{"id":47966,"date":"2016-10-23T00:09:57","date_gmt":"2016-10-22T16:09:57","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=47966"},"modified":"2016-10-25T08:54:39","modified_gmt":"2016-10-25T00:54:39","slug":"%e6%ae%8a%e9%80%94%e5%90%8c%e5%bd%92-%e4%b8%8d%e9%a5%b1%e5%92%8c%e7%a1%ab%e8%be%b9%e7%bc%98%e6%95%88%e5%ba%94-%e8%b5%9d%e7%94%b5%e5%ae%b9%e6%9c%ba%e5%88%b6%e5%85%b1%e5%bb%ba","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=47966","title":{"rendered":"\u201c\u6b8a\u9014\u540c\u5f52\u201d—\u4e0d\u9971\u548c\u786b\u8fb9\u7f18\u6548\u5e94 & \u8d5d\u7535\u5bb9\u673a\u5236\u5171\u5efa\u4f18\u5f02\u7684\u94a0\u79bb\u5b50\u7535\u6c60"},"content":{"rendered":"

<\/p>\n

\u3010<\/strong>\u6210\u679c\u7b80\u4ecb<\/strong>\u3011<\/strong><\/p>\n

\u6709\u5173\u94a0\u79bb\u5b50\u7535\u6c60\u7684\u62a5\u9053\u6301\u7eed\u5237\u65b0\u7740\u6211\u4eec\u5bf9\u8fd9\u4e00\u719f\u6089\u800c\u53c8\u964c\u751f\u9886\u57df\u7684\u8ba4\u77e5\uff0c\u65b0\u7684\u7535\u6781\u6750\u6599\u6216\u53cd\u5e94\u673a\u7406\u6b63\u88ab\u4e0d\u65ad\u6316\u6398\u3002\u5728\u4e09\u79cd\u6269\u6563\u63a7\u5236\u7684\u7535\u6c60\u53cd\u5e94\u673a\u7406\uff08\u8131\u5d4c\u3001\u6c27\u5316\u8fd8\u539f\u3001\u5408\u91d1\u5316\uff09\u4e2d\uff0c\u5408\u91d1\u5316\u5411\u6765\u4ee5\u9ad8\u5bb9\u91cf\u81ea\u5c45\uff0c\u800c\u7535\u6c60\u7684\u5bb9\u91cf\u4e0e\u500d\u7387\u4e0d\u80fd\u5171\u5b58\u4f3c\u4e4e\u5df2\u88ab\u5927\u5bb6\u9ed8\u8ba4\u3002\u4e3a\u4e86\u6fc0\u53d1\u7535\u6781\u500d\u7387\u6027\u80fd\uff0c\u79d1\u5b66\u5bb6\u4eec\u5df2\u5728\u4f20\u7edf\u7684\u81ea\u7531\u8131\u5d4c\u3001\u6c27\u5316\u8fd8\u539f\u3001\u751a\u81f3\u5408\u91d1\u5316\u53cd\u5e94\u673a\u5236\u7684\u7535\u6c60\u6750\u6599\u4e2d\uff0c\u901a\u8fc7\u5bf9\u6750\u6599\u7ed3\u6784\u7684\u7269\u7406\u8c03\u63a7\uff0c\u53d1\u73b0\u4e86\u8d5d\u7535\u5bb9\u8d21\u732e\u7684\u5b58\u5728\u3002\u76f8\u5bf9\u4e8e\u6269\u6563\u673a\u5236\uff0c\u6b64\u8d5d\u7535\u5bb9\u673a\u5236\u5df2\u88ab\u8bc1\u5b9e\u5177\u6709\u5feb\u901f\u5145\u653e\u7535\u7684\u7279\u6027\u3002<\/p>\n

