{"id":37969,"date":"2016-09-05T14:00:13","date_gmt":"2016-09-05T06:00:13","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=37969"},"modified":"2016-09-05T12:02:43","modified_gmt":"2016-09-05T04:02:43","slug":"angew-chem-int-edit-%e5%a4%a9%e6%b4%a5%e5%a4%a7%e5%ad%a6-%e8%96%84%e5%bc%82%e8%b4%a8%e7%bb%93%e5%92%8c%e7%a9%ba%e9%97%b4%e5%88%86%e7%a6%bb%e7%9a%84%e5%85%b1%e5%82%ac%e5%8c%96%e5%89%82","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=37969","title":{"rendered":"Angew \u5929\u6d25\u5927\u5b66\u6784\u5efa\u8584\u5f02\u8d28\u7ed3\u548c\u7a7a\u95f4\u5206\u79bb\u5171\u50ac\u5316\u5242\u964d\u4f4e\u5149\u50ac\u5316\u5242\u4f53\u76f8\u548c\u8868\u9762\u7535\u8377\u91cd\u7ec4"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u5149\u50ac\u5316\u53cd\u5e94\u5728\u89e3\u51b3\u80fd\u6e90\u548c\u73af\u5883\u76f8\u5173\u95ee\u9898\u65b9\u9762\u524d\u666f\u5de8\u5927\uff0c\u800c\u6709\u6548\u7684\u7535\u8377\u5206\u79bb\u548c\u5149\u5438\u6536\u662f\u56fa\u4f53\u50ac\u5316\u5242\u5b9e\u73b0\u592a\u9633\u80fd\u8f6c\u6362\u7684\u5173\u952e\u3002\u5f02\u8d28\u7ed3\u53ef\u4ee5\u6709\u6548\u5730\u63d0\u9ad8\u7535\u8377\u5206\u79bb\uff0c\u7136\u800c\u5f53\u7535\u8377\u8f6c\u79fb\u5230\u8868\u9762\u65f6\uff0c\u5982\u679c\u5b83\u4eec\u7684\u6269\u6563\u957f\u5ea6\u5c0f\u4e8e\u5f02\u8d28\u7ed3\u7684\u6df1\u5ea6\uff0c\u90a3\u4e48\u5f02\u8d28\u754c\u9762\u7684\u5206\u79bb\u7535\u8377\u4ecd\u7136\u4f1a\u53d1\u751f\u91cd\u7ec4\uff0c\u56e0\u6b64\u8981\u964d\u4f4e\u8868\u9762\u548c\u754c\u9762\u95f4\u7684\u8ddd\u79bb\u3002\u4e0d\u540c\u79cd\u7c7b\u7684\u5171\u50ac\u5316\u5242\u53ef\u4ee5\u4f5c\u4e3a\u7535\u5b50\uff08\u7a7a\u7a74\uff09\u7684\u6355\u83b7\u5668\uff0c\u4fc3\u8fdb\u7535\u8377\u5206\u79bb\u3002\u7136\u800c\uff0c\u968f\u673a\u5206\u5e03\u7684\u5171\u50ac\u5316\u5242\u7684\u7b80\u5355\u52a0\u5165\u540c\u6837\u4f1a\u589e\u52a0\u91cd\u7ec4\u7684\u53ef\u80fd\u6027\uff0c\u5bfc\u81f4\u4e25\u91cd\u7684\u9006\u53cd\u5e94\u3002\u4e3a\u4e86\u89e3\u51b3\u8fd9\u4e2a\u95ee\u9898\uff0c\u5df2\u6709\u4eba\u63d0\u51fa\u4e86\u6c27\u5316\u548c\u8fd8\u539f\u5171\u50ac\u5316\u5242\u7684\u7a7a\u95f4\u5206\u79bb\u3002\u7136\u800c\uff0c\u8fd9\u4e9b\u50ac\u5316\u5242\u53ea\u80fd\u6709\u6548\u5730\u63d0\u9ad8\u8868\u9762\u7535\u8377\u5206\u79bb\