{"id":61247,"date":"2017-01-19T14:00:41","date_gmt":"2017-01-19T06:00:41","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=61247"},"modified":"2017-01-17T20:57:19","modified_gmt":"2017-01-17T12:57:19","slug":"adv-mater-%e5%be%ae%e7%b1%b3%e5%b0%ba%e5%ba%a6%e9%87%91%e5%b1%9e%e7%bb%93%e6%9e%84%e7%9a%84%e5%a2%9e%e6%9d%90%e5%88%b6%e9%80%a0%e6%8a%80%e6%9c%af","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=61247","title":{"rendered":"Adv. Mater. : \u5fae\u7c73\u5c3a\u5ea6\u91d1\u5c5e\u7ed3\u6784\u7684\u589e\u6750\u5236\u9020\u6280\u672f"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u8fd1\u5e74\u6765\uff0c\u4f5c\u4e3a\u4e00\u79cd\u91c7\u7528\u6750\u6599\u9010\u6e10\u7d2f\u52a0\u7684\u65b9\u6cd5\u5236\u9020\u5b9e\u4f53\u96f6\u4ef6\u7684\u6280\u672f\uff0c\u589e\u6750\u5236\u9020\uff08Additive Manufacturing, AM\uff09\u6280\u672f\u5f97\u5230\u4e86\u975e\u5e38\u8fc5\u901f\u7684\u53d1\u5c55\u3002\u76f8\u6bd4\u4e8e\u4f20\u7edf\u7684\u201c\u53bb\u9664\u5f0f\u201d\u7684\u5236\u9020\u6280\u672f\uff0c\u5b83\u53ef\u4ee5\u5feb\u901f\u7cbe\u5bc6\u7684\u5236\u9020\u51fa\u5f62\u72b6\u590d\u6742\u7684\u96f6\u4ef6\uff0c\u5e76\u5927\u5927\u51cf\u5c0f\u4e86\u52a0\u5de5\u5de5\u5e8f\uff0c\u7f29\u77ed\u4e86\u52a0\u5de5\u5468\u671f\u3002\u7136\u800c\uff0c\u5bf9\u4e8e\u5fae\u7c73\u5c3a\u5ea6\u91d1\u5c5e\u7ed3\u6784\u7684AM\uff0c\u76ee\u524d\u867d\u7136\u63d0\u51fa\u4e86\u4e00\u4e9b\u65b0\u7684\u5de5\u827a\u65b9\u6cd5\uff0c\u4f46\u662f\u4ecd\u7136\u6ca1\u6709\u975e\u5e38\u6210\u719f\u7684\u89e3\u51b3\u65b9\u6848\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u6765\u81ea\u745e\u58eb\u82cf\u9ece\u4e16\u8054\u90a6\u7406\u5de5\u5b66\u9662\u7684Tomaso Zambelli\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u56e2\u961f\u5728Advenced Materials\u671f\u520a\u4e0a\u4ee5\u201cAdditive Manufacturing of Metal Structures at the Micrometer Scale\u201d\u4e3a\u9898\u53d1\u8868\u4e86\u4e00\u7bc7\u5173\u4e8e\u5fae\u7c73\u5c3a\u5ea6\u91d1\u5c5e\u7ed3\u6784AM\u7684\u7efc\u8ff0\u6027\u6587\u7ae0\u3002\u4ed6\u4eec\u9488\u5bf9\u8fd1\u5e74\u6765\u63d0\u51fa\u5e76\u53d1\u5c55\u8d77\u6765\u7684\u51e0\u79cdAM\u6280\u672f\uff0c\u5206\u522b\u603b\u7ed3\u4e86\u5b83\u4eec\u7684\u57fa\u672c\u539f\u7406\u3001\u4eea\u5668\u8bbe\u7f6e\u3001\u7279\u5f81\u5c3a\u5bf8\u3001\u5fae\u89c2\u7ed3\u6784\u7b49\u65b9\u9762\u7684\u5185\u5bb9\uff0c\u5e76\u5bf9\u672a\u6765\u7684\u6280\u672f\u53d1\u5c55\u8d8b\u52bf\u8fdb\u884c\u4e86\u8ba8\u8bba\u548c\u5c55\u671b\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe1 \u5fae\u7c73\u5c3a\u5ea6\u91d1\u5c5eAM\u6280\u672f\u6982\u89c8\uff08\u4e0a\u9762\u4e00\u884c\u7684\u6280\u672f\u4f9d\u8d56\u9884\u5408\u6210\u6750\u6599\u7684\u8f6c\u79fb\uff0c\u4e0b\u9762\u4e00\u884c\u7684\u6280\u672f\u5229\u7528\u91d1\u5c5e\u6750\u6599\u7684\u6c89\u79ef\u8fc7\u7a0b\uff09<\/strong><\/p>\n

\"\"<\/p>\n

\u76f4\u63a5\u58a8\u6c34\u4e66\u5199\uff08Direct ink writing, DIW\uff09\u6280\u672f\uff1a\u901a\u8fc7\u5fae\u7c73\u5c3a\u5bf8\u7684\u73bb\u7483\u6bdb\u7ec6\u7ba1\u55b7\u51fa\u526a\u5207\u7a00\u5316\u7684\u7eb3\u7c73\u9897\u7c92\u58a8\u6c34\uff1b<\/p>\n