\u6839\u636eACS Nano\u5b98\u7f51\u5728\u7ebf\u53d1\u8868\u7684\u4e00\u6761\u6700\u65b0\u8fdb\u5c55\uff0c\u5357\u6d0b\u7406\u5de5\u5927\u5b66\u8054\u5408\u9ed1\u9f99\u6c5f\u79d1\u6280\u5927\u5b66\u3001\u4e2d\u56fd\u8ba1\u91cf\u5927\u5b66\u3001\u6d59\u6c5f\u5927\u5b66\u3001\u83ab\u65af\u79d1\u56fd\u7acb\u5927\u5b66\u5171\u540c\u5408\u4f5c\u901a\u8fc7\u4e00\u6b65\u6cd5\u6210\u529f\u5236\u5907\u81ea\u5206\u679d\u4e8c\u7ef4SnS2<\/sub>\u7eb3\u7c73\u9635\u5217\u67d4\u6027\u7535\u6781\u3002\u4f20\u7edf\u4e09\u7ef4\u67d4\u6027\u7535\u6781\u5177\u6709\u8f7d\u91cf\u4f4e\u7684\u81f4\u547d\u7f3a\u70b9\uff08\u901a\u5e38\u5c0f\u4e8e1mg\/cm2<\/sup>\uff09\uff0c\u800c\u81ea\u5206\u679d\u7ed3\u6784\u67d4\u6027\u7535\u6781\u53ef\u5c06\u5176\u8f7d\u91cf\u63d0\u9ad8\u5230~4 mg\/cm2<\/sup>\uff0c\u6781\u5927\u7a0b\u5ea6\u63d0\u9ad8\u4e86\u4e09\u7ef4\u67d4\u6027\u7535\u6781\u7684\u5b9e\u7528\u4ef7\u503c\u3002\u7b2c\u4e00\u6027\u539f\u7406\u8ba1\u7b97\u5206\u6790\u663e\u793a\uff0c\u5206\u679d\u4e0a\u5145\u5206\u66b4\u9732\u7684\u4e0d\u9971\u548c\u786b\u8fb9\u7f18\u5177\u6709\u66f4\u4e3a\u7a33\u5b9a\u7684\u7ed3\u6784\u4e14\u63d0\u4f9b\u66f4\u591a\u7535\u5316\u5b66\u6d3b\u6027\u4f4d\u3002\u5bf9\u6bd4\u65e0\u5206\u679dSnS2<\/sub>\uff0c\u81ea\u5206\u679dSnS2<\/sub>\u5177\u6709\u66f4\u9ad8\u7684\u5bb9\u91cf3.7 mAh cm-2<\/sup> (900 mAh g-1<\/sup>)\uff0c\u4ee5\u53ca\u500d\u7387\u5bb9\u91cf1.6 mAh cm-2<\/sup> (400 mAh g-1<\/sup>) at 40 mA cm-2<\/sup> (10 A g-1<\/sup>)\u3002\u5206\u6790\u8fd8\u53d1\u73b0\uff0c\u6b64\u5408\u91d1\u5316\u57fa\u4e8c\u7ef4SnS2<\/sub>\u7535\u6781\u7684\u9ad8\u500d\u7387\u6027\u80fd\u4e0e\u8d5d\u7535\u5bb9\u8d21\u732e\u5b58\u5728\u7740\u5bc6\u4e0d\u53ef\u5206\u7684\u5173\u8054\uff0c\u4e14\u81ea\u5206\u679d\u7535\u6781\u7684\u8d5d\u7535\u5bb9\u8d21\u732e\u8981\u660e\u663e\u5927\u4e8e\u65e0\u5206\u679d\u7535\u6781\u3002\u6b64\u5916\uff0c\u539f\u4f4d\u62c9\u66fc\u5149\u8c31\u5bf9\u7535\u6781\u7535\u5316\u5b66\u8fc7\u7a0b\u7684\u5206\u6790\u4ea6\u63ed\u793a\u4e86\u81ea\u5206\u679d\u7535\u6781\u5177\u6709\u8f83\u5feb\u7684\u500d\u7387\u54cd\u5e94\u7279\u6027\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb<\/strong>\u3011<\/strong><\/p>\n

\u56fe1<\/strong>\uff1a\u8fc7\u7a0b\u5e72\u9884\u6cd5\u4e00\u6b65\u5236\u5907\u81ea\u5206\u679d<\/strong>SnS2<\/sub><\/strong>\u7eb3\u7c73\u9635\u5217\u67d4\u6027\u7535\u6781<\/strong><\/p>\n