uff0c\u5374\u4e0d\u80fd\u88ab\u6291\u5236\u4f53\u76f8\u4e2d\u7684\u7535\u8377\u91cd\u7ec4\u3002\u56e0\u6b64\uff0c\u8feb\u5207\u9700\u8981\u8bbe\u8ba1\u4e00\u79cd\u50ac\u5316\u5242\u53ef\u4ee5\u540c\u65f6\u51cf\u5c11\u4f53\u76f8\u548c\u8868\u9762\u7535\u8377\u7684\u91cd\u7ec4\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u00a0<\/strong>\u8fd1\u65e5\uff0c\u5929\u6d25\u5927\u5b66\u5de9\u91d1\u9f99\u6559\u6388<\/strong>\uff08\u901a\u8baf\u4f5c\u8005\uff09\u7b49\u4eba\u5728\u56fd\u9645\u671f\u520aAngewandte Chemie International Edition<\/strong>\u4e0a\u53d1\u8868\u4e86\u4e00\u7bc7\u540d\u4e3aThin Heterojunctions and Spatially Separated Cocatalysts To Simultaneously Reduce Bulk and Surface Recombination in Photocatalysts\u7684\u6587\u7ae0\u3002\u8be5\u6587\u4ecb\u7ecd\u4e86\u4e00\u79cd\u9ad8\u6548\u5149\u50ac\u5316\u6c27\u5316\u7684\u4ecb\u5b54\u7a7a\u5fc3\u7403Pt@TiO2@In2O3@MnOx (PTIM-MSs\uff0c\u4e0b\u540c)\u7684\u8bbe\u8ba1\u4e0e\u5408\u6210\uff0c\u8be5\u7ed3\u6784\u540c\u65f6\u5229\u7528\u4e86\u7a7a\u95f4\u5206\u79bb\u7684\u5171\u50ac\u5316\u5242(Pt\u548cMnOx))\u548c\u8584\u5f02\u8d28\u7ed3(TiO2@In2O3\u58f3)\u7684\u4f18\u70b9\uff0c\u8fbe\u5230\u4e86\u964d\u4f4e\u4f53\u76f8\u548c\u8868\u9762\u7535\u8377\u91cd\u7ec4\u7684\u76ee\u7684\u3002\u7814\u7a76\u7ed3\u679c\u8868\u660e\u7a7a\u95f4\u5206\u79bb\u7684\u5171\u50ac\u5316\u5242\u9a71\u52a8\u8868\u9762\u9644\u8fd1\u7684\u7535\u5b50\u548c\u7a7a\u7a74\u5f80\u76f8\u53cd\u7684\u65b9\u5411\u6d41\u52a8\uff0c\u4ee5\u51cf\u5c11\u5b83\u4eec\u7684\u91cd\u7ec4\u3002\u8584\u5f02\u8d28\u7ed3\u80fd\u6709\u6548\u5730\u5206\u79bb\u4f53\u76f8\u4e2d\u7684\u7535\u8377\uff0c\u4f7f\u5b83\u4eec\u8f6c\u79fb\u5230\u8868\u9762\u53ca\u8868\u9762\u4ee5\u4e0b\u533a\u57df\uff0c\u4ee5\u4fbf\u5171\u50ac\u5316\u5242\u6355\u83b7\u5b83\u4eec\u6765\u53d1\u751f\u8868\u9762\u53cd\u5e94\u3002\u6b64\u5916\uff0cIn2O3\u4f5c\u4e3a\u654f\u5316\u5242\u53ef\u4ee5\u63d0\u9ad8\u5149\u7684\u5438\u6536\u3002\u7528\u4f5c\u6c34\u548c\u9152\u7cbe\u7684\u6c27\u5316\u65f6\uff0cPTIM-MSs\u7cfb\u7edf\u8868\u73b0\u51fa\u9ad8\u7684\u5149\u50ac\u5316\u6d3b\u6027\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe<\/strong>1 PTIM-MS<\/strong>\u7684\u7ed3\u6784\u53ca\u5149\u50ac\u5316\u6c27\u5316\u673a\u7406<\/strong><\/p>\n