\u7535\u6d41\u4f53\u5370\u5237\uff08Electrohydrodynamic printing, EHD printing\uff09\u6280\u672f\uff1a\u901a\u8fc7\u7535\u6d41\u4f53\u7684\u52a8\u529b\u6765\u9a71\u52a8\u55b7\u5c04\u7eb3\u7c73\u9897\u7c92\u58a8\u6c34\u4e2d\u7684\u4e9a\u5fae\u7c73\u5c3a\u5ea6\u6db2\u6ef4\uff1b<\/p>\n

\u6fc0\u5149\u8f85\u52a9\u7535\u6cf3\u6c89\u79ef\uff08Laser-assisted electrophoretic deposition\uff09\u6280\u672f\uff1a\u901a\u8fc7\u6fc0\u5149\u6765\u5c40\u90e8\u805a\u96c6\u6eb6\u6db2\u4e2d\u7684\u7eb3\u7c73\u7c92\u5b50\uff0c\u540c\u65f6\u65bd\u52a0\u7535\u573a\u4f7f\u7c92\u5b50\u6c89\u79ef\u5e76\u81f4\u5bc6\u5316\uff1b<\/p>\n

\u6fc0\u5149\u8bf1\u5bfc\u8f6c\u79fb\uff08Laser-induced forward transfer, LIFT\uff09\u6280\u672f\uff1a\u91d1\u5c5e\u8584\u819c\u5438\u6536\u6fc0\u5149\u8109\u51b2\uff0c\u4ece\u800c\u55b7\u51fa\u7194\u878d\u91d1\u5c5e\u6db2\u6ef4\uff0c\u6db2\u6ef4\u968f\u540e\u5728\u57fa\u5e95\u4e0a\u56fa\u5316\uff1b<\/p>\n

\u5f2f\u6708\u9762\u9650\u5236\u7684\u7535\u9540\uff08Meniscus-confined electroplating\uff09\u6280\u672f\uff1a\u5c06\u5f2f\u6708\u9762\u4e2d\u7684\u91d1\u5c5e\u76d0\u6eb6\u6db2\u4fdd\u6301\u5728\u57fa\u5e95\u548c\u4e9a\u5fae\u7c73\u7ea7\u73bb\u7483\u6bdb\u7ec6\u7ba1\u4e4b\u95f4\uff0c\u5bf9\u57fa\u5e95\u7684\u9634\u6781\u7535\u52bf\u4fc3\u4f7f\u91d1\u5c5e\u79bb\u5b50\u5728\u5f2f\u6708\u9762\u4e0a\u53d1\u751f\u7535\u5316\u5b66\u8fd8\u539f\uff1b<\/p>\n

\u6db2\u4f53\u5c40\u57df\u5206\u914d\u79bb\u5b50\u7535\u9540\uff08Electroplating of locally dispensed ions in liquid\uff09\u6280\u672f\uff1a\u901a\u8fc7\u6d78\u6ce1\u5728\u652f\u6301\u7535\u89e3\u8d28\u4e2d\u7684\u4e9a\u5fae\u7c73\u5c3a\u5bf8\u55b7\u5634\u5c06\u91d1\u5c5e\u79bb\u5b50\u6eb6\u6db2\u8fdb\u884c\u5c40\u57df\u5206\u914d\uff0c\u5bf9\u57fa\u5e95\u7684\u9634\u6781\u7535\u52bf\u4f1a\u4fc3\u4f7f\u5c40\u57df\u7684\u7535\u5316\u5b66\u6c89\u79ef\uff1b<\/p>\n

\u6fc0\u5149\u611f\u5e94\u5149\u81f4\u8fd8\u539f\uff08Laser-induced photoreduction\uff09\u6280\u672f\uff1a\u901a\u8fc7\u53cc\u5149\u5b50\u5438\u6536\u4f5c\u7528\u6765\u6fc0\u53d1\u611f\u5149\u6027\u6eb6\u6db2\u4e2d\u91d1\u5c5e\u79bb\u5b50\u7684\u5c40\u57df\u5149\u81f4\u8fd8\u539f\u4f5c\u7528\uff1b<\/p>\n

\u805a\u7126\u7535\u5b50\/\u79bb\u5b50\u675f\u8bf1\u5bfc\u6c89\u79ef\uff08Focused electron\/ion beam induced deposition, FEBID\/FIBID\uff09\u6280\u672f\uff1a\u901a\u8fc7\u4e0e\u7535\u5b50\u675f\u6216\u79bb\u5b50\u675f\u7684\u5c40\u57df\u76f8\u4e92\u4f5c\u7528\uff0c\u5c06\u524d\u9a71\u6c14\u4f53\u5206\u79bb\u6210\u91d1\u5c5e\u7684\u6210\u5206\u548c\u6709\u673a\u7684\u6210\u5206\uff0c\u7406\u60f3\u60c5\u51b5\u4e0b\uff0c\u91d1\u5c5e\u7684\u6210\u5206\u4f1a\u6c89\u79ef\uff0c\u800c\u65e0\u673a\u7684\u6210\u5206\u4f1a\u84b8\u53d1\u6389\u3002<\/p>\n