<\/p>\n

\u56fe1\u4ecb\u7ecd\u4e86\u4e00\u79cd\u4f4e\u6e29\u5feb\u901f\u5408\u6210\u5c42\u72b6SnS2<\/sub>\u9635\u5217\u7684\u65b9\u6cd5\uff0c\u901a\u8fc7\u6d53\u5ea6\u63a7\u5236\u7684\u65b9\u6cd5\u53ef\u5f97\u5230\u5927\u7247\u6216\u5c0f\u7247\u7684SnS2<\/sub>\u9635\u5217\uff0c\u8fdb\u4e00\u6b65\u901a\u8fc7\u5e72\u9884\u53cd\u5e94\u8fc7\u7a0b\u7684\u65b9\u6cd5\u5b9e\u73b0\u4e86\u81ea\u5206\u679d\u7ed3\u6784SnS2<\/sub>\u5206\u5c42\u9635\u5217\uff08\u5c0f\u7247\u5206\u679d@\u5927\u7247\u5185\u6838\uff09\u3002<\/p>\n

(a)\u5408\u6210\u8fc7\u7a0b\u6f14\u793a\u56fe\uff0c\u4e8c\u7ef4\u81ea\u5206\u679dSnS2<\/sub>\u9635\u5217\u751f\u957f\u4e8e\u8f7b\u8d28\u67d4\u6027\u5bfc\u7535\u7684\u4e09\u7ef4\u77f3\u58a8\u70ef\u57fa\u5e95\u4e0a\uff1b\uff08b\uff09SEM\u7ed3\u6784\u5206\u6790\uff0c\u81ea\u5206\u679d\u7ed3\u6784\u7531200-500 nm\u5927\u7247\u53ca~50 nm\u5c0f\u7247\u7ec4\u6210\uff1b\uff08c-e\uff09\u4e0d\u540c\u53cd\u5e94\u65f6\u95f4\u7ed3\u6784\u6f14\u53d8\u56fe\u3002<\/p>\n

\u56fe<\/strong>2<\/strong>\uff1a\u81ea\u5206\u679d<\/strong>SnS2<\/sub><\/strong>\u7eb3\u7c73\u9635\u5217\u7684\u7ed3\u6784\u53ca\u6bd4\u8868\u9762\u5206\u6790<\/strong><\/p>\n

<\/p>\n

(a-c)\u5206\u522b\u4e3a\u81ea\u5206\u679dSnS2<\/sub>\u7684\u6574\u4f53TEM\u5f62\u8c8c\u3001\u5927\u7247\u6838\u90e8\u4f4dTEM\u53ca\u5c0f\u7247\u5206\u679d\u90e8\u4f4dTEM\uff0c\u8868\u660e\u5927\u7247\u7ea6\u4e3a12\u5c42\uff0c\u5c0f\u7247\u7ea6\u4e3a4\u5c42\u539a\u5ea6\uff1b<\/p>\n

(d)\u4e3a\u5c0f\u5206\u679d\u7247\u7684HRTEM\u5206\u6790\uff0c\u663e\u793a\u5c0f\u7247\u4e3a\u5fae\u5b54\u7ed3\u6784\uff0c\u5177\u67095nm\u5de6\u53f3\u5927\u5c0f\u7684\u7eb3\u7c73\u6676\u7c92\u7ec4\u6210\uff1b(e)\u4e3aEDX\u5143\u7d20\u5206\u5e03\uff1b(f) SnS2<\/sub>\u6676\u4f53\u7ed3\u6784\u793a\u610f\u56fe\uff1b<\/p>\n

(g) XRD\u6676\u4f53\u7ed3\u6784\u5206\u6790\uff1b(h,i) \u6bd4\u8868\u9762\u53ca\u5fae\u5b54\u5927\u5c0f\u5206\u6790\uff1b<\/p>\n

\u56fe<\/strong>3<\/strong>\uff1a\u81ea\u5206\u679d<\/strong>SnS2<\/sub><\/strong>\u7eb3\u7c73\u9635\u5217\u7684\u94a0\u79bb\u5b50\u5b58\u8d2e\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

