{"id":67330,"date":"2017-06-13T06:30:00","date_gmt":"2017-06-12T22:30:00","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=67330"},"modified":"2017-06-09T20:50:51","modified_gmt":"2017-06-09T12:50:51","slug":"nat-commun-%ef%bc%9a%e5%9b%9b%e9%85%b0%e8%83%ba%e5%ae%98%e8%83%bd%e5%8c%96%e7%9a%84mofs%e5%86%85%e5%bc%82%e5%b8%b8%e4%b9%99%e7%82%94%e5%92%8c%e4%ba%8c%e6%b0%a7%e5%8c%96%e7%a2%b3%e5%90%b8%e9%99%84","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=67330","title":{"rendered":"Nat. Commun. \uff1a\u56db\u9170\u80fa\u5b98\u80fd\u5316\u7684MOFs\u5185\u5f02\u5e38\u4e59\u7094\u548c\u4e8c\u6c27\u5316\u78b3\u5438\u9644\u6027\u80fd"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u80fd\u6e90\u662f\u4eba\u7c7b\u6d3b\u52a8\u7684\u7269\u8d28\u57fa\u7840\u3002\u5f53\u4eca\u4e16\u754c\uff0c\u80fd\u6e90\u5df2\u6210\u4e3a\u5f71\u54cd\u4e2d\u56fd\u793e\u4f1a\u7ecf\u6d4e\u53d1\u5c55\u7684\u91cd\u5927\u95ee\u9898\u3002\u5728\u4f17\u591a\u7684\u80fd\u6e90\u6750\u6599\u4e2d\uff0c\u6c22\u6c14\u3001\u7532\u70f7\u7b49\u53ef\u71c3\u6c14\u4f53\u56e0\u5177\u6709\u4f4e\u6c61\u67d3\u3001\u9ad8\u80fd\u6548\u800c\u6210\u4e3a\u7fd8\u695a\uff0c\u4f46\u6b64\u7c7b\u6c14\u4f53\u5728\u50a8\u5b58\u53ca\u5408\u7406\u4f7f\u7528\u65b9\u9762\u4ecd\u65e7\u9762\u4e34\u7740\u5de8\u5927\u7684\u56f0\u96be\u548c\u6311\u6218\u3002MOFs\u56e0\u62e5\u6709\u8f83\u5927\u7684\u6bd4\u8868\u9762\u79ef\u4ee5\u53ca\u53ef\u8c03\u63a7\u7684\u5b54\u9053\uff0c\u5728\u6c14\u4f53\u50a8\u5b58\u9886\u57df\u5145\u6ee1\u4e86\u5e7f\u9614\u7684\u524d\u666f\u3002\u867d\u53d6\u5f97\u4e86\u4e00\u5b9a\u7684\u7814\u7a76\u8fdb\u5c55\uff0c\u4f46\u662f\u8fdb\u4e00\u6b65\u7406\u89e3\u6c14\u4f53\u5438\u9644\u5242\u7684\u53cd\u5e94\u673a\u7406\u662f\u6539\u8fdb\u6c14\u4f53\u50a8\u5b58\u6750\u6599\u7684\u91cd\u8981\u524d\u63d0\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\u66fc\u5f7b\u65af\u7279\u5927\u5b66\u5316\u5b66\u5b66\u9662Sihai Yang\uff08\u901a\u8baf\u4f5c\u8005\uff09\u548cMartin Schr\u00f6der\uff08\u901a\u8baf\u4f5c\u8005\uff09\u7b49\u4eba<\/strong>\u5728Nat. Commun.<\/strong> \u4e0a\u53d1\u8868\u4e86\u4e00\u7bc7\u9898\u4e3a\u201cUnravelling exceptional acetylene and carbon dioxide adsorption within a tetra-amide functionalized metal-organic framework\u201d\u6587\u7ae0<\/strong>\u3002\u6587\u4e2d\u63d0\u51fa\u4e86\u5728\u7ed3\u6676\u5206\u8fa8\u7387\u4e0b\uff0c\u56db\u9170\u80fa\u529f\u80fd\u5316\u91d1\u5c5e\u6709\u673a\u6846\u67b6MFM-188a\u4e2d\u4e8c\u6c27\u5316\u78b3\u548c\u4e59\u7094\u7684\u7ed3\u5408\u3002\u867d\u7136\u8868\u73b0\u51fa\u4e86\u4e2d\u7b49\u5b54\u9699\u7387\uff0c\u4f46\u662f\u8131\u6eb6\u5242\u5316\u7684MFM-188a\u663e\u793a\u51fa\u5f02\u5e38\u9ad8\u7684\u4e8c\u6c27\u5316\u78b3\u548c\u4e59\u7094\u7684\u5438\u6536\u7387\uff0c\u5176\u4e2d\u4e59\u7094\u7684\u5438\u6536\u7387\uff08232cm3<\/sup>g-1<\/sup>\u5728295K\u548c1bar\u6761\u4ef6\u4e0b\uff09\u662f\u76ee\u524d\u6240\u77e5\u7684\u591a\u5b54\u6750\u6599\u5438\u6536\u4e59\u7094\u91cf\u7684\u6700\u5927\u503c\u3002\u4e2d\u5b50\u884d\u5c04\u548c\u975e\u5f39\u6027\u4e2d\u5b50\u6563\u5c04\u7814\u7a76\u80fd\u591f\u76f4\u63a5\u89c2\u5bdf\u9170\u80fa\u57fa\u56e2\u5728\u5e95\u7269\u7ed3\u5408\u4e2d\u7684\u4f5c\u7528\uff0c\u7528\u8be5\u65b9\u6cd5\u63a2\u6d4b\u6c14\u4f53 – \u9170\u80fa\u57fa\u7ed3\u5408\u76f8\u4e92\u4f5c\u7528\u7684\u5b9e\u4f8b\u4e5f\u8bc1\u660e\u4e86\u8fd9\u4e00\u70b9\u3002\u8fd9\u9879\u7814\u7a76\u63ed\u793a\uff0c\u9170\u80fa\u57fa\u3001\u5f00\u653e\u7684\u91d1\u5c5e\u4f4d\u70b9\u3001\u9002\u5f53\u7684\u591a\u5b54\u5f62\u72b6\u548c\u5ba2\u4f53\u5206\u5b50\u4e4b\u95f4\u7684\u76f8\u4e92\u5f71\u54cd\u5bfc\u81f4\u4e86MFM-188a\u4e2d\u4e59\u7094\u548c\u4e8c\u6c27\u5316\u78b3\u7684\u9ad8\u6444\u53d6\u91cf\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe<\/strong>1. <\/strong>\u56db\u9170\u80fa\u516b\u7fa7\u9178\u916f\u8fde\u63a5\u4f53\u3002<\/strong><\/p>\n