\u56fe2 \u76f4\u63a5\u58a8\u6c34\u4e66\u5199\uff08Direct ink writing, DIW\uff09\u6280\u672f<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u539f\u7406\uff1a\u901a\u8fc7\u5fae\u7c73\u5c3a\u5bf8\u7684\u73bb\u7483\u6bdb\u7ec6\u7ba1\u55b7\u51fa\u526a\u5207\u7a00\u5316\u7684\u7eb3\u7c73\u9897\u7c92\u58a8\u6c34\uff1b<\/p>\n

(b) \u9897\u7c92\u6d53\u5ea6\u5bf9\u58a8\u6c34\u7684\u7c98\u5f39\u6027\u548c\u526a\u5207\u7a00\u5316\u6027\u80fd\u7684\u5f71\u54cd\uff1b<\/p>\n

(c) \u5229\u7528\u53e0\u5c42\u6253\u5370\u6280\u672f\u5236\u9020\u7684\u4e09\u7ef4\u91d1\u5c5e\u94f6\u7ed3\u6784\u7684SEM\u7167\u7247\uff1b<\/p>\n

(d) \u6b63\u5728\u8fdb\u884c\u4e2d\u7684\u6253\u5370\u8fc7\u7a0b\uff1b<\/p>\n

(e) \u94f6\u7ebf\u5728\u4e0d\u540c\u6e29\u5ea6\u9000\u706b\u540e\u7684\u4fef\u89c6\u56fe\u53ca\u622a\u9762SEM\u7167\u7247\uff1b<\/p>\n

(f) \u5229\u7528DIW\u6280\u672f\u5728\u4e00\u4e2a4 \u00d7 4\u7684\u53d1\u5149\u4e8c\u6781\u7ba1\u9635\u5217\u4e0a\u5236\u9020\u7684\u7535\u5b50\u8fde\u63a5\u7ebf\u7684SEM\u7167\u7247\uff1b<\/p>\n

(g) \u6fc0\u5149DIW\u6280\u672f\u8fc7\u7a0b\uff1b<\/p>\n

(h) \u5728\u4e00\u4e2a\u5851\u6599\u57fa\u5e95\u4e0a\u7528\u6fc0\u5149DIW\u6280\u672f\u5236\u9020\u7684\u94f6\u7ebf\u5708\uff1b<\/p>\n

(i) \u901a\u8fc7\u53d8\u5316\u6fc0\u5149\u7684\u5f3a\u5ea6\u6765\u63a7\u5236\u9000\u706b\u7684\u7a0b\u5ea6\uff0c\u4ece\u800c\u8c03\u8282\u7535\u963b\u7387\uff0c\u672c\u56fe\u8868\u793a\u7684\u662f\u4e00\u4e2a\u6fc0\u5149DIW\u5236\u9020\u7684\u91d1\u5c5e\u7ebf\u7531\u4e8e\u53d8\u5316\u7684\u7535\u963b\u52a0\u70ed\u800c\u4ea7\u751f\u7684\u7ea2\u5916\u53d1\u5c04\u60c5\u51b5\u3002<\/p>\n

\u56fe3 \u7535\u6d41\u4f53\u5370\u5237\uff08Electrohydrodynamic printing, EHD printing\uff09\u6280\u672f<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u539f\u7406\uff1a\u901a\u8fc7\u7535\u6d41\u4f53\u7684\u52a8\u529b\u6765\u9a71\u52a8\u55b7\u5c04\u7eb3\u7c73\u9897\u7c92\u58a8\u6c34\u4e2d\u7684\u4e9a\u5fae\u7c73\u5c3a\u5ea6\u6db2\u6ef4\uff1b<\/p>\n

(b) \u4ece\u4e00\u4e2a\u5355\u4e00\u7684\u5c0f\u6db2\u6ef4\u6c89\u79ef\u7684\u91d1\u7eb3\u7c73\u9897\u7c92\u7684SEM\u7167\u7247\uff1b<\/p>\n

(c) \u6db2\u6ef4\u76f4\u5f84\u53ca\u55b7\u51fa\u9891\u7387\u968f\u5916\u52a0\u55b7\u51fa\u7535\u538b\u7684\u53d8\u5316\u60c5\u51b5\uff1b<\/p>\n

(d) \u5229\u7528EHD printing\u6280\u672f\u5236\u9020\u7684\u91d1\u7eb3\u7c73\u67f1\u7684SEM\u7167\u7247\uff1b<\/p>\n

(e) \u5728\u4e00\u4e2a\u9540\u819c\u7684\u73bb\u7483\u7247\u4e0a\u5229\u7528EHD printing\u6280\u672f\u5236\u9020\u7684\u7684\u91d1\u7eb3\u7c73\u67f1\u7684SEM\u7167\u7247\uff1b<\/p>\n

