFe-LDH electrode in 1 M NaOH with Na2<\/sub>S at different scan times; (e) Open-circuit potential curves of Sc-NiFe-LDH after CE with different times in NaOH, with Na2<\/sub>S being injected subsequently. (f) Chronopotentiometric curves of Sc-NiFe-LDH at 100 mA\/cm2<\/sup>; (g) UV-vis spectra during SOR; (h) Schematic illustration of CE-SOR over Sc-NiFe-LDH.<\/p>\n\n\n\n

\"\"<\/figure>\n\n\n\n

\u56fe4. (a) Output potentials and (b) Chronoamperometric curves at CE and PE modes. (c) Removal rates of S2<\/sup>–<\/sup> and coulombic efficiencies under different potentials at CE model; (d) Output potentials of a pulsed square wave with different high and low potential duration times; (e) Removal rates of S2<\/sup>–<\/sup> and coulombic efficiencies at PE model (E0.9<\/sub> = 1\u20135 s, E0<\/sub> = 1 s); (f) Concentration changes of S2<\/sup>–<\/sup> and Sn<\/sub>2<\/sup>–<\/sup> at PE mode (E0.9<\/sub> = 2 s, E0<\/sub> = 1 s); (g) UV-vis spectra during SOR; (h) Open-circuit potential curves of Sc-NiFe-LDH at PE model; (i) SEM images of the catalysts after reaction at either CE or PE model.<\/p>\n\n\n\n

\"\"<\/figure>\n\n\n\n

\u56fe5. In-situ<\/em> Raman spectra collected at (a) CE mode; (b) PE mode; (c) CE for 5 min then PE for 6 min; Ex situ XPS spectroscopy of Sc-NiFe-LDH electrode for SOR during the time course of 10 to 40 min at (d) CE mode; (e) PE mode; (f) Schematic illustration of the mechanism of Sc-NiFe-LDH catalyzed SOR at PE mode.<\/p>\n\n\n\n

\"\"<\/figure>\n\n\n\n

\u56fe6 (a) Schematic diagram of stacked MEA system consisting of five stacked modules; (b) LSV curves of Sc-NiFe-LDH in 1 L of 1 M NaOH with or without 1 M Na2<\/sub>S in MEA; (c) Catalyst\u2019s durability tests at PE and CE mode (replacing fresh electrolyte every 52 h); (d) Comparison of the catalytic performances of Sc-NiFe-LDH with the state-of the art electrocatalysts; (e) Comparisons of the power consumptions between Sc-NiFe-LDH and literature-reported muti-functional electrocatalysts.<\/p>\n\n\n\n

\"\"<\/figure>\n\n\n\n

\u56fe7 (a) Schematic illustration of the integrated process of sulfide contaminant recycling, sulfur production, and purification; (b) Comparison of a hybrid seawater-SOR electrolyzer system with different hydrogen production techniques in energy equivalent input and CO2<\/sub> equivalent emission; (c) Durability of Sc-NiFe-LDH for the electrochemical removal of H2<\/sub>S from industrial syngas (2% H2<\/sub>S) in 1 M NaOH solution; (d) XRD of prepared S8<\/sub>; (e) XRD of obtained sodium formate; (f) Sankey diagram for the mass flow of industrial syngas upcycling; (g) SOR profit comparisons before and after sulfur purification.<\/p>\n\n\n\n

\u603b\u7ed3\u4e0e\u5c55\u671b<\/strong><\/strong><\/h1>\n\n\n\n

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