\"\"<\/p>\n

\u7528\u4e8e\u5408\u6210MFM-188\u7684\u56db\u9170\u80fa\u516b\u7fa7\u9178\u916f\u8fde\u63a5\u4f53\u7684\u5316\u5b66\u7ed3\u6784\u3002\u6587\u7ae0\u901a\u8fc7\u7c89\u672bX\u5c04\u7ebf\u884d\u5c04\u548c\u5143\u7d20\u5206\u6790\u68c0\u6d4b\u4e86MFM-188\u7684\u7eaf\u5ea6\u3002<\/p>\n

\u56fe<\/strong>2.<\/strong> MFM-188<\/strong>\u6676\u4f53\u7ed3\u6784\u56fe\u3002<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u4e09\u79cd\u7b3c\u72b6\u7ed3\u6784\u7684\u7acb\u4f53\u7ed3\u6784\uff1aA\uff08\u516b\u9762\u4f53\uff09\uff0cB\u548cC\uff08\u7acb\u65b9\u516b\u9762\u4f53\uff09\u3002<\/p>\n

\uff08b\uff09\u8fd9\u4e9b\u7b3c\u72b6\u7ed3\u6784\u57283D\u7a7a\u95f4\u4e2d\u7684\u7ec4\u88c5\u5f62\u6210MFM-188\u6846\u67b6\u3002\u84dd\u8272\u3001\u9ec4\u8272\u3001\u7eff\u8272\u5206\u522b\u5bf9\u5e94\u7b3cA\u3001B\u3001C\u3002<\/p>\n