(f) \u5229\u7528EHD printing\u6280\u672f\u5236\u9020\u7684\u4e00\u79cd\u91d1\u5899\u53e0\u5c42\u7ed3\u6784\u7684SEM\u7167\u7247\uff1b<\/p>\n

(g) \u5229\u7528EHD printing\u6280\u672f\u5236\u9020\u7684\u4e00\u79cd\u590d\u5408\u6750\u6599\uff08\u9ed1\u8272\u4e3a\u78b3\u6c22\u5316\u5408\u7269\u84bd\uff0c\u7070\u8272\u4e3a\u91d1\u5c5e\u94f6\uff09\u7ed3\u6784\u7684SEM\u7167\u7247\uff1b<\/p>\n

(h) \u4e00\u79cd\u7eb5\u6a2a\u6bd4\u4e3a2.3\u3001\u7ebf\u76f4\u5f84\u4e3a80 nm\u7684\u91d1\u7f51\u683c\u900f\u660e\u7535\u6781\uff1b<\/p>\n

(i) \u7531\u76f4\u5f84\u4e3a120 nm\u7684\u91d1\u7eb3\u7c73\u67f1\u6784\u6210\u7684\u9762\u79ef\u4e3a200 \u00d7 175 \u03bcm2\u7684\u5927\u5438\u6536\u5f3a\u53cd\u5dee\u56fe\u50cf\uff1b<\/p>\n

(j) \u7528\u4e09\u7ef4\u94f6\u8fde\u63a5\u7ebf\u6765\u8054\u7ed3\u4e24\u4e2a\u67d4\u6027\u7684\u57fa\u5e95\uff1b<\/p>\n

(k) \u5177\u6709\u4e0d\u540c\u5b54\u5f84\u5c3a\u5bf8\u7684\u5e73\u9762\u5916\u6c14\u5b54\uff0c\u7528\u6765\u7814\u7a76\u7ec6\u80de\u8fc1\u79fb\u53ef\u5851\u6027\u3002<\/p>\n

\u56fe4 \u6fc0\u5149\u8f85\u52a9\u7535\u6cf3\u6c89\u79ef\uff08Laser-assisted electrophoretic deposition\uff09\u6280\u672f<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u901a\u8fc7\u6fc0\u5149\u6765\u5c40\u90e8\u805a\u96c6\u6eb6\u6db2\u4e2d\u7684\u7eb3\u7c73\u7c92\u5b50\uff0c\u540c\u65f6\u65bd\u52a0\u7535\u573a\u4f7f\u7c92\u5b50\u6c89\u79ef\u5e76\u81f4\u5bc6\u5316\uff1b<\/p>\n

(b) \u5229\u7528\u6fc0\u5149\u8f85\u52a9\u7535\u6cf3\u6c89\u79ef\u5236\u9020\u7684\u91d1\u7ebf\u5708\u7684SEM\u7167\u7247\uff1b<\/p>\n

(c) \u83b7\u5f97\u7684\u7279\u5f81\u5c3a\u5bf8\u968f\u6fc0\u5149\u5f3a\u5ea6\u7684\u53d8\u5316\u60c5\u51b5\uff1b<\/p>\n

(d) \u8be5\u6280\u672f\u53ef\u4ee5\u5236\u9020\u76f4\u5f84\u4e3a500 nm\u7684\u7eb3\u7c73\u7ebf\uff1b<\/p>\n

(e) FIB\u6a2a\u622a\u9762\u8868\u73b0\u51fa\u591a\u5b54\u7684\u5fae\u89c2\u7ed3\u6784\u3002<\/p>\n

\u56fe5 \u6fc0\u5149\u8bf1\u5bfc\u8f6c\u79fb\uff08Laser-induced forward transfer, LIFT\uff09\u6280\u672f<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u539f\u7406\uff1a\u91d1\u5c5e\u8584\u819c\u5438\u6536\u6fc0\u5149\u8109\u51b2\uff0c\u4ece\u800c\u55b7\u51fa\u7194\u878d\u91d1\u5c5e\u6db2\u6ef4\uff0c\u6db2\u6ef4\u968f\u540e\u5728\u57fa\u5e95\u4e0a\u56fa\u5316\uff1b<\/p>\n

(b) \u4e0a\u56fe\u548c\u4e0b\u56fe\u5206\u522b\u8868\u793a\u55b7\u51fa\u901f\u5ea6\u4f4e\u548c\u9ad8\u65f6\u56fa\u5316\u7684\u94dc\u6db2\u6ef4\uff0c\u8868\u73b0\u51fa\u4e0d\u540c\u7684\u51b2\u51fb\u548c\u56fa\u5316\u884c\u4e3a\uff1b<\/p>\n

(c) \u5236\u9020\u51fa\u7684\u53e0\u5c42\u7ed3\u6784\u7684\u540c\u5fc3\u5706\u67f1\u4f53\uff1b<\/p>\n

(d) \u901a\u8fc7\u5806\u579b\u6db2\u6ef4\u751f\u6210\u7684\u5782\u76f4\u548c\u503e\u659c\u94dc\u7eb3\u7c73\u67f1\uff1b<\/p>\n

