{"id":67771,"date":"2017-02-28T06:30:16","date_gmt":"2017-02-27T22:30:16","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=67771"},"modified":"2017-02-28T19:30:35","modified_gmt":"2017-02-28T11:30:35","slug":"adv-energy-mater-%ef%bc%9a%e6%99%b6%e7%95%8c%e5%b7%a5%e7%a8%8b%e6%8f%90%e9%ab%98n%e5%9e%8b%e6%96%b9%e9%92%b4%e7%9f%bf%e7%83%ad%e7%94%b5%e6%80%a7%e8%83%bd","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=67771","title":{"rendered":"Adv. Energy Mater.\uff1a\u6676\u754c\u5de5\u7a0b\u63d0\u9ad8n\u578b\u65b9\u94b4\u77ff\u70ed\u7535\u6027\u80fd"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

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\u5f88\u591a\u4f53\u7cfb\uff08\u5982PbTe\u63ba\u6742Ag\u7eb3\u7c73\u70b9\u3001Yb0.26<\/sub>Co4<\/sub>Sb12<\/sub>\/GaSb\u7eb3\u7c73\u590d\u5408\u7269\u3001\u7eb3\u7c73\u5b6a\u6676Cu-Ni\u5408\u91d1\uff09\u90fd\u9a8c\u8bc1\u4e86\u6676\/\u76f8\u754c\u5bf9\u8f7d\u6d41\u5b50\u548c\u58f0\u5b50\u7684\u4f20\u8f93\u7279\u6027\u6709\u91cd\u8981\u5f71\u54cd\uff0c\u56e0\u6b64\u901a\u8fc7\u63a7\u5236\u6676\u754c\u5229\u7528\u5176\u5c4f\u853d\u4f4e\u80fd\u91cf\u7535\u5b50\u8f7d\u6d41\u5b50\u7684\u80fd\u91cf\u8fc7\u6ee4\u6548\u5e94\uff0c\u6709\u671b\u80fd\u591f\u589e\u5927Seebeck\u7cfb\u6570\u3002\u800c\u4e00\u4e9b\u4f53\u7cfb\u4e5f\u8868\u660e\u5927\u89d2\u5ea6\u6676\u754c\u548c\u975e\u5171\u683c\u6676\u754c\u867d\u7136\u80fd\u591f\u589e\u5927Seebeck\u7cfb\u6570\u4f46\u540c\u65f6\u4e5f\u4f1a\u51cf\u5c0f\u8f7d\u6d41\u5b50\u8fc1\u79fb\u7387\uff0c\u6700\u540e\u5bfc\u81f4ZT\u503c\u63d0\u9ad8\u4e0d\u660e\u663e\u3002\u56e0\u6b64\uff0c\u5982\u4f55\u901a\u8fc7\u6676\u754c\u5de5\u7a0b\u660e\u663e\u63d0\u9ad8Seebeck\u7cfb\u6570\u540c\u65f6\u51cf\u5c0f\u6676\u683c\u70ed\u5bfc\u7387\u3001\u7565\u5fae\u51cf\u5c0f\u8f7d\u6d41\u5b50\u8fc1\u79fb\u7387\uff0c\u6700\u7ec8\u663e\u8457\u63d0\u9ad8ZT\u503c\u662f\u4e00\u4e2a\u96be\u9898\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb<\/b><\/strong>\u3011<\/p>\n

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\u3010\u56fe\u6587\u5bfc\u8bfb<\/b><\/strong>\u3011<\/p>\n

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\"\"<\/strong><\/p>\n

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c\uff09\u56feb\uff0920\u00b0~40\u00b0XRD\u56fe\u8c31\u7684\u653e\u5927\u56fe<\/p>\n

\u56fe2. \u6837\u54c1TEM\u56fe\u50cf<\/b><\/strong><\/p>\n

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\n a\uff09\u6837\u54c1\u5feb\u6dec\u5e26\u4f4e\u500dTEM\u56fe\u50cf<\/p>\n

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c\uff09Co\u3001Sb\u3001Yb\u5143\u7d20STEM-EDS\u9762\u5206\u5e03\u56fe<\/p>\n

d\uff09\u56feb\u4e2dA\u533a\u57df\u653e\u5927\u56fe\u50cf\uff0c\u5185\u63d2\u56fe\u4e3a\u9ec4\u8272\u5706\u5708\u6807\u6ce8\u7684\u4e24\u4e2a\u6676\u7c92\u7684FFT\u56fe\u50cf<\/p>\n

e\uff09\u56fed\u4e2d\u9ec4\u8272\u65b9\u6846\u533a\u57df\u9ad8\u500dTEM\u56fe\u50cf<\/p>\n