\u56fe<\/strong>3. MFM-188a<\/strong>\u7684\u6c14\u4f53\u5438\u9644\u7b49\u6e29\u7ebf\u3002<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09MFM-188a\u5728273-298K\u548c1.0bar\u4e0b\u7684CO2<\/sub>\u548cC2<\/sub> H2<\/sub>\u5438\u9644\u7b49\u6e29\u7ebf\u6bd4\u8f83\u3002<\/p>\n

\uff08b\uff09MFM-188a\u4e2dCO2<\/sub>\u548cC2<\/sub>H2<\/sub>\u5438\u9644\u7684\u5438\u9644\u7b49\u6e29\u70ed\u7684\u53d8\u5316\u3002<\/p>\n

\uff08c\uff09\u4f5c\u4e3a\u6240\u9009\u62e9\u7684MOF\u7684\u5f00\u653e\u91d1\u5c5e\u4f4d\u70b9\u548c\u5b98\u80fd\u56e2\u7684BET\u8868\u9762\u79ef\u548c\u603b\u91cd\u91cf\u6d53\u5ea6\u7684\u51fd\u6570\u7684295K \u00a0C2<\/sub>H2<\/sub>\u5438\u6536\u76843D\u56fe\u3002 \u4e3a\u4e86\u6e05\u695a\u8d77\u89c1\uff0c\u5728\u56fe\u4e2d\u4ec5\u793a\u51fa\u6700\u4f73\u884c\u4e3a\u548c\u4ee3\u8868\u6027\u7684MOF\uff08*\u6570\u636e\u5728298K\u4e0b\u83b7\u5f97\uff09\u3002<\/p>\n

\u56fe<\/strong>4. MFM-188a<\/strong>\u4e2d\u4e09\u79cd\u7c7b\u578b\u7b3c\u72b6\u7ed3\u6784\u4e2d\u5438\u9644\u7684\u6c14\u4f53\u5206\u5b50\u7684\u5206\u5e03\u3002<\/strong><\/p>\n

\"\"<\/p>\n

\u4e0a\u4e0b\u4e24\u56fe\u5206\u522b\u8868\u793a\u57281.75 CO2<\/sub>\/Cu \u548c3.2 C2<\/sub>D2<\/sub>\/Cu\u8d1f\u8f7d\u4e0bMFM-188a\u7684\u7b3cA\u3001B\u3001C\u4e2d\u7684 C2<\/sub>D2<\/sub> \uff08\u9876\u90e8\uff09\u548cCO2<\/sub> \uff08\u5e95\u90e8\uff09\u4f4d\u7f6e\u3002\u786e\u5b9a\u5404\u4f4d\u7f6e\u7684\u5f69\u8272\u7403\u534a\u5f84\u4e0e\u76f8\u5e94\u7684\u6676\u4f53\u5360\u636e\u7387\u6210\u6bd4\u4f8b\u3002<\/p>\n

\u56fe<\/strong>5 CO2<\/sub><\/strong>\u548c<\/strong>C2<\/sub>H2<\/sub><\/strong>\u5728<\/strong>MFM-188a<\/strong>\u4e2d\u7ed3\u5408\u7684\u6676\u4f53\u5b66\u5206\u8fa8\u7387\u3002<\/strong><\/p>\n

\"\"<\/p>\n

\u9aa8\u67b6\u539f\u5b50\uff1aC\uff0c\u9ed1\u8272\uff1bO\uff0c\u7ea2\u8272\uff1bH\uff0c\u767d\u8272\uff1bN\uff0c\u84dd\u8272\uff1bCu\uff0c\u84dd\u8272\u3002\u5176\u4ed6\u7684\u9aa8\u67b6\u6c14\u4f53\u5206\u5b50\u6839\u636e\u5b83\u4eec\u5360\u636e\u7684\u7ed3\u5408\u4f4d\u70b9\u8fdb\u884c\u7a0d\u5fae\u653e\u5927\u548c\u7740\u8272\u3002\u8ddd\u79bb\u7528\u00c5\u8868\u793a\u3002\u5728\u4f4d\u7f6e1\uff08a\uff09\uff0c2\uff08b\uff09\u548c4\uff08c\uff09\u5904\u5438\u9644\u7684CO2<\/sub>\u5206\u5b50\u7684\u7ed3\u5408\u56fe\u3002\uff08d\uff09\u4e3a\u5728\u6846\u67b6C\u5185\u5438\u9644\u7684CO2<\/sub>\u5206\u5b50\u7684\u5806\u780c\u56fe\u3002\u5728\u4f4d\u70b91\uff0c2\uff0c4\uff08e\uff09\u548c\u4f4d\u70b93\uff08f\uff09\u5904\u5438\u9644\u7684C2<\/sub>H2<\/sub>\u5206\u5b50\u7684\u534f\u540c\u7ed3\u5408\u56fe\u3002<\/p>\n