(e) \u5f62\u6210\u70ed\u8bf1\u5bfc\u55b7\u5634\u540e\u65bd\u63d0\u8584\u819c\u7684\u793a\u610f\u56fe\u53caSEM\u7167\u7247\uff1b<\/p>\n

(f) \u5de6\u56fe\u548c\u53f3\u56fe\u5206\u522b\u8868\u793a\u7528LIFT\u6280\u672f\u6253\u5370\u7684\u590d\u5408\u6750\u6599\u7ed3\u6784\u5728\u7ecf\u5386\u523b\u8680\u5de5\u827a\u524d\u540e\u7684SEM\u7167\u7247\uff1b<\/p>\n

(g) \u5229\u7528LIFT\u5236\u9020\u7684\u4e00\u79cd\u94dc\u7ed3\u6784\u7684FIB\u6a2a\u622a\u9762\uff1b<\/p>\n

(h) \u901a\u8fc7\u6fc0\u5149\u8bf1\u5bfc\u6765\u8f6c\u79fb\u7eb3\u7c73\u9897\u7c92\u7cca\u72b6\u7269\u8fc7\u7a0b\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

(i) \u901a\u8fc7\u65b9\u5f62\u6fc0\u5149\u675f\u55b7\u5c04\u51fa\u7684\u4e00\u5806\u94f6\u6b63\u65b9\u5757\uff1b<\/p>\n

(j) \u4e00\u4e2a\u5927\u7684\u6b63\u65b9\u5757\uff0c\u65c1\u8fb9\u8fd8\u6709\u4e24\u4e2a\u5c0f\u7684\u5706\u5f62\u5feb\uff0c\u8bf4\u660e\u8be5\u6280\u672f\u53ef\u4ee5\u52a8\u6001\u6539\u53d8\u91d1\u5c5e\u5757\u7684\u5c3a\u5bf8\u548c\u5f62\u72b6\uff1b<\/p>\n

(k) \u7ecf\u8fc7\u4e0d\u540c\u9000\u706b\u5904\u7406\u540e\u7684\u8f6c\u79fb\u94f6\u6d46\u6599\u7684\u8868\u9762\u7ed3\u6784\u3002<\/p>\n

\u56fe6 \u5f2f\u6708\u9762\u9650\u5236\u7684\u7535\u9540\uff08Meniscus-confined electroplating\uff09\u6280\u672f<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u539f\u7406\uff1a\u5c06\u5f2f\u6708\u9762\u4e2d\u7684\u91d1\u5c5e\u76d0\u6eb6\u6db2\u4fdd\u6301\u5728\u57fa\u5e95\u548c\u4e9a\u5fae\u7c73\u7ea7\u73bb\u7483\u6bdb\u7ec6\u7ba1\u4e4b\u95f4\uff0c\u5bf9\u57fa\u5e95\u7684\u9634\u6781\u7535\u52bf\u4fc3\u4f7f\u91d1\u5c5e\u79bb\u5b50\u5728\u5f2f\u6708\u9762\u4e0a\u53d1\u751f\u7535\u5316\u5b66\u8fd8\u539f\uff1b<\/p>\n

(b) \u5229\u7528\u5f2f\u6708\u9762\u9650\u5236\u7684\u7535\u9540\u6280\u672f\u5236\u9020\u7684\u4e00\u4e2a\u94dc\u7eb3\u7c73\u67f1\u7684SEM\u7167\u7247\uff1b<\/p>\n

(c) \u63d0\u68d2\u901f\u5ea6\u548c\u79bb\u5b50\u7535\u6d41\u5bf9\u83b7\u5f97\u7684\u91d1\u5c5e\u7ebf\u76f4\u5f84\u7684\u5f71\u54cd\uff0c\u7ed3\u679c\u663e\u793a\uff0c\u63d0\u68d2\u901f\u5ea6\u8d8a\u6162\uff0c\u79bb\u5b50\u7535\u6d41\u8d8a\u9ad8\uff0c\u5f97\u5230\u7684\u91d1\u5c5e\u7ebf\u76f4\u5f84\u8d8a\u5927\uff1b<\/p>\n

(d) \u4e0a\u56fe\u8868\u793a\u7528FIB\u6539\u8fdb\u7684\u73bb\u7483\u5438\u7ba1\uff0c\u4ee5\u4fc3\u8fdb\u6c34\u5e73\u5f2f\u6708\u9762\u7684\u63a7\u5236\uff0c\u4e0b\u56fe\u8868\u793a\u5236\u9020\u7684\u94dc\u7eb3\u7c73\u4e1d\uff1b<\/p>\n

(e) \u5728AFM\u63a2\u9488\u4e0a\u5236\u9020\u7684\u4e00\u4e2a\u94c2\u7eb3\u7c73\u7ebf\uff1b<\/p>\n

