{"id":84245,"date":"2017-07-08T06:30:57","date_gmt":"2017-07-07T22:30:57","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=84245"},"modified":"2017-07-04T14:30:28","modified_gmt":"2017-07-04T06:30:28","slug":"acs-nano-%e5%88%a9%e7%94%a8%e6%89%a9%e6%95%a3%e9%97%b4%e7%9a%84%e7%9b%b8%e4%ba%92%e4%bd%9c%e7%94%a8%e5%90%88%e6%88%90%e4%ba%8c%e7%bb%b4mof%e5%90%8c%e6%97%b6%e8%a1%a8%e5%be%81ti3c2tx%e7%ba%b3%e7%b1%b3","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=84245","title":{"rendered":"ACS Nano: \u5229\u7528\u76f8\u4e92\u6269\u6563\u8f85\u52a9\u590d\u5408\u4e8c\u7ef4MOF\u548cTi3C2Tx\u7eb3\u7c73\u8584\u7247\u7528\u4e8e\u7535\u50ac\u5316\u6790\u6c27\u53cd\u5e94"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/span><\/p>\n

\u968f\u7740\u5bf9\u5316\u77f3\u71c3\u6599\u71c3\u70e7\u5f15\u53d1\u7684\u7a7a\u6c14\u6c61\u67d3\u548c\u5168\u7403\u6c14\u5019\u53d8\u5316\u7684\u65e5\u8d8b\u5173\u6ce8\uff0c\u71c3\u6599\u7535\u6c60\u3001\u91d1\u5c5e-\u7a7a\u6c14\u84c4\u7535\u6c60\u3001\u7535\u89e3\u6c34\u7b49\u6709\u6548\u7684\u7535\u5316\u5b66\u80fd\u6e90\u8f6c\u5316\u548c\u5b58\u50a8\u6280\u672f\u8d8a\u6765\u8d8a\u5177\u6709\u91cd\u5927\u610f\u4e49\u3002\u5728\u8fd9\u4e9b\u57fa\u4e8e\u80fd\u6e90\u7684\u5e94\u7528\u4e2d\u7535\u5316\u5b66\u6790\u6c27\u53cd\u5e94(OER)\u662f\u91cd\u8981\u7684\u8fc7\u7a0b\u3002\u5c3d\u7ba1\u73b0\u6709\u7684\u57fa\u4e8e\u91d1\u5c5e\u7684\u6c27\u5316\u5242(\u5982RuO2<\/sub>\u548c IrO2<\/sub> )\u5bf9\u4e8eOER\u53cd\u5e94\u6765\u8bf4\u6d3b\u6027\u5f88\u9ad8\uff0c\u4f46\u7531\u4e8e\u7a00\u7f3a\u5bfc\u81f4\u6210\u672c\u8fc7\u9ad8\u3002\u4e8c\u7ef4(2D)\u91d1\u5c5e\u6709\u673a\u6846\u67b6(MOF)\u7eb3\u7c73\u7247\u8fd1\u6765\u88ab\u8ba4\u4e3a\u662f\u5178\u578b\u7684\u7535\u50ac\u5316\u5242\uff0c\u5f97\u76ca\u4e8e\u5176\u591a\u7a7a\u7ed3\u6784\uff0c\u5c42\u95f4\u7684\u8d28\u91cf\u548c\u79bb\u5b50\u5feb\u901f\u4f20\u9012\uff0c\u5f88\u5927\u90e8\u5206\u7684\u66b4\u9732\u7684\u6d3b\u6027\u91d1\u5c5e\u4f4d\u70b9\u3002\u7136\u800c\uff0c\u5927\u90e8\u5206MOFs\u7684\u7535\u5bfc\u6027\u8f83\u4f4e\uff0c\u56e0\u6b64\u5c062D MOFs\u548c\u5177\u6709\u7535\u5bfc\u6027\u7684\u7eb3\u7c73\u7ed3\u6784\u7ed3\u5408\u6709\u671b\u63d0\u9ad8\u5728\u591a\u79cd\u7535\u50ac\u5316\u8fc7\u7a0b\u4e2d\u7684\u50ac\u5316\u6027\u80fd\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/span><\/p>\n