\"1\"<\/p>\n

a) \u53cd\u5e94\u8fc7\u7a0b\u3002A\u4ee3\u8868\u7535\u5b50\u53d7\u4f53\uff0c\u8be5\u6587\u7528\u7684\u662fNaIO3<\/sub>\u3002Pt\u548cMnOx\u7531TiO2\u2014In2O3\u5f02\u6784\u53cc\u5c42\u58f3\u7a7a\u95f4\u5206\u79bb\u3002<\/p>\n

b) \u50ac\u5316\u5242\u7684\u7b80\u5316\u80fd\u5e26\u7ed3\u6784\u3002\u4ee5\u6807\u51c6\u6c22\u7535\u6781\u4f5c\u53c2\u8003\uff0cIn2O3\u548cTiO2\u7684\u5bfc\u5e26\u4f4d\u7f6e\u5206\u522b\u5728-0.63\u548c-0.40 eV\uff0c\u6839\u636e\u5e26\u9699\u8ba1\u7b97\u51fa\u5b83\u4eec\u4ef7\u5e26\u4f4d\u7f6e\u5206\u522b\u572817\u548c2.80 eV\u3002<\/p>\n

\u56fe<\/strong>2 <\/strong>\u7c92\u5b50\u7ed3\u6784\u7684\u6f14\u53d8<\/strong><\/p>\n

\"2\"<\/p>\n

a-d) TI-MSs\u7684EDS\u9762\u626b\u63cf: a) HAADF-STEM\u56fe\u50cf\uff1bb) In\u7684\u4fe1\u53f7\uff1bc) Ti\u7684\u4fe1\u53f7\uff1bd) In\u548cTi\u7684\u53e0\u52a0\u4fe1\u53f7\u3002<\/p>\n

e) SPTIS\u7684HAADF-STEM\u56fe\u50cf\u3002<\/p>\n

f) PTI-MSs\u7684TEM\u56fe\u50cf\u3002<\/p>\n

g) (f)\u56fe\u4e2d\u865a\u7ebf\u6846\u5904\u7684HRTEM\u56fe\u50cf\u3002<\/p>\n

h) PTI-MSs\u7684TEM\u56fe\u50cf\u3002\u63d2\u56fe\u4e3a\uff1aPTIM-MSs\u7684\u793a\u610f\u56fe\u3002<\/p>\n

i) (h)\u56fe\u4e2d\u865a\u7ebf\u6846\u5904\u7684HRTEM\u56fe\u50cf\u3002<\/p>\n

j) PTI-MSs\u7684EDS\u7ebf\u626b\u63cf\u3002\u66f2\u7ebf(1)-(4)\u5206\u522b\u4ee3\u8868Ti\uff0cIn\uff0cMn\u548cPt\u7684\u4fe1\u53f7\u3002<\/p>\n

k) \u653e\u5927\u540e\u7684EDS\u7ebf\u626b\u63cf\u3002\u672a\u663e\u793aIn\u548cMn\u7684\u4fe1\u53f7<\/p>\n

\u56fe<\/strong>3 <\/strong>\u5149\u50ac\u5316\u6d3b\u6027\u53ca\u5176\u52a8\u529b\u5b66\u7814\u7a76<\/strong><\/p>\n

\"3\"<\/p>\n

a) \u50ac\u5316\u5242\u7684PL\u5149\u8c31(\u03bbex=260 nm)\u3002<\/p>\n

b) \u5728\u6a21\u62df\u592a\u9633\u5149\uff08\u7d2b\u5916\/\u53ef\u89c1\u5149\uff09\u7684\u7167\u5c04\u4e0b\uff0c\u51e0\u79cd\u5149\u50ac\u5316\u5242\u5728\u6c34\u6c27\u5316\u53cd\u5e94\u4e2d\u7684\u6d3b\u6027\u3002<\/p>\n

c) \u5728\u6a21\u62df\u592a\u9633\u5149\u7684\u7167\u5c04\u4e0b\uff0c\u51e0\u79cd\u5149\u50ac\u5316\u5242\u5728\u4e59\u9187\u6c27\u5316\u53cd\u5e94\u4e2d\u7684\u6d3b\u6027\u3002<\/p>\n

d) \u76f8\u5e94\u7684\u52a8\u529b\u5b66\u7814\u7a76\u3002<\/p>\n

(c)\u548c(d)\u4e2d\u7684(1)\u2013(9)\u5206\u522b\u4ee3\u8868\u9ed1\u6697\u548c\u65e0\u50ac\u5316\u5242\u7684\u6761\u4ef6\u4e0bPTIM-MSs\uff0cPTM-MSs\uff0cTI\/P\/M-MSs\uff0cPTI-MSs\uff0cTI-MSs\uff0cT-MSs.\uff0cI-MSs\u548c PTM-MSs\u3002(1)\u2013(7)\u548c(9) \u662f\u5728\u6a21\u62df\u592a\u9633\u5149\u7167\u5c04\u4e0b\u83b7\u5f97\u3002\u50ac\u5316\u5242\u7684\u91cf\u4e3a0.06g\u3002<\/p>\n