(f) \u901a\u8fc7\u8c03\u6574\u5f2f\u6708\u9762\u84b8\u53d1\u901f\u7387\u4ee5\u53ca\u6c89\u79ef\u7535\u52bf\u5206\u5e03\u56fe\uff0c\u53ef\u4ee5\u5f71\u54cd\u6c89\u79ef\u7269\u7684\u5f62\u6001\uff0c\u4ece\u800c\u5236\u9020\u51fa\u591a\u5b54\u3001\u7a20\u5bc6\u6216\u8005\u7a7a\u5fc3\u7684\u7ed3\u6784\u3002<\/p>\n

\u56fe7 \u6db2\u4f53\u5c40\u57df\u5206\u914d\u79bb\u5b50\u7535\u9540\uff08Electroplating of locally dispensed ions in liquid\uff09\u6280\u672f<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u539f\u7406\uff1a\u901a\u8fc7\u6d78\u6ce1\u5728\u652f\u6301\u7535\u89e3\u8d28\u4e2d\u7684\u4e9a\u5fae\u7c73\u5c3a\u5bf8\u55b7\u5634\u5c06\u91d1\u5c5e\u79bb\u5b50\u6eb6\u6db2\u8fdb\u884c\u5c40\u57df\u5206\u914d\uff0c\u5bf9\u57fa\u5e95\u7684\u9634\u6781\u7535\u52bf\u4f1a\u4fc3\u4f7f\u5c40\u57df\u7684\u7535\u5316\u5b66\u6c89\u79ef\uff1b<\/p>\n

(b) \u4e0d\u540c\u53cd\u9988\u673a\u5236\uff0c\u4e0a\u56fe\u548c\u4e0b\u56fe\u5206\u522b\u8868\u793aFluidFM\u7cfb\u7edf\u4ee5\u53caSICM\u7cfb\u7edf\uff1b<\/p>\n

(c) \u5229\u7528SICM\u7cfb\u7edf\u5236\u9020\u7684\u9ad8\u6a2a\u7eb5\u6bd4\u7ed3\u6784\uff1b<\/p>\n

(d) \u5229\u7528SICM\u7cfb\u7edf\u5236\u9020\u7684\u7a81\u51fa\u7ed3\u6784\uff1b<\/p>\n

(e) SICM\u7cfb\u7edf\u53ef\u4ee5\u8fdb\u884c\u539f\u4f4d\u7684\u5f62\u6001\u626b\u63cf\uff1b<\/p>\n

(f) \u5229\u7528FluidFM\u7cfb\u7edf\u5236\u9020\u7684\u53e0\u5c42\u5f0f\u4e09\u91cd\u87ba\u65cb\u7ed3\u6784\uff1b<\/p>\n

(g) \u5229\u7528FluidFM\u7cfb\u7edf\u5236\u9020\u7684\u53e0\u5c42\u5f0f\u94dc\u5899\u7ed3\u6784\uff1b<\/p>\n

(h) \u5229\u7528FluidFM\u7cfb\u7edf\u5236\u9020\u7684\u94dc\u7ed3\u6784\u7684FIB\u6a2a\u622a\u9762\u3002<\/p>\n

\u56fe8 \u6fc0\u5149\u611f\u5e94\u5149\u81f4\u8fd8\u539f\uff08Laser-induced photoreduction\uff09\u6280\u672f<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u539f\u7406\uff1a\u901a\u8fc7\u53cc\u5149\u5b50\u5438\u6536\u4f5c\u7528\u6765\u6fc0\u53d1\u611f\u5149\u6027\u6eb6\u6db2\u4e2d\u91d1\u5c5e\u79bb\u5b50\u7684\u5c40\u57df\u5149\u81f4\u8fd8\u539f\u4f5c\u7528\uff1b<\/p>\n

(b) \u4e00\u7ef4\u94f6\u6c89\u79ef\u7684\u5c3a\u5bf8\u968f\u6fc0\u5149\u529f\u7387\u548c\u66dd\u5149\u65f6\u95f4\u7684\u53d8\u5316\u60c5\u51b5\uff0c\u7ed3\u679c\u8868\u660e\uff0c\u6fc0\u5149\u529f\u7387\u8d8a\u5c0f\uff0c\u66dd\u5149\u65f6\u95f4\u8d8a\u77ed\uff0c\u5f97\u5230\u7684\u5355\u4e2a\u70b9\u7684\u76f4\u5f84\u8d8a\u5c0f\uff1b<\/p>\n

(c) \u5728\u4e00\u4e2a\u7531\u7eafAgNO3\u6eb6\u6db2\u5408\u6210\u7684\u73bb\u7483\u57fa\u7247\u4e0a\u5236\u9020\u7684\u4e09\u7ef4\u94f6\u7ed3\u6784\u7684SEM\u7167\u7247\uff1b<\/p>\n

(d) \u5728\u4e00\u4e2a\u7531AgNO3\u6eb6\u6db2\u53ca\u611f\u5149\u67d3\u6599\u5408\u6210\u7684\u73bb\u7483\u57fa\u7247\u4e0a\u5236\u9020\u7684\u4e09\u7ef4\u94f6\u7ed3\u6784\u7684SEM\u7167\u7247\uff1b<\/p>\n