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h\uff09\u56feg\u4e2d\u9ec4\u8272\u65b9\u6846\u533a\u57df\u9ad8\u500dTEM\u56fe\u50cf\uff0c\u5185\u63d2\u56fe\u4e3a\u865a\u7ebf\u533a\u57df\u7684IFFT\u56fe\uff0c\u7ea2\u8272\u6807\u8bb0\u4e3a\u97e7\u578b\u4f4d\u9519<\/p>\n

\u56fe3. <\/b><\/strong>Yb<\/b><\/strong>0.3<\/b><\/sub><\/strong>Co<\/b><\/strong>4<\/b><\/sub><\/strong>Sb<\/b><\/strong>12+x%<\/b><\/sub><\/strong>\u00a0(x = 0, 10, 20, 30)<\/b><\/strong>\u4f20\u8f93\u7279\u6027\u66f2\u7ebf\u56fe<\/b><\/strong><\/p>\n

\"\"<\/b><\/strong><\/p>\n

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b\uff09Seebeck\u7cfb\u6570\u4e0e\u6e29\u5ea6\u66f2\u7ebf\u56fe<\/p>\n

c\uff09\u529f\u7387\u56e0\u5b50\u4e0e\u6e29\u5ea6\u66f2\u7ebf\u56fe<\/p>\n

d\uff09\u529f\u7387\u56e0\u5b50\u4e0e\u73b0\u4eca\u524d\u6cbf\u7684\u5176\u4ed6\u586b\u5145\u578b\u65b9\u94b4\u77ff\u6750\u6599\u7684\u6bd4\u8f83<\/p>\n

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\u56fe4. \u8f7d\u6d41\u5b50\u6d53\u5ea6\u5f71\u54cd\u56e0\u7d20<\/b><\/strong><\/p>\n

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b\uff09\u8f7d\u6d41\u5b50\u6d53\u5ea6\u4e0eSeebeck\u7cfb\u6570\u5173\u7cfb\u66f2\u7ebf\u56fe<\/p>\n

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\u56fe5. \u70ed\u4f20\u8f93\u7279\u6027\u66f2\u7ebf\u56fe<\/b><\/strong><\/p>\n

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b\uff09Yb0.3<\/sub>Co4<\/sub>Sb12+x%<\/sub>\u00a0(x = 0, 10, 20, 30)\u6676\u683c\u70ed\u5bfc\u7387\u4e0e\u6e29\u5ea6\u5173\u7cfb\u66f2\u7ebf\u56fe\u53ca\u5176\u4e0eLi\u7b49\u4eba\u5236\u5907\u7684Yb0.3<\/sub>Co4<\/sub>Sb12.05<\/sub>\u7684\u6bd4\u8f83<\/p>\n

c\uff09\u6676\u683c\u70ed\u5bfc\u7387\u4e0eYb\u586b\u5145\u5206\u6570\u5173\u7cfb\u66f2\u7ebf\u56fe<\/p>\n

\u56fe6.<\/b><\/strong>\u00a0Yb<\/b><\/strong>0.3<\/b><\/sub><\/strong>Co<\/b><\/strong>4<\/b><\/sub><\/strong>Sb<\/b><\/strong>12+x%<\/b><\/sub><\/strong>\u00a0(x = 0, 20<\/b><\/strong>)\u5feb\u6dec\u5e26\u7684\u6676\u683c\u70ed\u5bfc\u7387\u4e0e\u6e29\u5ea6\u5173\u7cfb\u66f2\u7ebf\u56fe<\/b><\/strong><\/p>\n

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b\uff09\u7ea2\u8272\u865a\u7ebf\u662f20%Sb\u5feb\u6dec\u5e26\u5728\u5e94\u53d8\u573a\u4e0b\u7684\u8ba1\u7b97\u503c<\/p>\n

c\uff09\u6a59\u8272\u7bad\u5934\u8868\u793a\u901a\u8fc7\u6676\u754c\u5904\u5bc6\u96c6\u4f4d\u9519\u9635\u5217\uff0c20%Sb\u5feb\u6dec\u5e26\u6676\u683c\u70ed\u5bfc\u7387\u964d\u4f4e\u7684\u7a0b\u5ea6<\/p>\n