\u8fd1\u65e5\uff0cACS Nano<\/strong>\u00a0<\/strong>\u520a\u767b\u4e86\u4e00\u7bc7\u9898\u4e3a\u201cInterdiffusion Reaction-Assisted Hybridization of Two-Dimensional Metal\u2212Organic Frameworks and Ti3<\/sub>C2<\/sub>Tx<\/sub><\/strong>\u00a0<\/strong>Nanosheets for Electrocatalytic Oxygen Evolution\u201d<\/strong>\u7684\u6587\u7ae0\uff0c\u62a5\u9053\u4e86\u5357\u4eac\u90ae\u7535\u5927\u5b66\u674e\u7ecd\u5468\u6559\u6388\u3001\u5357\u4eac\u5de5\u4e1a\u5927\u5b66\u9ec4\u7ef4\u6559\u6388\u3001\u9ec4\u6653\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09\u7b49\u4eba<\/strong>\uff0c\u8fd0\u7528\u5185\u90e8\u6269\u6563\u76f8\u8f85\u52a9\u7684\u8fc7\u7a0b\u539f\u4f4d\u5408\u6210CoBDC\uff0c\u5e76\u5c06Ti3C2Tx \u7eb3\u7c73\u7247\u4e0e\u4e4b\u590d\u5408\u3002\u5c06\u5f97\u5230\u7684\u590d\u5408\u6750\u6599\u5e94\u7528\u4e8e\u7535\u5316\u5b66\u6790\u6c27\u53cd\u5e94(OER)\u4e2d\uff0c\u57280.1M KOH\u7684\u7535\u89e3\u6db2\u4e0b\uff0c\u76f8\u5bf9\u4e8e\u53ef\u9006\u6c22\u7535\u6781\u57281.64V\u7535\u52bf\u4e0b\u80fd\u8fbe\u5230\u7535\u6d41\u5bc6\u5ea6\u4e3a10mA cm\u2212<\/sup>2<\/sup> \u53ca\u5854\u83f2\u5c14\u659c\u7387\u4e3a48.2mV dec–<\/sup>1<\/sup>\u3002\u8fd9\u4e9b\u6027\u80fd\u8d85\u51fa\u90a3\u4e9b\u57fa\u4e8e IrO2<\/sub>\u7684\u50ac\u5316\u5242\u751a\u81f3\u6bd4\u6b64\u524d\u62a5\u9053\u7684\u66f4\u5148\u8fdb\u7684\u57fa\u4e8e\u8fc7\u6e21\u91d1\u5c5e\u7684\u50ac\u5316\u5242\u3002\u7531\u4e8eCoBDC\u5c42\u63d0\u4f9b\u591a\u5b54\u7ed3\u6784\u548c\u8f83\u5927\u7684\u6d3b\u6027\u8868\u9762\u79ef\u4e14Ti3C2Tx\u7eb3\u7c73\u7247\u7684\u4f18\u826f\u7684\u7535\u5bfc\u6027\u548c\u4eb2\u6c34\u6027\u4f7f\u5f97\u7535\u8377\u548c\u79bb\u5b50\u5728\u590d\u5408\u5f97\u5230\u7684Ti3<\/sub>C2<\/sub>Tx<\/sub>\u2212CoBDC\u754c\u9762\u4e0a\u5feb\u901f\u4f20\u9012\u3002\u540c\u65f6\u4e5f\u4fbf\u4e8e\u6c34\u6027\u7535\u89e3\u6db2\u63a5\u8fd1\u50ac\u5316\u7684\u6d3b\u6027CoBDC\u8868\u9762\u3002\u8fd9\u79cd\u7eb3\u7c73\u8584\u7247\u8fdb\u4e00\u6b65\u7ec4\u88c5\u5230\u7a7a\u6c14\u9634\u6781\u5f62\u6210\u53ef\u5145\u7535\u7684\u950c-\u7a7a\u6c14\u7535\u6c60\uff0c\u5e76\u6210\u529f\u5e26\u52a8LED\u53d1\u5149\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/span><\/p>\n

\u56fe\u4e00\uff1a\u5236\u5907<\/strong>Ti3<\/sub>C2<\/sub>Tx<\/sub>-CoBDC<\/strong>\u590d\u5408\u7269\u8fdb\u884c\u6790\u6c27\u53cd\u5e94\u7684\u793a\u610f\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

\u6b65\u9aa4a\u3001b\u5c55\u793a\u4e86Ti3<\/sub>C2<\/sub>Tx<\/sub>\u7684\u751f\u6210\uff0c\u6b65\u9aa4c\u5c55\u793a\u4e86Ti3<\/sub>C2<\/sub>Tx<\/sub>-MOF\u590d\u5408\u7269\u7684\u5f62\u6210\uff0c\u6b65\u9aa4d\u5c55\u793a\u7684\u662f\u8fdb\u884c\u6790\u6c27\u53cd\u5e94\u7684\u8fc7\u7a0b\u3002<\/p>\n

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\uff08a\uff09\u5c42\u53e0\u72b6Ti3<\/sub>C2<\/sub>Tx<\/sub>\u7ed3\u6784\u7684TEM\u56fe\u50cf<\/p>\n

\uff08b\uff09\u901a\u8fc7\u5c06\u5c42\u72b6Ti3<\/sub>C2<\/sub>Tx<\/sub>\u00a0\u9897\u7c92\u901a\u8fc7\u8d85\u58f0\u5904\u7406\u5f97\u5230\u7684Ti3<\/sub>C2<\/sub>Tx<\/sub>\u7eb3\u7c73\u8584\u7247SEM\u56fe\u50cf<\/p>\n

