{"id":63965,"date":"2017-02-07T06:30:41","date_gmt":"2017-02-06T22:30:41","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=63965"},"modified":"2017-02-06T13:00:07","modified_gmt":"2017-02-06T05:00:07","slug":"macromolecules%ef%bc%9a%e6%b8%85%e5%8d%8e%e5%a4%a7%e5%ad%a6-%e8%81%9a%e9%9b%86%e6%80%81%e8%af%b1%e5%af%bc%e5%8f%91%e5%85%89%ef%bc%88aie%ef%bc%89%e4%b8%8e%e8%87%aa%e7%bb%84%e8%a3%85%e8%81%9a%e5%90%88","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=63965","title":{"rendered":"Macromolecules\uff1a\u6e05\u534e\u5927\u5b66-\u805a\u96c6\u6001\u8bf1\u5bfc\u53d1\u5149\uff08AIE\uff09\u4e0e\u81ea\u7ec4\u88c5\u805a\u5408\u7269\u7eb3\u7c73\u7ed3\u6784\u76f8\u5173\u6027\u7814\u7a76"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u805a\u96c6\u8bf1\u5bfc\u53d1\u5149\uff08AIE\uff09\u662f\u4e00\u7c7b\u53d1\u5149\u5206\u5b50\u7684\u72ec\u7279\u7684\u5149\u7269\u7406\u73b0\u8c61\uff0c\u8fd9\u7c7b\u5206\u5b50\u5728\u826f\u6eb6\u5242\u4e2d\u53d1\u5149\u6216\u4e0d\u53d1\u5149\uff0c\u4f46\u5728\u805a\u96c6\u72b6\u6001\u4e0b\u662f\u9ad8\u5ea6\u53d1\u5149\u7684\uff0c\u8fd9\u4f7f\u5f97AIE\u6d3b\u6027\u67d3\u6599\u6210\u4e3a\u7528\u4e8e\u89c2\u5bdf\u5904\u4e8e\u805a\u96c6\u72b6\u6001\u7684\u6750\u6599\u7684\u4f18\u826f\u63a2\u9488\u3002\u636e\u62a5\u9053\u5177\u6709AIE\u6548\u5e94\u7684\u805a\u5408\u7269\u5149\u81f4\u53d1\u5149\u6027\u8d28\u4e0e\u7ec4\u4ef6\u7684\u7eb3\u7c73\u7ed3\u6784\u6709\u5173\uff0c\u867d\u7136\u5bf9\u7814\u7a76\u4eba\u5458\u5bf9\u8be5\u65b9\u9762\u5df2\u7ecf\u505a\u4e86\u8bb8\u591a\u7814\u7a76\uff0c\u4f46\u662f\u4e00\u76f4\u7f3a\u4e4f\u7cfb\u7edf\u6027\u7684\u7814\u7a76\u3002\u805a\u5408\u8bf1\u5bfc\u81ea\u7ec4\u88c5\uff08PISA\uff09\u662f\u4e00\u79cd\u65b0\u5174\u7684\u6280\u672f\uff0c\u7528\u4ee5\u5236\u5907\u5177\u6709\u9ad8\u6d53\u5ea6\u7684\u4e0d\u540c\u7eb3\u7c73\u7ed3\u6784\u7684\u81ea\u7ec4\u88c5\u805a\u5408\u7269\u3002\u5b83\u53ef\u4ee5\u7b80\u5316\u805a\u5408\u7269\u81ea\u7ec4\u88c5\u4f53\u7684\u5c3a\u5bf8\u548c\u5f62\u6001\u63a7\u5236\u7684\u56e0\u7d20\uff0c\u5e76\u5927\u5927\u589e\u52a0\u81ea\u7ec4\u88c5\u7684\u6d53\u5ea6\uff0c\u53ef\u4f5c\u4e3a\u5236\u5907\u805a\u5408\u7269\u7ec4\u4ef6\u7684\u53ef\u9760\u624b\u6bb5\u3002\u56e0\u6b64\uff0c\u53ef\u901a\u8fc7\u5c06AIE\u6d3b\u6027\u8367\u5149\u56e2\u7ed3\u5408\u5230PISA\u7cfb\u7edf\u4e2d\u63ed\u793a\u7eb3\u7c73\u7ed3\u6784\u4e0eAIE\u6d3b\u6027\u805a\u5408\u7269\u7ec4\u4ef6\u7684\u5149\u81f4\u53d1\u5149\u884c\u4e3a\u7684\u76f8\u5173\u6027\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u9274\u4e8e\u6b64\uff0c\u6ed1\u94c1\u5362\u5927\u5b66\