\u56fe7. \u5c0f\u89d2\u5ea6\u6676\u754c\u5bc6\u96c6\u4f4d\u9519\u9635\u5217\u5bf9\u8f7d\u6d41\u5b50\u548c\u58f0\u5b50\u4f20\u8f93\u7684\u5f71\u54cd\u673a\u5236\u793a\u610f\u56fe<\/b><\/strong><\/p>\n

\"\"<\/b><\/strong><\/p>\n

a\uff09\u9ad8\u80fd\u91cf\u7684\u8f7d\u6d41\u5b50\u80fd\u591f\u901a\u8fc7\u5c0f\u89d2\u5ea6\u6676\u754c\u800c\u80fd\u91cf\u4f4e\u7684\u8f7d\u6d41\u5b50\u53ef\u4ee5\u88ab\u6709\u6548\u5c4f\u853d<\/p>\n

b\uff09\u58f0\u5b50\u5728\u5c0f\u89d2\u5ea6\u6676\u754c\u5904\u7531\u4e8e\u5bc6\u96c6\u7684\u4f4d\u9519\u9635\u5217\u6563\u5c04\u589e\u5f3a<\/p>\n

\u56fe8. \u586b\u5145\u578b\u65b9\u94b4\u77ff\u6750\u6599ZT\u503c<\/b><\/strong><\/p>\n

\"\"
\n <\/b><\/strong>
\n a\uff09Yb0.3<\/sub>Co4<\/sub>Sb12+x%<\/sub>\u00a0(x = 0, 10, 20, 30)ZT\u503c\u4e0eLi\u7b49\u4eba\u5236\u5907\u7684Yb0.3<\/sub>Co4<\/sub>Sb12.05<\/sub>\u7684ZT\u503c\u5bf9\u6bd4\u56fe<\/p>\n

b\uff09\u76ee\u524d\u6700\u524d\u6cbf\u7684\u4e00\u4e9b\u65b9\u94b4\u77ff\u7814\u7a76\u6210\u679cZT\u503c\u5bf9\u6bd4<\/p>\n

c\uff09\u56feb\uff09\u4e2d\u63d0\u5230\u7684\u6750\u6599\u7684\u5e73\u5747ZT\u503c<\/p>\n

\u3010\u5c0f\u7ed3<\/b><\/strong>\u3011<\/p>\n

\u8be5\u7814\u7a76\u5229\u7528\u6db2\u76f8\u51dd\u7ed3\u7684\u65b9\u6cd5\u6210\u529f\u5236\u5f97\u5177\u6709\u5e26\u5bc6\u96c6\u4f4d\u9519\u9635\u5217\u7684\u5c0f\u89d2\u5ea6\u6676\u754c\u7684Yb\u586b\u5145CoSb3<\/sub>\u6750\u6599\uff0c\u8fd9\u79cd\u6676\u754c\u5177\u6709\u80fd\u91cf\u8fc7\u6ee4\u6548\u5e94\uff0c\u80fd\u591f\u5728\u7565\u5fae\u51cf\u5c0f\u8fc1\u79fb\u7387\u4f46\u662f\u663e\u8457\u589e\u5927Seebeck\u7cfb\u6570\uff0c\u540c\u65f6\u964d\u4f4e\u6676\u683c\u70ed\u5bfc\u7387\uff0c\u63d0\u9ad8\u529f\u7387\u56e0\u5b50\u548c\u70ed\u7535\u4f18\u503c\uff0c\u5728300K\u5f97\u5230\u8d85\u9ad8\u529f\u7387\u56e0\u5b50PF\u224847 \u03bcW cm\u22122<\/sup>\u00a0K\u22121<\/sup>\uff0c\u5728300~850K\u5f97\u5230\u5e73\u5747ZT\u22481.08\u3002\u8be5\u7814\u7a76\u5229\u7528\u6676\u754c\u5de5\u7a0b\u63d0\u9ad8\u65b9\u94b4\u77ff\u6750\u6599\u7684\u70ed\u7535\u6027\u80fd\u7684\u65b9\u6cd5\uff0c\u5bf9\u4e8e\u5176\u4ed6\u70ed\u7535\u6750\u6599\u70ed\u7535\u6027\u80fd\u7684\u63d0\u9ad8\u4e5f\u5c06\u6709\u542f\u793a\u4f5c\u7528\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/b><\/strong>Grain Boundary Engineering for Achieving High Thermoelectric Performance in n-Type Skutterudites<\/a>\uff08Adv. Energy Mater.,\u00a02017, DOI: 10.1002\/aenm.201602582\uff09<\/p>\n

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