{"id":59057,"date":"2016-12-30T06:30:00","date_gmt":"2016-12-29T22:30:00","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=59057"},"modified":"2017-03-18T21:39:53","modified_gmt":"2017-03-18T13:39:53","slug":"%e3%80%90%e5%be%85%e5%ae%a1%e6%a0%b8%ef%bc%8c%e5%ae%a1%e6%a0%b8%e5%90%8e%e8%af%b7%e9%87%8d%e6%96%b0%e5%ae%9a%e6%97%b6%e3%80%91jacs%ef%bc%9a%e9%9d%a2%e5%90%91%e9%ab%98%e6%80%a7%e8%83%bd%e5%85%89","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=59057","title":{"rendered":"JACS\uff1a\u9762\u5411\u9ad8\u6027\u80fd\u5149\u7535\u63a2\u6d4b\u5668\u7684\u4e8c\u7ef4\u9499\u949b\u77ff\u6676\u4f53"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u8fd1\u5e74\u6765\u6709\u673a\u65e0\u673a\u6742\u5316\u578b\u9499\u949b\u77ff\u6750\u6599\u5728\u5149\u7535\u5668\u4ef6\uff0c\u4f8b\u5982\u5728\u592a\u9633\u80fd\u7535\u6c60\u3001\u53d1\u5149\u4e8c\u6781\u7ba1\u3001\u5149\u7535\u63a2\u6d4b\u5668\u7b49\u65b9\u9762\u5177\u6709\u663e\u8457\u7684\u5e94\u7528\u524d\u666f\u3002\u7279\u522b\u662f2015\u5e74\u6768\u57f9\u4e1c\u8bfe\u9898\u7ec4\u901a\u8fc7\u6db2\u76f8\u6cd5\u6210\u529f\u5236\u5907\u51fa\u5ba4\u6e29\u5177\u6709\u5f3a\u8367\u5149\u7684\u4e8c\u7ef4\u5c42\u72b6\u6676\u4f53 (C4<\/sub>H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\uff0c\u4f7f\u5f97\u4e8c\u7ef4\u5355\u6676\u9499\u949b\u77ff\u6750\u6599\u8fc5\u901f\u6210\u4e3a\u7814\u7a76\u70ed\u70b9\u3002\u4e8c\u7ef4\u5355\u6676\u6709\u673a\u65e0\u673a\u6742\u5316\u9499\u949b\u77ff\u6750\u6599\u4e2d\uff0c\u65e0\u673a\u6210\u5206\u63d0\u4f9b\u4e86\u9ad8\u7684\u8f7d\u6d41\u5b50\u8fc1\u79fb\u7387\u548c\u5bbd\u7684\u5e26\u9699\u8303\u56f4\uff0c\u800c\u6709\u673a\u90e8\u5206\u5219\u63d0\u4f9b\u7ed3\u6784\u5dee\u5f02\u3001\u9ad8\u6548\u53d1\u5149\u7b49\u6027\u80fd\u3002\u66f4\u4e3a\u91cd\u8981\u7684\u662f\uff0c\u4e8c\u7ef4\u5c42\u72b6\u9499\u949b\u77ff\u6676\u4f53\u56e0\u5177\u6709\u76f4\u63a5\u5e26\u9699\u548c\u9ad8\u6001\u5bc6\u5ea6\u800c\u5c55\u73b0\u51fa\u4e30\u5bcc\u7684\u5149\u5b66\u6027\u8d28\uff0c\u4f8b\u5982\u6df1\u84dd\u8272\u53d1\u5149\u3001\u6fc0\u53d1\u6548\u5e94\u3001\u9ad8\u6548\u5438\u6536\u6027\u3002\u6b64\u5916\uff0c\u76f8\u6bd4\u4e8e\u4f20\u7edf\u7684\u591a\u6676\u9499\u949b\u77ff\u8584\u819c\uff0c\u4e8c\u7ef4\u5355\u6676\u9499\u949b\u77ff\u7f3a\u9677\u66f4\u5c11\uff0c\u4ee5\u81f3\u4e8e\u8f7d\u6d41\u5b50\u6269\u6563\u957f\u5ea6\u663e\u8457\u589e\u52a0\u3002\u56e0\u6b64\u8fd9\u79cd\u6db2\u76f8\u5236\u5907\u7684\u9499\u949b\u77ff\u6676\u4f53\u5f88\u53ef\u80fd\u5c06\u5728\u5fae\u7eb3\u5149\u7535\u5668\u4ef6\u5177\u6709\u663e\u8457\u7684\u5149\u5b66\u548c\u7535\u5b66\u6027\u8d28\u3002\u4f46\u662f\uff0c\u5728\u5fae\u7eb3\u5668\u4ef6\u5236\u5907\u8fc7\u7a0b\uff0c\u4e8c\u7ef4\u5c42\u72b6\u5355\u6676 (C4<\/sub>H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u5728\u4e00\u4e9b\u6eb6\u5242\uff08\u4e19\u916e\u6216\u8005\u6c34\uff09\u6781\u5177\u4e0d\u7a33\u5b9a\u6027\uff0c\u5355\u4e2a\u4e8c\u7ef4\u9499\u949b\u77ff\u6676\u4f53\u5fae\u7eb3\u5668\u4ef6\u8fd8\u5c1a\u672a\u5236\u5907\u6210\u529f\u3002\u56e0\u6b64\uff0c\u5982\u4f55\u514b\u670d\u9499\u949b\u77ff\u6750\u6599\u7684\u4e0d\u7a33\u5b9a\u6027\u548c\u8bbe\u8ba1\u4e8c\u7ef4\u5355\u6676\u9499\u949b\u77ff\u5668\u4ef6\u52a0\u5de5\u5de5\u827a\u662f\u4e9f\u5f85\u89e3\u51b3\u7684\u79d1\u7814\u95ee\u9898\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u5317\u4eac\u65f6\u95f412\u670814\u65e5\uff0cJACS\u5728\u7ebf\u53d1\u8868\u4e86\u9898\u4e3a\u201c\u9ad8\u6027\u80fd\u7684\u4e8c\u7ef4\u5355\u6676 (C4<\/sub>H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub> \u9499\u949b\u77ff\u5149\u7535\u63a2\u6d4b\u5668\u201d(Two-Dimensional (C4<\/sub>H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub> Perovskite Crystals for High Performance Photodetector)\u7684\u7814\u7a76\u8bba\u6587\uff0c\u5317\u4eac\u5927\u5b66\u5f6d\u6d77\u7433\u6559\u6388\u548c\u5218\u5fe0\u8303\u9662\u58eb\u4e3a\u5171\u540c\u901a\u8baf\u4f5c\u8005\u3002<\/strong><\/p>\n