<\/p>\n

\u4f7f\u7528\u4e09\u7ef4\u77f3\u58a8\u70ef\u57fa\u5e95\u751f\u957f\u7684SnS2<\/sub>\u9635\u5217\u67d4\u6027\u7535\u6781\u5207\u7247\uff0c\u76f4\u63a5\u4f5c\u4e3a\u94a0\u79bb\u5b50\u7535\u6c60\u8d1f\u6781\u6750\u6599\uff0c\u907f\u514d\u4e86\u4f20\u7edf\u7535\u6781\u4e2d\u4f7f\u7528Cu\/Al\u96c6\u6d41\u4f53\uff0c\u70ad\u9ed1\u5bfc\u7535\u5242\u53caPVDF\u7c98\u63a5\u5242\u7b49\u53ef\u80fd\u5bfc\u81f4\u6027\u80fd\u8870\u9000\u6216\u589e\u52a0\u989d\u5916\u7535\u6781\u8d28\u91cf\u7684\u6750\u6599\u3002\u4e09\u7ef4\u77f3\u58a8\u70ef\u4e0d\u4ec5\u4f5c\u4e3a\u751f\u957f\u786b\u5316\u9521\u7684\u9aa8\u67b6\u652f\u6491\uff0c\u4f18\u826f\u7535\u5b50\u4f20\u5bfc\u7684\u8f7b\u8d28\u591a\u5b54\u96c6\u6d41\u4f53\uff0c\u540c\u65f6\u517c\u5177\u4e00\u5b9a\u67d4\u6027\u53ca\u53ef\u538b\u7f29\u6027\u3002<\/p>\n

(a-b)\u4e3a\u81ea\u5206\u679d\u53ca\u65e0\u5206\u679d\u7ed3\u6784\u5bf9\u6bd4\u4e0b\u7684CV\u66f2\u7ebf\u53ca\u7535\u5316\u5b66\u5145\u653e\u7535\u66f2\u7ebf\u3002\u5bf9\u6bd4\u53d1\u73b0\uff0c\u867d\u7136\u8d28\u91cf\u6bd4\u5bb9\u91cf\u63a5\u8fd1\uff0c\u4f46\u662f\u9762\u79ef\u5bb9\u91cf\u76f8\u5dee\u8fd14\u500d\uff1b<\/p>\n

(c-d) \u81ea\u5206\u679d\u53ca\u65e0\u5206\u679d\u7ed3\u6784\u5bf9\u6bd4\u4e0b\u7684\u500d\u7387\u5145\u653e\u7535\u66f2\u7ebf\u3002\u81ea\u5206\u679dSnS2<\/sub>\u5145\u653e\u7535\u8fc7\u7a0b\u5c55\u793a\u4e86\u503e\u659c\u7684\u5e73\u53f0\uff0c\u8fd9\u6697\u793a\u7740\u7535\u5bb9\u673a\u5236\u7684\u5b58\u5728\uff1b<\/p>\n

(e)\u4e3a \u8d28\u91cf\u6bd4\u5bb9\u91cf\u3001\u9762\u79ef\u5bb9\u91cf\u4e0e\u5176\u4ed6\u673a\u5236\u94a0\u7535\u8d1f\u6781\u6027\u80fd\uff0c\u53ca\u4e00\u4e9b\u9502\u7535\u8d1f\u6781\u6027\u80fd\u7684\u5bf9\u6bd4\u3002\u663e\u793a1.6 mAh cm-2<\/sup> (400 mAh g-1<\/sup>) at 40 mA cm-2<\/sup> (10 A g-1<\/sup>)\u8fd9\u4e00\u9762\u79ef\u500d\u7387\u5bb9\u91cf\u751a\u81f3\u8d85\u8d8a\u4e86\u5f53\u4e0b\u4f17\u591a\u9502\u7535\u6750\u6599\u3002<\/p>\n

(f-g)\u4e3a\u51e0\u79cd\u4e0d\u540c\u8fb9\u7f18\u7684DFT\u5206\u6790\u53ca\u8fb9\u7f18\u5f62\u6210\u80fd\u8ba1\u7b97\uff0c\u663e\u793aSn-S \u8fb9\u7f18\u5177\u6709\u6700\u7a33\u5b9a\u7ed3\u6784\uff1b<\/p>\n