\u56fe<\/strong>4 <\/strong>\u4f53\u76f8\u548c\u8868\u9762\u533a\u57df\u7535\u8377\u91cd\u7ec4\u7684\u63a2\u7a76<\/strong><\/p>\n

\"4\"<\/p>\n

a) T-MSs\uff0cPTM-MSs\u548cPTIMMSs\u7684\u65f6\u95f4\u5206\u8fa8PL\u5149\u8c31\u3002\u6e05\u9664\u5242\u6eb6\u6db2\u4e2d\u7684\u50ac\u5316\u5242\u8868\u793a\u4e3a\uff1a-sca\uff0c\u6837\u54c1\u5728355nm\u5904\u88ab\u6fc0\u53d1\uff0c\u5e76\u5728480nm\u5904\u8fdb\u884cPL\u76d1\u6d4b\u3002\u89c2\u5bdf\u5230\u7684\u6570\u636e\u7531\u70b9\u8868\u793a\uff0c\u62df\u5408\u540e\u4e3a\u5149\u6ed1\u66f2\u7ebf\u3002<\/p>\n

b) PTIM-MSs\u7ed3\u6784\u793a\u610f\u56fe\u3002<\/p>\n

c)\u58f3\u7684\u5e73\u5747\u539a\u5ea6\u548c\u8584\u5f02\u8d28\u7ed3\u4e0e\u7a7a\u95f4\u5206\u79bb\u7684\u5171\u50ac\u5316\u5242\u7684\u534f\u540c\u4f5c\u7528\u3002<\/p>\n

d-f) \u6ca1\u6709\u6e05\u9664\u5242\u5b58\u5728\u65f6\uff0c\u50ac\u5316\u5242\u7684\u6807\u79f0\u6269\u6563\u957f\u5ea6\u3002<\/p>\n

g\u2013i) \u6709\u6e05\u9664\u5242\u5b58\u5728\u65f6\uff0c\u50ac\u5316\u5242\u7684\u6807\u79f0\u6269\u6563\u957f\u5ea6\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u8584\u5f02\u8d28\u7ed3\u548c\u7a7a\u95f4\u5206\u79bb\u7684\u5171\u50ac\u5316\u5242\u7684\u534f\u540c\u4f5c\u7528\u53ef\u4ee5\u6709\u6548\u5730\u964d\u4f4e\u4f53\u76f8\u548c\u8868\u5c42\u533a\u57df\u7684\u7535\u8377\u91cd\u7ec4\u3002\u6b64\u5916\uff0cIn2O3\u53ef\u4ee5\u5c06TiO2\u7684\u5438\u6536\u5149\u8c31\u6269\u5c55\u5230\u53ef\u89c1\u5149\u533a\u57df\uff08510 nm\uff09\u3002\u4ece\u63d0\u9ad8\u5149\u5438\u6536\u3001\u7535\u8377\u5206\u79bb\u548c\u8868\u9762\u53cd\u5e94\u7684\u89d2\u5ea6\u6765\u770b\uff0cPTIM-MS\u7ed3\u6784\u4e3a\u5176\u4ed6\u5149\u50ac\u5316\u7cfb\u7edf\uff08\u5982\u5149\u8f85\u52a9CO2\u8fd8\u539f\uff09\u63d0\u4f9b\u4e86\u65b0\u601d\u8def\u3002<\/p>\n