\u672c\u6587\u4eae\u70b9\uff1a\u4e3a\u4e86\u89e3\u51b3\u4e8c\u7ef4\u9499\u949b\u77ff\u6676\u4f53\u5728\u5fae\u7eb3\u5668\u4ef6\u5236\u5907\u8fc7\u7a0b\u7684\u4e0d\u7a33\u5b9a\u6027\u95ee\u9898\uff0c\u5229\u7528\u5355\u5c42\u77f3\u58a8\u70ef\u4f5c\u4e3a\u4fdd\u62a4\u6750\u6599\u548c\u7535\u6781\u6750\u6599\uff0c\u6210\u529f\u5236\u5907\u51fa\u7b2c\u4e00\u4e2a\u4e8c\u7ef4\u5355\u6676\u9499\u949b\u77ff\u5149\u7535\u63a2\u6d4b\u5668\u3002\u5728\u6b64\u57fa\u7840\u4e0a\uff0c\u8bbe\u8ba1\u77f3\u58a8\u70ef\u53c9\u6307\u7535\u6781\uff0c\u5728\u5355\u4e2a\u4e8c\u7ef4\u9499\u949b\u77ff\u6676\u4f53\u4e0a\u5c55\u73b0\u51fa\u4f18\u5f02\u7684\u5149\u7535\u6027\u80fd\uff1a\u6781\u4f4e\u7684\u6697\u7535\u6d41\uff08~0.1 nA\uff09\u548c\u9ad8\u7684\u7535\u6d41\u5f00\u5173\u6bd4\uff0810\u7684\u4e09\u6b21\u65b9\uff09\uff0c\u5b9e\u73b0\u9ad8\u8fbe2100A\/W\u7684\u5149\u7535\u54cd\u5e94\u5ea6\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe<\/strong>1. <\/strong>\u4e8c\u7ef4\u5c42\u72b6<\/strong> (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub><\/strong>\u7ed3\u6784\u8868\u5f81\u56fe\u3001\u5668\u4ef6\u5236\u5907\u793a\u610f\u56fe\u4ee5\u53ca\u76f8\u5e94\u8fc7\u7a0b\u7684\u5149\u5b66\u56fe\u7247<\/strong><\/p>\n