\u56fe<\/strong>6 MFM-188a<\/strong>\u7684<\/strong>INS<\/strong>\u5149\u8c31\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

\u65e0\u5438\u9644MFM-188a\u4e0e\u5438\u9644\uff08a\uff09CO2<\/sub>\u548c\uff08b\uff09C2<\/sub>H2<\/sub>\u7684MFM-188a\u7684INS\u5149\u8c31\u7684\u6bd4\u8f83\u3002<\/p>\n

\uff08c\uff09MFM-188a\u7684\u5b9e\u9a8c\u548cDFT\u8ba1\u7b97\u7684INS\u5149\u8c31\u7684\u6bd4\u8f83\u3002 \u88f8MFM-188a\u4e0e\u8d1f\u8f7d\uff08d\uff09CO2<\/sub>\u548c\uff08e\uff09C2<\/sub>H2<\/sub>\u7684MFM-188a\u7684INS\u5149\u8c31\u7684\u5dee\u5f02\u56fe\u4e0e\u56fa\u6001\u7684\u6d53\u7f29\uff08e\uff09C2<\/sub>H2<\/sub>\u7684\u5b9e\u9a8cINS\u5149\u8c31\u7684\u5dee\u5f02\u56fe\u7684\u6bd4\u8f83\u3002\uff08f\uff09\u663e\u793aC2H2\u5185\u90e8\u632f\u52a8\u6a21\u5f0f\u7684INS\u5149\u8c31\u7684\u653e\u5927\u7ec6\u8282\u3002<\/p>\n

\u3010\u7ed3\u8bba\u3011<\/strong><\/p>\n

MFM-188a \u8868\u73b0\u51fa\u4e86\u4f18\u5f02\u7684C2<\/sub>H2<\/sub>\uff0827.0wt\uff05\uff09\u548cCO2<\/sub>\uff0823.7wt\uff05\uff09\u5438\u9644\u6027\u80fd\u3002\u56fe3c\u76843D\u56fe\u603b\u7ed3\u4e86\u8bb8\u591a\u8fc4\u4eca\u4e3a\u6b62\u6240\u62a5\u9053\u7684\u6700\u597d\u7684MOFs\u7684BET\u8868\u9762\u79ef\u3001\u7ed3\u6784\u4e2d\u201cOMSs\u5b98\u80fd\u56e2\u201d\u7684\u5bc6\u5ea6\u548cC2<\/sub>H2<\/sub>\u7684\u5438\u6536\u4e4b\u95f4\u7684\u5173\u7cfb\u3002\u663e\u7136\uff0c\u4e3a\u4e86\u5b9e\u73b0\u9ad8C2<\/sub>H2<\/sub>\u5438\u5bb9\u7387\uff0c\u9700\u8981\u5728\u5b54\u7ed3\u6784\u4e2d\u7ed3\u5408\u9ad8BET\u8868\u9762\u79ef\uff08\u548c\u66f4\u5bbd\u8303\u56f4\u7684\u5b54\u9699\u7387\uff09\u4ee5\u53ca\u9ad8\u5bc6\u5ea6\u7684\u7ed3\u5408\u4f4d\u70b9\u3002\u7136\u800c\uff0c\u8fd9\u901a\u5e38\u662f\u5b58\u5728\u56fa\u6709\u77db\u76fe\u7684\uff0c\u56e0\u4e3a\u9ad8\u8868\u9762\u79ef\/\u5b54\u9699\u7387\u5c06\u81ea\u7136\u7a00\u91ca\u5b54\u4e2d\u7684\u7ed3\u5408\u4f4d\u70b9\uff0c\u5bfc\u81f4\u8fd9\u4e24\u4e2a\u56e0\u7d20\u4e4b\u95f4\u6709\u4e0d\u53ef\u907f\u514d\u7684\u6743\u8861\u3002\u7531\u4e8eMFM-188a\u7684\u9aa8\u67b6\u62d3\u6251\u548c\u5b54\u51e0\u4f55\u5f62\u72b6\uff0c\u5176\u663e\u793a\u51fa\u9002\u5f53\u9ad8\u7684BET\u8868\u9762\u79ef\u548c\u9ad8\u5bc6\u5ea6\u7684\u7ed3\u5408\u4f4d\u70b9\uff0c\u56e0\u6b64\u663e\u793a\u51fa\u8f83\u597d\u7684C2<\/sub>H2<\/sub>\u5438\u6536\u6027\u80fd\u3002<\/p>\n