(e) \u5728\u4e00\u4e2a\u7531AgNO3\u6eb6\u6db2\u53caNDSS\u6eb6\u6db2\u5408\u6210\u7684\u73bb\u7483\u57fa\u7247\u4e0a\u5236\u9020\u7684\u4e09\u7ef4\u94f6\u7ed3\u6784\u7684SEM\u7167\u7247\uff1b<\/p>\n

(f) \u5728\u4e00\u4e2a\u7531AgNO3\u6eb6\u6db2\u53caNDSS\u6eb6\u6db2\u5408\u6210\u7684\u73bb\u7483\u57fa\u7247\u4e0a\u5236\u9020\u7684\u4e09\u7ef4\u94f6\u7ed3\u6784\u7684SEM\u7167\u7247\uff1b<\/p>\n

(g) \u4e0a\u56fe\u548c\u4e0b\u56fe\u5206\u522b\u8868\u793a\u5728AgNO3\u6eb6\u6db2\u4e2d\u6dfb\u52a0\u548c\u4e0d\u6dfb\u52a0\u611f\u5149\u67d3\u6599\u5236\u9020\u7684\u94f6\u7eb3\u7c73\u70b9\u7684SEM\u7167\u7247\uff1b<\/p>\n

(h) \u5728Ag(NH3)2\u548c\u7535\u89e3\u6db2\u7684\u6df7\u5408\u6db2\u4e2d\u6dfb\u52a0\u4e0d\u540c\u6d53\u5ea6\u7684\u8868\u9762\u6d3b\u6027NDSS\u6eb6\u6db2\u5236\u9020\u7684\u94f6\u7eb3\u7c73\u7ebf\u7684SEM\u7167\u7247\u3002<\/p>\n

\u56fe9 \u805a\u7126\u7535\u5b50\/\u79bb\u5b50\u675f\u8bf1\u5bfc\u6c89\u79ef\uff08Focused electron\/ion beam induced deposition, FEBID\/FIBID\uff09\u6280\u672f<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u539f\u7406\uff1a\u901a\u8fc7\u4e0e\u7535\u5b50\u675f\u6216\u79bb\u5b50\u675f\u7684\u5c40\u57df\u76f8\u4e92\u4f5c\u7528\uff0c\u5c06\u524d\u9a71\u6c14\u4f53\u5206\u79bb\u6210\u91d1\u5c5e\u7684\u6210\u5206\u548c\u6709\u673a\u7684\u6210\u5206\uff0c\u7406\u60f3\u60c5\u51b5\u4e0b\uff0c\u91d1\u5c5e\u7684\u6210\u5206\u4f1a\u6c89\u79ef\uff0c\u800c\u65e0\u673a\u7684\u6210\u5206\u4f1a\u84b8\u53d1\u6389\uff1b<\/p>\n

(b) \u5229\u7528\u4e0d\u540c\u5149\u675f\u76f4\u5f84\u5236\u9020\u7684\u94c2\u68d2\u7684SEM\u7167\u7247\uff1b<\/p>\n

(c) \u5728\u81ea\u7531\u7a7a\u95f4\u4e2d\u751f\u957f\u7684\u4e00\u4e2a\u6c34\u5e73DLC\u7ebf\u7684SEM\u7167\u7247\uff1b<\/p>\n

(d) \u5728\u81ea\u7531\u7a7a\u95f4\u4e2d\u5236\u9020\u7684\u4e00\u4e2a\u76f4\u5f84\u4e3a8 nm\u68d2\u7684\u94a8\u7ed3\u6784\u7684TEM\u7167\u7247\uff1b<\/p>\n

(e) \u5de6\u56fe\u548c\u53f3\u56fe\u5206\u522b\u8868\u793a\u4e00\u79cd\u91d1\u87ba\u65cb\u7ed3\u6784\u5728\u70ed\u5904\u7406\u524d\u540e\u7684\u663e\u5fae\u7167\u7247\uff1b<\/p>\n

(f) \u5de6\u56fe\u8868\u793a\u501f\u52a9\u8ba1\u7b97\u6a21\u62df\u7528FEBID\u65b9\u6cd5\u5236\u9020\u7684\u94c2\u4e8c\u5341\u9762\u4f53\u7684SEM\u7167\u7247\uff0c\u53f3\u56fe\u8868\u793a\u8ba1\u7b97\u6a21\u62df\u7ed9\u51fa\u7684\u7535\u5b50\u675f\u4e0e\u6c89\u79ef\u7269\u4e4b\u95f4\u7684\u76f8\u4e92\u4f5c\u7528\uff1b<\/p>\n

(g) \u4e00\u79cd\u542b\u94c2\u7684\u6c89\u79ef\u7269\u7684TEM\u7167\u7247\uff1b<\/p>\n

(h) \u4e0a\u56fe\u548c\u4e0b\u56fe\u5206\u522b\u8868\u793a\u4ee5\u4e0d\u542b\u78b3\u7684PF3AuCl\u548c\u6709\u673a\u7684Me2Au(tfa)\u4f5c\u4e3a\u524d\u9a71\u4f53\u5229\u7528FEBID\u6280\u672f\u5236\u9020\u7684\u4e8c\u7ef4\u6c89\u79ef\u7269\u7684SEM\u7167\u7247\uff1b<\/p>\n