<\/p>\n

(a). \u4e8c\u7ef4\u5c42\u72b6 (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u7ed3\u6784\u793a\u610f\u56fe<\/p>\n

(b). \u4e8c\u7ef4\u5c42\u72b6 (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u7684\u4f4e\u500dSEM\u56fe<\/p>\n

(c). (b) \u56fe\u4e2d\u6837\u54c1\u76f8\u5e94\u7684\u9009\u533a\u7535\u5b50\u884d\u5c04\u56fe<\/p>\n

(d). \u5355\u5c42\u77f3\u58a8\u70ef\u8f85\u52a9\u7684\u4e8c\u7ef4\u5c42\u72b6 (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u5668\u4ef6\u52a0\u5de5\u8fc7\u7a0b\u793a\u610f\u56fe<\/p>\n

(e). \u8f6c\u79fb\u77f3\u58a8\u70ef\u4e4b\u524d\uff0c\u751f\u957f\u5728\u7845\u7247\u4e0a\u7684\u4e8c\u7ef4 (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u6676\u4f53\u5149\u5b66\u56fe\u7247<\/p>\n

(f). \u5e72\u6cd5\u8f6c\u79fb\u77f3\u58a8\u70ef\u548c\u6d78\u6ce1\u4e19\u916e\u4e4b\u540e\u7684\u4e8c\u7ef4 (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u6676\u4f53\u5149\u5b66\u56fe\u7247<\/p>\n

(g). \u672a\u8fdb\u884c\u5668\u4ef6\u6c9f\u9053\u52a0\u5de5\u524d\uff0c\u77f3\u58a8\u70ef\u4fdd\u62a4\u4e0b\u7684\u4e8c\u7ef4 (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u6676\u4f53\u5149\u5b66\u56fe\u7247<\/p>\n

(h). \u5229\u7528\u5355\u5c42\u77f3\u58a8\u70ef\u4f5c\u7535\u6781\u7684\u4e8c\u7ef4 (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u5668\u4ef6\u5149\u5b66\u56fe\u7247<\/p>\n

\u5e72\u6cd5\u8f6c\u79fb\u77f3\u58a8\u70ef\u8986\u76d6\u5728\u4e8c\u7ef4 (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u6676\u4f53\u4e0a\uff0c\u5728\u5fae\u7eb3\u5668\u4ef6\u52a0\u5de5\u4e2d\u80fd\u591f\u4fdd\u62a4\u4e8c\u7ef4\u9499\u949b\u77ff\u6750\u6599\uff0c\u907f\u514d\u5176\u5728\u6eb6\u5242\u4e2d\u7684\u4e0d\u7a33\u5b9a\u6027\u3002<\/p>\n