\u56fe<\/strong>4<\/strong>\uff1a\u8d5d\u7535\u5bb9\u8ba1\u7b97\u5206\u6790\u94a0\u79bb\u5b50\u9ad8\u500d\u7387\u5b58\u8d2e\u673a\u5236<\/strong><\/p>\n

<\/p>\n

(a) \u4e3a\u81ea\u5206\u679dSnS2<\/sub> \u7eb3\u7c73\u9635\u5217\u4e0d\u540c\u626b\u901f\u4e0b\u7684CV\u56fe\uff1b<\/p>\n

(b) \u5cf0\u7535\u6d41\u5904\u5e38\u6570b\u503c\u7684\u5206\u6790\u8ba1\u7b97\uff1b<\/p>\n

(c) 1 mV\/s\u626b\u901f\u4e0b\uff0c\u7535\u5bb9\u8d21\u732e\u5360\u603b\u5bb9\u91cf\u8d21\u732e\u7684\u6bd4\u4f8b\u56fe\uff0c\u81ea\u5206\u679d\u7535\u6781\u7684\u7535\u5bb9\u5206\u6790\u8868\u660e\u517674%\u5bb9\u91cf\u8d21\u732e\u6e90\u81ea\u4e8e\u7535\u5bb9\u7c7b\u8d21\u732e\uff0c\u65e0\u5206\u679d\u4ec5\u4e3a58%\uff1b<\/p>\n

(d)\u968f\u7740\u626b\u901f\u589e\u5927\uff0c\u5176\u7535\u5bb9\u8d21\u732e\u4e5f\u9010\u6e10\u589e\u5927\uff1b<\/p>\n

\u56fe<\/strong>5<\/strong>\uff1a\u81ea\u5206\u679d<\/strong>SnS2<\/sub><\/strong>\u7eb3\u7c73\u9635\u5217\u7535\u5316\u5b66\u8fc7\u7a0b\u5206\u6790<\/strong><\/p>\n

<\/p>\n

(a)\u81ea\u5206\u679d\u7535\u6781\u5145\u653e\u7535\u66f2\u7ebf\u53ca\u7ed3\u6784\u6f14\u53d8\u793a\u610f\u56fe\uff1b<\/p>\n

(b-f)\u4e3a\u7535\u5316\u5b66\u8fc7\u7a0b\u539f\u4f4d\u963b\u6297\u5206\u6790\u3001\u975e\u539f\u4f4dTEM\u5206\u6790\uff1b<\/p>\n

(g-h)\u4e3a\u7535\u5316\u5b66\u8fc7\u7a0b\u539f\u4f4d\u62c9\u66fc\u5206\u6790\u3002\u7531\u4e8e\u7535\u5316\u5b66\u8fc7\u7a0b\u4ea7\u751f\u4f17\u591a\u7684\u975e\u6676\u4ea7\u7269\uff0cTEM\u53caXRD\u4e00\u5b9a\u7a0b\u5ea6\u9650\u5236\u4e86\u5176\u7535\u5316\u5b66\u8fc7\u7a0b\u5206\u6790\uff0c\u56e0\u6b64\u62c9\u66fc\u5206\u6790\u5728\u8fd9\u91cc\u66f4\u5177\u6709\u610f\u4e49\u3002\u7ed3\u679c\u663e\u793a\uff0c\u81ea\u5206\u679d\u7ed3\u6784SnS2<\/sub>\u5373\u4f7f\u5728\u9ad8\u500d\u7387\u5145\u653e\u7535\u8fc7\u7a0b\u4e2d\uff0c\u4ecd\u7136\u5177\u6709\u8f83\u5feb\u7684\u7ed3\u6784\u53d8\u5316\u76f8\u5e94\uff0c\u800c\u65e0\u5206\u679d\u7ed3\u6784\u5728\u9ad8\u500d\u7387\u4e0b\u201c\u6765\u4e0d\u53ca\u201d\u53cd\u5e94\uff0c\u663e\u793a\u4e86\u81ea\u5206\u679d\u7ed3\u6784\u7684\u4f18\u8d8a\u6027\u3002<\/p>\n