(i) \u7528FEBID\u65b9\u6cd5\u5236\u9020\u7684\u4e00\u79cd\u94c2\u7ed3\u6784SEM\u7167\u7247\uff0c\u901a\u8fc7\u539f\u4f4d\u7684\u70ed\u5904\u7406\u6765\u6539\u5584\u7ed3\u6784\u7684\u5f62\u72b6\u7a33\u5b9a\u6027\uff1b<\/p>\n

(j) \u5728\u5546\u4e1aAFM\u63a2\u9488\u4e0a\u7528FEBID\u65b9\u6cd5\u5236\u9020\u7684\u94c1\u7eb3\u7c73\u7ebf\uff1b<\/p>\n

(k) \u4e00\u79cd\u75316 \u00d7 6\u87ba\u65cb\u7ed3\u6784\u9635\u5217\u7ec4\u6210\u7684\u5149\u5b66\u8d85\u6750\u6599\uff0c\u6bcf\u4e2a\u87ba\u65cb\u7ed3\u6784\u7531\u4e09\u4e2a\u76f8\u4e92\u7f20\u7ed5\u7684\u94c2\u87ba\u65cb\u7ebf\u6784\u6210\uff1b<\/p>\n

(l) \u51b7\u6c89\u6dc0FEBID\u65b9\u6cd5\u7684\u57fa\u672c\u539f\u7406\uff1b<\/p>\n

(m) \u572830\u79d2\u5185\u7528\u51b7\u6c89\u6dc0FEBID\u65b9\u6cd5\u5236\u9020\u7684\u94c2\u6b63\u65b9\u5757\u7684SEM\u7167\u7247\uff1b<\/p>\n

(n) \u5728\u8fde\u7eed\u4e94\u4e2a\u805a\u5408-\u66b4\u9732\u5faa\u73af\u4e2d\u7528\u51b7\u6c89\u6dc0FEBID\u65b9\u6cd5\u5236\u9020\u7684\u4e09\u7ef4\u94c2\u7ed3\u6784\u3002<\/p>\n

\u56fe10 \u5fae\u7c73\u5c3a\u5ea6\u91d1\u5c5eAM\u6280\u672f\u529f\u80fd\u53ca\u7279\u5f81\u6c47\u603b<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u6bcf\u79cd\u6280\u672f\u6709\u80fd\u529b\u5236\u9020\u7684\u51e0\u4f55\u5f62\u72b6\u7ed3\u6784\u7684\u793a\u610f\u56fe\uff0c\u7eff\u8272\u8868\u793a\u662f\u6b64\u6280\u672f\u7684\u57fa\u672c\u6784\u9020\u5355\u5143\uff0c\u84dd\u8272\u8868\u793a\u5bf9\u4e8e\u6b64\u6280\u672f\u53ef\u80fd\u53ef\u884c\uff0c\u7ea2\u8272\u8868\u793a\u4f5c\u8005\u8ba4\u4e3a\u5bf9\u4e8e\u6b64\u6280\u672f\u51e0\u4e4e\u4e0d\u592a\u53ef\u884c\uff1b<\/p>\n

(b) \u6bcf\u79cd\u6280\u672f\u7684\u7ed3\u6784\u5c3a\u5bf8\u5f52\u4e00\u5316\u540e\u7684\u5236\u9020\u901f\u5ea6\u4e0e\u4e8c\u7ef4\u7279\u5f81\u5c3a\u5bf8\u5173\u7cfb\u7684\u5bf9\u6bd4\u60c5\u51b5\uff1b<\/p>\n

(c) \u5df2\u7ecf\u88ab\u6bcf\u79cd\u6280\u672f\u5e94\u7528\u7684\u5143\u7d20\u5728\u5468\u671f\u8868\u4e2d\u7684\u4f4d\u7f6e\u60c5\u51b5\uff0c\u6df1\u7eff\u8272\u8868\u793a\u5f97\u5230\u7eaf\u7684\u6c89\u79ef\u7269\uff0c\u6d45\u7eff\u8272\u8868\u793a\u5f97\u5230\u91d1\u5c5e\u548c\u6709\u673a\u7269\u590d\u5408\u7684\u6c89\u79ef\u7269\uff0c\u84dd\u8272\u8868\u793a\u4f5c\u8005\u8ba4\u4e3a\u53ef\u4ee5\u7528\u6b64\u6280\u672f\u8fdb\u884c\u5236\u9020\u7684\u5143\u7d20\uff1b<\/p>\n

(d) \u6bcf\u79cd\u6280\u672f\u5f97\u5230\u7684\u539f\u59cb\u6c89\u79ef\u7269\u548c\u9000\u706b\u6001\u7684\u5fae\u89c2\u7ec4\u7ec7\u53ca\u7535\u963b\u7387\u7684\u5bf9\u6bd4\u60c5\u51b5\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5<\/strong>\uff1aAdditive Manufacturing of Metal Structures at the Micrometer Scale<\/a>\uff08Adv. Mater. , 2017, DOI: 10.1002\/adma.201604211\uff09<\/p>\n

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