u7684\u738b\u6653\u677e\u526f\u6559\u6388\u3001\u6e05\u534e\u5927\u5b66\u5371\u5ca9\u6559\u6388\u548c\u8881\u91d1\u9896\u6559\u6388<\/strong>\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09\u7b49\u4eba\u901a\u8fc7\u5c06AIE\u6d3b\u6027\u8367\u5149\u56e2\u7ed3\u5408\u5230PISA\u7cfb\u7edf\u4e2d\u63ed\u793a\u4e86\u7eb3\u7c73\u7ed3\u6784\u4e0eAIE\u6d3b\u6027\u805a\u5408\u7269\u7ec4\u4ef6\u7684\u5149\u81f4\u53d1\u5149\u884c\u4e3a\u7684\u76f8\u5173\u6027\u5e76\u5bf9\u5176\u8fdb\u884c\u4e86\u7cfb\u7edf\u7684\u7814\u7a76\u3002\u7814\u7a76\u4eba\u5458\u901a\u8fc7RAFT\u805a\u5408\u5236\u5907\u4e86\u5177\u6709\u4e0d\u540c\u5c3a\u5bf8\u548c\u5f62\u6001\u7684AlE-\u6d3b\u6027\uff08PDMA-P\uff08BzMA-TPE\uff09\uff08BZMA\uff1a\u7532\u57fa\u4e19\u70ef\u9178\u82c4\u916f\u3001TPE\uff1a1-\u4e59\u70ef\u57fa-4-\uff081,2,2-\u4e09\u82ef\u57fa\u4e59\u70ef\u57fa\uff09-\u82ef\u3001PDMA\uff1a\u805a\uff08N\uff0cN-\u4e8c\u7532\u57fa\u6c28\u57fa\u4e59\u57fa\uff09(RAFT\u8bd5\u5242)\uff09\u7ec4\u4ef6\uff0c\u5e76\u4e14\u8bc1\u660e\u4e86AIE\u6548\u5e94\u4e0e\u8fd9\u4e9b\u7ec4\u4ef6\u7684\u7eb3\u7c73\u7ed3\u6784\u7684\u76f8\u5173\u6027\u3002\u7814\u7a76\u8868\u660e\uff1a\uff081\uff09\u8367\u5149\u5f3a\u5ea6\u548c\u91cf\u5b50\u4ea7\u7387\u6309\u7167\u56ca\u6ce1>\u8815\u866b\u72b6\u80f6\u675f>\u7403\u72b6\u80f6\u675f\u7684\u987a\u5e8f\u589e\u52a0\uff1b\uff082\uff09\u5bf9\u4e8e\u7403\u5f62\u80f6\u675f\uff0cAIE\u6548\u5e94\u968f\u7740\u80f6\u675f\u5c3a\u5bf8\u7684\u589e\u52a0\u800c\u589e\u5f3a\uff1b\uff083\uff09\u4e0e\u7ed3\u6784\u76f8\u5173\u7684\u5149\u5b66\u6027\u8d28\u548c\u805a\u96c6\u4f53\u4e2d\u5f62\u6210\u6838\u7684\u94fe\u7684\u5e94\u529b\u53d8\u5316\u6709\u5173\uff1b\uff084\uff09\u56ca\u6ce1\u7684\u91cf\u5b50\u4ea7\u7387\u4e0e\u56ca\u6ce1\u58c1\u7684\u539a\u5ea6\u6210\u6b63\u6bd4\uff0c\u8868\u660e\u819c\u5e94\u529b\u968f\u7740\u56ca\u6ce1PISA\u805a\u5408\u8fc7\u7a0b\u7684\u751f\u957f\u800c\u589e\u52a0\uff0c\u8fd9\u4e0e\u901a\u8fc7\u4f20\u7edf\u65b9\u6cd5\u83b7\u5f97\u7684\u56ca\u6ce1\u76f8\u53cd\u3002\u6700\u7ec8\u7814\u7a76\u8bc1\u660eAIE\u6d3b\u6027\u67d3\u6599\u53ef\u4f5c\u4e3a\u63a2\u7a76\u805a\u5408\u7269\u7ec4\u88c5\u7684\u6709\u6548\u63a2\u9488\u3002\u8be5\u6210\u679c\u4ee5\u201cPolymer Assemblies with Nanostructure Correlated Aggregation-Induced Emission<\/strong>\u201d\u4e3a\u9898\u4e8e2017\u5e741\u670825\u65e5\u53d1\u8868\u5728\u671f\u520aMacromolecules\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00 \u901a\u8fc7PISA\u5236\u5907AIE\u6d3b\u6027\u7ec4\u4ef6\u7684\u793a\u610f\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