\u5c3d\u7ba1\u5b66\u754c\u5e7f\u6cdb\u8ba4\u4e3a\u5b54\u4e2d\u7684\u9170\u80fa\u57fa\u56e2\u5c06\u901a\u8fc7\u6c22\u952e\u79ef\u6781\u53c2\u4e0e\u6c14\u4f53\u5438\u9644\uff0c\u4f46\u8fc4\u4eca\u5c1a\u672a\u62a5\u9053\u6709\u5b9e\u9a8c\u8bc1\u636e\u3002\u672c\u7814\u7a76\u901a\u8fc7\u4e2d\u5b50\u884d\u5c04\u548c\u5149\u8c31\u6280\u672f\u7684\u7ec4\u5408\u5bf9\u56db\u9170\u80fa\u5b98\u80fd\u5316MOF\u4e2d\u7684\u6c14\u4f53-\u5438\u9644\u5242\u7ed3\u5408\u76f8\u4e92\u4f5c\u7528\u7684\u7efc\u5408\u7814\u7a76\u63d0\u4f9b\u4e86\u4e00\u4e2a\u72ec\u7279\u7684\u5b9e\u4f8b\u3002\u8fd9\u4e9b\u5b9e\u9a8c\u4ece\u6676\u4f53\u5b66\u548c\u52a8\u6001\u7684\u89d2\u5ea6\u63d0\u4f9b\u5173\u4e8e\u8fd9\u4e2a\u4e3b\u5ba2\u4f53\u7cfb\u7edf\u7684\u5206\u5b50\u7ec6\u8282\u7684\u5173\u952e\u89c1\u89e3\u3002\u672c\u6587\u5728OMS\u548cMFM-188a\u5b54\u4e2d\u6e38\u79bb\u9170\u80fa\u57fa\u56e2\u4e2d\u53d1\u73b0\u4e86CO2<\/sub>\u548cC2<\/sub>H2<\/sub>\u7684\u9ad8\u5ea6\u534f\u4f5c\u7684\u7ed3\u5408\u673a\u5236\uff0c\u5176\u4e2d\u4e00\u4e2a\u4f4d\u70b9\u589e\u5f3a\u53e6\u4e00\u4e2a\u4f4d\u70b9\u7684\u7ed3\u5408\u3002 \u8fd9\u9879\u5de5\u4f5c\u4e0d\u4ec5\u4e3a\u9ad8\u5bb9\u91cfCO2<\/sub>\u548cC2<\/sub>H2<\/sub>\u50a8\u5b58\u63d0\u4f9b\u4e86\u65b0\u7684\u591a\u5b54\u6750\u6599\uff0c\u800c\u4e14\u66f4\u91cd\u8981\u7684\u662f\uff0c\u6709\u52a9\u4e8e\u65b0\u578b\u591a\u5b54\u6750\u6599\u7684\u8bbe\u8ba1\u548c\u7ed3\u6784\u4f18\u5316\uff0c\u5176\u5177\u6709\u6539\u8fdb\u7684\u6c14\u4f53\u5438\u9644\u6027\u80fd\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Unravelling exceptional acetylene and carbon dioxide adsorption within a tetra-amide functionalized metal-organic framework<\/a>\u00a0\u00a0\uff08Nat. Commun.\uff0c2017\uff0cDOI: 10.1038\/ncomms14085\uff09<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8MOF\u7ec4Joanna\u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u7f16\u8f91\u6574\u7406\u3002\u6b22\u8fce\u52a0\u5165\u6750\u6599\u4ebaMOF\u5b66\u672f\u4ea4\u6d41\u7fa4\uff08120199039\uff09\uff01<\/p>\n

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