\uff08c\uff09\u901a\u8fc7\u5c06\u5c42\u72b6Ti3<\/sub>C2<\/sub>Tx<\/sub>\u00a0\u9897\u7c92\u901a\u8fc7\u8d85\u58f0\u5904\u7406\u5f97\u5230\u7684Ti3<\/sub>C2<\/sub>Tx<\/sub>\u7eb3\u7c73\u8584\u7247TEM\u56fe\u50cf<\/p>\n

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\uff08e\uff09Ti3<\/sub>C2<\/sub>Tx<\/sub>\u7eb3\u7c73\u8584\u7247\u8fb9\u7f18\u90e8\u5206\u4fa7\u89c6\u56fe\u7684TEM\u56fe\u50cf<\/p>\n

\uff08f\uff09Ti3<\/sub>AlC2<\/sub>\u7c89\u672b\u548c\u4ec5\u6709Ti3<\/sub>C2<\/sub>Tx<\/sub>\u7eb3\u7c73\u8584\u7247\u7684XRD\u56fe\u50cf<\/p>\n

\u56fe\u4e09\uff1a<\/strong>SEM<\/strong>\u3001<\/strong>TEM<\/strong>\u3001<\/strong>XRD<\/strong>\u3001<\/strong>XPS<\/strong>\u7b49\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

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\uff08b\uff09Ti3<\/sub>C2<\/sub>Tx<\/sub>-CoBDC\u590d\u5408\u7269\u7eb3\u7c73\u8584\u7247\u7684SEM\u56fe\u50cf<\/p>\n

\uff08c\uff09Ti3<\/sub>C2<\/sub>Tx<\/sub>-CoBDC\u590d\u5408\u7269\u7eb3\u7c73\u8584\u7247\u7684TEM\u56fe\u50cf<\/p>\n

\uff08d\uff09\u5c11\u91cf\u5806\u53e0\u7684Ti3<\/sub>C2<\/sub>Tx<\/sub>-CoBDC\u590d\u5408\u7269\u7eb3\u7c73\u8584\u7247\u7684\u622a\u9762\u56fe<\/p>\n

\uff08e\uff09\u5c11\u91cf\u5806\u53e0\u7684Ti3<\/sub>C2<\/sub>Tx<\/sub>-CoBDC\u590d\u5408\u7269\u7eb3\u7c73\u8584\u7247\u7684STEM\u56fe\u50cf\u548cEDX\u6620\u5c04\u56fe<\/p>\n

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\u56fe\u56db\uff1a\u7535\u6027\u80fd\u8868\u5f81<\/strong><\/p>\n

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\u3010\u5c0f\u7ed3\u3011<\/strong><\/span><\/p>\n

\u5728\u8fd9\u9879\u5de5\u4f5c\u4e2d\uff0c\u7814\u7a76\u4eba\u5458\u5229\u7528\u6269\u6563\u95f4\u7684\u76f8\u4e92\u4f5c\u7528\u5408\u6210\u4e8c\u7ef4\u91d1\u5c5e-\u6709\u673a\u7269\u7ed3\u6784\u540c\u65f6\u8868\u5f81Ti3<\/sub>C2<\/sub>Tx<\/sub>\u7eb3\u7c73\u8584\u7247\u7684\u6c27\u6790\u51fa\u7535\u50ac\u5316\u6027\u80fd\u3002CoBDC\u5c42\u8d1f\u8f7d\u5728\u5e26\u8d1f\u7535\u7684Ti3<\/sub>C2<\/sub>Tx<\/sub>\u7eb3\u7c73\u8584\u7247\u7684\u8868\u9762\uff0c\u5408\u6210\u5f97\u5230\u7684\u826f\u597d\u7684Ti3<\/sub>C2<\/sub>Tx<\/sub>\u2212CoBDC\u754c\u9762\u80fd\u591f\u5b9e\u73b0\u5feb\u901f\u5145\u7535\u548c\u79bb\u5b50\u4ea4\u6362\uff0c\u540c\u65f6\u4e5f\u4fbf\u4e8e\u6c34\u6027\u7535\u89e3\u6db2\u901a\u8fc7\u50ac\u5316\u7684\u6d3b\u6027CoBDC\u8868\u9762\u3002\u8fd9\u9879\u7814\u7a76\u7684\u6210\u529f\u5b9e\u73b0\uff0c\u672a\u6765\u5c06MXenes\u548c2D MOFs\u5e94\u7528\u4e8e\u80fd\u91cf\u50a8\u5b58\u65b9\u9762\u4f1a\u66f4\u591a\u7684\u673a\u4f1a\u3002<\/span><\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Interdiffusion Reaction-Assisted Hybridization of Two-Dimensional Metal\u2212Organic Frameworks and Ti3C2Tx Nanosheets for Electrocatalytic Oxygen Evolution<\/a><\/span>\uff08ACS Nano, \u00a02017, DOI: 10.1021\/acsnano.7b01409\uff09<\/span><\/p>\n

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