BZMA\uff08\u7532\u57fa\u4e19\u70ef\u9178\u82c4\u916f\uff09\u3001TPE\uff081-\u4e59\u70ef\u57fa-4-\uff081,2,2-\u4e09\u82ef\u57fa\u4e59\u70ef\u57fa\uff09-\u82ef\uff09<\/p>\n

PDMA\u805a\uff08N\uff0cN-\u4e8c\u7532\u57fa\u6c28\u57fa\u4e59\u57fa\uff09(RAFT\u8bd5\u5242)<\/p>\n

\u56fe\u4e8c DLS\u4e0e TEM\u6027\u80fd\u6d4b\u8bd5<\/strong><\/p>\n

\"\"<\/p>\n

a) \u7ec4\u4ef6\u5728\u4e59\u9187\u6eb6\u6db2\u4e2d\u7684DLS\uff08\u52a8\u6001\u5149\u6563\u5c04\uff09\u6d4b\u8bd5\u3002\u4ece\u56fe\u4e2d\u53ef\u4ee5\u770b\u51fa\u5e73\u5747\u6d41\u4f53\u52a8\u529b\u5b66\u76f4\u5f84\uff08D h\uff09\u968f\u7740BzMA \/ PDMA\u7684\u6dfb\u52a0\u6bd4\u4f8b\u589e\u52a0\u800c\u589e\u52a0\u3002<\/p>\n

b) \u7ec4\u4ef6\u5728\u6c34\u6eb6\u6db2\u4e2d\u7684DLS\uff08\u52a8\u6001\u5149\u6563\u5c04\uff09\u6d4b\u8bd5\u3002\u53d1\u73b0\u5f53\u7528\u6c34\u4f5c\u4e3a\u7ec4\u4ef6\u7684\u6eb6\u5242\u65f6\uff0c\u7531\u4e8e\u6c34\u7684\u6eb6\u89e3\u80fd\u529b\u6bd4\u4e59\u9187\u66f4\u5dee\uff0c\u6c34\u4e2d\u7684\u5e73\u5747\u5c3a\u5bf8\u5c0f\u4e8e\u4e59\u9187\u4e2d\u7684\u5e73\u5747\u5c3a\u5bf8\u3002<\/p>\n

c-e) \u4e59\u9187\u4e2d\u80f6\u4f53\u7684TEM\u56fe\u50cf\u3002<\/p>\n

f-h) \u6c34\u4e2d\u80f6\u4f53\u7684TEM\u56fe\u50cf\u3002\u901a\u8fc7\u8fd9\u4e24\u7ec4\u56fe\u50cf\u8fdb\u884c\u5bf9\u6bd4\u53d1\u73b0\uff0c\u6539\u53d8\u6eb6\u5242\u7ec4\u4ef6\u7684\u5f62\u6001\u4e0d\u53d1\u751f\u53d8\u5316\uff0c\u8fd9\u4e0e\u5176\u4ed6\u6587\u732e\u62a5\u9053\u7684\u4e00\u81f4\u3002<\/p>\n