\u4e00\u53e5\u8bdd\u603b\u7ed3<\/strong>\uff1a<\/strong><\/p>\n

\u8be5\u5de5\u4f5c\u901a\u8fc7\u5bf9\u4e8c\u7ef4SnS2<\/sub>\u9635\u5217\u5408\u6210\u8fc7\u7a0b\u7684\u63a7\u5236\u5f97\u5230\u4e00\u79cd\u81ea\u5206\u679d\u7ed3\u6784\u7684\u67d4\u6027\u7535\u6781\uff0c\u63d0\u51fa\u4e86\u4e0d\u9971\u548c\u786b\u8fb9\u7f18\u5bf9\u7535\u5316\u5b66\u6d3b\u6027\u4f4d\u7684\u63d0\u9ad8\uff0c\u540c\u65f6\u9a8c\u8bc1\u4e86\u8d5d\u7535\u5bb9\u8d21\u732e\u7684\u5b58\u5728\u5bf9\u500d\u7387\u63d0\u5347\u7684\u610f\u4e49\u3002\u4ece\u800c\u5b9e\u73b0\u4e86\u9ad8\u5bb9\u91cf\u53ca\u9ad8\u500d\u7387\u5171\u5b58\u7684\u94a0\u79bb\u5b50\u7535\u6781\u4f53\u7cfb\u3002\u672c\u6587\u4f5c\u8005\u8054\u7cfb\u65b9\u5f0f: \u6641\u680b\u6881 \uff08S120055@e.ntu.edu.sg<\/a>\uff09<\/p>\n

\u53cb\u60c5\u63d0\u793a\uff1a\u6b64\u62a5\u9053\u4e3a\u8be5\u8bfe\u9898\u7ec4\u524d\u671fNat. Commun.\u5de5\u4f5c\u7684\u5ef6\u7eed\uff0c\u6750\u6599\u4eba\u4ea6\u5bf9\u5176\u8fdb\u884c\u4e86\u8be6\u7ec6\u62a5\u9053\uff0c\u89c1\uff1ahttp:\/\/www.cailiaoniu.com\/24923.html<\/a>\u00a0\u00a0\u00a0 (Nat. Commun. \u5357\u6d0b\u7406\u5de5\u5927\u5b66\u63d0\u51fa\u5bb9\u91cf\u4e0e\u500d\u7387\u5171\u5b58\u94a0\u79bb\u5b50\u7535\u6c60\u7684\u6784\u5efa\u673a\u5236).<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Dongliang Chao, Pei Liang, Zhen Chen, Linyi Bai, He Shen, Xiaoxu Liu, Xinhui Xia, Yanli Zhao, Serguei V Savilov, Jianyi Lin, and Ze Xiang Shen<\/p>\n

Pseudocapacitive Na-Ion Storage Boosts High-Rate and Areal Capacity of Self-Branched 2D Layered Metal Chalcogenide Nanoarrays<\/p>\n

http:\/\/pubs.acs.org\/doi\/abs\/10.1021\/acsnano.6b05566<\/a><\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u65b0\u80fd\u6e90\u5b66\u672f\u7ec4 blank \u4f9b\u7a3f\uff0c\u70b9\u8fd9\u91cc\u52a0\u5165\u6750\u6599\u4eba\u7684\u5927\u5bb6\u5ead<\/a>\u3002\u53c2\u4e0e\u65b0\u80fd\u6e90\u8bdd\u9898\u8ba8\u8bba\u8bf7\u52a0\u5165\u201c\u6750\u6599\u4eba\u65b0\u80fd\u6e90\u6750\u6599\u4ea4\u6d41\u7fa4 422065952\u201d\uff0c\u6b22\u8fce\u5173\u6ce8\u5fae\u4fe1\u516c\u4f17\u53f7\uff0c\u5fae\u4fe1\u641c\u7d22\u201c\u65b0\u80fd\u6e90\u524d\u7ebf\u201d\u6216\u626b\u7801\u5173\u6ce8\u3002<\/p>\n

\"6\"<\/p>\n","protected":false},"excerpt":{"rendered":"

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