\u56fe<\/strong>2. <\/strong>\u4ee5\u77f3\u58a8\u70ef\u505a\u6e90\u6f0f\u7535\u6781\uff0c\u4e8c\u7ef4\u5355\u6676<\/strong> (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub><\/strong>\u5149\u7535\u63a2\u6d4b\u5668\u7684\u5149\u7535\u6027\u80fd\u8868\u5f81<\/strong><\/p>\n

<\/p>\n

(a). \u4ee5\u77f3\u58a8\u70ef\u505a\u6e90\u6f0f\u7535\u6781\uff0c\u4e8c\u7ef4\u5355\u6676 (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u5149\u7535\u63a2\u6d4b\u5668\u793a\u610f\u56fe<\/p>\n

(b). \u5668\u4ef6\u7684SEM\u56fe<\/p>\n

(c). \u5728\u6ce2\u957f\u4e3a470 nm\u7684\u5165\u5c04\u5149\u4e0b\u4ea7\u751f\u7684\u5149\u7535\u6d41\u5206\u5e03\u56fe<\/p>\n

(d). \u5149\u7535\u6d41\u4e0e\u5165\u5c04\u5149\u6ce2\u957f\u7684\u51fd\u6570\u5173\u7cfb\u56fe<\/p>\n

(e). \u5149\u7535\u6d41\u4e0e\u5165\u5c04\u5149\u529f\u7387\u3001\u504f\u538b\u5927\u5c0f\u7684\u4e09\u7ef4\u51fd\u6570\u5173\u7cfb\u56fe<\/p>\n

\u56fe<\/strong>3. <\/strong>\u8bbe\u8ba1\u77f3\u58a8\u70ef\u53c9\u6307\u7535\u6781\u540e\uff0c\u4e8c\u7ef4\u5355\u6676<\/strong> (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub><\/strong>\u5149\u7535\u63a2\u6d4b\u5668\u7684\u5149\u7535\u6027\u80fd\u8868\u5f81<\/strong><\/p>\n

<\/p>\n

(a). \u77f3\u58a8\u70ef\u53c9\u6307\u7535\u6781\u7684\u4e8c\u7ef4\u5355\u6676 (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u5149\u7535\u63a2\u6d4b\u5668\u793a\u610f\u56fe<\/p>\n

(b). \u5668\u4ef6\u7684SEM\u56fe<\/p>\n

(c). \u5728\u6ce2\u957f\u4e3a470 nm\u7684\u5165\u5c04\u5149\u4e0b\u4ea7\u751f\u7684\u5149\u7535\u6d41\u5206\u5e03\u56fe<\/p>\n

(d). \u5355\u4e2a\u5668\u4ef6\u5728\u65e0\u5149\u7167\u548c\u4e0d\u540c\u5149\u7167\u5f3a\u5ea6\u4e0b\u7684\u5178\u578bI<\/em>SD<\/sub>–V<\/em>SD<\/sub>\u66f2\u7ebf<\/p>\n

(e). \u65f6\u95f4\u6a21\u5f0f\u4e0b\u5668\u4ef6\u7684\u7535\u6d41\u5f00\u5173\u54cd\u5e94\u56fe\uff0c\u6fc0\u5149\u5927\u5c0f\u4e3a1 mm2<\/sup>, \u5149\u5f3a\u4e3a10 \u03bcW\uff0c\u504f\u538b\u4e3a0.5 V<\/p>\n

(f). \u6709\u65e0\u5149\u7167\u5207\u6362\u4e0b\u7684\u5149\u7535\u6d41\u54cd\u5e94\u653e\u5927\u56fe<\/p>\n

\u77f3\u58a8\u70ef\u53c9\u6307\u7535\u6781\u80fd\u591f\u4fc3\u8fdb\u4e8c\u7ef4\u9499\u949b\u77ff\u6676\u4f53\u5bf9\u5149\u7684\u5438\u6536\u8303\u56f4\u548c\u52a0\u5f3a\u5149\u548c\u7269\u8d28\u7684\u76f8\u4e92\u4f5c\u7528\uff0c\u4f7f\u5f97\u5149\u7535\u6027\u80fd\u5927\u4e3a\u6539\u5584\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u4e0e\u5c55\u671b\u3011<\/strong><\/p>\n