i-k) \u5229\u7528PISA\u805a\u5408\u5f97\u5230\u7684\u4e0d\u540c\u5355\u4f53\u542b\u91cf\u5bf9\u5e94\u7684\u805a\u5408\u4ea7\u7269\u7684\u4e0d\u540c\u5f62\u6001\u3002\u5176\u4e2di\u4e3aPDMA 39 -P\uff08BzMA-TPE\uff09-120\uff0c\u5f97\u5230\u5e73\u5747\u6d41\u4f53\u52a8\u529b\u5b66\u76f4\u5f84\uff08Dh\uff09\u4e3a41.3\u00b14.2nm\u7684\u7403\u5f62\u80f6\u675f\u3002j\u4e3aPDMA 39 -P\uff08BzMA-TPE\uff09-240\uff0c\u5f97\u5230\u5e73\u5747\u6d41\u4f53\u52a8\u529b\u5b66\u76f4\u5f84\uff08Dh\uff09\u4e3a51.7\u00b16.0nm\u7684\u8815\u866b\u72b6\u80f6\u675f\u3002k\u4e3aPDMA 39-P\uff08BzMA-TPE\uff09-360\uff0c\u5f97\u5230\u66f4\u5927\u548c\u66f4\u4eae\u7684\u7403\u4f53\u3002<\/p>\n

\u56fe\u4e09 \u5355\u4f53\u542b\u91cf\u4e0eAIE\u6548\u5e94\u7684\u5173\u7cfb\u53ca\u8367\u5149\u8c31\u6d4b\u8bd5\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

a) PDMA 39 -P\uff08BzMA-TPE\uff09-120\u5728THF\u548c\u6c34\u4e2d\u7684FL\u5149\u8c31\uff08\u8367\u5149\u5149\u8c31\uff09\u3002\u901a\u8fc7\u5bf9\u6bd4\u53d1\u73b0PDMA 39 -P\uff08BzMA-TPE\uff09-120\u5d4c\u6bb5\u5171\u805a\u7269\u5728THF\u6eb6\u6db2\u4e0b480nm\u5904\u4e0d\u663e\u793a\u8367\u5149\u8c31\u5cf0\uff0c\u800c\u5728\u6c34\u6027\u5206\u6563\u4f53\u4e0b480nm\u5904\u5177\u6709\u5f3a\u7684\u8367\u5149\u8c31\u5cf0\u3002<\/p>\n

b) \u5728\u6c34\u4e2d\u7684PDMA 39-P\uff08BzMA-TPE\uff09-120\uff0c-240\u548c-360\u7ec4\u4ef6\u7684FL\u5149\u8c31\u3002<\/p>\n

c) \u5728\u4e59\u9187\u4e2d\u7684PDMA 39-P\uff08BzMA-TPE\uff09-120\uff0c-240\u548c-360\u7ec4\u4ef6\u7684FL\u5149\u8c31\u3002\u901a\u8fc7b\u548cc\u5bf9\u6bd4\u53d1\u73b0\u7ec4\u4ef6\u5728\u6c34\u548c\u4e59\u9187\u4e2d\u7684\u8367\u5149\u5f3a\u5ea6\u968f\u7ec4\u4ef6\u5f62\u6001\u800c\u53d8\u5316\u3002\u4e14\u5728480nm\u5904\u7684\u8c31\u5cf0\u5f3a\u5ea6\u6709\u5982\u4e0b\u5173\u7cfbPDMA 39 -P\uff08BzMA-TPE\uff09-120\uff08\u80f6\u675f\uff09<PDMA 39 -P\uff08BzMA-TPE\uff09-240\uff08\u8815\u866b\u72b6\u80f6\u675f\uff09<PDMA 39 -P -TPE\uff09-360\uff08\u56ca\u6ce1\uff09\u3002\u800c\u5bf9\u4e8e\u76f8\u540c\u7684\u805a\u5408\u7269\uff0c\u5728\u6c34\u4e2d\u6bd4\u5728\u4e59\u9187\u4e2d\u5177\u6709\u66f4\u5f3a\u7684\u8367\u5149\u5f3a\u5ea6\u3002<\/p>\n

d) PDMA 39 -P\uff08BzMA-TPE\uff09-x\u7ec4\u4ef6\uff08x = 120,240\u548c360\uff09\u5728\u4e59\u9187\u548c\u6c34\u4e2d\u7684\u91cf\u5b50\u4ea7\u7387\u3002\u53ef\u4ee5\u770b\u51fa\u5728\u6c34\u4e2d\u7684\u91cf\u5b50\u4ea7\u7387\u660e\u663e\u5927\u4e8e\u4e59\u9187\u4e2d\u7684\u91cf\u5b50\u4ea7\u7387\u3002<\/p>\n