\u5de9\u91d1\u9f99\u6559\u6388\u7b80\u4ecb\uff1a<\/strong><\/p>\n

\u5de9\u91d1\u9f99\uff0c\u7f8e\u56fd\u5fb7\u514b\u8428\u65af\u5927\u5b66\u5965\u65af\u6c40\u5206\u6821\u5316\u5b66\u5de5\u7a0b\u535a\u58eb\uff082008\u5e74\uff09\uff0c\u7f8e\u56fd\u54c8\u4f5b\u5927\u5b66George Whitesides\u5b9e\u9a8c\u5ba4\u535a\u58eb\u540e\u3002\u73b0\u4efb\u5929\u6d25\u5927\u5b66\u5316\u5de5\u5b66\u9662\u6559\u6388\u3001\u535a\u58eb\u751f\u5bfc\u5e08\u3001\u526f\u9662\u957f\uff08\u79d1\u7814\uff09\uff0c\u56fd\u5bb6\u6770\u51fa\u9752\u5e74\u57fa\u91d1\u83b7\u5f97\u8005\u3002\u4e3b\u8981\u4ece\u4e8b\u591a\u76f8\uff08\u5149\uff09\u50ac\u5316\u3001\u80fd\u6e90\u5316\u5de5\u5e94\u7528\u57fa\u7840\u7814\u7a76\uff0c\u5728\u56fa\u4f53\u8868\u9762\u7269\u7406\u5316\u5b66\u3001\u591a\u76f8\u50ac\u5316\u6a21\u578b\u4f53\u7cfb\u548c\u591a\u76f8\u50ac\u5316\u539f\u4f4d\u52a8\u6001\u7814\u7a76\u65b9\u6cd5\u7b49\u65b9\u9762\u53d6\u5f97\u7cfb\u7edf\u7814\u7a76\u8fdb\u5c55\u3002\u5148\u540e\u4e3b\u6301\u56fd\u5bb6\u81ea\u7136\u79d1\u5b66\u57fa\u91d1\u59d4\u91cd\u70b9\u57fa\u91d1\u3001\u79d1\u6280\u90e8863\u9879\u76ee10\u4f59\u9879\u3002\u5728Nature Commun\u3001J Am Chem Soc\u3001Angew Chem Int Ed\u3001AIChE J\u3001Adv Mater\u3001Chem Rev\u3001Acc Chem Res\u3001Chem Soc Rev\u3001Nano Lett\u3001Energy Environ Sci\u7b49\u56fd\u9645\u671f\u520a\u4e0a\u53d1\u8868\u8bba\u6587150\u4f59\u7bc7\uff0c\u88ab\u5f15\u75283500\u4f59\u6b21\uff1b\u7533\u8bf7\u7f8e\u56fd\u3001\u4e2d\u56fd\u53d1\u660e\u4e13\u522952\u9879\uff0c\u5176\u4e2d17\u9879\u5df2\u83b7\u6388\u6743\u3002\u7814\u7a76\u6210\u679c\u591a\u6b21\u88abChemical & Engineering News\u3001Nature China\u7b49\u56fd\u9645\u65b0\u95fb\u5a92\u4f53\u3001\u79d1\u5b66\u6742\u5fd7\u9074\u9009\u4e3a\u7814\u7a76\u4eae\u70b9\u62a5\u9053\uff1b\u7814\u7a76\u8bba\u658730\u4f59\u6b21\u88abJACS\u3001Adv Mater\u3001Chem Soc Rev\u3001Acc Chem Res\u3001Energy Environ Sci\u3001Chem Comm\u3001Small\u3001Nanoscale\u7b49\u671f\u520a\u9009\u4e3a\u5c01\u9762\u8bba\u6587\u520a\u767b\u3002\uff08\u901a\u8baf\u4f5c\u8005\u4fe1\u606f\u6765\u6e90\u4e8e\u5929\u6d25\u5927\u5b66\u5316\u5de5\u5b66\u9662\u5b98\u65b9\u7f51\u7ad9<\/a>\u00a0\uff09<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1aThin Heterojunctions and Spatially Separated Cocatalysts To Simultaneously Reduce Bulk and Surface Recombination in Photocatalysts<\/a>\uff08Angew. Chem. Int. Ed.\uff0c2016\uff0cDOI: <\/span>10.1002\/anie.201607765<\/span>\uff09<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u65b0\u80fd\u6e90\u5b66\u672f\u7ec4\u5c65\u51b0\u4f9b\u7a3f\uff0c\u70b9\u6211\u52a0\u5165\u7f16\u8f91\u90e8\u3002<\/a><\/p>\n

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