\u81ea\u6210\u529f\u5236\u5907\u51fa\u4e8c\u7ef4\u5355\u6676\u6709\u673a\u65e0\u673a\u6742\u5316\u9499\u949b\u77ff\u4ee5\u6765\uff0c\u867d\u7136\u5176\u5177\u6709\u826f\u597d\u7684\u5149\u5b66\u6027\u8d28\uff0c\u5374\u6ca1\u6709\u50cf\u5176\u4ed6\u4e8c\u7ef4\u6750\u6599\u5728\u5fae\u7eb3\u5668\u4ef6\u65b9\u5411\u5f00\u5c55\u5e7f\u6cdb\u7684\u5e94\u7528\u3002\u800c\u672c\u6587\u7684\u7814\u7a76\u56e2\u961f\u5229\u7528\u77f3\u58a8\u70ef\u4fdd\u62a4\u4e8c\u7ef4\u5355\u6676\u9499\u949b\u77ff\u6750\u6599\uff0c\u514b\u670d\u4e86\u5176\u5728\u5fae\u7eb3\u5668\u4ef6\u52a0\u5de5\u4e2d\u7684\u4e0d\u7a33\u5b9a\u6027\uff0c\u9996\u6b21\u6210\u529f\u5236\u5907\u51fa\u5355\u4e2a\u4e8c\u7ef4 \u00a0\u00a0\u00a0\u00a0\u00a0(C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u5149\u7535\u63a2\u6d4b\u5668\u5e76\u7814\u7a76\u4e86\u5176\u672c\u5f81\u5149\u7535\u54cd\u5e94\u884c\u4e3a\u3002\u5229\u7528\u77f3\u58a8\u70ef\u53c9\u6307\u7535\u6781\uff0c\u4e8c\u7ef4 (C4H9<\/sub>NH3<\/sub>)2<\/sub>PbBr4<\/sub>\u5149\u7535\u63a2\u6d4b\u5668\u7684\u6027\u80fd\u5f97\u5230\u4e86\u6781\u5927\u7684\u63d0\u5347\u3002\u8fd9\u9879\u5de5\u4f5c\u521b\u9020\u6027\u5730\u8bbe\u8ba1\u4e86\u4e8c\u7ef4\u5355\u6676\u9499\u949b\u77ff\u5fae\u7eb3\u5668\u4ef6\u52a0\u5de5\u7684\u5de5\u827a\uff0c\u4e3a\u4e8c\u7ef4\u5355\u6676\u9499\u949b\u77ff\u5728\u5149\u7535\u5b50\u5b66\u5e94\u7528\u9886\u57df\u5f00\u8f9f\u4e86\u9053\u8def\u3002\u968f\u7740\u7814\u7a76\u7684\u8fdb\u4e00\u6b65\u6df1\u5165\u5c55\u5f00\uff0c\u76f8\u4fe1\u4e8c\u7ef4\u5355\u6676\u9499\u949b\u77ff\u6750\u6599\u4f1a\u7ed9\u6211\u4eec\u5e26\u6765\u66f4\u591a\u7684\u60ca\u559c\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Two-Dimensional (C4H9NH3)2PbBr4 Perovskite Crystals for High Performance Photodetector.<\/a>(J. Am. Chem. Soc, 2016, DOI: 10.1021\/jacs.6b11683)<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u65b0\u80fd\u6e90\u5b66\u672f\u7ec4\u6f20\u6cb3\u4ee5\u5317\u4f9b\u7a3f\u3002<\/p>\n

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\u6750\u6599\u6d4b\u8bd5\uff0c\u6570\u636e\u5206\u6790\uff0c\u4e0a<\/strong>\u6d4b\u8bd5\u8c37<\/a>\uff01<\/strong><\/p>\n","protected":false},"excerpt":{"rendered":"

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