\u56fe\u56db \u4e3a\u5177\u6709\u4e0d\u540c\u5c3a\u5bf8\u7684PDMA 67 -P\uff08BzMA-TPE\uff09\u80f6\u675f\u7684\u8367\u5149\u5149\u8c31<\/strong><\/p>\n

\"\"<\/p>\n

a) \u4e3a\u5177\u6709\u4e0d\u540c\u5c3a\u5bf8\u7684PDMA 67 -P\uff08BzMA-TPE\uff09\u80f6\u675f\u7684\u6c34\u6027\u5206\u6563\u4f53\u7684\u8367\u5149\u5149\u8c31\u3002<\/p>\n

b) \u5c06480nm\u5904\u7684\u8367\u5149\u5f3a\u5ea6\u5bf9\u80f6\u675f\u7684\u5927\u5c0f\u4f5c\u56fe\u3002\u53d1\u73b0\u8367\u5149\u5f3a\u5ea6\u968f\u7740\u80f6\u675f\u7684\u76f4\u5f84\u4ece36.4nm\u589e\u52a0\u523086.6nm\u800c\u589e\u52a0\uff0c\u800c\u968f\u7740\u76f4\u5f84\u4ece86.6nm\u589e\u52a0\u5230150.3nm\uff0c\u5f3a\u5ea6\u7565\u5fae\u51cf\u5c0f\u3002<\/p>\n

c) \u4e3a\u91cf\u5b50\u4ea7\u7387\u4e0e\u5e73\u5747\u6d41\u4f53\u52a8\u529b\u5b66\u534a\u5f84\uff08Dh\uff09\u7684\u5173\u7cfb\uff0c\u53d1\u73b0QY\uff08\u91cf\u5b50\u4ea7\u7387\uff09\u968f\u4e9b\u7ec4\u4ef6\u7684D h\u503c\u589e\u52a0\u800c\u589e\u52a0\u3002<\/p>\n

\u56fe\u4e94 \u4e3a\u56ca\u6ce1\u7684\u58c1\u539a\u4e0eAIE\u7684\u5173\u7cfb<\/strong><\/p>\n

\"\"<\/p>\n

a) \u5728\u6c34\u4e2d\u7684PDMA 67 -P\uff08BzMA-TPE\uff09-x\u80f6\u675f\u7684FL\u5149\u8c31\u3002<\/p>\n

b) \u6c34\u4e2dPDMA 39 -P\uff08BzMA-TPE\uff09-x\u56ca\u6ce1\u7684FL\u6700\u5927\u503c\u4e0e\u56ca\u6ce1\u58c1\u539a\u7684\u5173\u7cfb\u3002<\/p>\n

c) \u6c34\u4e2dPDMA 39 -P\uff08BzMA-TPE\uff09-x\u56ca\u6ce1\u7684QY\u4e0e\u56ca\u6ce1\u58c1\u539a\u7684\u5173\u7cfb\u3002\u53d1\u73b0QY\uff08\u91cf\u5b50\u4ea7\u7387\uff09\u968f\u56ca\u6ce1\u58c1\u539a\u7684\u589e\u52a0\u800c\u589e\u5927\uff0cAIE\u6548\u5e94\u4e5f\u968f\u7740\u56ca\u6ce1\u58c1\u539a\u5ea6\u7684\u589e\u52a0\u800c\u589e\u5f3a\uff0c\u8868\u660e\u5728PISA\u805a\u5408\u8fc7\u7a0b\u4e2d\u56ca\u6ce1\u5185\u819c\u5e94\u529b\u589e\u5f3a\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Polymer Assemblies with Nanostructure-Correlated Aggregation-Induced Emission<\/a>\uff08Macromolecules, 2017, DOI: 10.1021\/acs.macromol.6b02499\uff09<\/p>\n

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